CN108947725A - A method of comprehensive utilization livestock/poultry biogas slurry prepares aqueous liquid fertilizer - Google Patents

A method of comprehensive utilization livestock/poultry biogas slurry prepares aqueous liquid fertilizer Download PDF

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Publication number
CN108947725A
CN108947725A CN201810755091.8A CN201810755091A CN108947725A CN 108947725 A CN108947725 A CN 108947725A CN 201810755091 A CN201810755091 A CN 201810755091A CN 108947725 A CN108947725 A CN 108947725A
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CN
China
Prior art keywords
aqueous liquid
liquid fertilizer
biogas slurry
base
livestock
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Pending
Application number
CN201810755091.8A
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Chinese (zh)
Inventor
沈冰涛
肖新
高亚飞
孙冰清
陈红
唐小倩
孙星
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Anhui University of Science and Technology
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Anhui University of Science and Technology
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Application filed by Anhui University of Science and Technology filed Critical Anhui University of Science and Technology
Priority to CN201810755091.8A priority Critical patent/CN108947725A/en
Publication of CN108947725A publication Critical patent/CN108947725A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05BPHOSPHATIC FERTILISERS
    • C05B7/00Fertilisers based essentially on alkali or ammonium orthophosphates
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05CNITROGENOUS FERTILISERS
    • C05C3/00Fertilisers containing other salts of ammonia or ammonia itself, e.g. gas liquor
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C05G3/80Soil conditioners
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G5/00Fertilisers characterised by their form
    • C05G5/20Liquid fertilisers

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Soil Sciences (AREA)
  • Fertilizers (AREA)

Abstract

The invention discloses a kind of method that comprehensive utilization livestock/poultry biogas slurry prepares aqueous liquid fertilizer, the preparations of preparation and aqueous liquid fertilizer finished product including aqueous liquid fertilizer base-material;The preparation of aqueous liquid fertilizer base-material are as follows: after being separated by solid-liquid separation livestock breeding wastewater, pass through chemistry, physical reactions process, the filtrate being obtained by filtration, as aqueous liquid fertilizer base-material;The preparation of aqueous liquid fertilizer finished product are as follows: component element content detection is carried out to the base-material handled well, obtains component element content, further according to different plant nutrient demands, adds the component of different material and needs, vegetation water state fertilizer can be produced;Contain a large amount of beneficial elements in aqueous liquid fertilizer base-material of the invention, nutrient demand and soil measurement formula technology further according to different plants add the nutrient of different components, and vegetation water state fertilizer can be obtained, apply fertilizer to plant.Realize the mass production of aqueous liquid fertilizer.

