CN108936484A - A kind of jelly and preparation method thereof adding squid ink black pigment - Google Patents
A kind of jelly and preparation method thereof adding squid ink black pigment Download PDFInfo
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- CN108936484A CN108936484A CN201810820537.0A CN201810820537A CN108936484A CN 108936484 A CN108936484 A CN 108936484A CN 201810820537 A CN201810820537 A CN 201810820537A CN 108936484 A CN108936484 A CN 108936484A
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L21/00—Marmalades, jams, jellies or the like; Products from apiculture; Preparation or treatment thereof
- A23L21/10—Marmalades; Jams; Jellies; Other similar fruit or vegetable compositions; Simulated fruit products
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L5/00—Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
- A23L5/20—Removal of unwanted matter, e.g. deodorisation or detoxification
- A23L5/27—Removal of unwanted matter, e.g. deodorisation or detoxification by chemical treatment, by adsorption or by absorption
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- Coloring Foods And Improving Nutritive Qualities (AREA)
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Abstract
The present invention relates to food processing technology fields, a kind of jelly and preparation method thereof for adding squid ink black pigment is disclosed, the jelly includes vegetable oil, thickener, potassium chloride, white granulated sugar, fructose syrup, citric acid, sodium citrate, D-araboascorbic acid sodium, squid ink black pigment and water.The present invention reacts the glucose contained in the group and jelly that generate fishy smell in squid ink black pigment, glucose and squid ink polysaccharide are passed through into chemistry key connection, the fishy smell of squid ink black pigment is removed, while improving body to the absorbability of the squid ink polysaccharide in jelly.The squid ink black pigment that deodorization is handled is directly added into jelly feed liquid and squid ink black pigment is made into after powder circle by the present invention is added the two kinds of jelly of form preparation containing squid ink black pigment in jelly, solving the problems, such as squid ink black pigment, there are fishy smell and jelly nutritional ingredient to be not easy to absorb, the mouthfeel for increasing jelly enables people to more convenient supplement squid ink black pigment.
Description
Technical field
The present invention relates to food processing technology field more particularly to a kind of jelly for adding squid ink polysaccharide and its preparation sides
Method.The squid ink black pigment that deodorization is handled is directly added into jelly feed liquid and added after squid ink black pigment is made into powder circle by the present invention
Enter the two kinds of jelly of form preparation containing squid ink black pigment in jelly, solving squid ink black pigment, there are fishy smell and jelly nutrition
Ingredient is not easy the problem absorbed, increases the mouthfeel of jelly, enables people to more convenient supplement squid ink black pigment.
Background technique
In the past, squid ink and Cuttlefish Ink were usually considered as waste when eating squid and cuttlefish by people.Now, Ren Menyi
The gradually dish of association's culinary art and trial test former prepared Chinese ink squid and former prepared Chinese ink cuttlefish, such as Normal juice inkfish bean vermicelli stew and squid prepared Chinese ink
Meal, although looking at as " dark cooking ", by favor.With deepening continuously for marine organisms medical research, researcher's hair
Existing, squid ink, Cuttlefish Ink, which have, adjusts immune, antitumor and hemostasis and other effects.Squid ink, Cuttlefish Ink main chemical compositions be
Melanin and protein complex have antitumor, adjusting body's immunity, can be living with physiology such as inducing various cytokines
Property.Containing more organic matter, thick protein and total lipid in squid ink and Cuttlefish Ink, and the content of squid ink contains than cuttlefish
More 1.5~3 times or so of ink.Inorganic matter in squid ink is fewer than the content in Cuttlefish Ink, is probably the 1/3 of Cuttlefish Ink.Except iron
Outside zinc, the macroelement and microelement in squid ink are lower than Cuttlefish Ink.It is worth noting that, in squid ink and Cuttlefish Ink
Elements strontium and the content of copper are very rich.Strontium has important role in the bone growth of animal, has not replaceable function
Can, therefore quite attract attention in nutrition and health care field.
Squid ink is applied to jelly industry, using the property of squid integration of drinking and medicinal herbs, by the nutritive value of squid and health care
Function is condensed among jelly, and the leisure of jelly, convenient feature are applied among squid processing, is not only increased
The utility value of squid develops squid market, increases the technology content in squid process, and it is raw to have widened jelly
The raw material sources of production, thus there is vast potential for future development.However, due to containing a large amount of dietary fiber, digestion in jelly
Speed is very fast, and the nutrient of addition can be lost quickly with body metabolism, causes supplementary result unobvious.Meanwhile squid
The monomer of pitch-dark pigment includes DHI (5,6- dihydroxy indole), DHICA (5,6- dihydroxy indoles acid), Cys-Dopa (half Guang ammonia
Sour DOPA) and dopamine (simultaneously containing indoles and phenylpropyl alcohol thiazine structure) etc., the group of some nucleophilicities contained in melanin
(such as-SH ,-NH2), indoles and heterocycle ammonia nitrogenous compound have fishy smell, affect the eating mouth feel of squid ink black pigment.About
Nutrition in squid jelly process, which is easy to run off problem and squid ink black pigment, has the problem of fishy smell, and there is presently no good
Good solution.
Summary of the invention
In order to solve the above-mentioned technical problems, the present invention provides a kind of jelly for adding squid ink black pigment and its preparation sides
Method.The present invention uses and the squid ink black pigment that deodorization is handled is added directly into jelly feed liquid and squid ink black pigment is made into powder
After circle be added jelly in two kinds of forms prepare jelly, not only solve the fishy smell of squid ink black pigment, solve jelly nutrition at
Divide the problem for being not easy to absorb, the supplement squid ink black pigment for increasing the mouthfeel of jelly, and people capable of being made more convenient.
