CN109042770A - A kind of insect prevention liquid using arbor-vitae ancient tree branch juice preparation - Google Patents
A kind of insect prevention liquid using arbor-vitae ancient tree branch juice preparation Download PDFInfo
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- A—HUMAN NECESSITIES
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- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
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- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
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- A—HUMAN NECESSITIES
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Abstract
The invention discloses a kind of insect prevention liquid using arbor-vitae ancient tree branch juice preparation, are related to insect prevention liquid field；It is made of the raw material of following parts by weight: arbor-vitae ancient tree branch 60-80 parts of juice, 25-30 parts of aqueous areca nut extract, 10-15 parts of Cortex Meliae extractive liquid, 8-10 parts of Cortex hibisus syriacus extracting solution, 20-25 parts of peppermint oil, 12-16 parts of lavender oil, 6-8 parts of eucalyptus oil, 2-3 parts of cumyl peroxide, 100-120 parts of ethyl alcohol, 3-5 parts of hydrogen cyanide, 11-14 parts of prodan, 3-6 parts of copper sulphate, 5-6 parts of sodium lignin sulfonate, 320-350 parts of deionized water；The insect prevention liquid of preparation is while insect prevention, moreover it is possible to kill part pest, and insect prevention liquid environmental pollution itself is small, not will cause secondary pollution, compare conventional pesticides, greatly reduce to human injury's property, suitable for various plants, the insect prevention management of animal colony house.
Description
Technical field:
The present invention relates to insect prevention liquid fields, and in particular to a kind of insect prevention liquid using arbor-vitae ancient tree branch juice preparation.
Background technique:
Medicinal plant in the course of cultivation, by harmful organism infect or unsuitable environmental condition is influenced, it is normal new old
Metabolism is interfered, from physiological function to institutional framework on a series of variation and destruction occurs so that be in formalness
Existing unusual lesion phenomenon, such as withered, rotten, spot, mould powder, floral leaf, are referred to as disease.
The reason of causing medicinal plant to be fallen ill, including biological factor and abiotic factor.By biological factor such as fungi, carefully
Disease caused by the invaded plants body such as bacterium, virus, is infectious, referred to as infectious disease or parasitic disease, by abiotic
Factor such as drought, flood, severe cold, nutrient imbalance etc. influence or damage disease caused by physiological function, referred to as non-to invade without infectiousness
Metachromia disease or physiological disturbance.In infectious disease, pathogenic parasite is known as causal organism, wherein fungi, bacterium
Frequently referred to pathogen.There are many animal species for endangering medicinal plant, wherein mainly insect, in addition there is mite class, snail, muroid
Deng.Much belong to pest though having in insect, also has beneficial insect, beneficial insect should be protected, bred and be utilized.Therefore, recognize elder brother
Worm studies insect, grasps pest generation and Fluctuation, for pest control, protects medicinal plant to obtain good quality and high output, has
Significance.
Summary of the invention:
Technical problem to be solved by the present invention lies in provide a kind of insect prevention liquid using arbor-vitae ancient tree branch juice preparation, energy
Enough plant is protected not encroached on by insect pest, while insect prevention liquid environmental pollution is small, secondary pollution will not be caused to environment.
The following technical solution is employed for the technical problems to be solved by the invention to realize:
A kind of insect prevention liquid using arbor-vitae ancient tree branch juice preparation, is made of: arbor-vitae ancient tree branch the raw material of following parts by weight
60-80 parts of juice, 25-30 parts of aqueous areca nut extract, 10-15 parts of Cortex Meliae extractive liquid, 8-10 parts of Cortex hibisus syriacus extracting solution, peppermint oil
20-25 parts, 12-16 parts of lavender oil, 6-8 parts of eucalyptus oil, 2-3 parts of cumyl peroxide, 100-120 parts of ethyl alcohol, hydrogen cyanide
3-5 parts, 11-14 parts of prodan, 3-6 parts of copper sulphate, 5-6 parts of sodium lignin sulfonate, 320-350 parts of deionized water.
The aqueous areca nut extract, Cortex Meliae extractive liquid, Cortex hibisus syriacus extracting solution are the water extractions of betel nut, azedarach, Cortex hibisus syriacus
Liquid.