Description

A method of comprehensive utilization livestock/poultry biogas slurry prepares aqueous liquid fertilizer
Technical field
The invention belongs to livestock and poultry breeding industry environmental technology field, it is related to a kind of preparing aqueous liquid fertilizer using livestock/poultry biogas slurry Method.
Background technique
In recent years, with the propulsion of adjustment and the agriculture industrialization of China's structure of agricultural production, scale, intensive livestock and poultry are supported It grows industry to be rapidly developed, becomes the important component and the vast farmers population below the poverty line of China's agricultural economy, shake off poverty and set out on the road to prosperity Effective way.The wastewater discharge of the annual livestock and poultry cultivation in China is more than 10,000,000,000 tons, considerably beyond national industrial wastewater and life Wastewater discharge summation, China has the farm of certain scale to carry out waste water of livestock poultry processing at present, and there are also most of medium and small enterprises Industry does not have substantial contribution to put into wastewater treatment, causes waste water of livestock poultry largely the phenomenon that rural area is disorderly arranged, rural environmental pollution Problem is got worse, and becomes China's vast rural area pollution main source.Biogas slurry is mostly pig, ox, sheep urine;Containing a large amount of COD, BOD, nitrogen, phosphorus, potassium etc., serious waste.So can use our learned professions by our environmental careers personages, can be subject to It rationally utilizes, realizes protection environment and utilization of wastewater resource, turn waste into wealth.Therefore, by recycling livestock breeding wastewater, It can either turn waste into wealth, also protect the pollution of ecological environment, realize the unification of economic value and Social Ecology value.
The present invention provides a kind of comprehensive utilization livestock/poultry biogas slurry and prepares water in view of the above problems, the problems such as being based on economic cost The method of solution state fertilizer is prepared into aqueous liquid fertilizer base-material by livestock breeding wastewater comprehensive utilization of resources, can protect environment, Realize its ecological value.Energy recycling waste again realizes that its circular economy is worth.
Summary of the invention
To achieve the above object, the invention provides the following technical scheme: a kind of comprehensive utilization livestock/poultry biogas slurry prepares aqueous solution The method of state fertilizer, which is characterized in that it successively includes the preparation step of aqueous liquid fertilizer base-material and matching for aqueous liquid fertilizer finished product Step processed;
Wherein, the preparation step of the aqueous liquid fertilizer base-material are as follows:
(1) after being separated by solid-liquid separation livestock breeding wastewater, then liquid introduces fermentor by conduit and carries out anaeration in normal temperature hair Ferment processing;
(2) biogas slurry fermented in step (1) is collected by storage pool by pipeline;
(3) aeration Aerobic Process for Treatment, flocculation treatment are passed sequentially through to the substance in storage pool in step (2), then filtered;
(4) the filtered biogas slurry of step (3) is introduced into sealed fermenting tank and carries out deodorization and sterilizing using bacteria agent, can be obtained Base-material;
The preparation step of the aqueous liquid fertilizer finished product are as follows:
The base-material that step (4) is obtained introduces chelating digestion and fills, and carries out component element content detection to aqueous liquid fertilizer base-material, obtains To after component element content, further according to the nutritional need of different plants, nutriment is added, aqueous liquid fertilizer can be obtained.
Further, preferably, the nutriment of addition includes at least in the preparation step of the aqueous liquid fertilizer finished product Nitrogen, phosphorus, potassium nutrition element, humic acid, amino acid.
It further,, will after obtaining aqueous liquid fertilizer preferably, in the preparation step of the aqueous liquid fertilizer finished product It introduces agitator tank, stirs evenly, is re-introduced into holding vessel, enters filling production lines by pipeline and carries out filling, factory sale.
Further, preferably, in solution state fertilizer, humic acid content≤40g/L, nitrogen, phosphorus, potassium element containing total amount≤ 500g/L, single nitrogen, phosphorus or potassium are not less than 40g/L, and 1:250 times of diluted pH value is 3.0-9.0, and meets NY1107- 2010 require.
Further, preferably, the nutriment of addition further includes five in the preparation step of the aqueous liquid fertilizer finished product Brochanite, manganese sulfate, zinc sulfate, borax, ammonium molybdate, ferrous sulfate.
