CN108976922A - A kind of fire resistant special type coating and preparation method thereof - Google Patents
A kind of fire resistant special type coating and preparation method thereof Download PDFInfo
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- CN108976922A CN108976922A CN201810502497.5A CN201810502497A CN108976922A CN 108976922 A CN108976922 A CN 108976922A CN 201810502497 A CN201810502497 A CN 201810502497A CN 108976922 A CN108976922 A CN 108976922A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D125/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an aromatic carbocyclic ring; Coating compositions based on derivatives of such polymers
- C09D125/02—Homopolymers or copolymers of hydrocarbons
- C09D125/04—Homopolymers or copolymers of styrene
- C09D125/06—Polystyrene
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/18—Fireproof paints including high temperature resistant paints
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/63—Additives non-macromolecular organic
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/65—Additives macromolecular
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
Abstract
The invention discloses a kind of fire resistant special type coating and preparation method thereof, it is made by containing the following parts by weight: 65-85 parts of polystyrene, 3-(perfluor -5- methylhexyl) 15-25 parts of -2- hydroxy propyl methacrylate, 12-20 parts of filler, 1- [(2- ethoxy) amino] -4- [(2- hydroxypropyl) amino] -9,5-9 parts of 10- amerantrone, 5-9 parts of Nipasol, 3-5 parts of high temperature resistant auxiliary agent, 2,7- bis- (4,4,5,5- tetramethyl -1,3- dioxy -2- boryl) 0.5-1 parts of -9,9- dioctyl fluorene；Wherein, the high temperature resistant auxiliary agent is made by anthraquinone-2-sodium, the chloro- 5- nitroaniline of 3-, hydroxymethyl cellulose, isophorone diisocyanate.The present invention also provides a kind of preparation methods of fire resistant special type coating.
Description
Technical field
The invention belongs to paint field, in particular to a kind of fire resistant special type coating and preparation method thereof.
Background technique
High-temperature resistant coating generally refers to that 200 degrees Celsius of temperatures above can be born for a long time, and is able to maintain certain physical chemistry
Performance, the special functional coating that makes protected object in the high temperature environment and can normally play a role.It generally can be by by borosilicate
Silicate glass is filled into resin matrix as main stuffing, improves high temperature resistance, to form a kind of high-temperature resistant coating.
It wherein, is high-temperature resistant anti-corrosive of the organosilicon aluminium paint for aircraft engine with most common high-temperature resistant coating earliest
Coating, but due to organosilicon bad mechanical property itself, adhesive force is low, wears no resistance, solvent resistance is low, is not able to satisfy increasingly
Requirement of the modern times to heat-resisting material.
Summary of the invention
In view of the above requirements, invention especially provides a kind of fire resistant special type coating and preparation method thereof.
The purpose of the present invention can be achieved through the following technical solutions:
A kind of fire resistant special type coating, is made by containing the following parts by weight:
65-85 parts of polystyrene,
3-(perfluor -5- methylhexyl) 15-25 parts of -2- hydroxy propyl methacrylate,
12-20 parts of filler,
1- [(2- ethoxy) amino] -4- [(2- hydroxypropyl) amino] 5-9 parts of -9,10- amerantrone,
5-9 parts of Nipasol,
3-5 parts of high temperature resistant auxiliary agent,
0.5-1 parts of -9,9- dioctyl fluorene of 2,7- bis- (4,4,5,5- tetramethyl -1,3- dioxy -2- boryl)；
Wherein, the high temperature resistant auxiliary agent is by anthraquinone-2-sodium, the chloro- 5- nitroaniline of 3-, hydroxymethyl cellulose, isophorone
Diisocyanate is made.
The filler is the mixture of porcelain powder, aluminosilicate and manganese iso-octoate.
The mass ratio of porcelain powder, the aluminosilicate and the manganese iso-octoate described in the mixture is 1:1-2:0.5.
The high temperature resistant auxiliary agent is made by following methods: anthraquinone-2-sodium, the chloro- 5- nitroaniline of 3-, methylol is fine
Dimension element, isophorone diisocyanate under a nitrogen atmosphere, 110-120 DEG C, stir 3-6 hours under 22-24MPa.