The extracting method of the arbor-vitae ancient tree branch juice are as follows:
(1) branch for choosing arbor-vitae ancient tree, branch is put into 25-30 DEG C of water and impregnates 2-3h, cuts branch after immersion
2-3cm is grown into, radial full-size is the branch of 2cm, and branch is wrapped up with preservative film, is put into 80 DEG C of saturated vapour pressures and steams
20-30min naturally cools to room temperature, removes preservative film, is put into baking oven and dries, and is ground into powder；
(2) powder is immersed in pretreatment fluid and impregnates 1-1.5h, cleaned 3-4 times after immersion with deionized water, use cold wind
Machine drying；
(3) pretreated powder is put into 15-20 times of powder weight of ethyl alcohol, flow back 2-3h at 80-90 DEG C, returns
Recycling ethyl alcohol is concentrated under reduced pressure after stream, crude product juice is made；
(4) crude product juice and white wine are uniformly mixed according to volume ratio 3:2, are put into reaction kettle and are stood at 105-110 DEG C
2-3h is centrifuged after standing, takes upper layer juice, and arbor-vitae ancient tree branch juice is made.
The pretreatment fluid is made of the raw material of following parts by weight: 50-60 parts of potassium citrate, 8-10 parts of starch, bicarbonate
22-26 parts of sodium, 18-20 parts of calcium hydroxide, 16-20 parts of niacin, 25-30 parts of tert-butylhydroquinone, aliphatic alcohol polyethenoxy
35-45 parts of ether sodium sulfate, 16-18 parts of magnesium silicate.
The pretreatment fluid the preparation method comprises the following steps:
(1) potassium citrate is soluble in water, it is stirred under 150-200r/min revolving speed, and be slowly added in whipping process
Starch is tuned into paste, is then placed in baking oven and bakes 20-25min at 70-80 DEG C；
(2) sodium bicarbonate and calcium hydroxide is added in the mixture prepared to step (1), under 200-250r/min revolving speed
40-50min is stirred, niacin, tert-butylhydroquinone, sodium sulfate of polyethenoxy ether of fatty alcohol and magnesium silicate is added, is transferred to
In ball mill under 400-500r/min revolving speed ball milling 80-100min；
(3) mixture after ball milling is added in ethyl alcohol, the ultrasound 20min at 35-45 DEG C, is put into baking oven after ultrasound
Mixture after drying is added in 40-50 times of mixture weight of deionized water and stirs evenly by 60-70 DEG C of drying, is made pre-
Treatment fluid.
The insect prevention liquid the preparation method comprises the following steps:
(1) ethyl alcohol and deionized water are uniformly mixed, mixed liquor is heated to 35-45 DEG C, in 120-150r/min revolving speed
Lower stirring, is slowly added to hydrogen cyanide, copper sulphate, sodium lignin sulfonate while stirring, continues to stir 20-30min after being added completely into,
Mixed liquor is sealed after stirring, is put into vacuum oven at 50-55 DEG C and stands 2h, is reduced to room temperature after standing；
(2) prodan, cumyl peroxide are added into step (1) treated mixed liquor, in 50-60r/min
10-15min is stirred under revolving speed, surplus stock is added after stirring into mixed liquor, continues to stir 25-30min, insect prevention liquid is made.
The present invention provides a kind of insect prevention liquid using arbor-vitae ancient tree branch juice preparation, it has the advantage that:
(1) with the branch juice of Natural Platycladus orientalis ancient tree after processing is extracted, as insect prevention liquid primary raw material, to a variety of plants
Object have insect prevention, deinsectization effect, cooperation aqueous areca nut extract, Cortex Meliae extractive liquid, Cortex hibisus syriacus extracting solution, hydrogen cyanide, prodan,
The raw materials such as copper sulphate use, and the insect prevention liquid of preparation is while insect prevention, moreover it is possible to kill part pest, and insect prevention liquid itself is to ring
Border pollution it is small, not will cause secondary pollution, compare conventional pesticides, human injury's property is greatly reduced, be suitable for various plants,
The insect prevention management of animal colony house.