The specific technical proposal of the invention is: a kind of jelly for adding squid ink black pigment, the jelly includes following matter
Measure the component of percentage: vegetable oil 5-10%, thickener 0.9-1%, potassium chloride 0.1-0.2%, white granulated sugar 10-20%, fruit Portugal
Syrup 10-20%, citric acid 0.3-0.8%, sodium citrate 0.5-0.9%, D-araboascorbic acid sodium 0.2-1%, squid are pitch-dark
Pigment 5-10%, surplus are water.
Squid ink black pigment is added in jelly by the present invention, enables people to take in squid ink black pigment whenever and wherever possible.
Squid ink black pigment is a kind of good free radical scavenger, can effectively remove the free radicals such as hydroxyl radical free radical, oxygen radical,
With anticancer, oxidation resistant effect.Squid ink black pigment is cooperateed with citric acid can enhance in squid ink black pigment absorption human body
The effect of heavy metal ion.Vegetable oil is preferably coconut oil or palm oil, for increasing the soft mouthfeel of jelly.Thickener uses
Carragheen or flaxseed gum, for making configured jelly feed liquid form gel, meanwhile, flaxseed gum is that emulsifying effectiveness is excellent
Emulsifier makes jelly feed liquid become stable mixed solution.D-araboascorbic acid sodium is antisepsis antistaling agent, increases the preservation of jelly
Time.
Preferably, a kind of jelly adding squid ink black pigment, the squid ink black pigment extracting method are as follows: manually take squid
Fish ink, then uses lipase and fat and protein in neutral proteinase hydrolysis squid ink, the lipase and neutral protein
Total dosage of enzyme is the 0.5-3.0% of squid ink weight, is filtered to remove impurity；It is 90-98wt%'s that concentration is added in filtrate
Ethanol water precipitates squid ink black pigment, after filtering, by drying precipitate and crushes.
Also containing fat, protein in addition to melanin in squid ink, the present invention first uses lipase and neutral proteinase by rouge
Fat and protein hydrolysis, total dosage of two kinds of enzymes are the 0.5-3.0% of squid ink weight, and the dosage of enzyme excessively will cause the wave of enzyme
Take, while increasing production cost, and the dosage of enzyme is very few, the fat and protein removal that will lead in squid ink are not thorough, and
It will increase enzymolysis time, increase the time cost of production, production efficiency is low.Since squid ink black pigment is insoluble in ethyl alcohol, therefore
The ethanol water that concentration is 90-98wt% is added in filtrate precipitates squid ink black pigment, after filtering, by the squid ink of precipitating
Melanin, which is dried, can obtain squid ink black pigment.
Preferably, a kind of jelly adding squid ink black pigment, the method for squid ink black pigment deodorization processing are as follows: by squid
Melanin is added to the water, addition glucose, and the mass ratio of squid ink black pigment and glucose is 1-1.3:1, is heated with stirring to 55-
Formic acid is added after 70 DEG C of dissolutions, the additional amount of formic acid is the 2-5% of squid ink black pigment quality, stirs 2-3h.After reaction
Feed liquid is down to room temperature, and it is that 90-98%wt ethanol solution precipitates squid ink black pigment that concentration, which is added, filters, is 90- with concentration
The ethanol solution of 98wt% cleans precipitating repeatedly, and drying simultaneously crushes.
Since squid ink black pigment has fishy smell, and jelly itself, because containing a large amount of dietary fiber, digestion rate is very
Fastly, the nutrient of addition can be lost quickly with body metabolism, cause supplementary result unobvious.In order to solve squid ink black
There is element nutritional ingredient in fishy smell and jelly to be not easy the problem of absorbing, and the present invention obtains a squid ink by many experiments demonstration
The technique of melanin deodorization processing.The present invention is while removing fishy smell, the diet that will contain in squid ink black pigment and jelly
Fiber combines, and slows down the digestion rate of jelly, enhances absorption of the human body to squid ink black pigment in jelly, for this field skill
Deodorization treatment process of the invention is non-obvious for art personnel.
Specifically: the monomer of squid ink black pigment includes DHI (5,6- dihydroxy indole), DHICA (5,6- dihydroxy indoles
Acid), Cys-Dopa (cysteine DOPA) and dopamine (simultaneously containing indoles and phenylpropyl alcohol thiazine structure) etc., wherein DHI,
Fishy smell substance is all had in DHICA and phenylpropyl alcohol thiazine, these types of fishy smell substance contains indoles and heterocycle ammonia nitrogenous compound.Yin
Contain heterocycle ammonia nitrogenous compound in diindyl, the present invention carries out processing modification to Heterocyclic nitrogen ingredient for this feature, utilizes secondary amine
The response characteristic of base and aldehyde radical connects the glucose of a upper molecule on the nitrogen-atoms of heterocycle ammonia.Studies have shown that secondary amine and aldehyde
Base can react under the catalytic action of formic acid at 55-70 DEG C, and this reaction condition will not destroy on squid ink black pigment
Active group (- SH ,-NH2).After nitrogen-atoms on squid ink black pigment is connect with glucose, what is be rich on grape sugar chain is hydrophilic
The hydroxyl of property is contacted with hydrone outwardly, and hydrophobic alkyl is then coated on the ring around nitrogen-atoms.Glucose molecule is logical
Cross the fishy smell that the mode of the nitrogen-atoms cladding on heterocycle is removed to squid ink black pigment.Contain in fructose syrup in the ingredient of jelly
There is glucose, and the hydrolysate of white granulated sugar is also glucose, and glucose is selected not change the ingredient of jelly, while glucose
One kind of the dietary fiber contained in jelly is also belonged to, glucose carries out also can solve the nutrition in jelly while deodorization processing
The problem of element is easy to run off.With concentration it is that 90-98wt% ethanol solution precipitates by the squid ink black pigment after reaction, is used in combination
Concentration is the squid ink black pigment that 90-98wt% ethanol solution repeated flushing obtains, and removes the first adhered on squid ink black pigment
Then acid is dried to obtain deodorization treated squid ink black pigment.
