CN108999051A - A kind of waterproof material of resisting sea water erosion - Google Patents
A kind of waterproof material of resisting sea water erosion Download PDFInfo
- Publication number
- CN108999051A CN108999051A CN201810913065.3A CN201810913065A CN108999051A CN 108999051 A CN108999051 A CN 108999051A CN 201810913065 A CN201810913065 A CN 201810913065A CN 108999051 A CN108999051 A CN 108999051A
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- glass
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- composite
- cotton
- sea water
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Classifications
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- E—FIXED CONSTRUCTIONS
- E01—CONSTRUCTION OF ROADS, RAILWAYS, OR BRIDGES
- E01C—CONSTRUCTION OF, OR SURFACES FOR, ROADS, SPORTS GROUNDS, OR THE LIKE; MACHINES OR AUXILIARY TOOLS FOR CONSTRUCTION OR REPAIR
- E01C7/00—Coherent pavings made in situ
- E01C7/08—Coherent pavings made in situ made of road-metal and binders
- E01C7/32—Coherent pavings made in situ made of road-metal and binders of courses of different kind made in situ
-
- E—FIXED CONSTRUCTIONS
- E01—CONSTRUCTION OF ROADS, RAILWAYS, OR BRIDGES
- E01C—CONSTRUCTION OF, OR SURFACES FOR, ROADS, SPORTS GROUNDS, OR THE LIKE; MACHINES OR AUXILIARY TOOLS FOR CONSTRUCTION OR REPAIR
- E01C7/00—Coherent pavings made in situ
- E01C7/08—Coherent pavings made in situ made of road-metal and binders
- E01C7/35—Toppings or surface dressings; Methods of mixing, impregnating, or spreading them
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- Engineering & Computer Science (AREA)
- Architecture (AREA)
- Civil Engineering (AREA)
- Structural Engineering (AREA)
- Paints Or Removers (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
Abstract
The invention discloses a kind of waterproof materials of resisting sea water erosion, successively include from inside to outside, the bitumen layer and polyester film of tire base, dip-coating on tire base, and the tire base is graphene composite superfine glass fibre cotton.The material is magnetic oxygenated graphene nanometer composite composite superfine glass fibre, has extraordinary sea water corrosion resistant, while the bitumen layer of collaborative configuration is added, can play the effect of permanent seawater corrosion resistance；In the preparation process of graphene composite superfine glass fibre cotton, in order to achieve the effect that industrialized production, a small amount of Fe is added in ultra-fine fibre glass2O3And using the magnetism of magnetic oxygenated graphene nanometer composite, the additional amount for the magnetic oxygenated graphene nanometer composite for reaching extraordinary composite effect and efficiency, while also reducing is reduced costs；The present invention also has adjusted the additional amount of 10# pitch, it is therefore an objective to the hardness of bitumen layer is improved, to improve the composite effect with tire base.
Description
Technical field
The present invention relates to pavement technique field more particularly to a kind of waterproof materials of resisting sea water erosion.
Background technique
Asphalt water-proof coiled material, which refers to, dispenses roll made of abherent etc. with asphalt material, tire material and surface, again
Claim malthoid.It is usually used in posted waterproof layer.Asphalt water-proof coiled material has referred to tire coiled material and Padless coiled material.It is all to use ground paper or glass
The tires material such as glass silk cloth, asbestos cloth, linen-cotton fabric impregnate weblike material made of asphalt, are known as having tire coiled material；By asbestos, rubber
Rubber powder etc. mixes in asphalt material, is rolled manufactured weblike material and is known as roll-in coiled material i.e. Padless coiled material.Asphalt water-proof coiled material
At low cost, tensile strength and elongation percentage are low, and temperature stability is poor, and high temperature easily trickles, fragile under low temperature to split；Resistance to ag(e)ing is poor, makes
It is short with the time limit, belong to low-grade waterproof roll.
In order to expand the application range of asphalt water-proof coiled material, the present invention provides a kind of waterproof materials of resisting sea water erosion.
Summary of the invention
Technical problems based on background technology, the invention proposes a kind of waterproof material of resisting sea water erosion and its systems
Preparation Method.
Technical scheme is as follows:
A kind of waterproof material of resisting sea water erosion successively includes from inside to outside, bitumen layer on tire base of tire base, dip-coating and
Polyester film, the tire base are graphene composite superfine glass fibre cotton.