(2) it in the extracting method of arbor-vitae ancient tree branch juice, is first soaked in water, increases the moisture of branch, retain the new of branch
Freshness is put into saturated vapour pressure after being wrapped up with preservative film and steams, and while softening branch, increases the maturity of branch, reduces
The acerbity of branch juice, be immersed in pretreatment fluid can make it is fat-soluble in branch separated with water-soluble substances, and soften fine
Tissue is tieed up, keeps plant cell wall thinning, is conducive to postorder juice and efficiently extracts, after extracting juice with alcohol reflux mode,
By juice and white wine reaction kettle high-temperature process, is conducive to activate the activity of flavone compound in juice, tannin, enhances juice
Repellency, reach enhancing vermins-proof effect.
(3) insect prevention liquid and preparation method thereof is simple, and raw material is gradually added, and raw material can be made to be substantially soluble in water and ethyl alcohol, and have
Time enough interaction, forms uniform mixed liquor.
Specific embodiment:
In order to be easy to understand the technical means, the creative features, the aims and the efficiencies achieved by the present invention, tie below
Specific embodiment is closed, the present invention is further explained.
Embodiment 1:
A kind of insect prevention liquid using arbor-vitae ancient tree branch juice preparation, is made of: arbor-vitae ancient tree branch the raw material of following parts by weight
60 parts of juice, 25 parts of aqueous areca nut extract, 10 parts of Cortex Meliae extractive liquid, 8 parts of Cortex hibisus syriacus extracting solution, 20 parts of peppermint oil, lavender oil
12 parts, 6 parts of eucalyptus oil, 2 parts of cumyl peroxide, 100 parts of ethyl alcohol, 3 parts of hydrogen cyanide, 11 parts of prodan, 3 parts of copper sulphate,
5 parts of sodium lignin sulfonate, 320 parts of deionized water.
The aqueous areca nut extract, Cortex Meliae extractive liquid, Cortex hibisus syriacus extracting solution are the water extractions of betel nut, azedarach, Cortex hibisus syriacus
Liquid.
Embodiment 2:
A kind of insect prevention liquid using arbor-vitae ancient tree branch juice preparation, is made of: arbor-vitae ancient tree branch the raw material of following parts by weight
80 parts of juice, 30 parts of aqueous areca nut extract, 15 parts of Cortex Meliae extractive liquid, 10 parts of Cortex hibisus syriacus extracting solution, 25 parts of peppermint oil, lavender oil
16 parts, 8 parts of eucalyptus oil, 3 parts of cumyl peroxide, 120 parts of ethyl alcohol, 5 parts of hydrogen cyanide, 14 parts of prodan, 6 parts of copper sulphate,
6 parts of sodium lignin sulfonate, 350 parts of deionized water.
The aqueous areca nut extract, Cortex Meliae extractive liquid, Cortex hibisus syriacus extracting solution are the water extractions of betel nut, azedarach, Cortex hibisus syriacus
Liquid.
The extracting method of the arbor-vitae ancient tree branch juice are as follows:
(1) branch for choosing arbor-vitae ancient tree, branch is put into 25 DEG C of water and impregnates 2h, grows into branch cutting after immersion
2cm, radial full-size are the branch of 2cm, and branch is wrapped up with preservative film, is put into 80 DEG C of saturated vapour pressures and steams 20min, from
It so is cooled to room temperature, preservative film is removed, is put into baking oven and dries, be ground into powder；
(2) powder is immersed in pretreatment fluid and impregnates 1h, cleaned 3 times after immersion with deionized water, dried up with air-cooler；
(3) pretreated powder is put into 15 times of powder weight of ethyl alcohol, flow back 2h at 80 DEG C, depressurizes after reflux
Crude product juice is made in concentration and recovery ethyl alcohol；
(4) crude product juice and white wine are uniformly mixed according to volume ratio 3:2, are put into reaction kettle in 105 DEG C of standing 2h, it is quiet
Centrifugation is postponed, upper layer juice is taken, arbor-vitae ancient tree branch juice is made.
The pretreatment fluid is made of the raw material of following parts by weight: 50 parts of potassium citrate, 8 parts of starch, 22 parts of sodium bicarbonate,
18 parts of calcium hydroxide, 16 parts of niacin, 25 parts of tert-butylhydroquinone, 35 parts of sodium sulfate of polyethenoxy ether of fatty alcohol, magnesium silicate
16 parts.