Compared with prior art, the beneficial effects of the present invention are:
(1) aqueous liquid fertilizer base-material can be made in livestock/poultry biogas slurry by technical solution through the invention, contained in aqueous liquid fertilizer base-material There are a large amount of beneficial elements, nutrient demand and soil measurement formula technology further according to different plants add the nutrient of different components, Vegetation water state fertilizer can be obtained, apply fertilizer to plant.
(2) according to the technical solution of the present invention, it can not only effectively turn waste into wealth, be conducive to environmental protection, to realize resource Recycle, for breeding wastewater provide one recycle way, improve ecological benefits, reduce economic cost.
(3) mass production for realizing aqueous liquid fertilizer according to the technical solution of the present invention, changes traditional fertilising Mode, entire production process is safe, fast, efficient, green, is conducive to promote the use of on a large scale.
(4) aqueous liquid fertilizer prepared by the present invention can do base manure application in flower, fruit and vegetable, cereal crops.
Specific embodiment
Below in conjunction in the embodiment of the present invention, technical solution in the embodiment of the present invention is clearly and completely retouched It states, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Based on the present invention In embodiment, every other implementation obtained by those of ordinary skill in the art without making creative efforts Example, shall fall within the protection scope of the present invention.
Embodiment 1:
A kind of preparation method of aqueous liquid fertilizer, the preparation of preparation and aqueous liquid fertilizer finished product including aqueous liquid fertilizer base-material:
Wherein, the preparation of aqueous liquid fertilizer base-material are as follows: after being separated by solid-liquid separation livestock breeding wastewater, the excreta of livestock is passed through Piping introduces fermentor and carries out anaerobic fermentation, then the biogas slurry fermented is collected into storage pool by overflow pipe, by aeration Aerobic Process for Treatment finally passes through flocculation, filtering, sterilizing, and introducing chelates digestion and fills.
Wherein, the preparation of aqueous liquid fertilizer finished product are as follows: component element content detection is carried out to aqueous liquid fertilizer base-material, is obtained After component element content, further according to the nutritional need of different plants, be added humic acid, calcium nitrate, potassium nitrate, ammonium dihydrogen phosphate, The a great number of elements water-soluble fertilizer containing humic acid can be obtained in the compounds such as sodium hydroxide.It introduces agitator tank to stir evenly, pass through Pipeline enters filling production lines and carries out filling, factory sale.
Embodiment 2:
It is identical as 1 preparation method of example, difference are as follows: further according to the nutritional need of different plants, different chemical elements is added Different aqueous liquid fertilizer is obtained, specifically:
A kind of preparation method of aqueous liquid fertilizer, the preparation of preparation and aqueous liquid fertilizer finished product including aqueous liquid fertilizer base-material:
Wherein, the preparation of aqueous liquid fertilizer base-material are as follows: after being separated by solid-liquid separation livestock breeding wastewater, the excreta of livestock is passed through Piping introduces fermentor and carries out anaerobic fermentation, then the biogas slurry fermented is collected into storage pool by overflow pipe, by aeration Aerobic Process for Treatment finally passes through flocculation, filtering, sterilizing, and introducing chelates digestion and fills;
Wherein, the preparation of aqueous liquid fertilizer are as follows: component element content detection is carried out to aqueous liquid fertilizer base-material, obtains component element After content, further according to the nutritional need of different plants, cupric sulfate pentahydrate, manganese sulfate, zinc sulfate, borax, ammonium molybdate, sulfuric acid is added Ferrous iron etc..The aqueous liquid fertilizer prepared, is diluted with water, and it is the same that the similar water-soluble fertilizer containing microelement can be obtained.Draw Enter agitator tank to stir evenly, filling production lines are entered by pipeline and carry out filling, factory sale.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with A variety of variations, modification, replacement can be carried out to these embodiments without departing from the principles and spirit of the present invention by understanding And modification, the scope of the present invention is defined by the appended.

