CN109023930A - A kind of heath-function material and its preparation method and application - Google Patents
A kind of heath-function material and its preparation method and application Download PDFInfo
- Publication number
- CN109023930A CN109023930A CN201810955234.XA CN201810955234A CN109023930A CN 109023930 A CN109023930 A CN 109023930A CN 201810955234 A CN201810955234 A CN 201810955234A CN 109023930 A CN109023930 A CN 109023930A
- Authority
- CN
- China
- Prior art keywords
- heath
- cellulose
- capsaicine
- essential oil
- function material
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F2/00—Monocomponent artificial filaments or the like of cellulose or cellulose derivatives; Manufacture thereof
- D01F2/06—Monocomponent artificial filaments or the like of cellulose or cellulose derivatives; Manufacture thereof from viscose
- D01F2/08—Composition of the spinning solution or the bath
- D01F2/10—Addition to the spinning solution or spinning bath of substances which exert their effect equally well in either
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
- D06M2101/06—Vegetal fibres cellulosic
Abstract
The invention discloses a kind of heath-function material, including complex, the complex includes cellulose matrix and the active material compound with the cellulose matrix, and the active material includes capsaicine and remaining active factors；The capsaicine is embedded in the inside and surface of the cellulose matrix, and the rest activity factor includes being sequentially distributed the tea oil in cellulose matrix outer layer, Peppermint essential oil and chamomile essential oil from inside to outside.The present invention also provides the preparation method and application of above-mentioned heath-function material.Heath-function material prepared by the present invention has the function of warming fever, bactericidal antiphlogistic.
Description
Technical field
The present invention relates to exothermic material technical fields, and in particular to a kind of heath-function material and preparation method thereof and answers
With.
Background technique
Cellulose is the most abundant natural polymer of content in nature, has renewable, degradable, biocompatibility etc.
Advantage.In recent years, it with the reduction of oil content, is had attracted more and more attention from people using material prepared by renewable resource.
Present cellulose is mainly used for the big industry of textile and paper two, and use cellulose as film made from raw material, fiber and other material all
With porous structure, aperture is mostly micron order, therefore has good mechanical property.
Capsaicine is the active constituent in capsicum, it includes that the mankind are irritant and can be in the oral cavity to mammal
Generate burning sensation.In addition, capsaicine has very strong anti-obesity activity, lipolysis can be promoted, heat is promoted to generate.It can
To be had an impact to a kind of muscle protein for being SERCA, it is generally the case that SERCA consume ATP (a kind of molecule fuel) by calcium from
Sub " pump " cell membrane (on calcium channel), this facilitates contracted muscle diastole and loosens.But the increase of capsaicine
Calcium channel can be closed, the ATP for causing SERCA to consume can only be discharged in the form of heat, and here it is so-called themogenesises.
Therefore it can use the heating function of capsaicine to prepare corresponding material, and cellulose is as common basis material, it can be with
The many materials such as hydrogel, aeroge, film, fiber are prepared by dissolving the regeneration of obtained cellulose solution, it not only can be with
The heath-function for playing capsaicine, can also improve the mechanical performance of material.Application No. is 20112054282.6 Chinese inventions
Patent application is placed in slippers using far-infared ceramic powder, magnetite, capsaicine as heater, may be used as warming drag
Shoes.But it can gradually weaken calorific intensity at any time, and application range is relatively narrow.Application No. is the China of CN20111002156.5
By capsaicine, surfactant in application for a patent for invention, emulsion is made in chitosan etc., is then protected by the method impregnated
Health-care function fabric.Its shortcomings that, is it is clear that method due to using dipping, capsaicine etc. are only distributed in fabric
Surface does not have stability, cannot reuse after wash.
Summary of the invention
In view of this, the purpose of the present invention is to provide a kind of heath-function materials and its preparation method and application.
In order to achieve the above purpose, described compound the present invention provides a kind of heath-function material, including complex
Body includes cellulose matrix and the active material compound with the cellulose matrix, the active material include capsaicine and remaining
Active factors；The capsaicine be embedded in the cellulose matrix inside and surface, the rest activity factor include from it is interior to
It is sequentially distributed the tea oil in cellulose matrix outer layer, Peppermint essential oil and chamomile essential oil outside.
Further, wherein the outer layer with a thickness of 50nm-2000nm, the functionality and physical and chemical performance of compound material,
Preferably 200-800nm.
Further, wherein the form of the heath-function material includes fiber, film or non-woven fabrics.
Further, wherein the heath-function material, by weight percentage, including following each component:
Capsaicine 0.01-10wt%；Tea oil 0.01-0.3wt%；Peppermint essential oil 0.01-0.05wt%；Chamomile essential oil
0.01-0.4wt%；Surplus is cellulose, film or non-woven fabrics.
