CN108990998A - A kind of Herbicidal combinations and its application containing trichlopyr and pyroxsulam - Google Patents

A kind of Herbicidal combinations and its application containing trichlopyr and pyroxsulam Download PDF

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CN108990998A
CN108990998A CN201810980141.2A CN201810980141A CN108990998A CN 108990998 A CN108990998 A CN 108990998A CN 201810980141 A CN201810980141 A CN 201810980141A CN 108990998 A CN108990998 A CN 108990998A
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pyroxsulam
trichlopyr
weeds
wheat
fresh weight
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陈国奇
张洪程
霍中洋
高辉
郭保卫
刘炳亮
魏海燕
张海鹏
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Yangzhou University
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Yangzhou University
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/90Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having two or more relevant hetero rings, condensed among themselves or with a common carbocyclic ring system
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/34Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom
    • A01N43/40Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom six-membered rings

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  • Agronomy & Crop Science (AREA)
  • Pest Control & Pesticides (AREA)
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  • Health & Medical Sciences (AREA)
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  • General Health & Medical Sciences (AREA)
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  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The invention discloses a kind of Herbicidal combinations, and by trichlopyr and pyroxsulam according to weight ratio (9.375~150): 1 proportion forms.The invention also discloses application of the above-mentioned Herbicidal combinations in prevention and control wheat weeds.Two kinds of medicaments can efficiently kill Different groups weeds respectively, and have apparent synergistic effect after being used in compounding, and accelerate drug effect to play, reduce herbicide dosage, to improve the safety to wheat.Two kinds of medicine component degrass spectrums are complementary, and mixed rear degrass spectrum can effectively cover various wheatland common weeds, and have high activity to the extremely refractory resistant weed of wheatland and elder weed, and market potential is huge.

Description

A kind of Herbicidal combinations and its application containing trichlopyr and pyroxsulam
Technical field
The invention belongs to agricultural technology fields, and in particular to a kind of Herbicidal combinations and its application.
Background technique
China is the maximum country of wheat yield in the world, about 2418.7 ten thousand hectares of annual wheat cultivated area (3.6 hundred million mu), Produce about 1.3 hundred million tons of wheat per year, cultivated area and yield account for 14.5% He of China crop sowing gross area and total output respectively 20.9%.Thereby it is ensured that wheat stable yields and Quality Safety are one of the basic tasks of China's planting industry.Weed infestation is that wheat is planted One of primary biological disaster faced in training, even if taking various prevention and control measures, the yield that wheat weeds harm directly results in is damaged Quenched 18%.It is at present still the most important means of China's wheatland crop smothering prevention and control, cornfield herbicidal by using herbicide weeding Agent dosage increases year by year, and wheat planting family is higher and higher to cornfield herbicidal drug cost budget, to cornfield herbicidal new product It is in urgent need.
There is an urgent need to lasting progress cornfield herbicidal varieties distributions in China.On the one hand, China's wheat weeds are to a variety of weedings The resistance of agent constantly aggravates and breaks out in flakes harm, and new herbicide kind is needed to come into operation.China's wheatland is bright at present The antiweed weeds really registered have 13 kinds of , Bao Kuo Wang grass (Beckmannia syzigachne), Alopecurus It is (Alopecurus japonicus), amur foxtail (Alopecurus aequalis), caput careless (Polypogon fugax), hard Grass (Sclerochloa dura), clearvers (Galium aparine), common vetch (Vicia sativa), shepherd's purse (Capsella bursa-pastoris), corn gromwell (Lithospermum arvense), Descurainia sophia (Descurainia Sophia), ox chickweed (Myosoton aquaticum), herba stellariae mediae (Stellaria media), indian rorippa herb (Rorippa indica);Herbicide involved in these resistant weeds be mainly aryloxyphenoxypropionate class fenoxapropPethyl and The pinoxaden of clodinafop-propargyl, neophyl pyrazolines, tribenuron-methyl, the mesosulfuron of sulfonylurea.What resistant weed was related to removes Careless agent is based on cauline leaf process agent, in this way, which the wheatland for weeds stem and leaf treatment after seedling can catch the flap with herbicide kind and see Elbow.There is an urgent need to efficiently and safely solve the problems, such as wheatland crop smothering in more practical herbicide type investment Wheat Productions for we While, delay weeds to break out resistance to existing medicament.On the other hand, efficient, safety, low-risk herbicide product are constantly researched and developed The herbicide kind that kind substitution dosage is big, residual is high, security risk is high had both met Demand of Nation and market trend.