Preferably, a kind of preparation method for the jelly adding squid ink black pigment, comprising the following steps:
(1) by white granulated sugar, fructose syrup investment water, heating stirring dissolution obtains syrup solution.
(2) squid ink black pigment after the thickener prepared in proportion, D-araboascorbic acid sodium, deodorization is put into step
(1) in the syrup solution obtained, vegetable oil is added after evenly dispersed, glue is boiled in heating after mixing evenly, is during which stirred continuously, will boil
Good feed liquid is shear agitation 1-20 minutes under conditions of temperature is 70-100 DEG C, revolving speed is 1000-5000r/min.
(3) dissolved citric acid and sodium citrate aqueous solution is added in through step (2) treated feed liquid, adjusts material
The pH to 3.5-5 of liquid.
(4) it filters after mixing evenly, takes out material and be fills up in jelly cup.
The present invention adds in the preparation method of the jelly of squid ink black pigment, heats water to 50-60 DEG C, and white granulated sugar is added
And fructose syrup, it dissolves while stirring, obtains syrup solution.After configured thickener, D-araboascorbic acid sodium, deodorization
Squid ink black pigment is added in syrup solution after mixing, is stirring evenly and then adding into vegetable oil, is uniformly dispersed, and is in temperature
Glue is boiled in heating under conditions of 70-100 DEG C, and is stirred continuously.By obtained feed liquid temperature be 70-100 DEG C, revolving speed 1000-
It is sheared homogeneous 1-20 minutes under conditions of 5000r/min, reduces the granularity of the various composition in feed liquid, keep feed liquid fine and smooth
It is even, while increasing the stability of feed liquid.Dissolved citric acid and sodium citrate aqueous solution are added into the feed liquid after shearing, adjusts
The pH to 3.5-5 of material-saving liquid.The too low gel force that can reduce jelly of pH makes the reduction of finished product elasticity.PH is excessively high to will lead to jelly
Taste bad.Finally feed liquid is fills up in jelly cup.
Preferably, a kind of another preparation method for the jelly adding squid ink black pigment, comprising the following steps:
(1) by white granulated sugar, fructose syrup investment water, heating stirring dissolution obtains syrup solution.
(2) in the syrup solution for obtaining the thickener prepared in proportion, D-araboascorbic acid sodium investment step (1),
Vegetable oil is added after even dispersion, after being uniformly dispersed heating boil glue, be during which stirred continuously, by well-done feed liquid temperature be 70-100
DEG C, revolving speed be 1000-5000r/min under conditions of shear agitation 1-20 minutes.
(3) dissolved sodium citrate aqueous solution is added in through step (2) treated feed liquid, adjust the pH of feed liquid to
3.5-5。
(4) powder circle is made with tapioca starch in the squid ink black pigment after deodorization.
(5) feed liquid that step (3) obtains is filtered after mixing evenly, takes out material and be fills up in jelly cup, powder is added in when filling
Circle.
The present invention adds in the preparation method of the jelly of squid ink black pigment, heats water to 50-60 DEG C, and white granulated sugar is added
And fructose syrup, it dissolves while stirring, obtains syrup solution.Configured thickener, D-araboascorbic acid sodium are uniformly mixed
After be added in syrup solution, be stirring evenly and then adding into vegetable oil, be uniformly dispersed, temperature be 70-100 DEG C under conditions of heat
Glue is boiled, and is stirred continuously.Obtained feed liquid is sheared under conditions of temperature is 70-100 DEG C, revolving speed is 1000-5000r/min
Homogeneous 1-20 minutes, the granularity of the various composition in feed liquid is reduced, it is fine and smooth uniformly to make feed liquid, while increasing the stabilization of feed liquid
Property.Dissolved citric acid and sodium citrate aqueous solution are added into the feed liquid after shearing, adjusts the pH to 3.5-5 of feed liquid.pH
The too low gel force that can reduce jelly makes the reduction of finished product elasticity.The excessively high taste bad that will lead to jelly of pH.By the squid after deodorization
Powder circle is made in the pitch-dark pigment of fish and tapioca starch, is added in jelly cup when filling jelly.Powder circle is made in squid ink black pigment, is added
Enter in jelly, not only can increase the mouthfeel of jelly, while also can further extend the digestion time of jelly, enhances human body to squid
The absorption of pitch-dark pigment.
Preferably, a kind of preparation method for the jelly adding squid ink black pigment, in step (2), well-done feed liquid exists
Shear agitation 10-15 minutes under conditions of temperature is 80-90 DEG C, revolving speed is 2300-2700r/min.
By well-done feed liquid under conditions of temperature is 80-90 DEG C, revolving speed is 2300-2700r/min shear agitation 10-15
Minute, temperature is too low, and jelly starts gel, is unfavorable for the shearing homogeneous of feed liquid.Revolving speed is excessively high, is easy to produce a large amount of bubbles, meeting
Shearing homogenizer is caused to damage, when revolving speed is too low, bulky grain sinks, also can damaging shear homogenizer.It can reach within 10-15 minutes
To good shearing homogenizing effect, the time is too short, and the particle of each component is difficult to reach uniform in feed liquid, and shear time is too long,
It is unfavorable for the stabilization of jelly feed liquid.