The pretreatment fluid the preparation method comprises the following steps:
(1) potassium citrate is soluble in water, it is stirred under 150r/min revolving speed, and starch is slowly added in whipping process
It is tuned into paste, is then placed in baking oven and bakes 20min at 70 DEG C；
(2) sodium bicarbonate and calcium hydroxide is added in the mixture prepared to step (1), is stirred under 200r/min revolving speed
40min adds niacin, tert-butylhydroquinone, sodium sulfate of polyethenoxy ether of fatty alcohol and magnesium silicate, is transferred in ball mill
The ball milling 80min under 400r/min revolving speed；
(3) mixture after ball milling is added in ethyl alcohol, the ultrasound 20min at 35 DEG C, is put into baking oven after ultrasound 60
DEG C drying, mixture after drying is added in 40 times of mixture weight of deionized water and is stirred evenly, pretreatment fluid is made.
Embodiment 3:
A kind of insect prevention liquid using arbor-vitae ancient tree branch juice preparation, is made of: arbor-vitae ancient tree branch the raw material of following parts by weight
70 parts of juice, 27 parts of aqueous areca nut extract, 12 parts of Cortex Meliae extractive liquid, 9 parts of Cortex hibisus syriacus extracting solution, 22 parts of peppermint oil, lavender oil
14 parts, 7 parts of eucalyptus oil, 2 parts of cumyl peroxide, 110 parts of ethyl alcohol, 4 parts of hydrogen cyanide, 12 parts of prodan, 4 parts of copper sulphate,
5 parts of sodium lignin sulfonate, 330 parts of deionized water.
The aqueous areca nut extract, Cortex Meliae extractive liquid, Cortex hibisus syriacus extracting solution are the water extractions of betel nut, azedarach, Cortex hibisus syriacus
Liquid.
The extracting method of the arbor-vitae ancient tree branch juice are as follows:
(1) branch for choosing arbor-vitae ancient tree, branch is put into 30 DEG C of water and impregnates 3h, grows into branch cutting after immersion
3cm, radial full-size are the branch of 2cm, and branch is wrapped up with preservative film, is put into 80 DEG C of saturated vapour pressures and steams 30min, from
It so is cooled to room temperature, preservative film is removed, is put into baking oven and dries, be ground into powder；
(2) powder is immersed in pretreatment fluid and impregnates 1.5h, cleaned 4 times after immersion with deionized water, blown with air-cooler
It is dry；
(3) pretreated powder is put into 20 times of powder weight of ethyl alcohol, flow back 3h at 90 DEG C, depressurizes after reflux
Crude product juice is made in concentration and recovery ethyl alcohol；
(4) crude product juice and white wine are uniformly mixed according to volume ratio 3:2, are put into reaction kettle in 110 DEG C of standing 3h, it is quiet
Centrifugation is postponed, upper layer juice is taken, arbor-vitae ancient tree branch juice is made.
The pretreatment fluid is made of the raw material of following parts by weight: 60 parts of potassium citrate, 10 parts of starch, sodium bicarbonate 26
Part, 20 parts of calcium hydroxide, 20 parts of niacin, 30 parts of tert-butylhydroquinone, 45 parts of sodium sulfate of polyethenoxy ether of fatty alcohol, silicic acid
18 parts of magnesium.
The pretreatment fluid the preparation method comprises the following steps:
(1) potassium citrate is soluble in water, it is stirred under 200r/min revolving speed, and starch is slowly added in whipping process
It is tuned into paste, is then placed in baking oven and bakes 25min at 80 DEG C；
(2) sodium bicarbonate and calcium hydroxide is added in the mixture prepared to step (1), is stirred under 250r/min revolving speed
50min adds niacin, tert-butylhydroquinone, sodium sulfate of polyethenoxy ether of fatty alcohol and magnesium silicate, is transferred in ball mill
The ball milling 100min under 500r/min revolving speed；
(3) mixture after ball milling is added in ethyl alcohol, the ultrasound 20min at 45 DEG C, is put into baking oven after ultrasound 70
DEG C drying, mixture after drying is added in 50 times of mixture weight of deionized water and is stirred evenly, pretreatment fluid is made.
