CN108956234A - A kind of sodium table status monitoring device and its operation method - Google Patents

A kind of sodium table status monitoring device and its operation method Download PDF

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Publication number
CN108956234A
CN108956234A CN201810972245.9A CN201810972245A CN108956234A CN 108956234 A CN108956234 A CN 108956234A CN 201810972245 A CN201810972245 A CN 201810972245A CN 108956234 A CN108956234 A CN 108956234A
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CN
China
Prior art keywords
cup
liquid
overflow
valve
level switch
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Pending
Application number
CN201810972245.9A
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Chinese (zh)
Inventor
张宇
赵东海
张建忠
常家强
梁雨晨
石岩
刘翔
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Jiangsu Nuclear Power Corp
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Jiangsu Nuclear Power Corp
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Application filed by Jiangsu Nuclear Power Corp filed Critical Jiangsu Nuclear Power Corp
Priority to CN201810972245.9A priority Critical patent/CN108956234A/en
Publication of CN108956234A publication Critical patent/CN108956234A/en
Pending legal-status Critical Current

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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q

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  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Control Of Non-Electrical Variables (AREA)

Abstract

The invention belongs to power station on-line chemical monitoring instrument signal processing technology fields, and in particular to a kind of sodium table status monitoring device and its operation method;It include: that sampling valve is connected with other valve, flowmeter and calibration valve in turn from the bottom to top;The calibration valve is connect with diffuser, and is arranged in alkalizing agent bottle;Alkalizing agent bottle connects measuring cup;Measuring cup connects transmitter, and the transmitter is also connected with air pump and overflow cup;The overflow cup, measuring cup are separately connected with catch basin;The other valve is connect with overflow cup.The present invention be used to solve sodium table at the scene in use because the start and stop state of make-up water preparation system change frequently trigger it is useless the technical issues of outranging warning message.