Preferably, a kind of preparation method for the jelly adding squid ink black pigment, the jelly after filling is in 75-90 DEG C of condition
Lower sterilization 5-30min.
The jelly filled is sterilized to 5-30min under the conditions of 75-90 DEG C can kill bacterium in jelly, improve jelly
Edible safety, extend the holding time of jelly.
It is compared with the prior art, the beneficial effects of the present invention are: the present invention is utilized using component sugar glucose original in jelly
The reaction mechanism of secondary amine and aldehyde radical carries out deodorization processing to squid ink black pigment, solves in jelly and seeks while removing fishy smell
It forms and point is not easy the shortcomings that being absorbed by the body.Jelly preparation step of the invention is simple, has both the two-fold advantage of leisure and health care.
Specific embodiment
The present invention will be further described with reference to the examples below.Related device, connection structure in the present invention
And method, if being device well known in the art, connection structure and method without refering in particular to.
Embodiment 1
A kind of preparation method for the jelly adding squid ink black pigment, steps are as follows:
(1) 55 DEG C are heated water to, it is 15% white granulated sugar and 15% fructose syrup that mass fraction, which is added, molten while stirring
Solution, obtains syrup solution.
(2) by mass fraction be 0.26% carragheen, 0.65% flaxseed gum, 0.4% D-araboascorbic acid sodium,
Treated that squid ink black pigment extract is added in syrup solution after mixing for 10% deodorization, stirs evenly, then
The vegetable oil that mass fraction is 10% is added, stirs evenly.By obtained feed liquid temperature be 85 DEG C, revolving speed 2700r/min
Under conditions of shear homogeneous 15 minutes, reduce the granularity of the various composition in feed liquid, it is fine and smooth uniformly to make feed liquid, while increasing material
The stability of liquid.
(3) mass fraction is added in through step (2) treated feed liquid is 0.5% citric acid and 0.5% lemon
Acid sodium aqueous solution adjusts the pH to 4.3 of feed liquid.
(4) it filters after mixing evenly, takes out material and be fills up in jelly cup.
(5) jelly after filling sterilizes 8min under the conditions of 90 DEG C.
The wherein extracting method of squid ink black pigment are as follows: manually take squid ink, then use lipase and neutral proteinase water
The fat and protein in squid ink are solved, total dosage of two kinds of enzymes is the 3% of squid ink weight, is filtered to remove impurity.In filtrate
95% edible ethanol of middle addition makes prepared Chinese ink melanin deposition, after filtering, will be deposited in 55 DEG C and is dried with vacuum drier, after dry
The fine grained of 100 mesh is crushed to stainless steel pulverizer.
The wherein method of squid ink black pigment deodorization processing are as follows: squid melanin is added to the water, glucose, squid is added
The mass ratio of pitch-dark pigment and glucose is 1.15:1, formic acid is added after being heated with stirring to 65 DEG C of dissolutions, the additional amount of formic acid is
The 2.5% of squid ink black pigment quality stirs 3h.Feed liquid after reaction is down to room temperature, it is that 98wt% ethyl alcohol is molten that concentration, which is added,
Liquid precipitates squid ink black pigment, filtering, and the ethanol solution for being 98wt% with concentration cleans precipitating repeatedly, and drying is simultaneously crushed to
The fine grained of 100 mesh.
Embodiment 2
A kind of preparation method for the jelly adding squid ink black pigment, steps are as follows:
(1) 50 DEG C are heated water to, it is 14% white granulated sugar and 16% fructose syrup that mass fraction, which is added, molten while stirring
Solution, obtains syrup solution.
(2) by mass fraction be 0.3% carragheen, 0.7% flaxseed gum, 0.5% D-araboascorbic acid sodium,
Treated that squid ink black pigment extract is added in syrup solution after mixing for 5% deodorization, stirs evenly, then plus
Entering mass fraction is 8% vegetable oil, is stirred evenly.By obtained feed liquid in the condition that temperature is 80 DEG C, revolving speed is 2500r/min
Lower shearing homogeneous 10 minutes, the granularity of the various composition in feed liquid is reduced, it is fine and smooth uniformly to make feed liquid, while increasing the steady of feed liquid
It is qualitative.
(3) mass fraction is added in through step (2) treated feed liquid is 0.3% citric acid and 0.7% lemon
Acid sodium aqueous solution adjusts the pH to 4.7 of feed liquid.
(4) it filters after mixing evenly, takes out material and be fills up in jelly cup.
(5) jelly after filling sterilizes 15min under the conditions of 80 DEG C.
The wherein extracting method of squid ink black pigment are as follows: manually take squid ink, then use lipase and neutral proteinase water
The fat and protein in squid ink are solved, total dosage of two kinds of enzymes is the 3% of squid ink weight, is filtered to remove impurity.In filtrate
98% edible ethanol of middle addition makes prepared Chinese ink melanin deposition, after filtering, will be deposited in 53 DEG C and is dried with vacuum drier, after dry
The fine grained of 100 mesh is crushed to stainless steel pulverizer.
