CN109042923A - It is a kind of with reduce cholesterol level, be exclusively used in barbecue edible blend oil - Google Patents
It is a kind of with reduce cholesterol level, be exclusively used in barbecue edible blend oil Download PDFInfo
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- CN109042923A CN109042923A CN201810771949.XA CN201810771949A CN109042923A CN 109042923 A CN109042923 A CN 109042923A CN 201810771949 A CN201810771949 A CN 201810771949A CN 109042923 A CN109042923 A CN 109042923A
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/007—Other edible oils or fats, e.g. shortenings, cooking oils characterised by ingredients other than fatty acid triglycerides
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/02—Other edible oils or fats, e.g. shortenings, cooking oils characterised by the production or working-up
- A23D9/04—Working-up
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- Life Sciences & Earth Sciences (AREA)
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- Fats And Perfumes (AREA)
Abstract
The invention discloses a kind of with the edible blend oil for reducing cholesterol level, being exclusively used in barbecue, it is related to edible oil technical field, edible blend oil of the invention is made of the feedstock oil of following parts by weight: 50~60 parts of sunflower oil, 5~15 parts of camellia seed oil, 10~20 parts of soybean oil, 1~10 part of rapeseed oil, 10~20 parts of linseed oil.Edible blend oil of the invention has followed the traditional diet of Chinese, also comply with the principle of content of fatty acid balance, the edible blend oil has that strong fragrance, flavour are palatable, nutritive value is high, are not easy oxidation deterioration, do not add chemical preservative, meet people and increasingly pursues delicious, nutrition eating habit, and it is squeezed using cold-press, avoid the loss of nutritional ingredient that nutritional ingredient is made to obtain maximum reservation to the maximum extent, obtained ready-mixed oil has the effects that reduce cholesterol, reduces blood pressure, prevents vascular sclerosis and prevention coronary heart disease.
Description
Technical field:
The present invention relates to edible oil technical fields, and in particular to it is a kind of with reduce cholesterol level, be exclusively used in barbecue
Edible blend oil.
Background technique:
Sunflower oil contains the beneficial substance of a variety of couples of mankind such as sterol, vitamin, linoleic acid, wherein natural VE
Content content highest in all main vegetable oils;And linoleic acid content is up to 70% or so.Linoleic acid is rouge needed by human
Fat acid plays the role of significantly reducing cholesterol, reduces blood pressure, prevents vascular sclerosis and prevention coronary heart disease.In addition, in sunflower oil
Also contain more vitamin E, has the function of good delay human body cell aging.Sunflower oil Linoleic acid content and dimension
The ratio of raw element E content is more balanced, utilizes convenient for absorption of human body.So sunflower oil is that nutritive value is very high, it is beneficial to people
The excellent edible oil of body health.
Camellia seed oil is a kind of natural advanced woody edible oil, and main ingredient is the insatiable hunger based on oleic acid and linoleic acid
And fatty acid, for content up to 90% or more, mid-oleic is more than 80%, is easily absorbed by the body, and oleic acid content is high, can be effective
Prevention three is high, softening blood vessel, removes human free radical.Camellia seed oil mycomycin cholesterol-free and yellow has improving eyesight brighten the hair, profit
Intestines defaecation and other effects.In addition, camellia seed oil is because of vitamin A rich in, E, D, K and other antioxidants.Use camellia seed oil
Fried food, color cadmium yellow, taste perfume (or spice) is palatable, is the high-grade oil plant of cooking food, processed can, making artificial cream.
Soybean oil is derived from soya seeds, is the grease that yield is most in the world.The Fatty acid compositions of soybean oil are preferable, it contains
The effect of having linoleic acid abundant, be significantly reduced serum cholesterol content, preventing cardiovascular disease, also containing more in soybean
Vitamin E, vitamin D and the lecithin abundant of amount, it is very useful to human health.In addition, the human body of soybean oil disappears
Change absorptivity and be up to 98%, so soybean oil is also a kind of very high excellent edible oil of nutritive value.
Rapeseed oil is to be squeezed out with rapeseed come golden yellow color or pale brown.Human body is very high to the absorptivity of rapeseed oil, reachable
99%, therefore the nutritional ingredients such as the unsaturated fatty acids such as linoleic acid contained by it and vitamin E can be absorbed by organisms well, tool
There is the effect of certain softening blood vessel, anti-aging.It, generally can be containing certain since the raw material of oil expression is the kind reality of plant
Seed phosphatide, it is particularly significant to the development of blood vessel, nerve, human brain.The cholesterol of rapeseed oil is with little or no containing, so being suitble to
The crowd of cholesterol is eaten less.