The chloro- 5- nitroaniline of the anthraquinone-2-sodium, the 3-, the hydroxymethyl cellulose, the isophorone two
The mass ratio of isocyanates is 1:2-7:8-20:0.2-1.
A kind of preparation method of fire resistant special type coating, method includes the following steps:
(1) by filler 12-20 parts by weight, high temperature resistant auxiliary agent 3-5 parts by weight and the (4,4,5,5- tetramethyl -1,3- two of 2,7- bis-
Oxygen -2- boryl) -9,9- dioctyl fluorene 0.5-1 parts by weight be added ball mill in mix 5-10 minutes；
(2) polystyrene 65-85 parts by weight, 3-(perfluor -5- methylhexyl are sequentially added) -2- hydroxy propyl methacrylate
15-25 parts by weight, 1- [(2- ethoxy) amino] -4- [(2- hydroxypropyl) amino] -9,10- amerantrone 5-9 parts by weight, oxybenzene third
Ester 5-9 parts by weight mix 15-30 minutes at 90-120 DEG C in an extruder, crush, sieving, obtain the fire resistant special type and apply
Material.
The filler is the mixture of porcelain powder, aluminosilicate and manganese iso-octoate.
The mass ratio of porcelain powder, the aluminosilicate and the manganese iso-octoate described in the mixture is 1:1-2:0.5.
The high temperature resistant auxiliary agent is made by following methods: anthraquinone-2-sodium, the chloro- 5- nitroaniline of 3-, methylol is fine
Dimension element, isophorone diisocyanate under a nitrogen atmosphere, 110-120 DEG C, stir 3-6 hours under 22-24MPa.
The chloro- 5- nitroaniline of the anthraquinone-2-sodium, the 3-, the hydroxymethyl cellulose, the isophorone two
The mass ratio of isocyanates is 1:2-7:8-20:0.2-1.
Compared with prior art, the present invention has the advantages that:
(1) fire resistant special type coating of the invention is by polystyrene, 3-(perfluor -5- methylhexyl) -2- hydroxypropylmethyl
Acrylate, filler, 1- [(2- ethoxy) amino] -4- [(2- hydroxypropyl) amino] -9,10- amerantrone, Nipasol,
The preparation such as high temperature resistant auxiliary agent and 2,7- bis- (4,4,5,5- tetramethyl -1,3- dioxy -2- boryl) -9,9- dioctyl fluorene
At, since the proportion of each component is all that have passed through stringent screening, and different component makes material have good mechanics strong
Degree and bond strength, have the stability of material and antioxygenic property also and largely improve,
(2) fire resistant special type coating of the invention has good heat-resisting quantity, and at a certain temperature, material surface will not be sent out
It is viscous, and mechanical strength remains to keep well, the stability of material is preferable.
(3) fire resistant special type coating of the present invention has good surface hardness, can resist a degree of scraping.
Specific embodiment
The present invention is further illustrated with reference to embodiments.
Embodiment 1
By the chloro- 5- nitroaniline 2kg of anthraquinone-2-sodium 1kg, 3-, hydroxymethyl cellulose 8kg, isophorone diisocyanate
0.2kg under a nitrogen atmosphere, 110 DEG C, stir 3 hours under 24MPa, obtain high temperature resistant auxiliary agent.
Embodiment 2
By the chloro- 5- nitroaniline 7kg of anthraquinone-2-sodium 1kg, 3-, hydroxymethyl cellulose 20kg, isophorone diisocyanate
1kg under a nitrogen atmosphere, 120 DEG C, stir 6 hours under 22MPa, obtain high temperature resistant auxiliary agent.
Embodiment 3
(1) by high temperature resistant the auxiliary agent 3kg and 2,7- in porcelain powder 4.8kg, aluminosilicate 4.8kg, manganese iso-octoate 2.4kg, embodiment 1
Two (4,4,5,5- tetramethyl -1,3- dioxy -2- boryl) -9,9- dioctyl fluorene 0.5kg are added in ball mill and mix 5 minutes；
(2) polystyrene 65kg, 3-(perfluor -5- methylhexyl is sequentially added) -2- hydroxy propyl methacrylate 15kg, 1-
[(2- ethoxy) amino] -4- [(2- hydroxypropyl) amino] -9,10- amerantrone 5kg, Nipasol 5kg, 90 DEG C in an extruder
Lower mixing 30 minutes, crushes, and sieving obtains fire resistant special type coating.