Further, wherein the heath-function material, by weight percentage, including following each component:
Capsaicine 0.3-5wt%；Tea oil 0.1-0.25wt%；Peppermint essential oil 0.02-0.03wt%；Chamomile essential oil
0.02-0.3wt%；Surplus is cellulose.
Further, wherein the capsaicine is selected from capsaicine, dihydrocapsaicin, homocapsaicin, homodihydrocapsaicin, drop
At least one of capsaicine, nordihydrocapsaicin, decoyl vanillylamide, nonoyl vanillylamide, caprinoyl vanilla amine；It is described peppery
Green pepper element is by naturally extracting to obtain or artificial synthesized obtain.
Further, wherein the cellulose is made by cellulose cotton pulp, bamboo pulp or jute pulp；The methyl of the cellulose is fine
It ties up cellulose content and is greater than 80wt%, degree of polymerization 200-1000.
The present invention also provides the preparation methods of above-mentioned heath-function material, comprising the following steps:
Capsaicine is added in dissolved cellulose solution, not similar shape is then prepared by solidification-regeneration
The cellulose substrate material of formula；Tea oil, Peppermint essential oil and chamomile essential oil are successively introduced by way of oiling later, i.e.,
?.
Further, wherein the solidification-regeneration includes at least one in wet spinning, casting film-forming or spun lacing
Kind.
Invention further provides a kind of textiles, including above-mentioned heath-function material.
Invention further provides a kind of medical products, including above-mentioned heath-function material.
The present invention has the advantages that
1, heath-function material provided by the present invention has porous structure, biocompatibility and good mechanics
Performance, the porous structure can help capsaicine to disperse and stablize, and still have preferable hair after repeatedly washing experiment test
Hot property, and the tea oil of outer layer, Peppermint essential oil, chamomile essential oil can not only play the role of slowing down the stimulation of capsaicine, also
It can have the function that bactericidal antiphlogistic, loosen calmness.
2, heath-function material provided by the present invention, warming heating principle is different from common physics gimmick, main
The complex stimulus process to be generated by the capsaicine of slow release to body, when use, need to can only produce with direct body contact
Heat effect, exothermic material is with good stability, using after 100-200 times still have apparent heating effect.
3, the preparation method of heath-function material provided by the present invention, by cellulose dissolution process or molten
It is added in solution after solution, to achieve the purpose that capsaicine slow release；Tea oil, Peppermint essential oil, chamomile essential oil pass through
The surface post processing mode of material is added, and the purpose of stimulation is generated to slow down capsaicine to the organism of contact.
Specific embodiment
The present invention provides one kind to have heath-function material, illustrates specific embodiment party below with specific embodiment
Formula, it should be understood that the specific embodiments described herein are merely illustrative of the present invention, is not intended to limit the present invention.
Embodiment 1
A kind of heath-function fibrous material, including complex, the complex include cellulose matrix and with the fibre
The active material of plain matrix composite is tieed up, the active material includes capsaicine and remaining active factors；The capsaicine is embedded in institute
The inside and surface of cellulose matrix are stated, the rest activity factor includes being sequentially distributed from inside to outside in cellulose matrix outer layer
Tea oil, Peppermint essential oil and the chamomile essential oil of (50nm)；Dissolved cellulose solution (the cellulose is added in capsaicine
Solution is the prezenta solution of 8wt%, and prezenta solution is adopted and prepared with method known in this field, herein no longer
Repeat) in, cellulose substrate material is then prepared by wet spinning technology；Tea oil, Peppermint essential oil and ocean later
Camomile essential oil successively introduced by way of oiling to get；By weight percentage, the heath-function fibrous material contains
The cellulose of 99.96wt%, the capsaicine of 0.01wt%, the tea oil of 0.01wt%, the Peppermint essential oil of 0.01wt%,
The chamomile essential oil of 0.01wt%；The strength of materials of the heath-function fibrous material is 3.0cN/dtex, elongation at break
It is 18%.There is heath-function fibrous material to wash described with the sodium dodecyl sulfate solution of 2wt%, washs
When number is 200 times, there is 95% or more of former heath-function.The heath-function fibrous material to Escherichia coli with
And the killing rate of staphylococcus aureus is 100%.
