CN108970811A - A kind of gutter oil microwave-heating gas is used for the method and device of coal slime flotation - Google Patents

A kind of gutter oil microwave-heating gas is used for the method and device of coal slime flotation Download PDF

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Publication number
CN108970811A
CN108970811A CN201810889204.3A CN201810889204A CN108970811A CN 108970811 A CN108970811 A CN 108970811A CN 201810889204 A CN201810889204 A CN 201810889204A CN 108970811 A CN108970811 A CN 108970811A
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CN
China
Prior art keywords
gas
microwave
flotation
gutter oil
coal slime
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201810889204.3A
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Chinese (zh)
Inventor
沈亮
焦瑞青
杨永琪
蔡川川
周伟
王超
朱金波
乔二乐
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Anhui University of Science and Technology
Original Assignee
Anhui University of Science and Technology
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Anhui University of Science and Technology filed Critical Anhui University of Science and Technology
Priority to CN201810889204.3A priority Critical patent/CN108970811A/en
Publication of CN108970811A publication Critical patent/CN108970811A/en
Pending legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B03SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
    • B03DFLOTATION; DIFFERENTIAL SEDIMENTATION
    • B03D1/00Flotation
    • B03D1/001Flotation agents
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10BDESTRUCTIVE DISTILLATION OF CARBONACEOUS MATERIALS FOR PRODUCTION OF GAS, COKE, TAR, OR SIMILAR MATERIALS
    • C10B55/00Coking mineral oils, bitumen, tar, and the like or mixtures thereof with solid carbonaceous material
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B03SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
    • B03DFLOTATION; DIFFERENTIAL SEDIMENTATION
    • B03D2201/00Specified effects produced by the flotation agents
    • B03D2201/02Collectors

Abstract

The invention discloses the method and devices that a kind of gutter oil microwave-heating gas is used for coal slime flotation.The specific method is as follows: being placed in the gutter oil in trench oil drum in three in microwave reactor mouthfuls of quartz flasks by the suction of pan feeding pipeline using peristaltic pump; it is pyrolyzed under certain microwave heating power; the pyrolysis gas that pyrolysis generates is passed directly into the flotation cell on flotation device, while the protective gas of conditions of certain gas flow being continually fed into three mouthfuls of quartz flasks by protective gas pipeline.By the above-mentioned means, the present invention can reduce coal slime flotation cost and improve flotation efficiency, have preferable social benefit, environmental benefit and economic benefit while gutter oil is effectively treated.

Description

A kind of gutter oil microwave-heating gas is used for the method and device of coal slime flotation
Technical field
The present invention relates to the method and devices that a kind of gutter oil microwave-heating gas is used for coal slime flotation, belong to the utilization of resources Technical field.
Background technique
With the development of economy, catering trade market persistently keeps good situation.It can be generated in catering trade actual operation A large amount of waste grease, that is, gutter oil.If gutter oil is without effective processing, it will bring some undesirable influences.One side Face, if being discharged into the Nature without processing, with certain pollution and the wasting of resources;On the other hand, if flowing again Enter catering market, it will bring potential threat to people's health.Therefore, it is carried out reasonably handling to reach sharp again With being a kind of urgent demand.And the non-polar hydrocarbon oil collecting agent used in the coal slime floating process in coal industry field There is close place with such oil, it, can be while solving the problems, such as gutter oil if the two can link together, and it can be significantly Reduce industrial cost.
Summary of the invention
The object of the present invention is to provide the method and devices that a kind of gutter oil microwave-heating gas is used for coal slime flotation;The party Method and device can convert gutter oil to the substance that can replace collecting agent used in coal slime floating process.The method both may be used To solve the environmental problem and social concern of gutter oil, the cost of coal slime flotation process also can be effectively reduced.
The technical solution adopted in the present invention is as follows:
The gutter oil in trench oil drum is pumped into three mouthfuls be placed in microwave reactor by pan feeding pipeline using peristaltic pump It in quartz flask, is pyrolyzed under certain microwave heating power, the pyrolysis gas for being pyrolyzed generation is direct by pyrolysis gas duct It is passed through in the flotation cell on flotation device, the protective gas in gas cylinder is with certain gas flow by being equipped with gas flowmeter Protective gas pipeline is continually fed into three mouthfuls of quartz flasks.
A kind of above-mentioned gutter oil microwave-heating gas is used for the method and device of coal slime flotation, the microwave reactor Working frequency be 915MHz.
A kind of above-mentioned gutter oil microwave-heating gas is used for the method and device of coal slime flotation, the microwave heating function Rate is 2000W-5000W.
A kind of above-mentioned gutter oil microwave-heating gas is used for the method and device of coal slime flotation, and the protective gas is Refer to nitrogen or argon gas.
A kind of above-mentioned gutter oil microwave-heating gas is used for the method and device of coal slime flotation, and the gas flow is 30-100ml/min。
Beneficial effects of the present invention are shown: converting institute in coal slime floating process for gutter oil using microwave-heating technology Using the substitute of collecting agent, on the one hand efficiently solve society and the environmental problem of gutter oil, on the other hand with traditional coal slime Flotation is compared with collecting agent, this substitute is passed through in gaseous form, is highly dispersed in flotation cell, has better flotation effect Fruit, while its price is more cheap.
Detailed description of the invention
Fig. 1 is a kind of schematic diagram of the gutter oil microwave-heating gas of the present invention for the method and device of coal slime flotation.
Appended drawing reference meaning in Fig. 1 is as follows:
1-trench oil drum, 2-pan feeding pipelines, 3-peristaltic pumps, 4-three mouthfuls of quartz flasks, 5-microwave reactors, 6-heat Solve gas pipeline, 7-flotation cells, 8-flotation devices, 9-gas cylinders, 10-protective gas pipelines, 11-gas flowmeters
Fig. 2 is the relationship in present example 1 between clean coal yield and ash content and collector dosage.
Specific embodiment
For ease of understanding, specific embodiments of the present invention are made described further below:
Embodiment 1: the gutter oil in trench oil drum is placed in microwave reactor by the suction of pan feeding pipeline using peristaltic pump In three mouthfuls of quartz flasks in and be pyrolyzed under 2000W heating condition, the pyrolysis gas for being pyrolyzed generation is passed directly on flotation device Flotation cell in, while continue be passed through into three mouthfuls of quartz flasks flow be 40ml/min nitrogen.
Embodiment 2: the gutter oil in trench oil drum is placed in microwave reactor by the suction of pan feeding pipeline using peristaltic pump In three mouthfuls of quartz flasks in and be pyrolyzed under 4000W heating condition, the pyrolysis gas for being pyrolyzed generation is passed directly on flotation device Flotation cell in, while continue be passed through into three mouthfuls of quartz flasks flow be 60ml/min argon gas.
This specification is only that preferred embodiments of the present invention will be described, is not limited the scope of the present invention Fixed, without departing from the spirit of the design of the present invention, those of ordinary skill in the art make technical solution of the present invention Various changes and improvements should fall within the scope of protection determined by the claims of the present invention.