Trichlopyr is pyridine oxycarboxylic acid class inner sucting conduction type low toxicity herbicide, and also known as lid fills energy, Triclopyr.By The blade face of plant and root system absorb, and complete stool is transmitted in plant, cause its root, stem, leaf deformity, and reserve substance exhausts, For vascular bundle by embolism or rupture, plant is gradually dead.Weeding is gone out fillings before afforesting suitable for forest, and maintenance fire line is helped and educates pine tree And stand conversion, broadleaf weeds and xylophyta are prevented and kill off for bare place.Sensibility of the gramineae plant to trichlopyr It is lower, there is drug resistance.Trichlopyr can be decomposed in the soil by edaphon, and half-life period is 30-46 days.
Pyroxsulam is inner sucting conduction type triazolopyrimidine sulfonamides herbicide, in wheatland as stem and leaf treatment after seedling agent Use, active superelevation can effectively prevent and kill off a variety of grass family and broadleaf class wheat weeds, as amur foxtail, Alopecurus, hard grass, Wild avena sativa, shepherd's purse, ox chickweed etc., however the performance of pyroxsulam drug effect is slower, and since pyroxsulam has super-active, Wheat paddock is larger using limiting.
Summary of the invention
Technical problem to be solved by the invention is to provide it is a kind of can efficiently and safely control of weed in wheat field weeding group Close object.
The present invention also technical problems to be solved are to provide the application of above-mentioned Herbicidal combinations.
In order to solve the above technical problems, The technical solution adopted by the invention is as follows:
A kind of Herbicidal combinations, by trichlopyr and pyroxsulam according to weight ratio (9.375~150): 1 proportion Composition.
Preferably, the weight ratio of trichlopyr and pyroxsulam is (9.375~75): 1.
It is furthermore preferred that the weight ratio of trichlopyr and pyroxsulam is (18.75~75): 1.
Application of the above-mentioned Herbicidal combinations in control of weed in wheat field is also within protection scope of the present invention.
Wherein, the weeds are gramineae weed or broad leaved weeds, and Bao is included but Bu Xian Yu Wang grass, amur foxtail, Japan The wheatlands such as amur foxtail, clearvers, field thistle, ox chickweed, shepherd's purse, Descurainia sophia common weed and intractable weed.
In addition, Herbicidal combinations antagonism weed control of the invention is significant.
In use, can be used in the 2 leaf phase of wheat or before wheat is turned green to jointing.
The utility model has the advantages that this re-compounded binary herbicide has the advantage that compared with existing wheatland Common Herbicides
(1) there is synergistic effect, two kinds of medicaments can efficiently kill Different groups weeds respectively, and have after being used in compounding bright Aobvious synergistic effect.
(2) two kinds of medicine component degrass spectrums are complementary, and mixed rear degrass spectrum can effectively cover grass family, broad leaved weeds, wrap The various common weeds of wheatlands such as Kuo Wang grass, amur foxtail, Alopecurus, clearvers, field thistle, ox chickweed, shepherd's purse, Descurainia sophia.
(3) pyroxsulam dosage is greatly reduced, improves the safety to wheat.
(4) it can be used for resistant weed improvement, two kinds of composite reagents can effectively administer the anti-aryloxy group benzene oxygen that wheatland causes disaster The gramineae weed of base propionic acid ester, neophyl pyrazolines etc. acetyl-CoA carboxylases (ACCase) inhibitor herbicides and The broadleaf weeds of the acetolactate synthases such as anti-sulfonylurea (ALS) inhibitor class herbicide.
(5) two kinds of composite reagents can greatly speed up the performance to pyroxsulam drug effect, 15 days weeds after optimal dose medication Mortality, 30 days weeds are substantially withered after medicine.Wheat can be made quickly to set up the competitive advantage to weeds in wheat paddock application, It lays the foundation for High-yield Wheat.
Specific embodiment
According to following embodiments, the present invention may be better understood.However, as it will be easily appreciated by one skilled in the art that real It applies content described in example and is merely to illustrate the present invention, without sheet described in detail in claims should will not be limited Invention.
Embodiment 1: trichlopyr pyroxsulam compounding agent formulation ratio screening test.
In order to screen the optimum formula proportion of trichlopyr and pyroxsulam, interior progress is a series of in the controlled environment chamber Whole strain bioassay.