Barbecue is a kind of multiplayer party leisure and entertainment, and people can talk at dinner in party, loosens mood, still
As the improvement of people's living standards, the pursuit to substance is also higher and higher, therefore edible oil used when barbecue will also meet
The nutrition-balanced pursuit of people, the food after enabling barbecue are fresher fragrant delicious.
Summary of the invention:
It is a kind of with the food for reducing cholesterol level, being exclusively used in barbecue technical problem to be solved by the present invention lies in providing
Use ready-mixed oil.
The following technical solution is employed for the technical problems to be solved by the invention to realize:
It is a kind of with reduce cholesterol level, be exclusively used in barbecue edible blend oil, be by the feedstock oil of following parts by weight
Composition: 50~60 parts of sunflower oil, 5~15 parts of camellia seed oil, 10~20 parts of soybean oil, 1~10 part of rapeseed oil, linseed oil 10
~20 parts.
The linseed oil the preparation method comprises the following steps:
(1) raw material screening: preferred maturity degree is suitable for, full grains, superior in quality linseed is as raw material;
(2) cleaning removal of impurities: being cleaned using mode of the combination sieve in conjunction with magnetic separator, and it is miscellaneous first to screen out size with combination
Matter, wherein the mesh size for screening out big impurity is 1.2mm × 20mm, the mesh size for screening out small impurity is 1.8~2.2mm;So
Irony is being screened out using magnetic separator afterwards, is screening out the impurity in linseed to greatest extent;
(3) strip plate: strip plate is carried out using hydraulic rolling mill, makes its thickness in 0.5mm or less;
(4) quenched: the linseed embryo piece that will have been rolled carries out low temperature drying, makes its moisture lower than 8%;
(5) low-temperature cold pressing: the linseed embryo piece merging twin-screw press after drying is extracted oil, oil outlet temperature 40
~55 DEG C;
(6) dregs of fat separate: gained linseed crude oil being filtered, filtered crude oil is refined again, and the dregs of fat carry out
Twice pressing;
(7) degumming: gained crude oil is injected in hydration tank, be added while stirring oil weigh 40 DEG C of 0.2%~0.3% it is dense
Degree is 5~10g/L saline solution, is filtered after reacting end and precipitating a period of time, and carry out vacuum dehydration;
(8) take off hardship: being 50~60 DEG C in oil temperature, under conditions of vacuum degree is 90~100kPa, be added oil weigh 0.1%~
0.5% adsorbent simultaneously stirs 20~40min or so with the revolving speed of 60~80r/min, is cooled to room temperature, breaks true after reaction
De- bitter linseed oil is obtained by filtration after sky;
(9) low temperature crystallization growing the grain: the oil after de- hardship is introduced into rapid cooling tank and is cooled down, after obtaining part wax nucleus
It into crystallization maturator, and is stirred with the revolving speed of 10~15r/min, oil temperature stops stirring when being cooled to 15 DEG C, continues cold
But to 5 DEG C, 8h is kept, then by being filtered for multiple times to obtain linseed oil.
The edible blend oil the preparation method comprises the following steps:
S1: under the protection of nitrogen, sunflower oil, camellia seed oil, soybean oil, rapeseed oil, linseed oil are added in proportion
Enter into blending tank, under normal temperature and pressure conditions, mix slowly 20~40min, stands, it is cooling, it is filling.
S2: exfactory inspection: carrying out exfactory inspection according to Q/JMZ 0001S-2017 standard, after the assay was approved, with qualification
Card can dispatch from the factory.
Preferably, the edible blend oil for having reduction cholesterol level, being exclusively used in roasting is by following parts by weight
Feedstock oil composition: 55 parts of sunflower oil, 10 parts of camellia seed oil, 15 parts of soybean oil, 5 parts of rapeseed oil, 15 parts of linseed oil.
The camellia seed oil, rapeseed oil, linseed oil pass through cold press preparation process and are prepared.
Adsorbent in the preparation method step (8) of the linseed oil is active carbon.
