CN108994999A - A kind of colouring method improving rattan anti-pollution characteristic - Google Patents
A kind of colouring method improving rattan anti-pollution characteristic Download PDFInfo
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- CN108994999A CN108994999A CN201810894596.2A CN201810894596A CN108994999A CN 108994999 A CN108994999 A CN 108994999A CN 201810894596 A CN201810894596 A CN 201810894596A CN 108994999 A CN108994999 A CN 108994999A
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K9/00—Chemical or physical treatment of reed, straw, or similar material
- B27K9/002—Cane, bamboo
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K3/00—Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
- B27K3/02—Processes; Apparatus
- B27K3/12—Impregnating by coating the surface of the wood with an impregnating paste
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K3/00—Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
- B27K3/16—Inorganic impregnating agents
- B27K3/22—Compounds of zinc or copper
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K3/00—Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
- B27K3/34—Organic impregnating agents
- B27K3/50—Mixtures of different organic impregnating agents
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K3/00—Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
- B27K3/52—Impregnating agents containing mixtures of inorganic and organic compounds
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K5/00—Treating of wood not provided for in groups B27K1/00, B27K3/00
- B27K5/0005—Cryogenic treatment
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K5/00—Treating of wood not provided for in groups B27K1/00, B27K3/00
- B27K5/0015—Treating of wood not provided for in groups B27K1/00, B27K3/00 by electric means
- B27K5/002—Electric discharges, plasma
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K5/00—Treating of wood not provided for in groups B27K1/00, B27K3/00
- B27K5/0025—Treating of wood not provided for in groups B27K1/00, B27K3/00 by magnetic fields
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K5/00—Treating of wood not provided for in groups B27K1/00, B27K3/00
- B27K5/0085—Thermal treatments, i.e. involving chemical modification of wood at temperatures well over 100°C
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K5/00—Treating of wood not provided for in groups B27K1/00, B27K3/00
- B27K5/02—Staining or dyeing wood; Bleaching wood
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K5/00—Treating of wood not provided for in groups B27K1/00, B27K3/00
- B27K5/04—Combined bleaching or impregnating and drying of wood
Abstract
The invention belongs to wicker plaiting article technical fields, especially a kind of colouring method for improving rattan anti-pollution characteristic, the specific method is as follows: (1) will carry out chilling treatment in the rattan merging refrigerating box after harvesting trimming, it takes out, steam treatment is taken out, is immersed in liquor zinci chloridi and impregnates, drip liquid is pulled out, and pretreatment rattan is obtained;(2) pretreatment rattan is immersed in coloring agent and is impregnated, drip agent is pulled out, and cold plasma processing is carried out, and being dried to moisture content is 8% ~ 10%, obtains pre-staining rattan;(3) coating agent is uniformly smeared on pre-staining rattan surface, magnetization treatment, being dried to moisture content is 4% ~ 6%, obtains dyeing rattan;So that rattan bright color is glossy, and it is colour-fast to meet salt chance light, with high color fastness, with high dyeing effect, the anti-pollution characteristic on rattan surface is effectively improved, so that spot is easily peeled off, effectively improves the color and glossiness on rattan surface, the using effect of rattan braided article is improved, visual effect is improved.
Description
Technical field
The invention belongs to wicker plaiting article technical field, especially a kind of colouring method for improving rattan anti-pollution characteristic.
Background technique
Rattan is a kind of liana strong but pliable in texture, figure is extremely long, and crust is bright in luster, and feel is smooth, elastic pole
It is good, seemingly slight rather than slights, therefore rattan is claimed to slight, it is a kind of first-class woven natural material, rattan chair, rattan case worked out using rattan etc. is daily
Apparatus technique is exquisite, numerous in variety, durable, is loved by consumers through the ages;But due to people's quality of the life
It is constantly promoted, requirement of the people to article used in everyday is also higher and higher, for example the rattan based article of color dullness can not
Meet people to the high pursuit of quality of the life and high request, in addition, its rattan product surface easily adheres to the dirts such as grease stain, so that rattan
The service performance and using effect of based article substantially reduce, and bring great worry, so a kind of raising should be invented
The colouring method of rattan anti-pollution characteristic, and then promote the further development of rattan product industry.
Summary of the invention
In view of the above-mentioned problems, the present invention is intended to provide a kind of colouring method for improving rattan anti-pollution characteristic.