1.1 for trying weeds: Wang grass, amur foxtail, clearvers, field thistle.In weeds control, wheat weeds are generally divided into two Major class: gramineae weed, broadleaf weeds.This test is that current wheatland endangers serious malignant weed for this 4 kinds of grass of examination, Zhong Wang grass, amur foxtail represent wheatland grass family malignant weed;Clearvers, field thistle represent wheatland broadleaf class malignant weed.
1.2 binary built agent prescriptions match the setting of screening test drug dose:
1) each single dose setting is as follows:
Trichlopyr (A): 0 (A0), 37.5 (A37.5), 75 (A75), 150 (A150) g a.i./hm2
Pyroxsulam (B): 0 (B0), 1 (B1), 2 (B2), 4 (B4) g a.i./hm2
2) binary built agent prescription proportion screening dosage setting is as shown in table 1:
Table is arranged in 1 binary built agent prescription of table proportion screening dosage
1.3 test method
It is cultivated in the square plastic plant that specification is 7 × 7 × 7cm and is packed into the organoclay that herbicide was not used in flowerpot (pH value 6.5, the content of organic matter 2.4%), adds water to saturation.Select full seed Wang grass, amur foxtail, clearvers, field thistle Seed, each small flower sow 20, cover one layer of fine earth (thickness about 3mm) on seed in small flower.Small flower is put into 44 The thickening plastics transferring box (clear water for being previously added 2cm depth) of × 33 × 10cm, is placed in phjytotron and cultivates, 15 DEG C of illumination 12 hours, 10 DEG C dark 12 hours, keep 0.5cm-1cm water layer logical in order to the soil in small whitepack in transferring box during test It crosses water suction and keeps wet.Sowing starts after 20 days to each small flower final singling, and each small flower retains the best children of 12 plants of growing ways Seedling.Each processing repeats 4 small flowers.Wang grass and amur foxtail seedling grow to 3-4 leaf phase, clearvers and field thistle seedling and grow to 6- Herbicide treatment is carried out using cauline leaf spray-on process when 8 leaf phase, control group sprays equivalent clear water.By spraying using Yangzhou University's gardening with The walking gesture voltage stabilization spray tower of plant protection institute is sprayed, spray height 20cm, flat Fan spray head spraying swath 50cm, pressure 200KPa.It is 45L water/hm that spray liquid measure, which corresponds to field spouting liquid,2.After application 45 days, acquires respectively and weigh each little Hua For trying weeds overground part fresh weight in basin.
Calculate the fresh weight inhibition rate (E) of weeds between single dose and binary built different disposal, theoretical fresh weight inhibition rate (E0)。 Using Gowing method by comparing E and E0The synergy type of value evaluation re-compounded binary herbicide.
Survey fresh weight inhibition rate (E)=(control group fresh weight-processing group fresh weight) ÷ control group fresh weight × 100%
Theoretical fresh weight inhibition rate (E0)=(X+Y-XY) × 100%
E in formula0Theoretical fresh weight inhibition rate after compounding for herbicide trichlopyr with pyroxsulam, X are trichlorine pyrrole The actual measurement fresh weight inhibition rate of fluoroacetic acid single dose, Y are the actual measurement fresh weight inhibition rate of pyroxsulam single dose.
Work as E-E0Indicate that two kinds of mixture of herbicides have synergistic effect when > 10%;Work as E-E0Two kinds of weedings are indicated when < -10% Agent compounding has antagonism;E-E0Value between -10% to 10% then for be added effect.
1.4 test result
1) synergy of trichlopyr and pyroxsulam Dui Wang grass
The actual measurement fresh weight inhibition rate E (%) of the trichlopyr pyroxsulam compounding agent Dui Wang grass of 2 different ratio of table
The theoretical fresh weight inhibition rate E of the trichlopyr pyroxsulam compounding agent Dui Wang grass of 3 different ratio of table0(%)
"/": the lower theoretical fresh weight inhibition rate (E of single dose processing0) it is equal to actual measurement fresh weight inhibition rate (E), synergy is not present
The trichlopyr of 4 different ratio of table and the synergy value [(E-E0) × 100] of pyroxsulam Dui Wang grass
Note: E-E0> 10% indicates synergistic effect "/": the lower theoretical fresh weight inhibition rate (E of single dose processing0) fresh equal to surveying Synergy is not present in weight inhibiting rate (E)
As shown in Table 2, trichlopyr single dose 150g a.i./hm2When inhibiting rate less than 8%;Pyroxsulam single dose 4g a.i./hm2When fresh weight inhibition rate be 28%, thus calculate the theoretical inhibiting rate that uses of two kinds of mixture of herbicides and be shown in Table 3.Pass through ratio Compared with the actual measurement inhibiting rate and theoretical inhibiting rate under two kinds of herbicide difference compounded combinations, and then two kinds of herbicides are investigated to barnyard grass Synergy is shown in Table 4, as a result, it has been found that having apparent synergy, trichlopyr in trichlopyr and pyroxsulam 37.5-150g a.i./hm2With pyroxsulam 1-4g a.i./hm2Between various dose combination to show actual measurement inhibiting rate super Theoretical 10% or more inhibiting rate out, that is, show synergistic effect.