Adsorbent in the preparation method step (8) of the linseed oil is compound adsorbent, preparation method are as follows:
(a) sour modification infusorial earth-attapulgite: diatomite, attapulgite, dispersing agent are dissolved in deionized water, added
After entering hydrochloric acid, 30~60 DEG C of 1~1.5h of stirring are mixed, and ultrasonic wave disperses 0.5h, and centrifugal dehydration is dried at 105 DEG C, grinding, mistake
200 meshes transfer to 400~500 DEG C of 2~3h of calcination activation of Muffle furnace, cooling, are sealed and are modified diatom to get to acid
Soil-attapulgite;
(b) it loads aluminum oxide: modification infusorial earth-attapulgite prepared by step (a) is added in alumina solution,
After air constant temperature oscillation 5h, being adjusted to pH is 5.5~6.5, after centrifugal dehydration, and aluminium oxide-diatomite-bumps are made in 105 DEG C of drying
Stick soil compound adsorbent.
The attapulgite clay compounded adsorbent of aluminium oxide-diatomite-is by the modified diatomite-attapulgite of acid in acid
Property under the conditions of with aluminium oxide react obtained through catalysis.
Diatomite in step (a) in the preparation method of the compound adsorbent, attapulgite, dispersing agent weight ratio be
100:100:6.
Dispersing agent is sodium pyrophosphate in step (a) in the preparation method of the compound adsorbent.
Concentration is in deionized water for diatomite, attapulgite in step (a) in the preparation method of the compound adsorbent
0.3g/ml, the concentration of hydrochloric acid being added are 0.1~3mol/L.
Weight percentage of the aluminium oxide in compound adsorbent in step (b) in the preparation method of the compound adsorbent
It is 10%~80%;Alumina solution concentration used is 0.1~1.0mol/L.
The reagent that pH is adjusted in the preparation method of the compound adsorbent is NaOH solution.
The beneficial effects of the present invention are:
1, proposed by the present invention that there is the edible blend oil for reducing cholesterol level, being exclusively used in barbecue, it is with sunflower oil
For matrix oil, deploy with camellia seed oil, soybean oil, rapeseed oil, cold pressed flax seed oil.This oil not only has followed China
The traditional diet of people, and its fatty acid composition meets n-3 polyunsaturated fatty acid: polyunsaturated fatty acid=1 n-6:
The principle of (4~6).
2, it is proposed by the present invention have reduce cholesterol level, be exclusively used in barbecue edible blend oil, have strong fragrance,
Flavour is palatable, nutritive value is high, content of fatty acid is balanced, is not easy oxidation deterioration, meets people and increasingly pursues delicious, nutrition drink
Dietary habits.
3, proposed by the present invention that there is the edible blend oil for reducing cholesterol level, being exclusively used in barbecue, it is anti-that chemistry is not added
Rotten agent, is squeezed using cold-press, avoids the loss of nutritional ingredient to the maximum extent, its nutritional ingredient is made to obtain maximum reservation,
Obtained ready-mixed oil has the effects that reduce cholesterol, reduces blood pressure, prevents vascular sclerosis and prevention coronary heart disease.
Specific embodiment:
In order to be easy to understand the technical means, the creative features, the aims and the efficiencies achieved by the present invention, tie below
Specific embodiment is closed, the present invention is further explained.
Embodiment 1
The preparation of compound adsorbent:
(a) sour modification infusorial earth-attapulgite: 5g diatomite, 5g attapulgite, 0.3g dispersing agent sodium pyrophosphate are placed in
In 250ml beaker, deionized water 40ml is added and dissolves to form aqueous solution, adds 0.5mol/L HCl 20ml, is placed in magnetic force and stirs
45 DEG C of stirring 1h of device to be mixed, are mixed, mixed liquor is then subjected to ultrasonic wave and disperses 0.5h, centrifugal dehydration is dried at 105 DEG C, grinding,
200 meshes are crossed, 450 DEG C of calcination activation 3h of Muffle furnace are transferred to, it is cooling, it is sealed to get sour modification infusorial earth-bumps are arrived
Stick soil;
(b) it loads aluminum oxide: modification infusorial earth-attapulgite made from 0.4g being taken to be added to 25ml 0.5mol/L's
In alumina solution, after air constant temperature oscillation 5h, being adjusted to pH with NaOH solution is 6.0, after centrifugal dehydration, 105 DEG C of drying
The attapulgite clay compounded adsorbent of aluminium oxide-diatomite-is made.
The preparation of linseed oil:
(1) raw material screening: preferred maturity degree be suitable for, full grains, superior in quality linseed 100kg.