The invention is realized by the following technical scheme:
A kind of colouring method improving rattan anti-pollution characteristic, the specific method is as follows:
(1) chilling treatment will be carried out in the rattan merging refrigerating box after harvesting trimming, taken out, the item for being 110 ~ 120 DEG C in temperature
Constant temperature steam handles 22 ~ 26min under part, takes out, and is immersed in 50 ~ 60min of immersion in liquor zinci chloridi, and drip liquid is pulled out, obtains pre- place
Manage rattan;
(2) pretreatment rattan being immersed in 220 ~ 240min of immersion in coloring agent, drip agent is pulled out, cold plasma processing is carried out,
It is 8% ~ 10% that moisture content is dried under conditions of temperature is 60 ~ 62 DEG C, obtains pre-staining rattan;
The coloring agent, is made of raw material from the following weight: 24 ~ 26 parts of orange skin, 15 ~ 17 parts of orange leaf, black rice 21 ~ 23
Part, 14 ~ 16 parts of fresh willow leaf, 15 ~ 17 parts of fresh camphortree leaf, 0.11 ~ 0.12 part of black cohosh root polysaccharide, 0.15 ~ 0.16 part of algal polysaccharides, horse
0.13 ~ 0.14 part of bitterroot polysaccharide, 140 ~ 160 parts of water;
(3) coating agent is uniformly smeared on pre-staining rattan surface, magnetic field strength be 770 ~ 790G under conditions of magnetization treatment 10 ~
12min, 15 ~ 17min of magnetization treatment under conditions of magnetic field strength is 1210 ~ 1230G, under conditions of temperature is 46 ~ 48 DEG C
Being dried to moisture content is 4% ~ 6%, obtains dyeing rattan;
The coating agent, is prepared according to the following steps:
A. raw material, 3.2 ~ 3.4 parts of vermiculite, 1.5 ~ 1.7 parts of borax, 2.6 ~ 2.8 parts of aloe polysaccharide, propylene yogurt are weighed by weight
110 ~ 120 parts of liquid;
B. constant temperature 19 ~ 21min of frying in the rotary frying pan for being 81 ~ 83 DEG C by vermiculite merging temperature, being immersed in mass fraction is 25%
28 ~ 32min is impregnated in ~ 27% ethanol solution, constant temperature 14 ~ 16min of frying in the rotary frying pan that merging temperature is 65 ~ 67 DEG C is ground
Be milled to powdery, be added to heat-insulation soaking 23 in the diphenylhydroxyethanone solution that temperature is 53 ~ 55 DEG C, mass fraction is 2.3% ~ 2.5% ~
25min is simultaneously stirred continuously, and filtering dries under conditions of temperature is 81 ~ 83 DEG C, obtains vermiculite power;
C. vermiculite power, borax, aloe polysaccharide are added in acrylic emulsion and are stirred evenly, be 1420 ~ 1460G in magnetic field strength
Under conditions of 28 ~ 30min of magnetization treatment, obtain coating agent.
As invention further embodiment: chilling treatment described in step (1), the condition for being -2.1 ~ -1.7 DEG C in temperature
Lower constant refrigeration handles 8 ~ 10min, and constant refrigeration handles 6 ~ 8min under conditions of temperature is 1.4 ~ 1.8 DEG C, and above-mentioned is one
Circulation, total circular treatment 5 times.
As invention further embodiment: liquor zinci chloridi described in step (1) is prepared: according to the following steps by 2.7
The zinc chloride of ~ 2.9 parts by weight and the Chinese yam polysaccharide of 0.21 ~ 0.23 parts by weight, which are put into the water of 130 ~ 150 parts by weight, to be stirred to molten
Solution, obtains liquor zinci chloridi.
As invention further embodiment: the processing of cold plasma described in step (2), in the condition that power is 33 ~ 35W
Lower cold plasma handles 80 ~ 90s, and cold plasma handles 120 ~ 130s under conditions of power is 89 ~ 91W, is in power
Cold plasma handles 100 ~ 110s under conditions of 65 ~ 67W, and above-mentioned is a circulation, altogether circular treatment 2 times.