Preferably, the preparation method of the graphene composite superfine glass fibre cotton, comprising the following steps:
A, binder solution uniform atomizing is sprayed at ultra-fine fibre glass surface；And be dispersed on forming net, it dries
It is drying at ultra-fine fibre glass cotton；
B, on a pet film by the absorption of ultra-fine fibre glass cotton；
C, it by after magnetic oxygenated graphene nanometer composite high speed dispersion, suspends in deionized water；
D, PET film is integrally immersed in the deionized water in step C, 5-8s takes out, and it is super to obtain magnetic oxygenated graphene-
Thin glass fiber cotton-PET film composite construction；
E, by graphene film-ultra-fine fibre glass cotton-PET film composite construction clear water repeated flushing, then PET film is shelled
From obtaining graphene composite superfine glass fibre cotton.
Preferably, in the step A, ultra-fine fibre glass diameter is 0.1-1 μm.
Preferably, in the step A, mass fraction is added in traditional ultra-fine fibre glass in ultra-fine fibre glass
For the Fe of 0.5-2%2O3。
The formula of traditional ultra-fine fibre glass refers to Chinese invention patent CN107012585, ultra-fine alkali-free glass
The formula in claim 1 in glass cellucotton and preparation method thereof.
The preparation method of the magnetic oxygenated graphene nanometer composite refers to Chinese invention patent CN103947675A,
Method for claim 3 in a kind of magnetic oxygenated graphene nanometer composite and its preparation method and application.
Preferably, the bitumen layer consists of the following components in percentage by weight: including following component: 90# pitch 18-
25%, 10# pitch 20-25%, machine oil 10-15%, dispersing agent 1-2%, rubber powder 5-8%, SBS 5-10%, SBR 2-5%, fill out
Expect surplus.
Usefulness of the present invention:
1, the waterproof material of resisting sea water erosion of the invention is with the main distinction of traditional waterproof material, uses
Tire base is graphene composite superfine glass fibre cotton；The material is magnetic oxygenated graphene nanometer composite composite superfine glass fibers
Dimension has extraordinary sea water corrosion resistant, while the bitumen layer of collaborative configuration is added, and can play permanent seawater corrosion resistance
Effect；
2, in the preparation process of graphene composite superfine glass fibre cotton, in order to achieve the effect that industrialized production,
A small amount of Fe is added in ultra-fine fibre glass2O3And using the magnetism of magnetic oxygenated graphene nanometer composite, reach extraordinary
Composite effect and efficiency, while the additional amount of the magnetic oxygenated graphene nanometer composite also reduced, reduce costs；
3, the difference of bitumen layer of the invention and traditional bitumen layer essentially consists in, and the additional amount of 10# pitch reaches 20-
25%, it is therefore an objective to the hardness of bitumen layer is improved, to improve the composite effect with tire base, if additional amount is very little, bitumen layer
Mobile performance is very good, will receive influence in conjunction with effect.
Specific embodiment
Embodiment 1:
A kind of waterproof material of resisting sea water erosion successively includes from inside to outside, bitumen layer on tire base of tire base, dip-coating and
Polyester film, the tire base are graphene composite superfine glass fibre cotton.
The preparation method of the graphene composite superfine glass fibre cotton, comprising the following steps:
A, binder solution uniform atomizing is sprayed at ultra-fine fibre glass surface；And be dispersed on forming net, it dries
It is drying at ultra-fine fibre glass cotton；
B, on a pet film by the absorption of ultra-fine fibre glass cotton；
C, it by after magnetic oxygenated graphene nanometer composite high speed dispersion, suspends in deionized water；
D, PET film is integrally immersed in the deionized water in step C, 6s takes out, and it is ultra-fine to obtain magnetic oxygenated graphene-
Glass fibre cotton-PET film composite construction；
E, by graphene film-ultra-fine fibre glass cotton-PET film composite construction clear water repeated flushing, then PET film is shelled
From obtaining graphene composite superfine glass fibre cotton.
In the step A, ultra-fine fibre glass diameter is 0.1-1 μm.
It is 0.8% that mass fraction is added in traditional ultra-fine fibre glass in the step A, in ultra-fine fibre glass
Fe2O3。
The formula of traditional ultra-fine fibre glass refers to Chinese invention patent CN107012585, ultra-fine alkali-free glass
The formula in claim 1 in glass cellucotton and preparation method thereof.