Embodiment 2
A kind of heath-function membrane material, including complex, the complex include cellulose matrix and with the fiber
The active material of plain matrix composite, the active material include capsaicine and remaining active factors；The capsaicine is embedded in described
The inside and surface of cellulose matrix, the rest activity factor include being sequentially distributed from inside to outside in cellulose matrix outer layer
Tea oil, Peppermint essential oil and the chamomile essential oil of (500nm)；Dissolved cellulose solution (the fiber is added in capsaicine
Plain solution is the prezenta solution of 8wt%, and prezenta solution is adopted and prepared with method known in this field, herein not
Repeat again) in, cellulose substrate material (film) is then prepared by casting film-forming technique；Tea oil, Peppermint essential oil later
And chamomile essential oil successively introduced by way of oiling to get；By weight percentage, the heath-function undulation degree
Cellulose of the material containing 99.08wt%, the capsaicine of 0.8wt%, the tea oil of 0.05wt%, the Peppermint essential oil of 0.03wt%,
The chamomile essential oil of 0.04wt%；The strength of materials of the heath-function fibrous material is 70Mpa, and elongation at break is
15%.There is heath-function material to wash described with the sodium dodecyl sulfate solution of 2wt%, washing times are
At 200 times, there is 95% or more of former heath-function.The heath-function membrane material is to Escherichia coli and golden yellow
Staphylococcic killing rate is 100%.
Embodiment 3
A kind of heath-function nonwoven cloth material, including complex, the complex include cellulose matrix and with it is described
The compound active material of cellulose matrix, the active material include capsaicine and remaining active factors；The capsaicine is embedded in
The inside and surface of the cellulose matrix, the rest activity factor include being sequentially distributed outside cellulose matrix from inside to outside
Tea oil, Peppermint essential oil and the chamomile essential oil of layer (2000nm)；Dissolved cellulose solution (the fibre is added in capsaicine
The prezenta solution that plain solution is 8wt% is tieed up, and prezenta solution is adopted and is prepared with method known in this field, herein
Repeat no more) in, cellulose substrate material (non-woven fabrics) is then prepared by water jet process；Tea oil, peppermint essence later
Oil and chamomile essential oil successively introduced by way of oiling to get；By weight percentage, the heath-function fiber
Material contains the cellulose of 98.55wt%, the capsaicine of 1.2wt%, the tea oil of 0.1wt%, the Peppermint essential oil of 0.05wt%,
The chamomile essential oil of 0.1wt%；The strength of materials of the heath-function fibrous material is 50Mpa, elongation at break 18%.With
The sodium dodecyl sulfate solution of 2wt% there is heath-function material to wash described, and washing times are 250 times
When, there is 95% or more of former heath-function.The heath-function nonwoven cloth material is to Escherichia coli and golden yellow
Staphylococcic killing rate is 100%.
Embodiment 4
A kind of heath-function fibrous material, including complex, the complex include cellulose matrix and with the fibre
The active material of plain matrix composite is tieed up, the active material includes capsaicine and remaining active factors；The capsaicine is embedded in institute
The inside and surface of cellulose matrix are stated, the rest activity factor includes being sequentially distributed from inside to outside in cellulose matrix outer layer
Tea oil, Peppermint essential oil and the chamomile essential oil of (800nm)；Dissolved cellulose solution (the fiber is added in capsaicine
Plain solution is the prezenta solution of 8wt%, and prezenta solution is adopted and prepared with method known in this field, herein not
Repeat again) in, cellulose substrate material (fiber) is then prepared by wet spinning technology；Tea oil, peppermint essence later
Oil and chamomile essential oil successively introduced by way of oiling to get；By weight percentage, the heath-function fiber
Material contains the cellulose of 97.77wt%, the capsaicine of 1.5wt%, the tea oil of 0.3wt%, the Peppermint essential oil of 0.03wt%,
The chamomile essential oil of 0.4wt%；The strength of materials of the heath-function fibrous material is 2.5cN/dtex, and elongation at break is
15%.There is heath-function material to wash described with the sodium dodecyl sulfate solution of 2wt%, washing times are
At 300 times, there is 95% or more of former heath-function.The heath-function fibrous material is to Escherichia coli and golden yellow
The staphylococcic killing rate of color is 100%.
Embodiment 5
A kind of heath-function membrane material, including complex, the complex include cellulose matrix and with the fiber
The active material of plain matrix composite, the active material include capsaicine and remaining active factors；The capsaicine is embedded in described
The inside and surface of cellulose matrix, the rest activity factor include being sequentially distributed from inside to outside in cellulose matrix outer layer
Tea oil, Peppermint essential oil and the chamomile essential oil of (1000nm)；Dissolved cellulose solution (the fiber is added in capsaicine
Plain solution is the prezenta solution of 8wt%, and prezenta solution is adopted and prepared with method known in this field, herein not
Repeat again) in, cellulose substrate material (film) is then prepared by casting film-forming technique；Tea oil, Peppermint essential oil later
And chamomile essential oil successively introduced by way of oiling to get；By weight percentage, the heath-function undulation degree
Expect the cellulose containing 97.67wt%, the capsaicine of 1.8wt%, tea oil 0.2wt%, Peppermint essential oil 0.03wt%, chamomile
Essential oil 0.3wt%；The strength of materials of the heath-function fibrous material is 70Mpa, elongation at break 13%.Use 2wt%
Sodium dodecyl sulfate solution to described there is heath-function material to wash, when washing times are 270 times, have
95% or more of former heath-function.The heath-function membrane material kills Escherichia coli and staphylococcus aureus
Rate of going out is 100%.