As invention further embodiment: coloring agent described in step (2) is prepared according to the following steps: black rice is set
Entering temperature is constant temperature 16 ~ 18min of frying in 74 ~ 78 DEG C of rotary frying pan, is ground to powdery, with the orange skin of co-grinding, fresh
Orange leaf, fresh willow leaf and fresh camphortree leaf are mixed evenly, and it is 59 ~ 61 DEG C that mild fire, which is heated to temperature, and water is added and stirs evenly, mild fire
Being heated to temperature is 83 ~ 85 DEG C, 220 ~ 240h of ferment at constant temperature in the fermenting case that merging temperature is 36 ~ 38 DEG C, is taken out, and filtering takes
Filtrate is added black cohosh root polysaccharide, algal polysaccharides and Polysaccharide from Portulaca oleracea and stirs to dissolution, obtains coloring agent.
Beneficial effects of the present invention: it is provided by the invention it is a kind of improve rattan anti-pollution characteristic colouring method, by rattan according to
It is secondary refrigerated, steam and liquor zinci chloridi immersion treatment, the outflow of lipid matter ingredient in rattan can be effectively facilitated, improve rattan
Porosity between fibr tissue, facilitates the infiltration and diffusion of coloring agent, moreover it is possible to effectively take out the dust etc. of rattan surface attachment
Attachment material improves coating effect;It is handled using staining reagent combination cold plasma of the invention, effective activation dyeing point
Son enhances combination and polymerizing power between dye molecule and rattan fiber tissue, so that rattan bright color is glossy, and meets salt
It is colour-fast to meet light, there is high color fastness, there is high dyeing effect;Finally rattan is carried out using coating agent of the invention
The coating of surface and magnetization treatment further promote polymerizeing for dye molecule and fibr tissue, so that forming stable stereoscopic graticule
Network structure effectively facilitates coating agent in conjunction with the strength of rattan, effectively improves the anti-pollution characteristic on rattan surface, effectively prevent rattan
Surface is covered and is adhered to by spot, and spot is easily peeled off, effectively improves the color and glossiness on rattan surface, effectively improve rattan
The using effect of knitting improves visual effect, green natural.
Specific embodiment
Illustrate the present invention with specific embodiment below, but is not limitation of the present invention.
Embodiment 1
In the embodiment of the present invention, a kind of colouring method improving rattan anti-pollution characteristic, the specific method is as follows:
(1) chilling treatment will be carried out in the rattan merging refrigerating box after harvesting trimming, taken out, under conditions of temperature is 110 DEG C
Constant temperature steam handles 22min, takes out, is immersed in liquor zinci chloridi and impregnates 50min, and drip liquid is pulled out, obtains pretreatment rattan;
(2) pretreatment rattan is immersed in coloring agent and impregnates 220min, drip agent is pulled out, cold plasma processing is carried out, in temperature
It is 8% ~ 10% that degree, which is dried to moisture content under conditions of being 60 DEG C, obtains pre-staining rattan;
The coloring agent, is made of raw material from the following weight: 24 parts of orange skin, 15 parts of orange leaf, 21 parts of black rice, fresh willow leaf
14 parts, 15 parts of fresh camphortree leaf, 0.11 part of black cohosh root polysaccharide, 0.15 part of algal polysaccharides, 0.13 part of Polysaccharide from Portulaca oleracea, 140 parts of water;
(3) coating agent is uniformly smeared on pre-staining rattan surface, under conditions of magnetic field strength is 770G magnetization treatment 10min,
Magnetization treatment 15min under conditions of magnetic field strength is 1210G, be dried under conditions of temperature is 46 DEG C moisture content be 4% ~
6%, obtain dyeing rattan;
The coating agent, is prepared according to the following steps:
A. raw material, 3.2 parts of vermiculite, 1.5 parts of borax, 2.6 parts of aloe polysaccharide, 110 parts of acrylic emulsion are weighed by weight;
B. constant temperature frying 19min in the rotary frying pan for being 81 DEG C by vermiculite merging temperature, being immersed in mass fraction is 25% ~ 27%
28min is impregnated in ethanol solution, constant temperature frying 14min in the rotary frying pan that merging temperature is 65 DEG C is ground to powdery, is added to
It heat-insulation soaking 23min and is stirred continuously, filters, in temperature in the diphenylhydroxyethanone solution that temperature is 53 DEG C, mass fraction is 2.3%
Degree is dried under conditions of being 81 DEG C, obtains vermiculite power;
C. vermiculite power, borax, aloe polysaccharide are added in acrylic emulsion and are stirred evenly, in the item that magnetic field strength is 1420G
Magnetization treatment 28min under part, obtains coating agent.