Description

A kind of sodium table status monitoring device and its operation method
Technical field
The invention belongs to power station on-line chemical monitoring instrument signal processing technology fields, and in particular to a kind of sodium table status monitoring dress It sets and its operation method.
Background technique
Sodium ion is one of the index that emphasis monitors in the water chemistry monitor system of power station, certain nuclear power station make up water treatment system It needs to be monitored Na ion concentration, to guarantee that the water quality indicator for process system is met the requirements.Existing make-up water preparation System uses intermittent duty mode, carries out water processed or stoppage in transit according to unit demand.When water manufacturing system is stopped transport, one side sample introduction stream Great changes have taken place when amount relatively operates normally, and instrument measurement numerical value also correspondingly generates relatively large deviation;On the other hand, instrument measurement cup Interior liquid level is insufficient, and under air pump purging, sodium ion electrode surface is in alternation of wetting and drying variable condition, causes measured value to have larger Fluctuation, more than the alarm limits of instrument, is frequent in master control room monitoring screen and outranges alarm.And in system shutdown state Under, such no practical significance of alarm, the alarm frequently occurred can influence in master control ASD picture brush screen instead and interference manipulates The normal monitoring of member and operation.If move back fortune instrument manually, but there are the response time slow (move back fortune and come into operation not in time), put into operation just The too long problem of phase instrument unavailable time.Therefore it is above-mentioned for solving to need to design a modified sodium table status monitoring device Problem.
Summary of the invention
Object of the present invention is to provide a kind of sodium table status monitoring device and its operation side in view of the above shortcomings of the prior art Method frequently triggers for solving start and stop state change of the sodium table at the scene in use because of make-up water preparation system and useless outranges The technical issues of warning message.
The technical scheme is that
A kind of sodium table status monitoring device, comprising: sampling valve is connected with other valve, flowmeter and calibration in turn from the bottom to top Valve;The calibration valve is connect with diffuser, and is arranged in alkalizing agent bottle;Alkalizing agent bottle connects measuring cup;Measuring cup connects Transmitter is connect, the transmitter is also connected with air pump and overflow cup;The overflow cup, measuring cup connect with catch basin respectively It connects;The other valve is connect with overflow cup.
Measuring electrode, reference electrode and temperature electrode are respectively arranged in measuring cup as described above.
Liquid-level switch, liquid-level switch contact, slide bar and magnetic float are additionally provided in overflow cup as described above;The overflow cup Nuclear power station is also respectively connected and operates normally I&C system and analyzer transmitter.
Slide bar as described above is vertically set on inside overflow cup, and slide bar upper end, magnetic float is arranged in the liquid-level switch contact It is arranged on slide bar, magnetic float floats up and down under buoyancy along slide bar.
Liquid-level switch as described above is integrated in the overflow cup in sampling valve downstream, and liquid-level switch contact is in normally open, It is connected on instrument signal output line, overflow cup is mounted on the position higher than measuring cup.
A kind of operation method of sodium table status monitoring device as described above, water sample enter gauge internal pipeline by sampling valve, Alkalization bottle is flowed through after other valve, flowmeter adjust flow, measuring cup is entered after sample alkalization, and air pump is continuous into measuring cell Bubble is blasted to believe the Na ion concentration chemistry in water sample to be measured with stirred sample and cleaning measuring electrode surface, electrode system It is exported through transmitter to monitoring screen after number being converted to electric signal;
When overflow cup liquid level reach a certain height, liquid-level switch contact is closed under magnetic float magneticaction;When water processed When system operates normally, overflow cup, which is in, is full of overflow situation, and magnetic float is close to liquid-level switch contact, and liquid-level switch contact is in magnetic It is closed under float magneticaction, instrument signal normally exports to nuclear power station and operates normally I&C system, and master control room ASD is normally shown Instrument currently measures indicating value;When water manufacturing system is stopped transport, sample introduction flow substantially reduces until stopping, at this time in overflow cup under liquid level Drop, magnetic float drop down onto overflow bottom of the tube, and two contacts of liquid-level switch disconnect, and instrument stops output signal, master control room monitoring screen Only exist channel failure warning note.
The invention has the following advantages:
When water manufacturing system is in stoppage in transit or inspecting state, liquid level decline in overflow cup, triggering liquid-level switch disconnects, stops Upload communication, will not frequently occur sodium ion in master control ASD transfinites value alarm, and channel failure alarm, operator only occurs in instrument State in conjunction with current system is the warning reason that can determine whether instrument, does not influence normal monitoring.Fortune and the instrument that comes into operation are moved back with manual It compares, a large amount of manpower and material resources costs can be saved, while also having many advantages, such as that the response time is fast, resetting time is short.
Detailed description of the invention
Fig. 1: being a kind of Na ion concentration table work flow diagram of sodium table status monitoring device designed by the present invention;
Fig. 2: being a kind of liquid-level switch wiring diagram of sodium table status monitoring device designed by the present invention;
Wherein, 1. sampling valve;2. side valve;3. flowmeter;4. demarcating valve;5. diffuser;6. alkalizing agent bottle;7. measurement Cup;8. measuring electrode;9. reference electrode;10. temperature electrode;11. transmitter;12. air pump;13. catch basin;14. liquid level is opened It closes;15. overflow cup;16. liquid-level switch contact;17. nuclear power station operates normally I&C system;18. magnetic float.
Specific embodiment
The technology of the present invention is described further below:
A kind of sodium table status monitoring device, comprising: sampling valve 1 is connected with other valve 2,3 and of flowmeter in turn from the bottom to top Demarcate valve 4;The calibration valve 4 is connect with diffuser 5, and is arranged in alkalizing agent bottle 6;Alkalizing agent bottle 6 connects measuring cup 7;Measuring cup 7 connects transmitter 11, and the transmitter 11 is also connected with air pump 12 and overflow cup 15;The overflow cup 15 is surveyed Measuring cup 7 is separately connected with catch basin 13;The other valve 2 is connect with overflow cup 15.
Measuring electrode 8, reference electrode 9 and temperature electrode 10 are respectively arranged in the measuring cup 7.
Liquid-level switch 14, liquid-level switch contact 16, slide bar and magnetic float 18 are additionally provided in the overflow cup 15;It is described to overflow Flow cup 15 is also respectively connected nuclear power station and operates normally I&C system 17 and analyzer transmitter.
The slide bar is vertically set on inside overflow cup 15, and slide bar upper end, magnetic float is arranged in the liquid-level switch contact 16 18 are arranged on slide bar, and magnetic float 18 floats up and down under buoyancy along slide bar.
The liquid-level switch 14 is integrated in the overflow cup 15 in 1 downstream of sampling valve, and liquid-level switch contact 16 is in normally opened shape State is connected on instrument signal output line, and overflow cup 15 is mounted on the position higher than measuring cup 17.
A kind of operation method of sodium table status monitoring device as described above, water sample enter gauge internal pipe by sampling valve 1 Road flows through alkalization bottle 6 after other valve 2, flowmeter 3 adjust flow, enters measuring cup 7 after sample alkalization, air pump 12 is to survey Amount pond in constantly blast bubble with stirred sample and cleaning 8 surface of measuring electrode, electrode system by the sodium in water sample to be measured from Sub- concentration chemical signal is exported through transmitter 11 to monitoring screen after being converted to electric signal;
When 15 liquid level of overflow cup reach a certain height, liquid-level switch contact 16 is closed under 18 magneticaction of magnetic float; When water manufacturing system operates normally, overflow cup 15, which is in, is full of overflow situation, and magnetic float 18 is close to liquid-level switch contact 16, liquid level Switch contact 16 is closed under 18 magneticaction of magnetic float, and instrument signal normally exports to nuclear power station and operates normally I&C system 17, master control room ASD is normal, and display instrument currently measures indicating value;When water manufacturing system is stopped transport, sample introduction flow substantially reduces until disconnected Stream, liquid level declines in overflow cup 15 at this time, and magnetic float 18 drops down onto overflow bottom of the tube, and two contacts of liquid-level switch disconnect, and instrument is stopped Only output signal, master control room monitoring screen only exist channel failure warning note, to outrange report to the frequent shwoot of instrument Police plays the role of automatic shield.
The present invention is explained in detail above in conjunction with embodiment, but the present invention is not limited to above-described embodiments, at this Field those of ordinary skill within the scope of knowledge, can also make various changes without departing from the purpose of the present invention Change.The content being not described in detail in the present invention can use the prior art.

