CN108936198A - One Plant Extracts prepare the preparation method of green preservative - Google Patents
One Plant Extracts prepare the preparation method of green preservative Download PDFInfo
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- CN108936198A CN108936198A CN201810863403.7A CN201810863403A CN108936198A CN 108936198 A CN108936198 A CN 108936198A CN 201810863403 A CN201810863403 A CN 201810863403A CN 108936198 A CN108936198 A CN 108936198A
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- 238000002360 preparation method Methods 0.000 title claims abstract description 49
- 239000003755 preservative agent Substances 0.000 title claims abstract description 28
- 230000002335 preservative effect Effects 0.000 title claims abstract description 28
- 239000000419 plant extract Substances 0.000 title claims abstract description 27
- 239000000284 extract Substances 0.000 claims abstract description 92
- 244000046052 Phaseolus vulgaris Species 0.000 claims abstract description 35
- 235000010627 Phaseolus vulgaris Nutrition 0.000 claims abstract description 35
- 240000004760 Pimpinella anisum Species 0.000 claims abstract description 34
- 235000012550 Pimpinella anisum Nutrition 0.000 claims abstract description 34
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 27
- 239000000463 material Substances 0.000 claims abstract description 25
- 235000007265 Myrrhis odorata Nutrition 0.000 claims abstract description 23
- 235000020748 rosemary extract Nutrition 0.000 claims abstract description 23
- 239000000945 filler Substances 0.000 claims abstract description 20
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 17
- 239000012153 distilled water Substances 0.000 claims abstract description 15
- 238000004321 preservation Methods 0.000 claims abstract description 10
- 239000000203 mixture Substances 0.000 claims abstract description 8
- 235000013312 flour Nutrition 0.000 claims abstract description 5
- 238000006243 chemical reaction Methods 0.000 claims description 54
- 239000000843 powder Substances 0.000 claims description 54
- 239000002904 solvent Substances 0.000 claims description 48
- 239000000126 substance Substances 0.000 claims description 46
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 36
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims description 36
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 34
- 239000002245 particle Substances 0.000 claims description 24
- 238000010992 reflux Methods 0.000 claims description 24
- 229910052757 nitrogen Inorganic materials 0.000 claims description 18
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 17
- 244000178870 Lavandula angustifolia Species 0.000 claims description 14
- 235000010663 Lavandula angustifolia Nutrition 0.000 claims description 14
- 239000001102 lavandula vera Substances 0.000 claims description 14
- 235000018219 lavender Nutrition 0.000 claims description 14
- 238000000605 extraction Methods 0.000 claims description 13
- 241001529742 Rosmarinus Species 0.000 claims description 12
- 125000003158 alcohol group Chemical group 0.000 claims description 12
- 238000003756 stirring Methods 0.000 claims description 9
- 238000007259 addition reaction Methods 0.000 claims description 6
- 239000013049 sediment Substances 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 5
- 238000002604 ultrasonography Methods 0.000 claims description 5
- 240000006927 Foeniculum vulgare Species 0.000 claims description 2
- 235000004204 Foeniculum vulgare Nutrition 0.000 claims description 2
- 235000013339 cereals Nutrition 0.000 claims 1
- 229940092258 rosemary extract Drugs 0.000 claims 1
- 239000001233 rosmarinus officinalis l. extract Substances 0.000 claims 1
- 239000003795 chemical substances by application Substances 0.000 abstract description 25
- 235000013305 food Nutrition 0.000 abstract description 11
- 239000007788 liquid Substances 0.000 abstract description 6
- 231100000252 nontoxic Toxicity 0.000 abstract description 4
- 230000003000 nontoxic effect Effects 0.000 abstract description 4
- 235000021056 liquid food Nutrition 0.000 abstract description 3
- 239000007787 solid Substances 0.000 abstract description 3
- 235000021055 solid food Nutrition 0.000 abstract description 3
- 230000002421 anti-septic effect Effects 0.000 abstract description 2
- 235000019441 ethanol Nutrition 0.000 description 20
- 241000238366 Cephalopoda Species 0.000 description 8
- 230000000694 effects Effects 0.000 description 7
- 238000000034 method Methods 0.000 description 7
- 239000005820 Prochloraz Substances 0.000 description 6