2) synergy of trichlopyr and pyroxsulam to amur foxtail
Actual measurement fresh weight inhibition rate E of the trichlopyr pyroxsulam compounding agent of 5 different ratio of table to amur foxtail (%)
Theoretical fresh weight inhibition rate E of the trichlopyr pyroxsulam compounding agent of 6 different ratio of table to amur foxtail0 (%)
"/": the lower theoretical fresh weight inhibition rate (E of single dose processing0) it is equal to actual measurement fresh weight inhibition rate (E), synergy is not present
The synergy value [(E-E0) × 100] of the trichlopyr of 7 different ratio of table and pyroxsulam to amur foxtail
Note: E-E0> 10% indicates synergistic effect "/": the lower theoretical fresh weight inhibition rate (E of single dose processing0) fresh equal to surveying Synergy is not present in weight inhibiting rate (E)
As shown in Table 5, trichlopyr single dose is to amur foxtail almost without inhibitory effect;Pyroxsulam single dose 4g a.i./hm2When fresh weight inhibition rate be more than 40%, thus calculate the theoretical inhibiting rate that uses of two kinds of mixture of herbicides and be shown in Table 6.Pass through Compare actual measurement inhibiting rate under two kinds of herbicide difference compounded combinations and theoretical inhibiting rate, and then investigates two kinds of herbicides to seeing wheat The synergy of ma is shown in Table 7, as a result, it has been found that having apparent synergy, trichlorine pyrrole oxygen in trichlopyr and pyroxsulam Acetic acid 37.5-150g a.i./hm2With pyroxsulam 1-4g a.i./hm2Between various dose combination show actual measurement inhibit Rate exceeds theoretical 10% or more inhibiting rate, that is, shows synergistic effect.
3) synergy of trichlopyr and pyroxsulam to clearvers
Actual measurement fresh weight inhibition rate E of the trichlopyr pyroxsulam compounding agent of 8 different ratio of table to clearvers (%)
Theoretical fresh weight inhibition rate E of the trichlopyr pyroxsulam compounding agent of 9 different ratio of table to clearvers0 (%)
"/": the lower theoretical fresh weight inhibition rate (E of single dose processing0) it is equal to actual measurement fresh weight inhibition rate (E), synergy is not present
The synergy value [(E-E0) × 100] of the trichlopyr of 10 different ratio of table and pyroxsulam to clearvers
Note: E-E0> 10% indicates synergistic effect "/": the lower theoretical fresh weight inhibition rate (E of single dose processing0) fresh equal to surveying Synergy is not present in weight inhibiting rate (E)
As shown in Table 8, trichlopyr single dose is inhibited to clearvers, 150g a.i./hm2When inhibiting rate 34%;Pyroxsulam single dose is not so good as the former to clearvers inhibitory effect, 4g a.i./hm2When fresh weight inhibition rate be 28%, thus It calculates the theoretical inhibiting rate that two kinds of mixture of herbicides use and is shown in Table 9.By comparing the reality under two kinds of herbicide difference compounded combinations Inhibiting rate and theoretical inhibiting rate are surveyed, and then investigates two kinds of herbicides and 10 is shown in Table to the synergy of clearvers, as a result, it has been found that three Chlorine pyrrole fluoroacetic acid and pyroxsulam have apparent synergy, trichlopyr 37.5-150g a.i./hm2With pyridine sulphur grass Amine 1-4g a.i./hm2Between various dose combination show actual measurement inhibiting rate and exceed theoretical 10% or more inhibiting rate, i.e. table Reveal synergistic effect.