The preparation method of the magnetic oxygenated graphene nanometer composite refers to Chinese invention patent CN103947675A,
Method for claim 3 in a kind of magnetic oxygenated graphene nanometer composite and its preparation method and application.
The bitumen layer consists of the following components in percentage by weight: including following component: 90# pitch 22%, 10# drip
Green 22%, machine oil 12%, dispersing agent 1.5%, rubber powder 6%, SBS 8%, SBR 3%, filler surplus.
Embodiment 2:
A kind of waterproof material of resisting sea water erosion successively includes from inside to outside, bitumen layer on tire base of tire base, dip-coating and
Polyester film, the tire base are graphene composite superfine glass fibre cotton.
The preparation method of the graphene composite superfine glass fibre cotton, comprising the following steps:
A, binder solution uniform atomizing is sprayed at ultra-fine fibre glass surface；And be dispersed on forming net, it dries
It is drying at ultra-fine fibre glass cotton；
B, on a pet film by the absorption of ultra-fine fibre glass cotton；
C, it by after magnetic oxygenated graphene nanometer composite high speed dispersion, suspends in deionized water；
D, PET film is integrally immersed in the deionized water in step C, 8s takes out, and it is ultra-fine to obtain magnetic oxygenated graphene-
Glass fibre cotton-PET film composite construction；
E, by graphene film-ultra-fine fibre glass cotton-PET film composite construction clear water repeated flushing, then PET film is shelled
From obtaining graphene composite superfine glass fibre cotton.
In the step A, ultra-fine fibre glass diameter is 0.1-1 μm.
It is 0.5% that mass fraction is added in traditional ultra-fine fibre glass in the step A, in ultra-fine fibre glass
Fe2O3。
The formula of traditional ultra-fine fibre glass refers to Chinese invention patent CN107012585, ultra-fine alkali-free glass
The formula in claim 1 in glass cellucotton and preparation method thereof.
The preparation method of the magnetic oxygenated graphene nanometer composite refers to Chinese invention patent CN103947675A,
Method for claim 3 in a kind of magnetic oxygenated graphene nanometer composite and its preparation method and application.
The bitumen layer consists of the following components in percentage by weight: including following component: 90# pitch 25%, 10# drip
Green 20%, machine oil 15%, dispersing agent 1%, rubber powder 8%, SBS 5%, SBR 5%, filler surplus.
Embodiment 3:
A kind of waterproof material of resisting sea water erosion successively includes from inside to outside, bitumen layer on tire base of tire base, dip-coating and
Polyester film, the tire base are graphene composite superfine glass fibre cotton.
The preparation method of the graphene composite superfine glass fibre cotton, comprising the following steps:
A, binder solution uniform atomizing is sprayed at ultra-fine fibre glass surface；And be dispersed on forming net, it dries
It is drying at ultra-fine fibre glass cotton；
B, on a pet film by the absorption of ultra-fine fibre glass cotton；
C, it by after magnetic oxygenated graphene nanometer composite high speed dispersion, suspends in deionized water；
D, PET film is integrally immersed in the deionized water in step C, 5s takes out, and it is ultra-fine to obtain magnetic oxygenated graphene-
Glass fibre cotton-PET film composite construction；
E, by graphene film-ultra-fine fibre glass cotton-PET film composite construction clear water repeated flushing, then PET film is shelled
From obtaining graphene composite superfine glass fibre cotton.
In the step A, ultra-fine fibre glass diameter is 0.1-1 μm.
It is 2% that mass fraction is added in traditional ultra-fine fibre glass in the step A, in ultra-fine fibre glass
Fe2O3。
The formula of traditional ultra-fine fibre glass refers to Chinese invention patent CN107012585, ultra-fine alkali-free glass
The formula in claim 1 in glass cellucotton and preparation method thereof.
The preparation method of the magnetic oxygenated graphene nanometer composite refers to Chinese invention patent CN103947675A,
Method for claim 3 in a kind of magnetic oxygenated graphene nanometer composite and its preparation method and application.
The bitumen layer consists of the following components in percentage by weight: including following component: 90# pitch 18%, 10# drip
Green 25%, machine oil 10%, dispersing agent 2%, rubber powder 5%, SBS 10%, SBR 2%, filler surplus.
Test 1: the sample of embodiment 1-3 is tested；
Test result shows that indices meet I type index of adhesive waterproof coil PY class in GB/T23457-2009.
Comparative example 1
Tire base in embodiment 1 is replaced with to conventional ultra-fine fibre glass cotton, remaining proportion is constant.