The insect prevention liquid the preparation method comprises the following steps:
(1) ethyl alcohol and deionized water are uniformly mixed, mixed liquor are heated to 35 DEG C, is stirred under 120r/min revolving speed,
It is slowly added to hydrogen cyanide, copper sulphate, sodium lignin sulfonate while stirring, continues to stir 20min after being added completely into, will be mixed after stirring
Liquid sealing is closed, is put into vacuum oven at 50 DEG C and stands 2h, be reduced to room temperature after standing；
(2) prodan, cumyl peroxide are added into step (1) treated mixed liquor, in 50r/min revolving speed
Lower stirring 10min, is added surplus stock into mixed liquor after stirring, continue to stir 25min, insect prevention liquid is made.
Embodiment 4:
A kind of insect prevention liquid using arbor-vitae ancient tree branch juice preparation, is made of: arbor-vitae ancient tree branch the raw material of following parts by weight
75 parts of juice, 28 parts of aqueous areca nut extract, 14 parts of Cortex Meliae extractive liquid, 9 parts of Cortex hibisus syriacus extracting solution, 24 parts of peppermint oil, lavender oil
15 parts, 6 parts of eucalyptus oil, 3 parts of cumyl peroxide, 115 parts of ethyl alcohol, 4 parts of hydrogen cyanide, 13 parts of prodan, 5 parts of copper sulphate,
5 parts of sodium lignin sulfonate, 340 parts of deionized water.
The aqueous areca nut extract, Cortex Meliae extractive liquid, Cortex hibisus syriacus extracting solution are the water extractions of betel nut, azedarach, Cortex hibisus syriacus
Liquid.
The extracting method of the arbor-vitae ancient tree branch juice are as follows:
(1) branch for choosing arbor-vitae ancient tree, branch is put into 25 DEG C of water and impregnates 3h, grows into branch cutting after immersion
3cm, radial full-size are the branch of 2cm, and branch is wrapped up with preservative film, is put into 80 DEG C of saturated vapour pressures and steams 30min, from
It so is cooled to room temperature, preservative film is removed, is put into baking oven and dries, be ground into powder；
(2) powder is immersed in pretreatment fluid and impregnates 1.5h, cleaned 3 times after immersion with deionized water, blown with air-cooler
It is dry；
(3) pretreated powder is put into 18 times of powder weight of ethyl alcohol, flow back 3h at 85 DEG C, depressurizes after reflux
Crude product juice is made in concentration and recovery ethyl alcohol；
(4) crude product juice and white wine are uniformly mixed according to volume ratio 3:2, are put into reaction kettle in 105 DEG C of standing 3h, it is quiet
Centrifugation is postponed, upper layer juice is taken, arbor-vitae ancient tree branch juice is made.
The pretreatment fluid is made of the raw material of following parts by weight: 55 parts of potassium citrate, 9 parts of starch, 24 parts of sodium bicarbonate,
19 parts of calcium hydroxide, 18 parts of niacin, 28 parts of tert-butylhydroquinone, 40 parts of sodium sulfate of polyethenoxy ether of fatty alcohol, magnesium silicate
17 parts.
The pretreatment fluid the preparation method comprises the following steps:
(1) potassium citrate is soluble in water, it is stirred under 180r/min revolving speed, and starch is slowly added in whipping process
It is tuned into paste, is then placed in baking oven and bakes 20min at 75 DEG C；
(2) sodium bicarbonate and calcium hydroxide is added in the mixture prepared to step (1), is stirred under 220r/min revolving speed
45min adds niacin, tert-butylhydroquinone, sodium sulfate of polyethenoxy ether of fatty alcohol and magnesium silicate, is transferred in ball mill
The ball milling 90min under 450r/min revolving speed；
(3) mixture after ball milling is added in ethyl alcohol, the ultrasound 20min at 35 DEG C, is put into baking oven after ultrasound 65
DEG C drying, mixture after drying is added in 45 times of mixture weight of deionized water and is stirred evenly, pretreatment fluid is made.
The insect prevention liquid the preparation method comprises the following steps:
(1) ethyl alcohol and deionized water are uniformly mixed, mixed liquor are heated to 45 DEG C, is stirred under 150r/min revolving speed,
It is slowly added to hydrogen cyanide, copper sulphate, sodium lignin sulfonate while stirring, continues to stir 30min after being added completely into, will be mixed after stirring
Liquid sealing is closed, is put into vacuum oven at 55 DEG C and stands 2h, be reduced to room temperature after standing；
(2) prodan, cumyl peroxide are added into step (1) treated mixed liquor, in 60r/min revolving speed
Lower stirring 15min, is added surplus stock into mixed liquor after stirring, continue to stir 30min, insect prevention liquid is made.