The wherein method of squid ink black pigment deodorization processing are as follows: squid melanin is added to the water, glucose, squid is added
The mass ratio of pitch-dark pigment and glucose is 1:1, formic acid is added after being heated with stirring to 63 DEG C of dissolutions, the additional amount of formic acid is squid
The 5% of pitch-dark chromatoplasm amount stirs 2.5h.Feed liquid after reaction is down to room temperature, it is that 95wt% ethanol solution makes that concentration, which is added,
Squid ink black pigment precipitating, filtering, the ethanol solution for being 95wt% with concentration clean precipitating repeatedly, and drying is simultaneously crushed to 100 mesh
Fine grained.
Embodiment 3
A kind of preparation method for the jelly adding squid ink black pigment, steps are as follows:
(1) 60 DEG C are heated water to, it is 10% white granulated sugar and 20% fructose syrup that mass fraction, which is added, molten while stirring
Solution, obtains syrup solution.
(2) by mass fraction be 0.3% carragheen, 0.7% flaxseed gum, 0.5% D-araboascorbic acid sodium,
Treated that squid ink black pigment extract is added in syrup solution after mixing for 10% deodorization, stirs evenly, then
Addition mass fraction is 10% vegetable oil, is stirred evenly.By obtained feed liquid temperature is 90 DEG C, revolving speed is 2300r/min's
Under the conditions of shear homogeneous 15 minutes, reduce the granularity of the various composition in feed liquid, it is fine and smooth uniformly to make feed liquid, while increasing feed liquid
Stability.
(3) mass fraction is added in through step (2) treated feed liquid is 0.8% citric acid and 0.7% lemon
Acid sodium aqueous solution adjusts the pH to 3.5 of feed liquid.
(4) it filters after mixing evenly, takes out material and be fills up in jelly cup.
(5) jelly after filling sterilizes 11min under the conditions of 83 DEG C.
The wherein extracting method of squid ink black pigment are as follows: manually take squid ink, then use lipase and neutral proteinase water
The fat and protein in squid ink are solved, total dosage of two kinds of enzymes is the 1.8% of squid ink weight, is filtered to remove impurity.It is filtering
95% edible ethanol is added in liquid makes prepared Chinese ink melanin deposition, after filtering, will be deposited in 55 DEG C of, dryings dry with vacuum drier
The fine grained of 100 mesh is crushed to stainless steel pulverizer afterwards.
The wherein method of squid ink black pigment deodorization processing are as follows: squid melanin is added to the water, glucose, squid is added
The mass ratio of pitch-dark pigment and glucose is 1.3:1, formic acid is added after being heated with stirring to 70 DEG C of dissolutions, the additional amount of formic acid is squid
The 2% of the pitch-dark chromatoplasm amount of fish stirs 2h.Feed liquid after reaction is down to room temperature, it is that 95wt% ethanol solution makes that concentration, which is added,
Squid ink black pigment precipitating, filtering, the ethanol solution for being 95wt% with concentration clean precipitating repeatedly, and drying is simultaneously crushed to 100 mesh
Fine grained.
Embodiment 4
A kind of preparation method for the jelly adding squid ink black pigment, steps are as follows:
(1) 60 DEG C are heated water to, it is 18% white granulated sugar and 12% fructose syrup that mass fraction, which is added, molten while stirring
Solution, obtains syrup solution.
(2) by mass fraction be 0.25% carragheen, 0.7% flaxseed gum, 0.3% D-araboascorbic acid sodium,
Treated that squid ink black pigment extract is added in syrup solution after mixing for 8% deodorization, stirs evenly, then plus
Entering mass fraction is 7% vegetable oil, is stirred evenly.By obtained feed liquid in the condition that temperature is 80 DEG C, revolving speed is 2500r/min
Lower shearing homogeneous 15 minutes, the granularity of the various composition in feed liquid is reduced, it is fine and smooth uniformly to make feed liquid, while increasing the steady of feed liquid
It is qualitative.
(3) mass fraction is added in through step (2) treated feed liquid is 0.15% citric acid and 0.85% lemon
Lemon acid sodium aqueous solution adjusts the pH to 5 of feed liquid.
(4) it filters after mixing evenly, takes out material and be fills up in jelly cup.
(5) jelly after filling sterilizes 20min under the conditions of 85 DEG C.
The wherein extracting method of squid ink black pigment are as follows: manually take squid ink, then use lipase and neutral proteinase water
The fat and protein in squid ink are solved, total dosage of two kinds of enzymes is the 1.8% of squid ink weight, is filtered to remove impurity.It is filtering
95% edible ethanol is added in liquid makes prepared Chinese ink melanin deposition, after filtering, will be deposited in 55 DEG C of, dryings dry with vacuum drier
The fine grained of 100 mesh is crushed to stainless steel pulverizer afterwards.
The wherein method of squid ink black pigment deodorization processing are as follows: squid melanin is added to the water, glucose, squid is added
The mass ratio of pitch-dark pigment and glucose is 1.2:1, formic acid is added after being heated with stirring to 65 DEG C of dissolutions, the additional amount of formic acid is squid
The 3% of the pitch-dark chromatoplasm amount of fish stirs 3h.Feed liquid after reaction is down to room temperature, it is that 95wt% ethanol solution makes that concentration, which is added,
Squid ink black pigment precipitating, filtering, the ethanol solution for being 95wt% with concentration clean precipitating repeatedly, and drying is simultaneously crushed to 100 mesh
Fine grained.
Embodiment 5
A kind of preparation method for the jelly adding squid ink black pigment, steps are as follows:
(1) 60 DEG C are heated water to, it is 15% white granulated sugar and 10% fructose syrup that mass fraction, which is added, molten while stirring
Solution, obtains syrup solution.