4) synergy of trichlopyr and pyroxsulam to field thistle
Actual measurement fresh weight inhibition rate E of the trichlopyr pyroxsulam compounding agent of 11 different ratio of table to field thistle (%)
Theoretical fresh weight inhibition rate E of the trichlopyr pyroxsulam compounding agent of 12 different ratio of table to field thistle0 (%)
"/": the lower theoretical fresh weight inhibition rate (E of single dose processing0) it is equal to actual measurement fresh weight inhibition rate (E), synergy is not present
The synergy value [(E-E0) × 100] of the trichlopyr of 13 different ratio of table and pyroxsulam to field thistle
Note: E-E0> 10% indicates synergistic effect "/": the lower theoretical fresh weight inhibition rate (E of single dose processing0) fresh equal to surveying Synergy is not present in weight inhibiting rate (E)
As shown in Table 11, trichlopyr single dose 150g a.i./hm2Handle the fresh weight inhibition rate to field thistle seedling Reach 38%;Pyroxsulam single dose 4g a.i./hm2Lower fresh weight inhibition rate 32% is handled, thus calculating two kinds of mixture of herbicides makes Theoretical inhibiting rate is shown in Table 12.Inhibit by comparing the actual measurement inhibiting rate under two kinds of herbicide difference compounded combinations with theoretical Rate, and then investigate two kinds of herbicides and 13 are shown in Table to the synergy of field thistle, as a result, it has been found that in trichlopyr and pyridine sulphur grass Amine has apparent synergy, trichlopyr 37.5-150g a.i./hm2With pyroxsulam 1-4g a.i./hm2Between Various dose combination shows actual measurement inhibiting rate and exceeds theoretical 10% or more inhibiting rate, that is, shows synergistic effect.
1.6 conclusion (of pressure testing)
4 kinds of weeds that this research is selected are that Qi Zhong of the common malignant weed , of wheatland Wang grass, amur foxtail represent wheatland grass Section's malignant weed;Clearvers, field thistle represent wheatland broadleaf class malignant weed.In summary result of study shows trichlorine pyrrole oxygen Acetic acid and pyroxsulam, which are used in compounding, all has inhibitory effect and synergy effect outstanding for all kinds of weeds.
Further analyze the proportion of trichlopyr and pyroxsulam compounded formula, trichlopyr 37.5-150g a.i./hm2With pyroxsulam 1-4g a.i./hm2Various combination compoundings show synergy, therefore, trichlopyr and pyridine The ratio range of sulphur grass amine is: trichlopyr: pyroxsulam=(9.375~150): 1.
Trichlopyr 37.5-150g a.i./hm2With pyroxsulam 2-4g a.i./hm2The connection of various combination compoundings Close threshold (E-E0) 25% or more, therefore, the more optimized ratio range of trichlopyr and pyroxsulam is: trichlorine Pyrrole fluoroacetic acid: pyroxsulam=(9.375~75): 1.
Trichlopyr 75-150g a.i./hm2With pyroxsulam 2-4g a.i./hm2The joint of various combination compoundings Threshold (E-E0) 35% or more, therefore, the more optimized ratio range of trichlopyr and pyroxsulam is: trichlorine pyrrole Fluoroacetic acid: pyroxsulam=(18.75~75): 1.
Embodiment 2: trichlopyr pyroxsulam compounding agent measures Safe to wheat
In order to measure safety of the compounding agent to wheat of trichlopyr pyroxsulam, in the controlled environment chamber in into A series of whole strain bioassay of row.Based on front as a result, with trichlopyr: pyroxsulam=37.5: 1 proportion is used for wheat Safety testing.
2.1 for studying object: raising wheat 23, Jimai 22.Wherein raising wheat 23 is suitable for planting in In Middle And Lower Reaches of Changjiang River, and Jimai 22 is suitable Suitable Northern Area of Huaihe River and the plantation of varieties in Huang-Huai-Hai Plain north piece.
2.2 dosage setting: trichlopyr+pyroxsulam: 0+0,75+2,150+4,300+8g a.i./hm2
2.3 test methods:
To Safe to wheat test respectively detection trichlopyr pyroxsulam compounding agent to the wheat 2-3 leaf phase, point The safety in tiller latter stage (before the jointing stage, stem starts jointing, jointing length < 1cm).