Comparative example 2
The content of 10# pitch in bitumen layer in embodiment 1 is reduced to 5%, remaining proportion is constant.
Test 2: by the waterproof material of each embodiment and comparative example, it is fitted in the concrete test block surface (comparison of 1m × 1m
Example is not bonded waterproof material), with a thickness of 50mm；Test block is put into the testing cassete of 1m × 1m, pouring into seawater, (real sea water takes
From Tianjin) in, the fresh seawater of replacement in every 1 month, taking out after 24 months (note that in test, seawater can not be contacted directly
Concrete test block).It is flat to Water soluble chloride ion at the compression strength of concrete test block, flexural strength, 2-2.5 centimetres of penetration depth
Equal mass fraction；It is investigated.Test result is shown in Table 1.
Table 1: sea water resistance test data
| Compression strength (MPa) | Flexural strength (Mpa) | Chloride ion average mass fraction % | |
| Before test | 48.5 | 6.7 | It is not detected |
| Embodiment 1 | 48.5 | 6.7 | It is not detected |
| Embodiment 2 | 48.5 | 6.7 | It is not detected |
| Embodiment 3 | 48.5 | 6.7 | It is not detected |
| Comparative example 1 | 24.2 | 2.7 | 0.311 |
| Comparative example 2 | 38.1 | 5.8 | 0.187 |
| Reference examples | 12.7 | 1.2 | 0.522 |
By the above test data it is recognised that the waterproof material of seawater corrosion resistance of the invention have to the salinity in seawater it is non-
Often good anticorrosion effect, has extraordinary protective effect to the concrete below waterproof material.
The foregoing is only a preferred embodiment of the present invention, but scope of protection of the present invention is not limited thereto,
Anyone skilled in the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention and its
Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.
Claims (5)
1. a kind of waterproof material of resisting sea water erosion, which is characterized in that from inside to outside successively include that tire base, dip-coating are on tire base
Bitumen layer and polyester film, the tire base be graphene composite superfine glass fibre cotton.
2. the waterproof material of resisting sea water erosion as described in claim 1, which is characterized in that the graphene composite superfine glass
The preparation method of glass cellucotton, comprising the following steps:
A, binder solution uniform atomizing is sprayed at ultra-fine fibre glass surface；And it is dispersed on forming net, drying system
At ultra-fine fibre glass cotton；
B, on a pet film by the absorption of ultra-fine fibre glass cotton；
C, it by after magnetic oxygenated graphene nanometer composite high speed dispersion, suspends in deionized water；
D, PET film is integrally immersed in the deionized water in step C, 5-8s takes out, and obtains the ultra-fine glass of magnetic oxygenated graphene-
Glass cellucotton-PET film composite construction；
E, by graphene film-ultra-fine fibre glass cotton-PET film composite construction clear water repeated flushing, then PET film is removed,
Obtain graphene composite superfine glass fibre cotton.
3. the waterproof material of resisting sea water erosion as claimed in claim 2, which is characterized in that in the step A, superfine glass
Fibre diameter is 0.1-1 μm.