Claims (7)

1. a kind of sodium table status monitoring device characterized by comprising sampling valve (1) is connected with other valve in turn from the bottom to top (2), flowmeter (3) and calibration valve (4);The calibration valve (4) connect with diffuser (5), and is arranged in alkalizing agent bottle (6) It is interior;Alkalizing agent bottle (6) connects measuring cup (7);Measuring cup (7) connects transmitter (11), and the transmitter (11) is also connected with Air pump (12) and overflow cup (15);The overflow cup (15), measuring cup (7) are separately connected with catch basin (13);The side Valve (2) is connect with overflow cup (15).
2. a kind of sodium table status monitoring device as described in claim 1, it is characterised in that: set respectively in the measuring cup (7) It is equipped with measuring electrode (8), reference electrode (9) and temperature electrode (10).
3. a kind of sodium table status monitoring device as claimed in claim 2, it is characterised in that: also set up in the overflow cup (15) There are liquid-level switch (14), liquid-level switch contact (16), slide bar and magnetic float (18);Core is also respectively connected in the overflow cup (15) Power station operates normally I&C system (17) and analyzer transmitter.
4. a kind of sodium table status monitoring device as claimed in claim 3, it is characterised in that: the slide bar is vertically set on overflow Cup (15) is internal, and slide bar upper end is arranged in the liquid-level switch contact (16), and magnetic float (18) is arranged on slide bar, magnetic float (18) It floats up and down under buoyancy along slide bar.
5. a kind of sodium table status monitoring device as claimed in claim 4, it is characterised in that: the liquid-level switch (14) is integrated in In the overflow cup (15) in sampling valve (1) downstream, liquid-level switch contact (16) are in normally open, are connected on instrument signal output line On, overflow cup (15) is mounted on the position higher than measuring cup (17).
6. it is a kind of according to claim 1 to one of 5 the sodium table status monitoring device operation method, it is characterised in that: Water sample enters gauge internal pipeline by sampling valve (1), flows through alkalization bottle (6) after other valve (2), flowmeter (3) adjust flow, Enter measuring cup (7) after sample alkalization, air pump (12) is constantly blasted bubble into measuring cell and surveyed with stirred sample and cleaning Electrode (8) surface is measured, electrode system is converted to the Na ion concentration chemical signal in water sample to be measured after electric signal through transmitter (11) it exports to monitoring screen.
7. a kind of operation method of sodium table status monitoring device as claimed in claim 6, it is characterised in that: when overflow cup (15) When liquid level reach a certain height, liquid-level switch contact (16) are closed under magnetic float (18) magneticaction;When water manufacturing system is normal When operation, overflow cup (15), which is in, is full of overflow situation, and magnetic float (18) is close to liquid-level switch contact (16), liquid-level switch contact (16) it being closed under magnetic float (18) magneticaction, instrument signal normally exports to nuclear power station and operates normally I&C system (17), Master control room ASD is normal, and display instrument currently measures indicating value;When water manufacturing system is stopped transport, sample introduction flow substantially reduces up to cutout, The interior liquid level decline of overflow cup (15) at this time, magnetic float (18) drop down onto overflow bottom of the tube, and two contacts of liquid-level switch disconnect, and instrument is stopped Only output signal, master control room monitoring screen only exist channel failure warning note.
CN201810972245.9A 2018-08-24 2018-08-24 A kind of sodium table status monitoring device and its operation method Pending CN108956234A (en)