As invention further embodiment: chilling treatment described in step (1), constant temperature under conditions of temperature is -2.1 DEG C
Chilling treatment 8min, constant refrigeration handles 6min under conditions of temperature is 1.4 DEG C, and above-mentioned is a circulation, altogether circular treatment 5
It is secondary.
As invention further embodiment: liquor zinci chloridi described in step (1) is prepared: according to the following steps by 2.7
The zinc chloride of parts by weight and the Chinese yam polysaccharide of 0.21 parts by weight put into stirring in the water of 130 parts by weight and it is molten to obtain zinc chloride to dissolving
Liquid.
As invention further embodiment: the processing of cold plasma described in step (2), under conditions of power is 33W
Cold plasma handles 80s, and cold plasma handles 120s under conditions of power is 89W, cold under conditions of power is 65W
Corona treatment 100s, above-mentioned is a circulation, altogether circular treatment 2 times.
As invention further embodiment: coloring agent described in step (2) is prepared according to the following steps: black rice is set
Entering temperature is constant temperature frying 16min in 74 DEG C of rotary frying pan, is ground to powdery, with the orange skin of co-grinding, orange leaf, fresh
Willow leaf and fresh camphortree leaf are mixed evenly, and it is 59 DEG C that mild fire, which is heated to temperature, and water is added and stirs evenly, mild fire is heated to temperature
Be 83 DEG C, merging temperature is ferment at constant temperature 220h in 36 DEG C of fermenting case, is taken out, and filtering takes filtrate, be added black cohosh root polysaccharide,
Algal polysaccharides and Polysaccharide from Portulaca oleracea are stirred to dissolution, obtain coloring agent.
150h is impregnated using the saline solution that temperature is 48 DEG C, mass fraction is 8% after dyeing, does not occur discoloration.
Embodiment 2
In the embodiment of the present invention, a kind of colouring method improving rattan anti-pollution characteristic, the specific method is as follows:
(1) chilling treatment will be carried out in the rattan merging refrigerating box after harvesting trimming, taken out, under conditions of temperature is 115 DEG C
Constant temperature steam handles 24min, takes out, is immersed in liquor zinci chloridi and impregnates 55min, and drip liquid is pulled out, obtains pretreatment rattan;
(2) pretreatment rattan is immersed in coloring agent and impregnates 230min, drip agent is pulled out, cold plasma processing is carried out, in temperature
It is 8% ~ 10% that degree, which is dried to moisture content under conditions of being 61 DEG C, obtains pre-staining rattan;
The coloring agent, is made of raw material from the following weight: 25 parts of orange skin, 16 parts of orange leaf, 22 parts of black rice, fresh willow leaf
15 parts, 16 parts of fresh camphortree leaf, 0.115 part of black cohosh root polysaccharide, 0.155 part of algal polysaccharides, 0.135 part of Polysaccharide from Portulaca oleracea, water 150
Part;
(3) coating agent is uniformly smeared on pre-staining rattan surface, under conditions of magnetic field strength is 780G magnetization treatment 11min,
Magnetization treatment 16min under conditions of magnetic field strength is 1220G, be dried under conditions of temperature is 47 DEG C moisture content be 4% ~
6%, obtain dyeing rattan;
The coating agent, is prepared according to the following steps:
A. raw material, 3.3 parts of vermiculite, 1.6 parts of borax, 2.7 parts of aloe polysaccharide, 115 parts of acrylic emulsion are weighed by weight;
B. constant temperature frying 20min in the rotary frying pan for being 82 DEG C by vermiculite merging temperature, is immersed in the ethyl alcohol that mass fraction is 26%
30min is impregnated in solution, constant temperature frying 15min in the rotary frying pan that merging temperature is 66 DEG C is ground to powdery, is added to temperature
It heat-insulation soaking 24min and is stirred continuously in the diphenylhydroxyethanone solution for being 2.4% for 54 DEG C, mass fraction, filters, be in temperature
It is dried under conditions of 82 DEG C, obtains vermiculite power;
C. vermiculite power, borax, aloe polysaccharide are added in acrylic emulsion and are stirred evenly, in the item that magnetic field strength is 1440G
Magnetization treatment 29min under part, obtains coating agent.