Comparative example:
The raw material and its parts by weight of botanical insect-proof liquid are as follows: 3 portions of lemongrass, 6 portions of Sculellaria barbatas, 4 portions of lavenders, 2 parts of peppermints, 1
Part honeysuckle, 1 part of vitamin B and 20 parts of ethyl alcohol.
Preparation method are as follows: above-mentioned perfume (or spice) is added in lemongrass, Sculellaria barbata, lavender, peppermint and the honeysuckle for weighing above-mentioned deal
3 times of total weight of the water of thatch, Sculellaria barbata, lavender, peppermint and honeysuckle, after ten minutes with high fire infusion, with small fire infusion 20
Minute, filtering takes filtrate, the vitamin B powder of above-mentioned filtrate and above-mentioned deal is added to the ethyl alcohol of above-mentioned deal, is shaken up both
?.
The Malus spectabilis of 50 plants of identical age of trees is divided into 5 groups, every group of the above various embodiments and comparison for being respectively adopted equivalent
The insect prevention liquid of example preparation after 3 months, detects Malus spectabilis disease incidence as caused by pear crown network pentatomidae and black peach aphid, as a result as follows:
| Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Comparative example | |
| Pear crown network pentatomidae disease incidence (%) | 10 | 10 | 0 | 0 | 30 |
| Black peach aphid disease incidence (%) | 0 | 0 | 0 | 0 | 20 |
The above shows and describes the basic principles and main features of the present invention and the advantages of the present invention.The technology of the industry
Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the above embodiments and description only describe this
The principle of invention, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, these changes
Change and improvement all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appended claims and its
Equivalent thereof.
Claims (6)
1. a kind of insect prevention liquid using arbor-vitae ancient tree branch juice preparation, which is characterized in that be made of the raw material of following parts by weight: side
60-80 parts of cypress Gu branch juice, 25-30 parts of aqueous areca nut extract, 10-15 parts of Cortex Meliae extractive liquid, 8-10 parts of Cortex hibisus syriacus extracting solution,
20-25 parts of peppermint oil, 12-16 parts of lavender oil, 6-8 parts of eucalyptus oil, 2-3 parts of cumyl peroxide, 100-120 parts of ethyl alcohol,
3-5 parts of hydrogen cyanide, 11-14 parts of prodan, 3-6 parts of copper sulphate, 5-6 parts of sodium lignin sulfonate, 320-350 parts of deionized water.
2. the insect prevention liquid according to claim 1 using arbor-vitae ancient tree branch juice preparation, which is characterized in that the betel nut mentions
Taking liquid, Cortex Meliae extractive liquid, Cortex hibisus syriacus extracting solution is the aqueous extract of betel nut, azedarach, Cortex hibisus syriacus.
3. the insect prevention liquid according to claim 1 using arbor-vitae ancient tree branch juice preparation, which is characterized in that the arbor-vitae is ancient
The extracting method of branch juice are as follows:
(1) branch for choosing arbor-vitae ancient tree, branch is put into 25-30 DEG C of water and impregnates 2-3h, is cut branch after immersion and is grown up
For 2-3cm, radial full-size is the branch of 2cm, and branch is wrapped up with preservative film, is put into 80 DEG C of saturated vapour pressures and steams 20-
30min naturally cools to room temperature, removes preservative film, is put into baking oven and dries, and is ground into powder；
(2) powder is immersed in pretreatment fluid and impregnates 1-1.5h, cleaned 3-4 times after immersion with deionized water, blown with air-cooler
It is dry；
(3) pretreated powder is put into 15-20 times of powder weight of ethyl alcohol, flow back 2-3h at 80-90 DEG C, after reflux
Recycling ethyl alcohol is concentrated under reduced pressure, crude product juice is made；
(4) crude product juice and white wine are uniformly mixed according to volume ratio 3:2, are put into reaction kettle in 105-110 DEG C of standing 2-3h,
It is centrifuged after standing, takes upper layer juice, arbor-vitae ancient tree branch juice is made.