(2) cleaning removal of impurities: being cleaned using mode of the combination sieve in conjunction with magnetic separator, and it is miscellaneous first to screen out size with combination
Matter, wherein the mesh size for screening out big impurity is 1.2mm × 20mm, the mesh size for screening out small impurity is 2.0mm;Then make
Irony is screened out with magnetic separator, screens out the impurity in linseed to greatest extent.
(3) strip plate: strip plate is carried out using hydraulic rolling mill, thickness is in 0.5mm or less.
(4) quenched: the linseed embryo piece that will have been rolled carries out low temperature drying, and moisture is lower than 8%.
(5) low-temperature cold pressing: the linseed embryo piece merging twin-screw press after drying is extracted oil, oil outlet temperature 45
℃。
(6) dregs of fat separate: gained linseed crude oil being filtered, filtered crude oil is refined again, and the dregs of fat carry out
Twice pressing.
(7) aquation degumming: gained crude oil is injected in hydration tank, and it is 5g/L's that 40 DEG C of 0.14kg concentration are added while stirring
Saline solution filters after reacting end and precipitating a period of time, and carries out vacuum dehydration.
(8) take off hardship: oil temperature be 50 DEG C, vacuum degree be 95kPa under conditions of, be added the compound adsorbent of 0.14kg and with
Revolving speed stirring 35min of 70r/min or so, is cooled to room temperature after reaction, and de- bitter linseed oil is obtained by filtration after vacuum breaker.
(9) low temperature crystallization growing the grain: the oil after de- hardship is introduced into rapid cooling tank and is cooled down, after obtaining part wax nucleus
It into crystallization maturator, and is stirred with the revolving speed of 15r/min, oil temperature stops stirring when being cooled to 15 DEG C, continues cool to 5
DEG C, 8h is kept, then by being filtered for multiple times to obtain linseed oil.
By sunflower oil 50kg, camellia seed oil 5kg, soybean oil 20kg, rapeseed oil 10kg, linseed oil 10kg in nitrogen
Protection under be added in blending tank, under normal temperature and pressure conditions, mix slowly 30min, stand, it is cooling, it is filling.
Exfactory inspection is carried out according to Q/JMZ 0001S-2017 standard to gained edible blend oil to have after the assay was approved
The certificate of competency can dispatch from the factory.
Embodiment 2
The preparation of compound adsorbent:
(a) sour modification infusorial earth-attapulgite: 5g diatomite, 5g attapulgite, 0.3g dispersing agent sodium pyrophosphate are placed in
In 250ml beaker, deionized water 40ml is added and dissolves to form aqueous solution, adds 0.5mol/L HCl 20ml, is placed in magnetic force and stirs
45 DEG C of stirring 1h of device to be mixed, are mixed, mixed liquor is then subjected to ultrasonic wave and disperses 0.5h, centrifugal dehydration is dried at 105 DEG C, grinding,
200 meshes are crossed, 450 DEG C of calcination activation 3h of Muffle furnace are transferred to, it is cooling, it is sealed to get sour modification infusorial earth-bumps are arrived
Stick soil;
(b) it loads aluminum oxide: modification infusorial earth-attapulgite made from 0.4g being taken to be added to 25ml 0.5mol/L's
In alumina solution, after air constant temperature oscillation 5h, being adjusted to pH with NaOH solution is 6.0, after centrifugal dehydration, 105 DEG C of drying
The attapulgite clay compounded adsorbent of aluminium oxide-diatomite-is made.
The preparation of linseed oil:
(1) raw material screening: preferred maturity degree be suitable for, full grains, superior in quality linseed 100kg.
(2) cleaning removal of impurities: being cleaned using mode of the combination sieve in conjunction with magnetic separator, and it is miscellaneous first to screen out size with combination
Matter, wherein the mesh size for screening out big impurity is 1.2mm × 20mm, the mesh size for screening out small impurity is 2.0mm;Then make
Irony is screened out with magnetic separator, screens out the impurity in linseed to greatest extent.
(3) strip plate: strip plate is carried out using hydraulic rolling mill, thickness is in 0.5mm or less.
(4) quenched: the linseed embryo piece that will have been rolled carries out low temperature drying, and moisture is lower than 8%.
(5) low-temperature cold pressing: the linseed embryo piece merging twin-screw press after drying is extracted oil, oil outlet temperature 45
℃。
(6) dregs of fat separate: gained linseed crude oil being filtered, filtered crude oil is refined again, and the dregs of fat carry out
Twice pressing.
(7) aquation degumming: gained crude oil is injected in hydration tank, and it is 5g/L's that 40 DEG C of 0.14kg concentration are added while stirring
Saline solution filters after reacting end and precipitating a period of time, and carries out vacuum dehydration.