- TVLSRXXIMLFWEO-UHFFFAOYSA-N prochloraz Chemical compound C1=CN=CN1C(=O)N(CCC)CCOC1=C(Cl)C=C(Cl)C=C1Cl TVLSRXXIMLFWEO-UHFFFAOYSA-N 0.000 description 6
- 235000012055 fruits and vegetables Nutrition 0.000 description 5
- 239000007789 gas Substances 0.000 description 5
- 238000005303 weighing Methods 0.000 description 5
- HFCYZXMHUIHAQI-UHFFFAOYSA-N Thidiazuron Chemical compound C=1C=CC=CC=1NC(=O)NC1=CN=NS1 HFCYZXMHUIHAQI-UHFFFAOYSA-N 0.000 description 4
- 239000003242 anti bacterial agent Substances 0.000 description 4
- 229940088710 antibiotic agent Drugs 0.000 description 4
- 230000008901 benefit Effects 0.000 description 3
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 3
- 230000001954 sterilising effect Effects 0.000 description 3
- 238000003860 storage Methods 0.000 description 3
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 description 2
- 241000251468 Actinopterygii Species 0.000 description 2
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 2
- 241000894006 Bacteria Species 0.000 description 2
- IMQLKJBTEOYOSI-GPIVLXJGSA-N Inositol-hexakisphosphate Chemical compound OP(O)(=O)O[C@H]1[C@H](OP(O)(O)=O)[C@@H](OP(O)(O)=O)[C@H](OP(O)(O)=O)[C@H](OP(O)(O)=O)[C@@H]1OP(O)(O)=O IMQLKJBTEOYOSI-GPIVLXJGSA-N 0.000 description 2
- IMQLKJBTEOYOSI-UHFFFAOYSA-N Phytic acid Natural products OP(O)(=O)OC1C(OP(O)(O)=O)C(OP(O)(O)=O)C(OP(O)(O)=O)C(OP(O)(O)=O)C1OP(O)(O)=O IMQLKJBTEOYOSI-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 238000007605 air drying Methods 0.000 description 2
- 230000003078 antioxidant effect Effects 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 235000013361 beverage Nutrition 0.000 description 2
- 235000013399 edible fruits Nutrition 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 235000013372 meat Nutrition 0.000 description 2
- 235000002949 phytic acid Nutrition 0.000 description 2
- 239000000467 phytic acid Substances 0.000 description 2
- 229940068041 phytic acid Drugs 0.000 description 2
- 108010064470 polyaspartate Proteins 0.000 description 2
- 235000010413 sodium alginate Nutrition 0.000 description 2
- 239000000661 sodium alginate Substances 0.000 description 2
- 229940005550 sodium alginate Drugs 0.000 description 2
- 238000004659 sterilization and disinfection Methods 0.000 description 2
- 244000025254 Cannabis sativa Species 0.000 description 1
- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 description 1
- 229910021380 Manganese Chloride Inorganic materials 0.000 description 1
- 229930003268 Vitamin C Natural products 0.000 description 1
- 150000001412 amines Chemical class 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 235000006708 antioxidants Nutrition 0.000 description 1
- 239000002775 capsule Substances 0.000 description 1
- 238000013329 compounding Methods 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- OXBLHERUFWYNTN-UHFFFAOYSA-M copper(I) chloride Chemical compound [Cu]Cl OXBLHERUFWYNTN-UHFFFAOYSA-M 0.000 description 1
- 230000002542 deteriorative effect Effects 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 150000002170 ethers Chemical class 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 229940099607 manganese chloride Drugs 0.000 description 1
- 239000011565 manganese chloride Substances 0.000 description 1
- OXOKTPUZOHPXSA-UHFFFAOYSA-L manganese(2+);n-propyl-n-[2-(2,4,6-trichlorophenoxy)ethyl]imidazole-1-carboxamide;dichloride Chemical compound Cl[Mn]Cl.C1=CN=CN1C(=O)N(CCC)CCOC1=C(Cl)C=C(Cl)C=C1Cl.C1=CN=CN1C(=O)N(CCC)CCOC1=C(Cl)C=C(Cl)C=C1Cl.C1=CN=CN1C(=O)N(CCC)CCOC1=C(Cl)C=C(Cl)C=C1Cl.C1=CN=CN1C(=O)N(CCC)CCOC1=C(Cl)C=C(Cl)C=C1Cl OXOKTPUZOHPXSA-UHFFFAOYSA-L 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000000575 pesticide Substances 0.000 description 1
- 230000000452 restraining effect Effects 0.000 description 1
- 230000001629 suppression Effects 0.000 description 1
- 239000000375 suspending agent Substances 0.000 description 1
- 239000004548 suspo-emulsion Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 235000019154 vitamin C Nutrition 0.000 description 1
- 239000011718 vitamin C Substances 0.000 description 1
- 239000004562 water dispersible granule Substances 0.000 description 1
- 239000004563 wettable powder Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L3/00—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
- A23L3/34—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals
- A23L3/3454—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals in the form of liquids or solids
- A23L3/3463—Organic compounds; Microorganisms; Enzymes
- A23L3/3472—Compounds of undetermined constitution obtained from animals or plants