(2) by mass fraction be 0.3% carragheen, 0.6% flaxseed gum, 0.3% D-araboascorbic acid sodium,
Treated that squid ink black pigment extract is added in syrup solution after mixing for 10% deodorization, stirs evenly, then
Addition mass fraction is 5% vegetable oil, is stirred evenly.By obtained feed liquid in the item that temperature is 80 DEG C, revolving speed is 2500r/min
It is sheared homogeneous 15 minutes under part, reduces the granularity of the various composition in feed liquid, it is fine and smooth uniformly to make feed liquid, while increasing feed liquid
Stability.
(3) mass fraction is added in through step (2) treated feed liquid is 0.65% citric acid and 0.55% lemon
Lemon acid sodium aqueous solution adjusts the pH to 4 of feed liquid.
(4) it filters after mixing evenly, takes out material and be fills up in jelly cup.
(5) jelly after filling sterilizes 30min under the conditions of 85 DEG C.
The wherein extracting method of squid ink black pigment are as follows: manually take squid ink, then use lipase and neutral proteinase water
The fat and protein in squid ink are solved, total dosage of two kinds of enzymes is the 1.8% of squid ink weight, is filtered to remove impurity.It is filtering
95% edible ethanol is added in liquid makes prepared Chinese ink melanin deposition, after filtering, will be deposited in 55 DEG C of, dryings dry with vacuum drier
The fine grained of 100 mesh is crushed to stainless steel pulverizer afterwards.
The wherein method of squid ink black pigment deodorization processing are as follows: squid melanin is added to the water, glucose, squid is added
The mass ratio of pitch-dark pigment and glucose is 1.25:1, formic acid is added after being heated with stirring to 65 DEG C of dissolutions, the additional amount of formic acid is
The 4% of squid ink black pigment quality stirs 3h.Feed liquid after reaction is down to room temperature, addition concentration is 95wt% ethanol solution
Squid ink black pigment is precipitated, is filtered, the ethanol solution for being 95wt% with concentration cleans precipitating repeatedly, and drying is simultaneously crushed to 100
Purpose fine grained.
Embodiment 6
A kind of preparation method for the jelly adding squid ink black pigment, steps are as follows:
(1) 55 DEG C are heated water to, it is 15% white granulated sugar and 15% fructose syrup that mass fraction, which is added, molten while stirring
Solution, obtains syrup solution.
(2) by mass fraction be 0.26% carragheen, 0.65% flaxseed gum, 0.4% D-araboascorbic acid sodium
It is added in syrup solution, stirs evenly after mixing, the vegetable oil that mass fraction is 10% is then added, stirs evenly.
Obtained feed liquid is sheared homogeneous 15 minutes under conditions of temperature is 85 DEG C, revolving speed is 2700r/min, is reduced each in feed liquid
It is fine and smooth uniformly to make feed liquid, while increasing the stability of feed liquid for the granularity of kind ingredient.
(3) mass fraction is added in through step (2) treated feed liquid is 0.5% citric acid and 0.5% lemon
Acid sodium aqueous solution adjusts the pH to 4.3 of feed liquid.
(4) by mass fraction be 10% deodorization treated squid ink black pigment extract and tapioca starch powder circle is made；
(5) feed liquid that step (3) obtains is filtered after mixing evenly, takes out material and is fills up in jelly cup, powder circle is added when filling.
(6) jelly after filling sterilizes 15min under the conditions of 85 DEG C.
Wherein the extracting method of squid ink black pigment and the method for squid ink black pigment deodorization processing are same as Example 1.
Embodiment 7
A kind of preparation method for the jelly adding squid ink black pigment, steps are as follows:
(1) 50 DEG C are heated water to, it is 14% white granulated sugar and 16% fructose syrup that mass fraction, which is added, molten while stirring
Solution, obtains syrup solution.
(2) by mass fraction be 0.3% carragheen, 0.7% flaxseed gum, 0.5% D-araboascorbic acid sodium mix
It is added in syrup solution, stirs evenly after closing uniformly, it is 8% vegetable oil that mass fraction, which is then added, is stirred evenly.It will obtain
Feed liquid sheared homogeneous 10 minutes under conditions of temperature is 80 DEG C, revolving speed is 2500r/min, reduce feed liquid in various composition
Granularity, it is fine and smooth uniformly to make feed liquid, while increasing the stability of feed liquid.
(3) mass fraction is added in through step (2) treated feed liquid is 0.3% citric acid and 0.7% lemon
Acid sodium aqueous solution adjusts the pH to 4.7 of feed liquid.
(4) by mass fraction be 5% deodorization treated squid ink black pigment extract and tapioca starch powder circle is made；
(5) feed liquid that step (3) obtains is filtered after mixing evenly, takes out material and is fills up in jelly cup, powder circle is added when filling.
(6) jelly after filling sterilizes 15min under the conditions of 80 DEG C.
Wherein the extracting method of squid ink black pigment and the method for squid ink black pigment deodorization processing are same as Example 2.
Embodiment 8
A kind of preparation method for the jelly adding squid ink black pigment, steps are as follows:
(1) 60 DEG C are heated water to, it is 10% white granulated sugar and 20% fructose syrup that mass fraction, which is added, molten while stirring
Solution, obtains syrup solution.
(2) by mass fraction be 0.3% carragheen, 0.7% flaxseed gum, 0.5% D-araboascorbic acid sodium mix
It is added in syrup solution, stirs evenly after closing uniformly, it is 10% vegetable oil that mass fraction, which is then added, is stirred evenly.Will
To feed liquid sheared homogeneous 15 minutes under conditions of temperature is 90 DEG C, revolving speed is 2300r/min, reduce feed liquid in it is various at
It is fine and smooth uniformly to make feed liquid, while increasing the stability of feed liquid for the granularity divided.