Claims (5)

1. the method and device that a kind of gutter oil microwave-heating gas is used for coal slime flotation, which is characterized in that peristaltic pump (3) is by ground Gutter oil in ditch oil drum (1) is pumped into three mouthfuls of quartz flasks (4) being placed in microwave reactor (5) by pan feeding pipeline (2), It is pyrolyzed under certain microwave heating power, the pyrolysis gas for being pyrolyzed generation is passed directly into flotation by pyrolysis gas duct (6) In flotation cell (7) on machine (8), the protective gas in gas cylinder (9) is with certain gas flow by being equipped with gas flowmeter Protective gas pipeline (10) be continually fed into three mouthfuls of quartz flasks (4).
2. a kind of gutter oil microwave-heating gas according to claim 1 is used for the method and device of coal slime flotation, special Sign is that the working frequency of the microwave reactor is 915MHz.
3. a kind of gutter oil microwave-heating gas according to claim 1 is used for the method and device of coal slime flotation, special Sign is that the microwave heating power is 2000W-5000W.
4. a kind of gutter oil microwave-heating gas according to claim 1 is used for the method and device of coal slime flotation, special Sign is that the protective gas refers to nitrogen or argon gas.
5. a kind of gutter oil microwave-heating gas according to claim 1 is used for the method and device of coal slime flotation, special Sign is that the gas flow is 30-100ml/min.
CN201810889204.3A 2018-08-07 2018-08-07 A kind of gutter oil microwave-heating gas is used for the method and device of coal slime flotation Pending CN108970811A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201810889204.3A CN108970811A (en) 2018-08-07 2018-08-07 A kind of gutter oil microwave-heating gas is used for the method and device of coal slime flotation

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201810889204.3A CN108970811A (en) 2018-08-07 2018-08-07 A kind of gutter oil microwave-heating gas is used for the method and device of coal slime flotation

Publications (1)

Publication Number Publication Date
CN108970811A true CN108970811A (en) 2018-12-11

Family

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CN201810889204.3A Pending CN108970811A (en) 2018-08-07 2018-08-07 A kind of gutter oil microwave-heating gas is used for the method and device of coal slime flotation

Country Status (1)

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CN (1) CN108970811A (en)

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2365492A (en) * 2000-08-07 2002-02-20 Finch Internat Ltd Method of combusting fuel in a compression-ignition engine
JP3898918B2 (en) * 2001-08-07 2007-03-28 俊正 板倉 Fertilizer manufacturing method
CN101058734A (en) * 2007-05-31 2007-10-24 张付舜 Device for industrially synthesizing biological diesel oil by microwave and method thereof
CN101058097A (en) * 2007-05-31 2007-10-24 张虎明 Resource using method for food and drink garbage
CN102580650A (en) * 2012-02-10 2012-07-18 中国石油大学(北京) Continuous reaction device and method for microwave biomass pyrolysis
CN204544468U (en) * 2015-04-25 2015-08-12 西安科技大学 A kind of coal slime flotation system based on gasification collecting agent
CN107674699A (en) * 2017-11-06 2018-02-09 南昌大学 A kind of method of the saponified fast pyrogenation of waste cooking oil

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2365492A (en) * 2000-08-07 2002-02-20 Finch Internat Ltd Method of combusting fuel in a compression-ignition engine
JP3898918B2 (en) * 2001-08-07 2007-03-28 俊正 板倉 Fertilizer manufacturing method
CN101058734A (en) * 2007-05-31 2007-10-24 张付舜 Device for industrially synthesizing biological diesel oil by microwave and method thereof
CN101058097A (en) * 2007-05-31 2007-10-24 张虎明 Resource using method for food and drink garbage
CN102580650A (en) * 2012-02-10 2012-07-18 中国石油大学(北京) Continuous reaction device and method for microwave biomass pyrolysis
CN204544468U (en) * 2015-04-25 2015-08-12 西安科技大学 A kind of coal slime flotation system based on gasification collecting agent
CN107674699A (en) * 2017-11-06 2018-02-09 南昌大学 A kind of method of the saponified fast pyrogenation of waste cooking oil

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Application publication date: 20181211