As invention further embodiment: chilling treatment described in step (1), constant temperature under conditions of temperature is -1.9 DEG C
Chilling treatment 9min, constant refrigeration handles 7min under conditions of temperature is 1.6 DEG C, and above-mentioned is a circulation, altogether circular treatment 5
It is secondary.
As invention further embodiment: liquor zinci chloridi described in step (1) is prepared: according to the following steps by 2.8
The zinc chloride of parts by weight and the Chinese yam polysaccharide of 0.22 parts by weight put into stirring in the water of 140 parts by weight and it is molten to obtain zinc chloride to dissolving
Liquid.
As invention further embodiment: the processing of cold plasma described in step (2), under conditions of power is 34W
Cold plasma handles 85s, and cold plasma handles 125s under conditions of power is 90W, cold under conditions of power is 66W
100 ~ 110s of corona treatment, above-mentioned is a circulation, altogether circular treatment 2 times.
As invention further embodiment: coloring agent described in step (2) is prepared according to the following steps: black rice is set
Entering temperature is constant temperature frying 17min in 76 DEG C of rotary frying pan, is ground to powdery, with the orange skin of co-grinding, orange leaf, fresh
Willow leaf and fresh camphortree leaf are mixed evenly, and it is 60 DEG C that mild fire, which is heated to temperature, and water is added and stirs evenly, mild fire is heated to temperature
Be 84 DEG C, merging temperature is ferment at constant temperature 230h in 37 DEG C of fermenting case, is taken out, and filtering takes filtrate, be added black cohosh root polysaccharide,
Algal polysaccharides and Polysaccharide from Portulaca oleracea are stirred to dissolution, obtain coloring agent.
150h is impregnated using the saline solution that temperature is 48 DEG C, mass fraction is 8% after dyeing, does not occur discoloration.
Embodiment 3
In the embodiment of the present invention, a kind of colouring method improving rattan anti-pollution characteristic, the specific method is as follows:
(1) chilling treatment will be carried out in the rattan merging refrigerating box after harvesting trimming, taken out, under conditions of temperature is 120 DEG C
Constant temperature steam handles 26min, takes out, is immersed in liquor zinci chloridi and impregnates 60min, and drip liquid is pulled out, obtains pretreatment rattan;
(2) pretreatment rattan is immersed in coloring agent and impregnates 240min, drip agent is pulled out, cold plasma processing is carried out, in temperature
It is 8% ~ 10% that degree, which is dried to moisture content under conditions of being 62 DEG C, obtains pre-staining rattan;
The coloring agent, is made of raw material from the following weight: 26 parts of orange skin, 17 parts of orange leaf, 23 parts of black rice, fresh willow leaf
16 parts, 17 parts of fresh camphortree leaf, 0.12 part of black cohosh root polysaccharide, 0.16 part of algal polysaccharides, 0.14 part of Polysaccharide from Portulaca oleracea, water 140 ~ 160
Part;
(3) coating agent is uniformly smeared on pre-staining rattan surface, under conditions of magnetic field strength is 790G magnetization treatment 12min,
Magnetization treatment 17min under conditions of magnetic field strength is 1230G, be dried under conditions of temperature is 48 DEG C moisture content be 4% ~
6%, obtain dyeing rattan;
The coating agent, is prepared according to the following steps:
A. raw material, 3.4 parts of vermiculite, 1.7 parts of borax, 2.8 parts of aloe polysaccharide, 120 parts of acrylic emulsion are weighed by weight;
B. constant temperature frying 21min in the rotary frying pan for being 83 DEG C by vermiculite merging temperature, is immersed in the ethyl alcohol that mass fraction is 27%
32min is impregnated in solution, constant temperature frying 16min in the rotary frying pan that merging temperature is 67 DEG C is ground to powdery, is added to temperature
It heat-insulation soaking 25min and is stirred continuously in the diphenylhydroxyethanone solution for being 2.5% for 55 DEG C, mass fraction, filters, be in temperature
It is dried under conditions of 83 DEG C, obtains vermiculite power;
C. vermiculite power, borax, aloe polysaccharide are added in acrylic emulsion and are stirred evenly, in the item that magnetic field strength is 1460G
Magnetization treatment 30min under part, obtains coating agent.