4. the waterproof material of resisting sea water erosion as claimed in claim 2, which is characterized in that in the step A, superfine glass
The Fe that mass fraction is 0.5-2% is added in fiber in traditional ultra-fine fibre glass2O3。
5. the waterproof material of resisting sea water erosion as described in claim 1, which is characterized in that the bitumen layer is by following weight
The group of percentage is grouped as: including following component: 90# pitch 18-25%, 10# pitch 20-25%, machine oil 10-15%, dividing
Powder 1-2%, rubber powder 5-8%, SBS 5-10%, SBR 2-5%, filler surplus.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810913065.3A CN108999051B (en) | 2018-08-10 | 2018-08-10 | Seawater erosion resistant waterproof material |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810913065.3A CN108999051B (en) | 2018-08-10 | 2018-08-10 | Seawater erosion resistant waterproof material |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN108999051A true CN108999051A (en) | 2018-12-14 |
| CN108999051B CN108999051B (en) | 2020-10-16 |
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ID=64596333
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810913065.3A Active CN108999051B (en) | 2018-08-10 | 2018-08-10 | Seawater erosion resistant waterproof material |
Country Status (1)
| Country | Link |
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| CN (1) | CN108999051B (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112300588A (en) * | 2020-11-12 | 2021-02-02 | 吴菊 | Preparation method of asphalt applied to coastal high-grade highway |
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|---|---|---|---|---|
| CN201121384Y (en) * | 2007-06-01 | 2008-09-24 | 潍坊市宏源防水材料有限公司 | Elastic modified asphalt waterproof coiled material |
| CN103408955A (en) * | 2013-08-14 | 2013-11-27 | 河南省华瑞防水防腐有限公司 | Waterproof coiled material and production method thereof |
| CN103947675A (en) * | 2014-04-11 | 2014-07-30 | 湖南大学 | Magnetic graphene oxide nanometer compound, preparation method and application thereof |
| CN106223549A (en) * | 2016-08-04 | 2016-12-14 | 合肥中科富华新材料有限公司 | A kind of high fire-retardance waterproof roll |
| CN106854343A (en) * | 2017-01-12 | 2017-06-16 | 四川航天五源复合材料有限公司 | Basalt fibre mixes reinforced resin and preparation method thereof, application with glass fibre |
| CN107310222A (en) * | 2017-07-25 | 2017-11-03 | 合肥威斯伏新材料有限公司 | A kind of heat-insulated antifreeze waterproof roll and preparation method |
| RU2637701C1 (en) * | 2017-01-11 | 2017-12-06 | Владимир Петрович Кудрявцев | Radar absorbent asphalt-concrete mixture and roadway covering made from this mixture |
| CN108081698A (en) * | 2018-01-30 | 2018-05-29 | 富华防水科技股份有限公司 | A kind of heat resist modification asphalt water-proof coiled material and preparation method thereof |
-
2018
- 2018-08-10 CN CN201810913065.3A patent/CN108999051B/en active Active
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN201121384Y (en) * | 2007-06-01 | 2008-09-24 | 潍坊市宏源防水材料有限公司 | Elastic modified asphalt waterproof coiled material |
| CN103408955A (en) * | 2013-08-14 | 2013-11-27 | 河南省华瑞防水防腐有限公司 | Waterproof coiled material and production method thereof |
| CN103947675A (en) * | 2014-04-11 | 2014-07-30 | 湖南大学 | Magnetic graphene oxide nanometer compound, preparation method and application thereof |
| CN106223549A (en) * | 2016-08-04 | 2016-12-14 | 合肥中科富华新材料有限公司 | A kind of high fire-retardance waterproof roll |
| RU2637701C1 (en) * | 2017-01-11 | 2017-12-06 | Владимир Петрович Кудрявцев | Radar absorbent asphalt-concrete mixture and roadway covering made from this mixture |
| CN106854343A (en) * | 2017-01-12 | 2017-06-16 | 四川航天五源复合材料有限公司 | Basalt fibre mixes reinforced resin and preparation method thereof, application with glass fibre |
| CN107310222A (en) * | 2017-07-25 | 2017-11-03 | 合肥威斯伏新材料有限公司 | A kind of heat-insulated antifreeze waterproof roll and preparation method |
| CN108081698A (en) * | 2018-01-30 | 2018-05-29 | 富华防水科技股份有限公司 | A kind of heat resist modification asphalt water-proof coiled material and preparation method thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112300588A (en) * | 2020-11-12 | 2021-02-02 | 吴菊 | Preparation method of asphalt applied to coastal high-grade highway |
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| Publication number | Publication date |
|---|---|
| CN108999051B (en) | 2020-10-16 |
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| PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A waterproof material resistant to seawater erosion Effective date of registration: 20210713 Granted publication date: 20201016 Pledgee: Nanxun Zhejiang rural commercial bank Limited by Share Ltd. and Fu sub branch Pledgor: ZHEJIANG WEILUN BUILDING MATERIAL Co.,Ltd. Registration number: Y2021330000832 |
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Date of cancellation: 20210728 Granted publication date: 20201016 Pledgee: Nanxun Zhejiang rural commercial bank Limited by Share Ltd. and Fu sub branch Pledgor: ZHEJIANG WEILUN BUILDING MATERIAL Co.,Ltd. Registration number: Y2021330000832 |
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| PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A waterproof material resistant to seawater erosion Effective date of registration: 20210728 Granted publication date: 20201016 Pledgee: Nanxun Zhejiang rural commercial bank Limited by Share Ltd. and Fu sub branch Pledgor: ZHEJIANG WEILUN BUILDING MATERIAL Co.,Ltd. Registration number: Y2021990000652 |