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Abstract
The present invention relates to the preparation methods that food antiseptic preservation field, specifically a Plant Extracts prepare green preservative；One Plant Extracts prepare the composition of green preservative are as follows: mass fraction is 10-15 parts of anise extract, 2-5 parts of Herba Lysimachiae foenumgraeci extract, 3-5 parts of bean dregs extract, 2-4 parts of Rosmarinus officinalis extract, 1-3 parts of orange bark extract, 20-30 parts of filler material；By come what is be prepared, being the nontoxic green product of overall safety using edible materials such as anise extract, Herba Lysimachiae foenumgraeci extract, bean dregs extract, Rosmarinus officinalis extract, orange bark extracts；And it is that can change its application field by the type for changing filler material, such as the distilled water of addition and the carry out mixed liquor of glycerol, its food that can be widely used in liquid type, if filler material is its antistaling agent that can be used as solid based food of flour, therefore its application range is very extensive, can be widely used in liquid and solid food.
Description
Technical field
The present invention relates to the systems that food antiseptic preservation field, specifically a Plant Extracts prepare green preservative
Preparation Method.
Background technique
Antistaling agent is a kind of processing food, to prevent food decay rotten, keeps nutritional ingredient and color, smell and taste constant, to food
Product carry out short-term fresh-keeping supplementary means and technical method.Now, main antistaling agent has chemical synthesis substance and natural materials
It is obtained as two ways.
Chinese patent application CN104472672B discloses a kind of fruit and vegetable fresh-keeping agent.The fruit and vegetable fresh-keeping agent active constituent is miaow
Fresh amine and Thidiazuron, Prochloraz are Prochloraz raw medicine or prochloraz-manganese chloride complex or prochloraz nantokite, and wherein Prochloraz accounts for preserving fruit and vegetable utilizing
The weight percent of agent is 10%-70%, and the weight percent that Thidiazuron accounts for fruit and vegetable fresh-keeping agent is 0.02%-5%, in pesticide
Allow to supply surplus using with acceptable auxiliary element, the weight ratio of Prochloraz and Thidiazuron is 5-500:1.Of the invention
Fruit and vegetable fresh-keeping agent can be prepared into suspending agent, suspoemulsion, wettable powder and water dispersible granules by known method.The present invention adopts
It is fresh-keeping for the postharvest storage of veterinary antibiotics with Prochloraz and compounding for Thidiazuron, not only to mould proof, the sterilization of veterinary antibiotics
Effect is good, extends the storage period of veterinary antibiotics, and protects green effect and protrude, and guarantees the storage quality of veterinary antibiotics, no chemistry
Residual, using conveniently, safely, at low cost, easily operated and popularization, still, it is using artificial synthesized that this method, which prepares antistaling agent,
Mode produced, therefore it is with certain toxicity, be not safety and environmental protection product.
Chinese patent application CN 104886225B discloses a kind of squid antistaling agent and its preservation method, by weight percentage
Content groups become: poly-aspartate 0.02%-0.2%, phytic acid 0.005%-0.05%, sodium alginate 0.1%-0.5%, more than water
Amount；Preservation method is: poly-aspartate is soluble in water, sodium alginate is then added and stirs evenly, is eventually adding phytic acid stirring
Uniformly, squid antistaling agent is prepared；New Fresh squid is cleaned, capsule is cut, is then cut into sheet, then is placed on the squid that temperature is 4 DEG C
It is uniformly impregnated in fish antistaling agent, squid fillet is pulled out and is drained, natural air drying under the conditions of being placed in 4 DEG C, the squid meat after air-drying
Piece surface will form one layer of antistaling film.Advantage is: antistaling agent is all made of natural green material, safe and non-toxic, does not generate to people
Body harmful substance, while can also play anti-oxidant, restraining and sterilizing bacteria keeps the multiple actions such as moisture, and fresh-keeping effect is significant, uses this
The freshness date of the fresh squid flesh of fish of antistaling agent facilitated the transport of squid meat to circulate up to -15 days 10 days, and comparatively it protects new
Period is shorter.