In the plastic casing that specification is 22 × 15 × 10cm, it is packed into and the organoclay of herbicide was not used (pH value 6.5, has Machine matter content 2.4%), soil layer height about 8cm in each box, plastic casing lower part is punched in order to absorb water.Plastic casing is put into 44 The thickening plastics transferring box (clear water for being previously added 2cm depth) of × 33 × 10cm, is placed in phjytotron and cultivates, 15 DEG C of illumination 12 hours, 10 DEG C dark 12 hours, keep about 0.5cm water layer in order to which the soil in plastic casing passes through in transferring box during test Water suction keeps wet.Each processing repeats 4 plastic casings.Stem is carried out before wheat 2-3 leaf phase, late tillering state start jointing respectively Leaf processing, control group spray equivalent clear water.The walking gesture voltage stabilization spray of Yangzhou University's gardening and plant protection institute is used by spraying Tower is sprayed, spray height 20cm, flat Fan spray head spraying swath 50cm, pressure 200KPa.Spray liquid measure corresponds to field hydrojet Amount is 45L water/hm2.After application 45 days, acquires and weighed in each plastic casing for trying wheat overground part fresh weight respectively, calculated not With the fresh weight inhibition rate for handling top over the ground.
Fresh weight inhibition rate=(control group fresh weight-processing group fresh weight) ÷ control group fresh weight × 100%
2.4 test result
Lower influence of the trichlopyr pyroxsulam compounding agent to wheat aerial part fresh weight of various dose processing is shown in Table 14, the results showed that, trichlopyr pyroxsulam is according to each for having under amount of reagent to wheat of 37.5: 1 proportion compounding agents There is preferable safety, < 10% equal to wheat fresh weight inhibition rate.
3 trichlopyr pyroxsulam compounding agent of table is to wheat overground part fresh weight inhibition rate
*: dosage is trichlopyr+pyroxsulam dosage.
2.5 conclusion (of pressure testing)
Trichlopyr pyroxsulam compounds 77-308g a.i./hm according to 37.5: 1 proportion2To small under processing Preferable safety was all had before wheat 2-3 leaf phase and tiller last jointing stage.
The inhibiting effect of 3 trichlopyr pyroxsulam compounding agent antagonism weeds of embodiment measures
Serious antiweed weeds are endangered to wheatland in order to measure the compounding agent of trichlopyr pyroxsulam Inhibiting effect, it is interior in the controlled environment chamber to carry out a series of whole strain bioassay.Comprehensively consider and the inhibiting rate and medicament of weeds are subtracted The principle used is measured, with trichlopyr: pyroxsulam=37.5: 1 proportion is for testing.
3.1 for trying weeds: anti-Jing dislikes azoles dogstail Ling Wang grass, anti-fenoxapropPethyl Alopecurus, anti-tribenuron-methyl and broadcasts ma Wormwood artemisia, anti-tribenuron-methyl ox chickweed, anti-tribenuron-methyl shepherd's purse, Chang Gui Wang grass, conventional Alopecurus, conventional Descurainia sophia, conventional ox chickweed, Conventional shepherd's purse.FenoxapropPethyl is aryloxyphenoxypropionate class herbicide, be wheat paddock dosage is maximum, application range most Wide gramineae weed cauline leaf process herbicide;Tribenuron-methyl is sulfonylurea herbicide, wealthy for the prevention and control of various regions wheat paddock for a long time Leaf weeds.Another aspect , Wang grass, Alopecurus, Descurainia sophia, ox chickweed and shepherd's purse are that China's wheatland sends out herbicide resistance The malignant weed of raw most serious.Therefore, the present embodiment is for trying object with above-mentioned Weed Resistance population, is pair with conventional population According to further research trichlopyr pyroxsulam is used for the potentiality that wheat paddock resistant weed is administered.