(3) mass fraction is added in through step (2) treated feed liquid is 0.8% citric acid and 0.7% lemon
Acid sodium aqueous solution adjusts the pH to 3.5 of feed liquid.
(4) by mass fraction be 10% deodorization treated squid ink black pigment extract and tapioca starch powder circle is made.
(5) feed liquid that step (3) obtains is filtered after mixing evenly, takes out material and be fills up in jelly cup, powder is added in when filling
Circle.
(6) jelly after filling sterilizes 11min under the conditions of 83 DEG C.
Wherein the extracting method of squid ink black pigment and the method for squid ink black pigment deodorization processing are same as Example 3.
Embodiment 9
A kind of preparation method for the jelly adding squid ink black pigment, steps are as follows:
(1) 60 DEG C are heated water to, it is 18% white granulated sugar and 12% fructose syrup that mass fraction, which is added, molten while stirring
Solution, obtains syrup solution.
(2) by mass fraction be 0.25% carragheen, 0.7% flaxseed gum, 0.3% D-araboascorbic acid sodium mix
It is added in syrup solution, stirs evenly after closing uniformly, it is 7% vegetable oil that mass fraction, which is then added, is stirred evenly.It will obtain
Feed liquid sheared homogeneous 15 minutes under conditions of temperature is 80 DEG C, revolving speed is 2500r/min, reduce feed liquid in various composition
Granularity, it is fine and smooth uniformly to make feed liquid, while increasing the stability of feed liquid.
(3) mass fraction is added in through step (2) treated feed liquid is 0.15% citric acid and 0.85% lemon
Lemon acid sodium aqueous solution adjusts the pH to 5 of feed liquid.
(4) by mass fraction be 8% deodorization treated squid ink black pigment extract and tapioca starch powder circle is made.
(5) feed liquid that step (3) obtains is filtered after mixing evenly, takes out material and be fills up in jelly cup, powder is added in when filling
Circle.
(6) jelly after filling sterilizes 20min under the conditions of 85 DEG C.
Wherein the extracting method of squid ink black pigment and the method for squid ink black pigment deodorization processing are same as Example 4.
Embodiment 10
A kind of preparation method for the jelly adding squid ink black pigment, steps are as follows:
(1) 60 DEG C are heated water to, it is 15% white granulated sugar and 10% fructose syrup that mass fraction, which is added, molten while stirring
Solution, obtains syrup solution.
(2) by mass fraction be 0.3% carragheen, 0.6% flaxseed gum, 0.3% D-araboascorbic acid sodium mix
It is added in syrup solution, stirs evenly after closing uniformly, it is 5% vegetable oil that mass fraction, which is then added, is stirred evenly.It will obtain
Feed liquid sheared homogeneous 15 minutes under conditions of temperature is 80 DEG C, revolving speed is 2500r/min, reduce feed liquid in various composition
Granularity, it is fine and smooth uniformly to make feed liquid, while increasing the stability of feed liquid.
(3) mass fraction is added in through step (2) treated feed liquid is 0.65% citric acid and 0.55% lemon
Lemon acid sodium aqueous solution adjusts the pH to 4 of feed liquid.
(4) by mass fraction be 10% deodorization treated squid ink black pigment extract and tapioca starch powder circle is made.
(5) feed liquid that step (3) obtains is filtered after mixing evenly, takes out material and be fills up in jelly cup, powder is added in when filling
Circle.
(6) jelly after filling sterilizes 30min under the conditions of 85 DEG C.
Wherein the extracting method of squid ink black pigment and the method for squid ink black pigment deodorization processing are same as Example 5.
Sensory evaluation: the present invention tests to the fishy smell of deodorization treated squid ink black pigment, carries out with control group
Comparison, control group is handled without deodorization, and using " the five-grade marking system ", score value is respectively 5,4,3,2,1, and evaluating member is made of 5 people,
Final assessment result takes 5 people to provide the average value of score value, and subjective appreciation standards of grading and specific appraisal result are shown in Tables 1 and 2.
1 squid ink black pigment subjective appreciation standards of grading of table
| Fishy smell | |
| Strong fishy smell | 5 |
| There is fishy smell | 4 |
| Slightly fishy smell | 3 |
| It is more pure and fresh | 2 |
| It is pure and fresh | 1 |
The fishy smell evaluation result of deodorization is handled in 2 embodiment 1-5 of table squid ink black pigment and control group (non-deodorization)
| Fishy smell | |
| Embodiment 1 | 1 |
| Embodiment 2 | 1.2 |
| Embodiment 3 | 1.8 |
| Embodiment 4 | 1.4 |
| Embodiment 5 | 1.4 |
| Control group | 5 |
The above is only presently preferred embodiments of the present invention, is not intended to limit the invention in any way, all technologies according to the present invention
Essence any simple modification, change and equivalent structure transformation to the above embodiments, still fall within the technology of the present invention side
The protection scope of case.
Claims (10)
1. a kind of jelly for adding squid ink black pigment, it is characterised in that: the jelly includes the following components'mass percentage:
Vegetable oil 5-10%, thickener 0.9-1%, potassium chloride 0.1-0.2%, white granulated sugar 10-20%, fructose syrup 10-20%, citric acid
0.3-0.8%, sodium citrate 0.5-0.9%, D-araboascorbic acid sodium 0.2-1%, squid ink black pigment 5-10%, surplus is water.