The performance test results of fire resistant special type coating obtained are as shown in table 1.
Embodiment 4
(1) by the high temperature resistant auxiliary agent 5kg and 2 in porcelain powder 5.7kg, aluminosilicate 11.4kg, manganese iso-octoate 2.9kg, embodiment 1,
(4,4,5,5- tetramethyl -1,3- dioxy -2- the boryl) -9,9- dioctyl fluorene 1kg of 7- bis-, which is added in ball mill, mixes 10 points
Clock；
(2) polystyrene 85kg, 3-(perfluor -5- methylhexyl is sequentially added) -2- hydroxy propyl methacrylate 25kg, 1-
[(2- ethoxy) amino] -4- [(2- hydroxypropyl) amino] -9,10- amerantrone 9kg, Nipasol 9kg, in an extruder 120
It mixes 15 minutes, crushes at DEG C, sieving obtains fire resistant special type coating.
The performance test results of fire resistant special type coating obtained are as shown in table 1.
Embodiment 5
(1) by the high temperature resistant auxiliary agent 4kg and 2 in porcelain powder 5.7kg, aluminosilicate 11.4kg, manganese iso-octoate 2.9kg, embodiment 2,
(4,4,5,5- tetramethyl -1,3- dioxy -2- the boryl) -9,9- dioctyl fluorene 0.8kg of 7- bis-, which is added in ball mill, mixes 8 points
Clock；
(2) polystyrene 73kg, 3-(perfluor -5- methylhexyl is sequentially added) -2- hydroxy propyl methacrylate 22kg, 1-
[(2- ethoxy) amino] -4- [(2- hydroxypropyl) amino] -9,10- amerantrone 7kg, Nipasol 7kg, in an extruder 100
It mixes 20 minutes, crushes at DEG C, sieving obtains fire resistant special type coating.
The performance test results of fire resistant special type coating obtained are as shown in table 1.
Embodiment 6
(1) by the high temperature resistant auxiliary agent 5kg and 2 in porcelain powder 5.7kg, aluminosilicate 11.4kg, manganese iso-octoate 2.9kg, embodiment 2,
(4,4,5,5- tetramethyl -1,3- dioxy -2- the boryl) -9,9- dioctyl fluorene 1kg of 7- bis-, which is added in ball mill, mixes 10 points
Clock；
(2) polystyrene 85kg, 3-(perfluor -5- methylhexyl is sequentially added) -2- hydroxy propyl methacrylate 25kg, 1-
[(2- ethoxy) amino] -4- [(2- hydroxypropyl) amino] -9,10- amerantrone 9kg, Nipasol 9kg, in an extruder 120
It mixes 15 minutes, crushes at DEG C, sieving obtains fire resistant special type coating.
The performance test results of fire resistant special type coating obtained are as shown in table 1.
Comparative example 1
(1) by the chloro- 5- nitroaniline 1kg of anthraquinone-2-sodium 0.2kg, 3-, hydroxymethyl cellulose 8kg, two isocyanide of isophorone
Acid esters 1kg, porcelain powder 4.8kg, aluminosilicate 4.8kg, 2,7- bis- (4,4,5,5- tetramethyl -1,3- dioxy -2- boryl) -9,
9- dioctyl fluorene 0.5kg is added in ball mill and mixes 5 minutes；
(2) polystyrene 65kg, 3-(perfluor -5- methylhexyl is added) -2- hydroxy propyl methacrylate 15kg, oxybenzene third
Ester 5kg is mixed 30 minutes at 90 DEG C in an extruder, is crushed, and sieving obtains fire resistant special type coating.
The fire resistant special type coating of embodiment 3-5 and comparative example 1 is used to test, concrete outcome is see table 1.
Table 1
| Test item | Surface hardness | 10 minutes at 380 DEG C |
| Embodiment 3 | 4H | It is unchanged |
| Embodiment 4 | 4H | It is unchanged |
| Embodiment 5 | 4H | It is unchanged |
| Comparative example 1 | H | Have under liquid flow |
The present invention is not limited to embodiment here, those skilled in the art's announcement according to the present invention does not depart from scope
The improvement and modification made all should be within protection scope of the present invention.