As invention further embodiment: chilling treatment described in step (1), constant temperature under conditions of temperature is -1.7 DEG C
Chilling treatment 10min, constant refrigeration handles 8min under conditions of temperature is 1.8 DEG C, and above-mentioned is a circulation, altogether circular treatment
5 times.
As invention further embodiment: liquor zinci chloridi described in step (1) is prepared: according to the following steps by 2.9
The zinc chloride of parts by weight and the Chinese yam polysaccharide of 0.23 parts by weight put into stirring in the water of 150 parts by weight and it is molten to obtain zinc chloride to dissolving
Liquid.
As invention further embodiment: the processing of cold plasma described in step (2), under conditions of power is 35W
Cold plasma handles 90s, and cold plasma handles 130s under conditions of power is 91W, cold under conditions of power is 67W
Corona treatment 110s, above-mentioned is a circulation, altogether circular treatment 2 times.
As invention further embodiment: coloring agent described in step (2) is prepared according to the following steps: black rice is set
Entering temperature is constant temperature frying 18min in 78 DEG C of rotary frying pan, is ground to powdery, with the orange skin of co-grinding, orange leaf, fresh
Willow leaf and fresh camphortree leaf are mixed evenly, and it is 61 DEG C that mild fire, which is heated to temperature, and water is added and stirs evenly, mild fire is heated to temperature
Be 85 DEG C, merging temperature is ferment at constant temperature 240h in 38 DEG C of fermenting case, is taken out, and filtering takes filtrate, be added black cohosh root polysaccharide,
Algal polysaccharides and Polysaccharide from Portulaca oleracea are stirred to dissolution, obtain coloring agent.
150h is impregnated using the saline solution that temperature is 48 DEG C, mass fraction is 8% after dyeing, does not occur discoloration.
Comparative example 1
A kind of colouring method improving rattan anti-pollution characteristic, the difference from embodiment 1 is that, step (1) is without described cold
Hiding processing, other conditions are all the same.
Comparative example 2
A kind of colouring method improving rattan anti-pollution characteristic, the difference from embodiment 1 is that, step (1) does not use the chlorine
Change zinc solution and carry out immersion treatment, other conditions are all the same.
Comparative example 3
A kind of colouring method improving rattan anti-pollution characteristic, the difference from embodiment 1 is that, step (2) is without described cold
Corona treatment, other conditions are all the same.
Comparative example 4
A kind of colouring method improving rattan anti-pollution characteristic, the difference from embodiment 1 is that, in coloring agent described in step (2)
It is added without black cohosh root polysaccharide, algal polysaccharides and Polysaccharide from Portulaca oleracea, other conditions are all the same.
Comparative example 5
A kind of colouring method improving rattan anti-pollution characteristic, the difference from embodiment 1 is that, in coating agent described in step (3)
It is added without vermiculite, borax and aloe polysaccharide, other conditions are all the same.
Comparative example 6
A kind of colouring method improving rattan anti-pollution characteristic, the difference from embodiment 1 is that, step (3) is without the magnetic
Change processing, other conditions are all the same.
Dyeing processing is carried out to same a collection of rattan using the method for embodiment and comparative example, dyeing after treatment detects rattan
The anti-pollution characteristic and dyeing effect of item, testing result is respectively such as table 1:
The comparing result of 1 embodiment and comparative example rattan resistant dyeing effect of table
As it can be seen from table 1 colouring method of the invention can be effectively reduced the surface energy and surface tension of rattan, so that its is resistance to
Dirty performance is significantly improved, moreover it is possible to which effectively the color fastness to light of enhancing rattan, dyeing effect are greatly improved.