2. a kind of jelly for adding squid ink black pigment according to claim 1, it is characterised in that squid ink black pigment mentions
Take method are as follows: manually take squid ink, then use lipase and fat and protein in neutral proteinase hydrolysis squid ink, filtering
Remove impurity；The ethanol water that concentration is 90-98wt% is added in filtrate precipitates squid ink black pigment, will after filtering
Drying precipitate simultaneously crushes.
3. a kind of jelly for adding squid ink black pigment according to claim 1 or 2, it is characterised in that squid ink black pigment
The method of deodorization processing are as follows: squid melanin is added to the water, glucose, the mass ratio of squid ink black pigment and glucose is added
For 1-1.3:1, formic acid is added after being heated with stirring to 55-70 DEG C of dissolution, the additional amount of formic acid is the 2- of squid ink black pigment quality
5%, stir 2-3h；Feed liquid after reaction is down to room temperature, it is that 90-98wt% ethanol solution keeps squid ink black pigment heavy that concentration, which is added,
It forms sediment, filtering, the ethanol solution for being 90-98wt% with concentration cleans precipitating repeatedly, and drying simultaneously crushes.
4. a kind of jelly for adding squid ink black pigment according to claim 1, it is characterised in that: the vegetable oil is coconut palm
At least one of seed oil, palm oil.
5. a kind of jelly for adding squid ink black pigment according to claim 1, it is characterised in that: the thickener is card
Draw at least one of glue, flaxseed gum.
6. a kind of jelly for adding squid ink black pigment according to claim 2, it is characterised in that: the lipase is in
Property protease total dosage be squid ink weight 0.5-3.0%.
7. a kind of jelly for adding squid ink black pigment according to claim 1, it is characterised in that the preparation of the jelly
Method the following steps are included:
(1) by white granulated sugar, fructose syrup investment water, heating stirring dissolution obtains syrup solution；
(2) squid ink black pigment after the thickener prepared in proportion, vegetable oil, D-araboascorbic acid sodium, deodorization is put into step
Suddenly in the syrup solution that (1) obtains, it is evenly dispersed after heating boil glue, be during which stirred continuously, by well-done feed liquid temperature be 70-
100 DEG C, revolving speed be 1000-5000r/min under conditions of shear agitation 1-20 minutes；
(3) dissolved sodium citrate aqueous solution is added in through step (2) treated feed liquid, adjusts the pH to 3.5- of feed liquid
5；
(4) it filters after mixing evenly, takes out material and be fills up in jelly cup.
8. a kind of jelly for adding squid ink black pigment according to claim 1, it is characterised in that the preparation of the jelly
Method the following steps are included:
(1) by white granulated sugar, fructose syrup investment water, heating stirring dissolution obtains syrup solution；
(2) in the syrup solution for obtaining the thickener prepared in proportion, vegetable oil, D-araboascorbic acid sodium investment step (1),
It is evenly dispersed after heating boil glue, be during which stirred continuously, by well-done feed liquid temperature be 70-100 DEG C, revolving speed 1000-
Shear agitation 1-20 minutes under conditions of 5000r/min；
(3) dissolved sodium citrate aqueous solution is added in through step (2) treated feed liquid, adjusts the pH to 3.5- of feed liquid
5；
(4) powder circle is made with tapioca starch in the squid ink black pigment after deodorization；
(5) feed liquid that step (3) obtains is filtered after mixing evenly, takes out material and is fills up in jelly cup, powder circle is added when filling.
9. a kind of preparation method of jelly for adding squid ink black pigment according to claim 7 or 8, it is characterised in that:
In step (2), well-done feed liquid shear agitation 10- under conditions of temperature is 80-90 DEG C, revolving speed is 2300-2700r/min
15 minutes.
10. a kind of preparation method of jelly for adding squid ink black pigment according to claim 7 or 8, it is characterised in that:
Jelly after filling sterilizes 5-30min under the conditions of 75-90 DEG C.
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|---|---|---|---|
| CN201810820537.0A CN108936484A (en) | 2018-07-24 | 2018-07-24 | A kind of jelly and preparation method thereof adding squid ink black pigment |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104544321A (en) * | 2013-10-21 | 2015-04-29 | 大连市沙河口区中小微企业服务中心 | Soluble squid inkiness pigment |
| CN107319449A (en) * | 2017-08-17 | 2017-11-07 | 阳江喜之郎果冻制造有限公司 | A kind of high konjak jelly and its production technology thoroughly |
| CN107410842A (en) * | 2017-05-02 | 2017-12-01 | 江南大学 | A kind of preparation of soluble squid ink black pigment through deodorant and its application in food |
| CN108236931A (en) * | 2017-12-05 | 2018-07-03 | 浙江海洋大学 | A kind of mussel boiling liquid takes off the preparation method of cadmium adsorbent |
-
2018
- 2018-07-24 CN CN201810820537.0A patent/CN108936484A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104544321A (en) * | 2013-10-21 | 2015-04-29 | 大连市沙河口区中小微企业服务中心 | Soluble squid inkiness pigment |
| CN107410842A (en) * | 2017-05-02 | 2017-12-01 | 江南大学 | A kind of preparation of soluble squid ink black pigment through deodorant and its application in food |
| CN107319449A (en) * | 2017-08-17 | 2017-11-07 | 阳江喜之郎果冻制造有限公司 | A kind of high konjak jelly and its production technology thoroughly |
| CN108236931A (en) * | 2017-12-05 | 2018-07-03 | 浙江海洋大学 | A kind of mussel boiling liquid takes off the preparation method of cadmium adsorbent |
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