(8) take off hardship: oil temperature be 50 DEG C, vacuum degree be 95kPa under conditions of, be added the compound adsorbent of 0.12kg and with
Revolving speed stirring 35min of 70r/min or so, is cooled to room temperature after reaction, and de- bitter linseed oil is obtained by filtration after vacuum breaker.
(9) low temperature crystallization growing the grain: the oil after de- hardship is introduced into rapid cooling tank and is cooled down, after obtaining part wax nucleus
It into crystallization maturator, and is stirred with the revolving speed of 15r/min, oil temperature stops stirring when being cooled to 15 DEG C, continues cool to 5
DEG C, 8h is kept, then by being filtered for multiple times to obtain linseed oil.
By sunflower oil 55kg, camellia seed oil 10kg, soybean oil 15kg, rapeseed oil 5kg, linseed oil 15kg in nitrogen
Protection under be added in blending tank, under normal temperature and pressure conditions, mix slowly 40min, stand, it is cooling, it is filling.
Exfactory inspection is carried out according to Q/JMZ 0001S-2017 standard to gained edible blend oil to have after the assay was approved
The certificate of competency can dispatch from the factory.
Embodiment 3
The preparation of compound adsorbent:
(a) sour modification infusorial earth-attapulgite: 5g diatomite, 5g attapulgite, 0.3g dispersing agent sodium pyrophosphate are placed in
In 250ml beaker, deionized water 40ml is added and dissolves to form aqueous solution, adds 0.5mol/L HCl 20ml, is placed in magnetic force and stirs
45 DEG C of stirring 1h of device to be mixed, are mixed, mixed liquor is then subjected to ultrasonic wave and disperses 0.5h, centrifugal dehydration is dried at 105 DEG C, grinding,
200 meshes are crossed, 450 DEG C of calcination activation 3h of Muffle furnace are transferred to, it is cooling, it is sealed to get sour modification infusorial earth-bumps are arrived
Stick soil;
(b) it loads aluminum oxide: modification infusorial earth-attapulgite made from 0.4g being taken to be added to 25ml 0.5mol/L's
In alumina solution, after air constant temperature oscillation 5h, being adjusted to pH with NaOH solution is 6.0, after centrifugal dehydration, 105 DEG C of drying
The attapulgite clay compounded adsorbent of aluminium oxide-diatomite-is made.
The preparation of linseed oil:
(1) raw material screening: preferred maturity degree be suitable for, full grains, superior in quality linseed 100kg.
(2) cleaning removal of impurities: being cleaned using mode of the combination sieve in conjunction with magnetic separator, and it is miscellaneous first to screen out size with combination
Matter, wherein the mesh size for screening out big impurity is 1.2mm × 20mm, the mesh size for screening out small impurity is 2.0mm;Then make
Irony is screened out with magnetic separator, screens out the impurity in linseed to greatest extent.
(3) strip plate: strip plate is carried out using hydraulic rolling mill, thickness is in 0.5mm or less.
(4) quenched: the linseed embryo piece that will have been rolled carries out low temperature drying, and moisture is lower than 8%.
(5) low-temperature cold pressing: the linseed embryo piece merging twin-screw press after drying is extracted oil, oil outlet temperature 45
℃。
(6) dregs of fat separate: gained linseed crude oil being filtered, filtered crude oil is refined again, and the dregs of fat carry out
Twice pressing.
(7) aquation degumming: gained crude oil is injected in hydration tank, and it is 5g/L's that 40 DEG C of 0.14kg concentration are added while stirring
Saline solution filters after reacting end and precipitating a period of time, and carries out vacuum dehydration.
(8) take off hardship: oil temperature be 50 DEG C, vacuum degree be 95kPa under conditions of, be added the compound adsorbent of 0.10kg and with
Revolving speed stirring 35min of 70r/min or so, is cooled to room temperature after reaction, and de- bitter linseed oil is obtained by filtration after vacuum breaker.
(9) low temperature crystallization growing the grain: the oil after de- hardship is introduced into rapid cooling tank and is cooled down, after obtaining part wax nucleus
It into crystallization maturator, and is stirred with the revolving speed of 15r/min, oil temperature stops stirring when being cooled to 15 DEG C, continues cool to 5
DEG C, 8h is kept, then by being filtered for multiple times to obtain linseed oil.