For above-mentioned there are problem, the antistaling agent of the advantages that researching and developing safety and environmental protection and longer service life a kind of meets city
Field demand seems even more important.
Summary of the invention
In order to achieve the purpose that in background technique, the system proposed by the present invention that green preservative is prepared using plant extracts
Preparation Method；By utilizing anise extract, Herba Lysimachiae foenumgraeci extract, bean dregs extract, Rosmarinus officinalis extract, orange bark extract etc.
Edible material is the nontoxic green product of overall safety come what is be prepared；And it passes through change filler material
Type be that can change its application field, such as be added distilled water and glycerol carry out mixed liquor, can be widely used in
The food of liquid type, if filler material is its antistaling agent that can be used as solid based food of flour, therefore its application range is very wide
It is general, liquid and solid food can be widely used in.
What the present invention realized by the following technical solutions
One Plant Extracts prepare the preparation method of green preservative the following steps are included:
(1) preparation of anise extract
In market, the aniseed of purchase is dried, and is then added into pulverizer and is crushed, granular size is
50-100 mesh is carried out refluxing extraction and is reacted 4-6 hour, and wherein reflux solvent is alcohol solvent, and aniseed powder
Mass ratio is 7:3, is filtered after fully reacting, remove filter residue, by obtained solution be added Rotary Evaporators in into
Row revolving, removes alcohol solvent, obtained substance is exactly anise extract, in the substance, contains a large amount of native hydroxyl fennel
The substances such as ethers can effectively play oxidation resistanct fresh-keeping effect.
(2) preparation of bean dregs extract
The bean dregs of collection are crushed, for powder particle diameter size in 10-20 mesh, then weighing its mass fraction is 20-
The ethyl acetate of 30 parts of bean dregs powder and 50-60 part is added in reaction kettle, then under the conditions of 60-70 DEG C, flow back anti-
It after answering 5-10 hours, is filtered, removes filter residue, obtained solution is added in Rotary Evaporators and is rotated, removed
Ethyl acetate solvent, obtained substance are exactly bean dregs extract,, can be with containing a large amount of natural acid Ester in the substance
It is effectively ensured with inoxidizability, reaches fresh-keeping effect.
(3) preparation of Herba Lysimachiae foenumgraeci extract
It after the lavender bar of collection is dried, is crushed, powder particle diameter size is in 20-30 mesh, then by it
Refluxing extraction is carried out to react 3-5 hours, wherein reflux solvent is alcohol solvent, and the mass ratio of lavender powder is 7:3,
It is filtered after fully reacting, removes filter residue, obtained solution is added in Rotary Evaporators and is rotated, remove ethyl alcohol
Solvent, obtained substance are exactly Herba Lysimachiae foenumgraeci extract, and the Lavender in the substance extract can effectively play sterilization
Effect.
(4) preparation of Rosmarinus officinalis extract
It after the rosemary of collection is dried, is crushed, then powder particle diameter size claims in 40-60 mesh
It takes in the powder from rosemary and 50-60 parts of acetone addition reaction kettle that its mass fraction is 10-15 parts, then in 50-65 DEG C of item
It under part, after carrying out back flow reaction 4-8 hours, is filtered, removes filter residue, obtained solution is added in Rotary Evaporators
It is rotated, removes acetone solvent, obtained substance is exactly Rosmarinus officinalis extract, in the substance, contains a large amount of natural lip shape
The soft acid of grass has inoxidizability.
(5) prepared by orange bark extract
The orange peel of collection is crushed, in 100-200 mesh, then weigh its mass fraction is powder particle diameter size
The distilled water of 10-30 parts of orange peel powder and 10-30 part is added in reaction kettle, then under the conditions of 30-50 DEG C, is reacted
After 4-5 hours, is carried out after standing 5-10 hours, carried out being separated off sediment, obtained substance is exactly orange peel
Extract in the substance, contains the suppression of the antioxidative substances and citric acid etc. such as a large amount of natural vitamin C, natural VE
Bacterium ingredient can effectively reach fresh-keeping effect.
(6) preparation of filler material
10-20 parts of distilled water and 1-2 parts of glycerol are carried out in the substances such as mixture prepared or flour
It is a kind of.