The setting of 3.2 doses:
Trichlopyr+pyroxsulam: 300+8g a.i./hm2
FenoxapropPethyl: 90g a.i./hm2
Tribenuron-methyl: 22.5g a.i./hm2
3.3 test methods:
It is cultivated in the square plastic plant that specification is 7 × 7 × 7cm and is packed into the organoclay that herbicide was not used in flowerpot (pH value 6.5, the content of organic matter 2.4%), adds water to saturation.Select full seed for trying weed seed, each small flower broadcasts Kind 20.One layer of fine earth (thickness about 3mm) is after planting covered on seed.Small flower is put into the thickening plastics of 44 × 33 × 10cm Transferring box (clear water for being previously added 2cm depth), is placed in phjytotron and cultivates, and 15 DEG C of illumination 12 hours, 10 DEG C of dark 12 are small When, keep 0.5cm or so water layer to keep wet by water suction in order to the soil in small whitepack in transferring box during test.15 days After start to each small flower final singling, each small flower retains the best seedling of 12 plants of growing ways.Each processing repeats 4 little Hua Basin.Wang grass and Alopecurus 3-4 leaf phase, Descurainia sophia, ox chickweed and shepherd's purse 6-8 leaf phase are using cauline leaf spray-on process progress herbicide Processing, control group spray equivalent clear water.The walking gesture voltage stabilization spray tower of Yangzhou University's gardening and plant protection institute is used by spraying It is sprayed, spray height 20cm, flat Fan spray head spraying swath 50cm, pressure 200KPa.Spray liquid measure corresponds to field spouting liquid For 45L water/hm2
After application 45 days, acquires and weighed in each plastic casing for trying plant above ground portion fresh weight respectively, calculate different disposal To the fresh weight inhibition rate of overground part.
Fresh weight inhibition rate=(control group fresh weight-processing group fresh weight) ÷ control group fresh weight × 100%
3.4 test result
The lower trichlopyr pyroxsulam compounding agent of various dose processing is to the weeds aerial part fresh weight for examination Influence is shown in Table 15 and table 16, the results showed that, trichlopyr pyroxsulam compounding agent is in 300+8g a.i./hm2At dosage Reason can effectively kill each resistant weed population and conventional weed population after 45 days, and combine the result of study of front, this test In trichlopyr and pyroxsulam compounding agent dose under to wheat safety.
The different herbicide antagonism of table 15 and Chang Gui Wang grass and the overground part fresh weight inhibition rate (%) of day too amur foxtail
The overground part fresh weight inhibition rate (%) of table 16 different herbicide antagonism and conventional broadleaf weeds
3.5 conclusion (of pressure testing)
Trichlopyr pyroxsulam can be used for the improvement of wheat paddock resistant weed, can be not only used for Chang Gui Wang grass, The prevention and treatment of Alopecurus, Descurainia sophia, ox chickweed, shepherd's purse, it can also be used to relevant resistant population prevention and control.
Embodiment 4: the quick-acting measurement of trichlopyr pyroxsulam compounding agent prevention and control weeds
In order to detect the quick-acting of trichlopyr pyroxsulam compounding agent management of weeds, in the controlled environment chamber in into A series of whole strain bioassay of row.Front is the result shows that trichlopyr 300g a.i./hm2+ pyroxsulam 8g a.i./hm2 Various weeds can effectively be killed and to wheat safety, therefore this research is careless using this dosage as trichlopyr pyridine sulphur The dosage of amine compounding agent is arranged.
4.1 for trying weeds: Wang grass, amur foxtail, shepherd's purse, Descurainia sophia.Qi Zhong Wang grass, amur foxtail represent wheat paddock grass family evil Property weeds;Shepherd's purse, Descurainia sophia represent wheat paddock broadleaf class malignant weed.
The setting of 4.2 doses:
T1: trichlopyr 300g a.i./hm2
T2: trichlopyr 300g a.i./hm2+ pyroxsulam 8g a.i./hm2
T3: pyroxsulam 8g a.i./hm2
T4: clear water control
4.3 test methods:
It is cultivated in the square plastic plant that specification is 7 × 7 × 7cm and is packed into the organoclay that herbicide was not used in flowerpot (pH value 6.5, the content of organic matter 2.4%), adds water to saturation.Select full seed Wang grass, amur foxtail, shepherd's purse, Descurainia sophia kind Son, each small flower sow 20.The thickening plastics transferring box that small flower is put into 44 × 33 × 10cm (is previously added 2cm depth Clear water), be placed in phjytotron and cultivate, 15 DEG C of illumination 12 hours, 10 DEG C dark 12 hours, protected in transferring box during test 0.5cm or so water layer is held in order to which the soil in small whitepack keeps wet by water suction.It is fixed to each small flower to start after 15 days Seedling, each small flower retain the best seedling of 12 plants of growing ways.Each processing repeats 4 small flowers.