By sunflower oil 60kg, camellia seed oil 15kg, soybean oil 10kg, rapeseed oil 1kg, linseed oil 20kg in nitrogen
Protection under be added in blending tank, under normal temperature and pressure conditions, mix slowly 20min, stand, it is cooling, it is filling.
Exfactory inspection is carried out according to Q/JMZ 0001S-2017 standard to gained edible blend oil to have after the assay was approved
The certificate of competency can dispatch from the factory.
Embodiment 4
The preparation of linseed oil:
(1) raw material screening: preferred maturity degree be suitable for, full grains, superior in quality linseed 100kg.
(2) cleaning removal of impurities: being cleaned using mode of the combination sieve in conjunction with magnetic separator, and it is miscellaneous first to screen out size with combination
Matter, wherein the mesh size for screening out big impurity is 1.2mm × 20mm, the mesh size for screening out small impurity is 2.0mm;Then make
Irony is screened out with magnetic separator, screens out the impurity in linseed to greatest extent.
(3) strip plate: strip plate is carried out using hydraulic rolling mill, thickness is in 0.5mm or less.
(4) quenched: the linseed embryo piece that will have been rolled carries out low temperature drying, and moisture is lower than 8%.
(5) low-temperature cold pressing: the linseed embryo piece merging twin-screw press after drying is extracted oil, oil outlet temperature 45
℃。
(6) dregs of fat separate: gained linseed crude oil being filtered, filtered crude oil is refined again, and the dregs of fat carry out
Twice pressing.
(7) aquation degumming: gained crude oil is injected in hydration tank, and it is 5g/L's that 40 DEG C of 0.14kg concentration are added while stirring
Saline solution filters after reacting end and precipitating a period of time, and carries out vacuum dehydration.
(8) take off hardship: oil temperature be 50 DEG C, vacuum degree be 95kPa under conditions of, be added 0.14kg acticarbon and with
Revolving speed stirring 35min of 70r/min or so, is cooled to room temperature after reaction, and de- bitter linseed oil is obtained by filtration after vacuum breaker.
(9) low temperature crystallization growing the grain: the oil after de- hardship is introduced into rapid cooling tank and is cooled down, after obtaining part wax nucleus
It into crystallization maturator, and is stirred with the revolving speed of 15r/min, oil temperature stops stirring when being cooled to 15 DEG C, continues cool to 5
DEG C, 8h is kept, then by being filtered for multiple times to obtain linseed oil.
By sunflower oil 55kg, camellia seed oil 10kg, soybean oil 15kg, rapeseed oil 5kg, linseed oil 15kg in nitrogen
Protection under be added in blending tank, under normal temperature and pressure conditions, mix slowly 30min, stand, it is cooling, it is filling.
Exfactory inspection is carried out according to Q/JMZ 0001S-2017 standard to gained edible blend oil to have after the assay was approved
The certificate of competency can dispatch from the factory.
Reference examples 1
The preparation of compound adsorbent:
5g diatomite, 5g attapulgite, 0.3g dispersing agent sodium pyrophosphate are placed in 250ml beaker, deionized water is added
40ml dissolves to form aqueous solution, adds 0.5mol/L HCl 20ml, is placed in 45 DEG C of stirring 1h of magnetic stirring apparatus, mixes, so
Mixed liquor is subjected to ultrasonic wave afterwards and disperses 0.5h, centrifugal dehydration is dried at 105 DEG C, and grinding crosses 200 meshes, transfers to Muffle
450 DEG C of calcination activation 3h of furnace, it is cooling, it is sealed to get compound adsorbent diatomite-attapulgite is arrived.
The preparation of linseed oil:
(1) raw material screening: preferred maturity degree be suitable for, full grains, superior in quality linseed 100kg.
(2) cleaning removal of impurities: being cleaned using mode of the combination sieve in conjunction with magnetic separator, and it is miscellaneous first to screen out size with combination
Matter, wherein the mesh size for screening out big impurity is 1.2mm × 20mm, the mesh size for screening out small impurity is 2.0mm;Then make
Irony is screened out with magnetic separator, screens out the impurity in linseed to greatest extent.
(3) strip plate: strip plate is carried out using hydraulic rolling mill, thickness is in 0.5mm or less.
(4) quenched: the linseed embryo piece that will have been rolled carries out low temperature drying, and moisture is lower than 8%.
(5) low-temperature cold pressing: the linseed embryo piece merging twin-screw press after drying is extracted oil, oil outlet temperature 45
℃。
(6) dregs of fat separate: gained linseed crude oil being filtered, filtered crude oil is refined again, and the dregs of fat carry out
Twice pressing.