4. the insect prevention liquid according to claim 3 using arbor-vitae ancient tree branch juice preparation, which is characterized in that the pretreatment
Liquid is made of the raw material of following parts by weight: 50-60 parts of potassium citrate, 8-10 parts of starch, 22-26 parts of sodium bicarbonate, calcium hydroxide
18-20 parts, 16-20 parts of niacin, 25-30 parts of tert-butylhydroquinone, 35-45 parts of sodium sulfate of polyethenoxy ether of fatty alcohol, silicon
Sour magnesium 16-18 parts.
5. the insect prevention liquid according to claim 4 using arbor-vitae ancient tree branch juice preparation, which is characterized in that the pretreatment
Liquid the preparation method comprises the following steps:
(1) potassium citrate is soluble in water, it is stirred under 150-200r/min revolving speed, and starch is slowly added in whipping process
It is tuned into paste, is then placed in baking oven and bakes 20-25min at 70-80 DEG C；
(2) sodium bicarbonate and calcium hydroxide is added in the mixture prepared to step (1), is stirred under 200-250r/min revolving speed
40-50min adds niacin, tert-butylhydroquinone, sodium sulfate of polyethenoxy ether of fatty alcohol and magnesium silicate, is transferred to ball milling
In machine under 400-500r/min revolving speed ball milling 80-100min；
(3) mixture after ball milling is added in ethyl alcohol, the ultrasound 20min at 35-45 DEG C, is put into baking oven after ultrasound in 60-
Mixture after drying is added in 40-50 times of mixture weight of deionized water and stirs evenly, pretreatment is made by 70 DEG C of drying
Liquid.
6. the insect prevention liquid according to claim 1 using arbor-vitae ancient tree branch juice preparation, which is characterized in that the insect prevention liquid
The preparation method comprises the following steps:
(1) ethyl alcohol and deionized water are uniformly mixed, mixed liquor is heated to 35-45 DEG C, stirred under 120-150r/min revolving speed
It mixes, is slowly added to hydrogen cyanide, copper sulphate, sodium lignin sulfonate while stirring, continue to stir 20-30min, stirring after being added completely into
Mixed liquor is sealed afterwards, is put into vacuum oven at 50-55 DEG C and stands 2h, is reduced to room temperature after standing；
(2) prodan, cumyl peroxide are added into step (1) treated mixed liquor, in 50-60r/min revolving speed
Lower stirring 10-15min, is added surplus stock into mixed liquor after stirring, continue to stir 25-30min, insect prevention liquid is made.
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| CN102283254A (en) * | 2010-03-17 | 2011-12-21 | 钟韬 | Plant source environmentally-friendly pesticide preparation |
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| KR20160028103A (en) * | 2014-09-03 | 2016-03-11 | 양철기 | Harmful pest and bacteria repellent and farmland fertiliser and methods for manufacturing the same |
| CN106689233A (en) * | 2016-11-25 | 2017-05-24 | 河池市农业科学研究所 | Organic insect repellant |
| CN107372661A (en) * | 2017-08-09 | 2017-11-24 | 福建小薇金匙科技孵化有限公司 | A kind of biological insecticides for preventing and treating high mountain paddy leaf roll snout moth's larva |
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|---|---|---|---|---|
| CN1152403A (en) * | 1996-10-23 | 1997-06-25 | 赵贵生 | Nontoxic pesticide made of pure traditional Chinese medicine |
| CN102283254A (en) * | 2010-03-17 | 2011-12-21 | 钟韬 | Plant source environmentally-friendly pesticide preparation |
| KR20160028103A (en) * | 2014-09-03 | 2016-03-11 | 양철기 | Harmful pest and bacteria repellent and farmland fertiliser and methods for manufacturing the same |
| CN104322591A (en) * | 2014-10-11 | 2015-02-04 | 赵敬哲 | Tea leaf insecticide and preparation method thereof |
| CN105230674A (en) * | 2015-10-27 | 2016-01-13 | 谷立鹏 | Bactericidal pesticide extracted from biota orientalis and rhubarb root |
| CN106689233A (en) * | 2016-11-25 | 2017-05-24 | 河池市农业科学研究所 | Organic insect repellant |
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