Claims (5)
1. a kind of colouring method for improving rattan anti-pollution characteristic, which is characterized in that the specific method is as follows:
(1) chilling treatment will be carried out in the rattan merging refrigerating box after harvesting trimming, taken out, the item for being 110 ~ 120 DEG C in temperature
Constant temperature steam handles 22 ~ 26min under part, takes out, and is immersed in 50 ~ 60min of immersion in liquor zinci chloridi, and drip liquid is pulled out, obtains pre- place
Manage rattan;
(2) pretreatment rattan being immersed in 220 ~ 240min of immersion in coloring agent, drip agent is pulled out, cold plasma processing is carried out,
It is 8% ~ 10% that moisture content is dried under conditions of temperature is 60 ~ 62 DEG C, obtains pre-staining rattan;
The coloring agent, is made of raw material from the following weight: 24 ~ 26 parts of orange skin, 15 ~ 17 parts of orange leaf, black rice 21 ~ 23
Part, 14 ~ 16 parts of fresh willow leaf, 15 ~ 17 parts of fresh camphortree leaf, 0.11 ~ 0.12 part of black cohosh root polysaccharide, 0.15 ~ 0.16 part of algal polysaccharides, horse
0.13 ~ 0.14 part of bitterroot polysaccharide, 140 ~ 160 parts of water;
(3) coating agent is uniformly smeared on pre-staining rattan surface, magnetic field strength be 770 ~ 790G under conditions of magnetization treatment 10 ~
12min, 15 ~ 17min of magnetization treatment under conditions of magnetic field strength is 1210 ~ 1230G, under conditions of temperature is 46 ~ 48 DEG C
Being dried to moisture content is 4% ~ 6%, obtains dyeing rattan;
The coating agent, is prepared according to the following steps:
A. raw material, 3.2 ~ 3.4 parts of vermiculite, 1.5 ~ 1.7 parts of borax, 2.6 ~ 2.8 parts of aloe polysaccharide, propylene yogurt are weighed by weight
110 ~ 120 parts of liquid;
B. constant temperature 19 ~ 21min of frying in the rotary frying pan for being 81 ~ 83 DEG C by vermiculite merging temperature, being immersed in mass fraction is 25%
28 ~ 32min is impregnated in ~ 27% ethanol solution, constant temperature 14 ~ 16min of frying in the rotary frying pan that merging temperature is 65 ~ 67 DEG C is ground
Be milled to powdery, be added to heat-insulation soaking 23 in the diphenylhydroxyethanone solution that temperature is 53 ~ 55 DEG C, mass fraction is 2.3% ~ 2.5% ~
25min is simultaneously stirred continuously, and filtering dries under conditions of temperature is 81 ~ 83 DEG C, obtains vermiculite power;
C. vermiculite power, borax, aloe polysaccharide are added in acrylic emulsion and are stirred evenly, be 1420 ~ 1460G in magnetic field strength
Under conditions of 28 ~ 30min of magnetization treatment, obtain coating agent.
2. the colouring method according to claim 1 for improving rattan anti-pollution characteristic, which is characterized in that described in step (1)
Chilling treatment, constant refrigeration handles 8 ~ 10min under conditions of temperature is -2.1 ~ -1.7 DEG C, the item for being 1.4 ~ 1.8 DEG C in temperature
Constant refrigeration handles 6 ~ 8min under part, and above-mentioned is a circulation, altogether circular treatment 5 times.
3. the colouring method according to claim 1 for improving rattan anti-pollution characteristic, which is characterized in that described in step (1)
Liquor zinci chloridi is prepared according to the following steps: by the Chinese yam of the zinc chloride of 2.7 ~ 2.9 parts by weight and 0.21 ~ 0.23 parts by weight
Polysaccharide puts into stirring in the water of 130 ~ 150 parts by weight and obtains liquor zinci chloridi to dissolving.
4. the colouring method according to claim 1 for improving rattan anti-pollution characteristic, which is characterized in that described in step (2)
Cold plasma processing, cold plasma handles 80 ~ 90s under conditions of power is 33 ~ 35W, in the item that power is 89 ~ 91W
Cold plasma handles 120 ~ 130s under part, and cold plasma handles 100 ~ 110s under conditions of power is 65 ~ 67W, above-mentioned
It is recycled for one, altogether circular treatment 2 times.
5. the colouring method according to claim 1 for improving rattan anti-pollution characteristic, which is characterized in that described in step (2)
Coloring agent is prepared according to the following steps: by black rice merging temperature be constant temperature frying 16 in 74 ~ 78 DEG C of rotary frying pan ~
18min is ground to powdery, is mixed evenly with orange skin, orange leaf, fresh willow leaf and the fresh camphortree leaf of co-grinding, mild fire
Being heated to temperature is 59 ~ 61 DEG C, and water is added and stirs evenly, and it is 83 ~ 85 DEG C that mild fire, which is heated to temperature, and merging temperature is 36 ~ 38 DEG C
Fermenting case in 220 ~ 240h of ferment at constant temperature, take out, filtering takes filtrate, and it is more that black cohosh root polysaccharide, algal polysaccharides and purslane is added
Sugar stirring obtains coloring agent to dissolving.
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