(7) aquation degumming: gained crude oil is injected in hydration tank, and it is 5g/L's that 40 DEG C of 0.14kg concentration are added while stirring
Saline solution filters after reacting end and precipitating a period of time, and carries out vacuum dehydration.
(8) take off hardship: oil temperature be 50 DEG C, vacuum degree be 95kPa under conditions of, be added the compound adsorbent of 0.14kg and with
Revolving speed stirring 35min of 70r/min or so, is cooled to room temperature after reaction, and de- bitter linseed oil is obtained by filtration after vacuum breaker.
(9) low temperature crystallization growing the grain: the oil after de- hardship is introduced into rapid cooling tank and is cooled down, after obtaining part wax nucleus
It into crystallization maturator, and is stirred with the revolving speed of 15r/min, oil temperature stops stirring when being cooled to 15 DEG C, continues cool to 5
DEG C, 8h is kept, then by being filtered for multiple times to obtain linseed oil.
By sunflower oil 55kg, camellia seed oil 10kg, soybean oil 15kg, rapeseed oil 5kg, linseed oil 15kg in nitrogen
Protection under be added in blending tank, under normal temperature and pressure conditions, mix slowly 30min, stand, it is cooling, it is filling.
Exfactory inspection is carried out according to Q/JMZ 0001S-2017 standard to gained edible blend oil to have after the assay was approved
The certificate of competency can dispatch from the factory.
Reference examples 2
The preparation of compound adsorbent:
5g diatomite and 5g attapulgite are placed in 250ml beaker, deionized water 40ml is added and dissolves to form aqueous solution,
45 DEG C of stirring 1h of magnetic stirring apparatus are placed in, are mixed, mixed liquor is then subjected to ultrasonic wave and disperses 0.5h, centrifugal dehydration, 105
DEG C drying, grinding crosses 200 meshes, transfers to 450 DEG C of calcination activation 3h of Muffle furnace, cooling, is sealed to get to compound
Adsorbent diatomite-attapulgite.
The preparation of linseed oil:
(1) raw material screening: preferred maturity degree be suitable for, full grains, superior in quality linseed 100kg.
(2) cleaning removal of impurities: being cleaned using mode of the combination sieve in conjunction with magnetic separator, and it is miscellaneous first to screen out size with combination
Matter, wherein the mesh size for screening out big impurity is 1.2mm × 20mm, the mesh size for screening out small impurity is 2.0mm;Then make
Irony is screened out with magnetic separator, screens out the impurity in linseed to greatest extent.
(3) strip plate: strip plate is carried out using hydraulic rolling mill, thickness is in 0.5mm or less.
(4) quenched: the linseed embryo piece that will have been rolled carries out low temperature drying, and moisture is lower than 8%.
(5) low-temperature cold pressing: the linseed embryo piece merging twin-screw press after drying is extracted oil, oil outlet temperature 45
℃。
(6) dregs of fat separate: gained linseed crude oil being filtered, filtered crude oil is refined again, and the dregs of fat carry out
Twice pressing.
(7) aquation degumming: gained crude oil is injected in hydration tank, and it is 5g/L's that 40 DEG C of 0.14kg concentration are added while stirring
Saline solution filters after reacting end and precipitating a period of time, and carries out vacuum dehydration.
(8) take off hardship: oil temperature be 50 DEG C, vacuum degree be 95kPa under conditions of, be added the compound adsorbent of 0.14kg and with
Revolving speed stirring 35min of 70r/min or so, is cooled to room temperature after reaction, and de- bitter linseed oil is obtained by filtration after vacuum breaker.
(9) low temperature crystallization growing the grain: the oil after de- hardship is introduced into rapid cooling tank and is cooled down, after obtaining part wax nucleus
It into crystallization maturator, and is stirred with the revolving speed of 15r/min, oil temperature stops stirring when being cooled to 15 DEG C, continues cool to 5
DEG C, 8h is kept, then by being filtered for multiple times to obtain linseed oil.
By sunflower oil 55kg, camellia seed oil 10kg, soybean oil 15kg, rapeseed oil 5kg, linseed oil 15kg in nitrogen
Protection under be added in blending tank, under normal temperature and pressure conditions, mix slowly 30min, stand, it is cooling, it is filling.
Exfactory inspection is carried out according to Q/JMZ 0001S-2017 standard to gained edible blend oil to have after the assay was approved
The certificate of competency can dispatch from the factory.