Wang grass and Alopecurus 3-4 leaf phase, Descurainia sophia, ox chickweed and shepherd's purse 6-8 leaf phase are carried out using cauline leaf spray-on process Herbicide treatment, control group spray equivalent clear water.The walking gesture pressure stabilizing of Yangzhou University's gardening and plant protection institute is used by spraying Spray tower is sprayed, spray height 20cm, flat Fan spray head spraying swath 50cm, pressure 200KPa.Spray liquid measure corresponds to field Spouting liquid is 45L water/hm2
After application 15 days, 30 days, 60 days, acquires and weighed in each small flower for trying weeds overground part fresh weight, meter respectively Calculate aerial part fresh weight inhibition rate.
4.4 test result
Different disposal herbicide using latter 15 days, 30 days and 60 days to the fresh weight inhibition rate of various weeds be shown in Table 17, table 18, Table 19.The result shows that trichlopyr compounds the quick-acting that can greatly promote herbicide with pyroxsulam, especially it is administered After 15 days.The inhibiting rate after medication 15 days as the result is shown of table 17, to gramineae weed and Cyperaceae under two kinds of medicament single doses processing The preventive effect of weeds is not high, however has great synergistic effect when being used in compounding.It the results are shown in Table 18 Hes within 30 days after medication Table 19, as a result also indicates that, trichlopyr is compounded with pyroxsulam substantially drug effect to be accelerated to play, and trichlorine pyrrole oxygen second Acid compounds the herbicide dosage that can be substantially reduced with pyroxsulam.
The different herbicide applications of table 17 are after 15 days to the fresh weight inhibition rate (%) for trying weeds
T1: trichlopyr 300g a.i./hm2;T2: trichlopyr 300g a.i./hm2+ pyroxsulam 8g a.i./hm2;T3: pyroxsulam 8g a.i./hm2.
The different herbicide applications of table 18 are after 30 days to the fresh weight inhibition rate (%) for trying weeds
T1: trichlopyr 300g a.i./hm2;T2: trichlopyr 300g a.i./hm2+ pyroxsulam 8g a.i./hm2;T3: pyroxsulam 8g a.i./hm2.
The different herbicide applications of table 19 are after 60 days to the fresh weight inhibition rate (%) for trying weeds
T1: trichlopyr 300g a.i./hm2;T2: trichlopyr 300g a.i./hm2+ pyroxsulam 8g a.i./hm2;T3: pyroxsulam 8g a.i./hm2.
4.5 conclusion (of pressure testing)
Trichlopyr is compounded with pyroxsulam can greatly promote drug effect, and target weeds are largely withered after application 15 days Extremely.Wheat Seedling gets rid of weed competition as early as possible, forms enough tillers early and jointing envelope row (thoroughly establishes the competition to weeds Advantage) it is most important, it is the basis of High-yield Wheat.Therefore, this test result shows trichlopyr pyroxsulam compounding With great application value.

Claims (7)

1. a kind of Herbicidal combinations, which is characterized in that it by trichlopyr and pyroxsulam according to weight ratio (9.375~ 150): 1 proportion composition.
2. Herbicidal combinations according to claim 1, which is characterized in that trichlopyr and pyroxsulam trichlorine pyrrole oxygen The weight ratio of acetic acid and pyroxsulam is (9.375~75): 1.
3. Herbicidal combinations according to claim 1, which is characterized in that the weight ratio of trichlopyr and pyroxsulam For (18.75~75): 1.
4. application of the Herbicidal combinations described in claim 1 in prevention and control wheat weeds.
5. application according to claim 4, which is characterized in that the weeds are gramineae weed, broad leaved weeds.
6. application according to claim 4, which is characterized in that the weeds are resistant weed.
7. application according to claim 4, which is characterized in that the herbicidal composition is used as cauline leaf process agent It can be used before wheat 2-3 leaf phase or wheat turn green to jointing.
CN201810980141.2A 2018-08-24 2018-08-24 A kind of Herbicidal combinations and its application containing trichlopyr and pyroxsulam Pending CN108990998A (en)

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Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1761395A (en) * 2003-03-13 2006-04-19 巴斯福股份公司 Synergistically acting herbicidal mixtures
CN102326567A (en) * 2011-10-21 2012-01-25 联保作物科技有限公司 Wheat field weeding composition and preparation thereof

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1761395A (en) * 2003-03-13 2006-04-19 巴斯福股份公司 Synergistically acting herbicidal mixtures
CN102326567A (en) * 2011-10-21 2012-01-25 联保作物科技有限公司 Wheat field weeding composition and preparation thereof

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Application publication date: 20181214