Claims (5)

1. a kind of method that comprehensive utilization livestock/poultry biogas slurry prepares aqueous liquid fertilizer, which is characterized in that it successively includes aqueous liquid The preparation step of fertile base-material and the preparation steps of aqueous liquid fertilizer finished product;
Wherein, the preparation step of the aqueous liquid fertilizer base-material are as follows:
(1) after being separated by solid-liquid separation livestock breeding wastewater, then liquid introduces fermentor by conduit and carries out anaeration in normal temperature hair Ferment processing;
(2) biogas slurry fermented in step (1) is collected by storage pool by pipeline;
(3) aeration Aerobic Process for Treatment, flocculation treatment are passed sequentially through to the substance in storage pool in step (2), then filtered;
(4) the filtered biogas slurry of step (3) is introduced into sealed fermenting tank and carries out deodorization and sterilizing using bacteria agent, can be obtained Base-material;
The preparation step of the aqueous liquid fertilizer finished product are as follows:
The base-material that step (4) is obtained introduces chelating digestion and fills, and carries out component element content detection to aqueous liquid fertilizer base-material, obtains To after component element content, further according to the nutritional need of different plants, nutriment is added, aqueous liquid fertilizer can be obtained.
2. a kind of method that comprehensive utilization livestock/poultry biogas slurry prepares aqueous liquid fertilizer according to claim 1, it is characterised in that: In the preparation step of the aqueous liquid fertilizer finished product, the nutriment of addition include at least nitrogen, phosphorus, potassium nutrition element, humic acid, Amino acid.
3. a kind of method that comprehensive utilization livestock/poultry biogas slurry prepares aqueous liquid fertilizer according to claim 1, it is characterised in that: In the preparation step of the aqueous liquid fertilizer finished product, after obtaining aqueous liquid fertilizer, it is introduced into agitator tank, is stirred evenly, again Holding vessel is introduced, filling production lines are entered by pipeline and carry out filling, factory sale.
4. a kind of method that comprehensive utilization livestock/poultry biogas slurry prepares aqueous liquid fertilizer according to claim 1, it is characterised in that: In solution state fertilizer, humic acid content≤40g/L, nitrogen, phosphorus, potassium element contain total amount≤500g/L, and single nitrogen, phosphorus or potassium is not low In 40g/L, 1:250 times of diluted pH value is 3.0-9.0, and meets NY1107-2010 requirement.
5. a kind of method that comprehensive utilization livestock/poultry biogas slurry prepares aqueous liquid fertilizer according to claim 1, it is characterised in that: In the preparation step of the aqueous liquid fertilizer finished product, the nutriment of addition further include cupric sulfate pentahydrate, manganese sulfate, zinc sulfate, Borax, ammonium molybdate, ferrous sulfate.
CN201810755091.8A 2018-07-11 2018-07-11 A method of comprehensive utilization livestock/poultry biogas slurry prepares aqueous liquid fertilizer Pending CN108947725A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111187120A (en) * 2020-03-24 2020-05-22 青岛格瑞盛环保工程有限公司 Liquid fertilizer for rooting and root-raising and preparation method thereof
CN113387732A (en) * 2021-07-26 2021-09-14 台州市椒江区农业技术推广中心 Production method and equipment of pig manure fertilizer influencing single-season late rice yield
CN115028499A (en) * 2022-07-07 2022-09-09 内蒙古御谷农牧科技有限公司 Production technology of organic liquid surface fertilizer after efficient separation treatment of cow dung and urine

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105461401A (en) * 2016-01-14 2016-04-06 邹伟龙 Preparation method of nutrient solution
CN106927870A (en) * 2015-12-31 2017-07-07 天津市凯润淡水养殖有限公司 A kind of production technology of biogas slurry fertilizer
CN107311702A (en) * 2017-08-09 2017-11-03 上海田应农业科技有限公司 A kind of method that livestock and poultry farm fecaluria biogas slurry integrated treatment recovery prepares Liquid Fertilizer

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106927870A (en) * 2015-12-31 2017-07-07 天津市凯润淡水养殖有限公司 A kind of production technology of biogas slurry fertilizer
CN105461401A (en) * 2016-01-14 2016-04-06 邹伟龙 Preparation method of nutrient solution
CN107311702A (en) * 2017-08-09 2017-11-03 上海田应农业科技有限公司 A kind of method that livestock and poultry farm fecaluria biogas slurry integrated treatment recovery prepares Liquid Fertilizer

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111187120A (en) * 2020-03-24 2020-05-22 青岛格瑞盛环保工程有限公司 Liquid fertilizer for rooting and root-raising and preparation method thereof
CN113387732A (en) * 2021-07-26 2021-09-14 台州市椒江区农业技术推广中心 Production method and equipment of pig manure fertilizer influencing single-season late rice yield
CN115028499A (en) * 2022-07-07 2022-09-09 内蒙古御谷农牧科技有限公司 Production technology of organic liquid surface fertilizer after efficient separation treatment of cow dung and urine

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Application publication date: 20181207

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