Based on embodiment 2, it is arranged in and does not load the reference examples 1 of aluminum oxide when preparing compound adsorbent, preparing
Dispersing agent and hydrochloric acid are not added when compound adsorbent and does not load the reference examples 2 of aluminum oxide.
It is utilized respectively the edible blend oil of embodiment 1-4, reference examples 1-2 preparation, wherein all raw materials are used with batch raw material.
Bitter substance removing test, test method are as follows: 1. take the Asia in 100g embodiment 1,2,3,4 are carried out to made linseed oil
Numb seed crude oil and linseed oil, linseed crude oil and linseed oil in reference examples 1,2 are dissolved in 100ml normal heptane, use 200ml
60% ethyl alcohol extracts three times, and lower aqueous layer is taken after static layering, and vacuum filtration removes ethyl alcohol;2. wet filter paper filtration step 1. in production
Object, remaining aqueous solution take 1ml to be dissolved in ethyl alcohol/diethyl ether solution of 1:1;3. taking the adsorption column of 50ml capacity, 20g silicon is filled
Rubber cement material is eluted with ether rinse using 20ml gradient elution agent;4. eluent is dissolved in 50% alcoholic solution, by
High performance liquid chromatography separation (250 × 4mm, 5 μm) measures ring octapeptide content, calculates bitter substance removal efficiency in linseed oil;Knot
Fruit such as table 1;Unsaturated fatty acid in each feedstock oil is detected, as a result such as table 2;How unsaturated in each embodiment and reference examples
The ratiometric result such as table 3 of content of fatty acid and n-6 content of polyunsaturated fatty acid and n-3 content of polyunsaturated fatty acid;To reality
It applies made edible blend oil in example and reference examples and carries out exfactory inspection, inspection result such as table 4, table 5.
Table 1
Test item | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Reference examples 1 | Reference examples 2 |
Bitter substance removal efficiency % | 94.19 | 94.27 | 95.12 | 94.92 | 75.65 | 66.89 |
Table 2
Table 3
Table 4
Table 5
The edible blend oil balanced fatty acid proportion it can be seen from the data in above table, nutritive value height and mouth
Feel, transparent color and luster, be not easy oxidation deterioration, do not add chemical preservative, meets people and increasingly pursue health, nutrition-balanced reason
It reads.
The above shows and describes the basic principles and main features of the present invention and the advantages of the present invention.The technology of the industry
Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the above embodiments and description only describe this
The principle of invention, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, these changes
Change and improvement all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appended claims and its
Equivalent thereof.
Claims (4)
1. a kind of with the edible blend oil for reducing cholesterol level, being exclusively used in barbecue, it is characterised in that: the edible blend oil
It is made of the feedstock oil of following parts by weight: 50~60 parts of sunflower oil, 5~15 parts of camellia seed oil, 10~20 parts of soybean oil, dish
1~10 part of seed oil, 10~20 parts of linseed oil.
2. according to claim 1 have the edible blend oil for reducing cholesterol level, being exclusively used in barbecue, feature exists
In: the edible blend oil is made of the feedstock oil of following parts by weight: 55 parts of sunflower oil, 10 parts of camellia seed oil, soybean oil
15 parts, 5 parts of rapeseed oil, 15 parts of linseed oil.
3. according to claim 1 have the edible blend oil for reducing cholesterol level, being exclusively used in barbecue, feature exists
In: the camellia seed oil, rapeseed oil, linseed oil pass through cold press preparation process and are prepared.
4. the edible blend oil according to claim 1-3 that there is reduction cholesterol level, be exclusively used in barbecue
Preparation method, which comprises the following steps:
S1: under the protection of nitrogen, sunflower oil, camellia seed oil, soybean oil, rapeseed oil, linseed oil are proportionally added into
In blending tank, under normal temperature and pressure conditions, 20~40min is mixed slowly, stood, it is cooling, it is filling;
S2: exfactory inspection: carrying out exfactory inspection according to Q/JMZ 0001S-2017 standard, after the assay was approved, has quality certification side
It can dispatch from the factory.
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN115152852A (en) * | 2022-07-19 | 2022-10-11 | 内蒙古金格勒食品有限公司 | Edible blend oil for preventing coronary heart disease |
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2018
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN115152852A (en) * | 2022-07-19 | 2022-10-11 | 内蒙古金格勒食品有限公司 | Edible blend oil for preventing coronary heart disease |
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