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CN108956234A true CN108956234A (en) 2018-12-07

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113740407A (en) * 2021-11-02 2021-12-03 南京柠檬科技发展有限公司 Sodium ion concentration analysis measuring equipment

Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2831116Y (en) * 2005-09-23 2006-10-25 金为民 Measurer for Na ion content in water
CN201368822Y (en) * 2009-03-20 2009-12-23 北京华科仪电力仪表研究所 Ammonia alkalization device used for online sodium analyzer
CN101975778A (en) * 2010-10-09 2011-02-16 中国神华能源股份有限公司 Device and method for detecting water quality stability
CN202018456U (en) * 2010-10-09 2011-10-26 中国神华能源股份有限公司 Water sampling cup and water quality detection system comprising same
CN202229959U (en) * 2011-07-11 2012-05-23 北京华科仪电力仪表研究所 Diisopropylamine alkalization device for online sodium analyzer
CN103454129A (en) * 2013-09-05 2013-12-18 贵阳学通仪器仪表有限公司 On-line sodium analyzer
CN106502225A (en) * 2016-11-10 2017-03-15 中铝广西国盛稀土开发有限公司 The information gathering of Rare Earth Production process materials and analysis intelligence control system
CN206788096U (en) * 2017-04-12 2017-12-22 北京华科仪科技股份有限公司 A kind of multi-passage sodion monitor
CN209102481U (en) * 2018-08-24 2019-07-12 江苏核电有限公司 A kind of sodium table status monitoring device

Patent Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2831116Y (en) * 2005-09-23 2006-10-25 金为民 Measurer for Na ion content in water
CN201368822Y (en) * 2009-03-20 2009-12-23 北京华科仪电力仪表研究所 Ammonia alkalization device used for online sodium analyzer
CN101975778A (en) * 2010-10-09 2011-02-16 中国神华能源股份有限公司 Device and method for detecting water quality stability
CN202018456U (en) * 2010-10-09 2011-10-26 中国神华能源股份有限公司 Water sampling cup and water quality detection system comprising same
CN202229959U (en) * 2011-07-11 2012-05-23 北京华科仪电力仪表研究所 Diisopropylamine alkalization device for online sodium analyzer
CN103454129A (en) * 2013-09-05 2013-12-18 贵阳学通仪器仪表有限公司 On-line sodium analyzer
CN106502225A (en) * 2016-11-10 2017-03-15 中铝广西国盛稀土开发有限公司 The information gathering of Rare Earth Production process materials and analysis intelligence control system
CN206788096U (en) * 2017-04-12 2017-12-22 北京华科仪科技股份有限公司 A kind of multi-passage sodion monitor
CN209102481U (en) * 2018-08-24 2019-07-12 江苏核电有限公司 A kind of sodium table status monitoring device

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113740407A (en) * 2021-11-02 2021-12-03 南京柠檬科技发展有限公司 Sodium ion concentration analysis measuring equipment
CN113740407B (en) * 2021-11-02 2022-02-18 南京柠檬科技发展有限公司 Sodium ion concentration analysis measuring equipment

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