Embodiment 6
A kind of heath-function nonwoven cloth material includes complex, the complex include cellulose matrix and with the fibre
The active material of plain matrix composite is tieed up, the active material includes capsaicine and remaining active factors；The capsaicine is embedded in institute
The inside and surface of cellulose matrix are stated, the rest activity factor includes being sequentially distributed from inside to outside in cellulose matrix outer layer
Tea oil, Peppermint essential oil and the chamomile essential oil of (700nm)；Dissolved cellulose solution (the fiber is added in capsaicine
Plain solution is the prezenta solution of 8wt%, and prezenta solution is adopted and prepared with method known in this field, herein not
Repeat again) in, cellulose substrate material (non-woven fabrics) is then prepared by water jet process；Tea oil, Peppermint essential oil later
And chamomile essential oil successively introduced by way of oiling to get；By weight percentage, the heath-function undulation degree
Cellulose of the material containing 97.55wt%, the capsaicine of 2wt%, the tea oil of 0.1wt%, the Peppermint essential oil of 0.05wt%,
The chamomile essential oil of 0.3wt%；The strength of materials of the heath-function fibrous material is 80Mpa, elongation at break 10%.
There is heath-function material to wash described with the sodium dodecyl sulfate solution of 2wt%, washing times are 40 times
When, there is 95% or more of former heath-function.The heath-function nonwoven cloth material is to Escherichia coli and golden yellow
Staphylococcic killing rate is 100%.
Claims (10)
1. a kind of heath-function material, which is characterized in that including complex, the complex include cellulose matrix and with institute
The compound active material of cellulose matrix is stated, the active material includes capsaicine and remaining active factors；The capsaicine is embedding
In the inside and surface of the cellulose matrix, the rest activity factor includes being sequentially distributed from inside to outside in cellulose matrix
Tea oil, Peppermint essential oil and the chamomile essential oil of outer layer.
2. heath-function material according to claim 1, which is characterized in that the outer layer with a thickness of 50nm-
2000nm, the form of the heath-function material include fiber, film or non-woven fabrics.
3. heath-function material according to claim 1, which is characterized in that by weight percentage, including it is following each
Component:
Capsaicine 0.01-10wt%；Tea oil 0.01-0.3wt%；Peppermint essential oil 0.01-0.05wt%；Chamomile essential oil
0.01-0.4wt%；Surplus is cellulose, film or non-woven fabrics.
4. heath-function material according to claim 3, which is characterized in that by weight percentage, including it is following each
Component:
Capsaicine 0.3-5wt%；Tea oil 0.1-0.25wt%；Peppermint essential oil 0.02-0.03wt%；Chamomile essential oil 0.02-
0.3wt%；Surplus is cellulose.
5. heath-function material according to claim 4, it is characterised in that: the capsaicine is selected from capsaicine, dihydro
Capsaicine, homocapsaicin, homodihydrocapsaicin, drop capsaicine, nordihydrocapsaicin, decoyl vanillylamide, nonoyl vanillylamide,
At least one of caprinoyl vanilla amine；The capsaicine is by naturally extracting to obtain or artificial synthesized obtain.
6. heath-function material according to claim 4, which is characterized in that the cellulose is by cellulose cotton pulp, bamboo
Slurry or jute pulp are made；The Methyl cellulose cellulose content of the cellulose is greater than 80wt%, degree of polymerization 200-1000.
7. a kind of preparation method of heath-function material described in any one of claims 1-6, which is characterized in that including following
Step:
Capsaicine is added in dissolved cellulose solution, is then prepared by solidification-regeneration various forms of
Cellulose substrate material；Later tea oil, Peppermint essential oil and chamomile essential oil successively introduced by way of oiling to get.
8. preparation method according to claim 7, which is characterized in that the solidification-regeneration includes wet spinning, stream
Prolong at least one of film forming or spun lacing.
9. a kind of textile, which is characterized in that including heath-function material described in any one of claims 1-6.
10. a kind of medical products, which is characterized in that including heath-function material described in any one of claims 1-6.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201810955234.XA CN109023930A (en) | 2018-08-21 | 2018-08-21 | A kind of heath-function material and its preparation method and application |
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| CN109023930A true CN109023930A (en) | 2018-12-18 |
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| CN110318255A (en) * | 2019-07-10 | 2019-10-11 | 桐庐雷泰生物科技有限公司 | A kind of spinning oil and its preparation method and application containing capsaicine |
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Application publication date: 20181218 |
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| RJ01 | Rejection of invention patent application after publication |