Claims (10)
1. a kind of fire resistant special type coating, which is characterized in that be made by containing the following parts by weight:
65-85 parts of polystyrene,
3-(perfluor -5- methylhexyl) 15-25 parts of -2- hydroxy propyl methacrylate,
12-20 parts of filler,
1- [(2- ethoxy) amino] -4- [(2- hydroxypropyl) amino] 5-9 parts of -9,10- amerantrone,
5-9 parts of Nipasol,
3-5 parts of high temperature resistant auxiliary agent,
0.5-1 parts of -9,9- dioctyl fluorene of 2,7- bis- (4,4,5,5- tetramethyl -1,3- dioxy -2- boryl)；
Wherein, the high temperature resistant auxiliary agent is by anthraquinone-2-sodium, the chloro- 5- nitroaniline of 3-, hydroxymethyl cellulose, isophorone
Diisocyanate is made.
2. fire resistant special type coating according to claim 1, which is characterized in that the filler be porcelain powder, aluminosilicate and
The mixture of manganese iso-octoate.
3. fire resistant special type coating according to claim 2, which is characterized in that porcelain powder described in the mixture, the aluminium
The mass ratio of silicate and the manganese iso-octoate is 1:1-2:0.5.
4. fire resistant special type coating according to claim 1, which is characterized in that the high temperature resistant auxiliary agent is by following methods system
: by anthraquinone-2-sodium, the chloro- 5- nitroaniline of 3-, hydroxymethyl cellulose, isophorone diisocyanate in condition of nitrogen gas
Under, 110-120 DEG C, stir 3-6 hours under 22-24MPa.
5. fire resistant special type coating according to claim 4, which is characterized in that the anthraquinone-2-sodium, the 3- are chloro-
5- nitroaniline, the hydroxymethyl cellulose, the isophorone diisocyanate mass ratio be 1:2-7:8-20:0.2-1.
6. the preparation method of fire resistant special type coating according to claim 1, which is characterized in that this method includes following step
It is rapid:
(1) by filler 12-20 parts by weight, high temperature resistant auxiliary agent 3-5 parts by weight and the (4,4,5,5- tetramethyl -1,3- two of 2,7- bis-
Oxygen -2- boryl) -9,9- dioctyl fluorene 0.5-1 parts by weight be added ball mill in mix 5-10 minutes；
(2) polystyrene 65-85 parts by weight, 3-(perfluor -5- methylhexyl are sequentially added) -2- hydroxy propyl methacrylate
15-25 parts by weight, 1- [(2- ethoxy) amino] -4- [(2- hydroxypropyl) amino] -9,10- amerantrone 5-9 parts by weight, oxybenzene third
Ester 5-9 parts by weight mix 15-30 minutes at 90-120 DEG C in an extruder, crush, sieving, obtain the fire resistant special type and apply
Material.
7. the preparation method of fire resistant special type coating according to claim 6, which is characterized in that the filler be porcelain powder,
The mixture of aluminosilicate and manganese iso-octoate.
8. the preparation method of fire resistant special type coating according to claim 7, which is characterized in that porcelain described in the mixture
The mass ratio of powder, the aluminosilicate and the manganese iso-octoate is 1:1-2:0.5.
9. the preparation method of fire resistant special type coating according to claim 6, which is characterized in that the high temperature resistant auxiliary agent by with
Lower section method is made: anthraquinone-2-sodium, the chloro- 5- nitroaniline of 3-, hydroxymethyl cellulose, isophorone diisocyanate are existed
Under condition of nitrogen gas, 110-120 DEG C, stir 3-6 hours under 22-24MPa.
10. the preparation method of fire resistant special type coating according to claim 9, which is characterized in that the anthraquinone-2-sulfonic acid
The chloro- 5- nitroaniline of sodium, the 3-, the hydroxymethyl cellulose, the isophorone diisocyanate mass ratio be 1:2-
7:8-20:0.2-1。
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110184562A (en) * | 2019-03-11 | 2019-08-30 | 苏州金言来新材料科技有限公司 | A kind of steel workpiece vacuum aluminizing method |
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