(7) preparation of antistaling agent
Temperature of reaction kettle is maintained 40-60 DEG C, mechanical agitator revolving speed is 250-350rpm, and nitrogen is passed through into reaction kettle
Gas is protected, and being passed through nitrogen flow rate is that 20-30 is added into reaction kettle after being passed through nitrogen 10-15 minutes by 60-100ml/min
Part filler material, stirring 2-5 minute after, then by mass fraction be 10-15 parts anise extract, 2-5 parts lavender extraction
Object, 3-5 parts of bean dregs extract, 2-4 parts of Rosmarinus officinalis extract, 1-3 parts of orange bark extract sequentially add in reaction kettle,
Then it after carrying out hybrid reaction 2-3 hours, after obtained substance is cooled to room temperature, is then added in ultrasonic machine and is surpassed
After sound 1-2 hours, it is sealed preservation, which is exactly that plant extracts prepares green preservative.
Beneficial to benefit
Green preservative prepared by the present invention, be by using anise extract, Herba Lysimachiae foenumgraeci extract, bean dregs extract,
The edible materials such as Rosmarinus officinalis extract, orange bark extract are nontoxic green of overall safety come what is be prepared
Color product；And it is that can change its application field by the type for changing filler material, such as the distilled water and glycerol being added
Mixed liquor is carried out, the food of liquid type can be widely used in, it can be used as solid based food if filler material is flour
Antistaling agent, therefore its application range is very extensive, can be widely used in liquid and solid food.
Specific embodiment
In order to keep the purpose of the present invention, technical scheme and beneficial effects clearer, below in conjunction with experimental data, to this
The preferred embodiment of invention is described in detail, to facilitate the technical staff to understand.
Embodiment 1
One Plant Extracts prepare the preparation method of green preservative the following steps are included:
(1) preparation of anise extract
In market, the aniseed of purchase is dried, and is then added into pulverizer and is crushed, granular size is
50-100 mesh is carried out refluxing extraction and is reacted 4-6 hour, and wherein reflux solvent is alcohol solvent, and aniseed powder
Mass ratio is 7:3, is filtered after fully reacting, remove filter residue, by obtained solution be added Rotary Evaporators in into
Row revolving, removes alcohol solvent, obtained substance is exactly anise extract.
(2) preparation of bean dregs extract
The bean dregs of collection are crushed, for powder particle diameter size in 10-20 mesh, then weighing its mass fraction is 30 parts
Bean dregs powder and 60 parts ethyl acetate be added reaction kettle in, then under the conditions of 60-70 DEG C, carry out back flow reaction 5-10 it is small
Shi Hou is filtered, and filter residue is removed, and obtained solution is added in Rotary Evaporators and is rotated, and removes ethyl acetate
Solvent, obtained substance are exactly bean dregs extract.
(3) preparation of Herba Lysimachiae foenumgraeci extract
It after the lavender bar of collection is dried, is crushed, powder particle diameter size is in 20-30 mesh, then by it
Refluxing extraction is carried out to react 3-5 hours, wherein reflux solvent is alcohol solvent, and the mass ratio of lavender powder is 7:3,
It is filtered after fully reacting, removes filter residue, obtained solution is added in Rotary Evaporators and is rotated, remove ethyl alcohol
Solvent, obtained substance are exactly Herba Lysimachiae foenumgraeci extract.
(4) preparation of Rosmarinus officinalis extract
It after the rosemary of collection is dried, is crushed, then powder particle diameter size claims in 40-60 mesh
It takes in the powder from rosemary and 60 parts of acetone addition reaction kettle that its mass fraction is 15 parts, then under the conditions of 50-65 DEG C, into
It after row back flow reaction 4-8 hours, is filtered, removes filter residue, obtained solution is added in Rotary Evaporators and is revolved
It steams, removes acetone solvent, obtained substance is exactly Rosmarinus officinalis extract.
(5) prepared by orange bark extract
The orange peel of collection is crushed, in 100-200 mesh, then weigh its mass fraction is powder particle diameter size
30 parts of orange peel powder and 30 parts of distilled water are added in reaction kettle, and then under the conditions of 30-50 DEG C, it is small to carry out reaction 4-5
Shi Hou is carried out after standing 5-10 hours, is carried out being separated off sediment, and obtained substance is exactly that orange peel extracts
Object.
(6) preparation of filler material
20 parts of distilled water and 1-2 parts of glycerol are carried out mixture prepared.
(7) preparation of antistaling agent
Temperature of reaction kettle is maintained 40-60 DEG C, mechanical agitator revolving speed is 250-350rpm, and nitrogen is passed through into reaction kettle
Gas is protected, and being passed through nitrogen flow rate is 60-100ml/min, and after being passed through nitrogen 10-15 minutes, 30 parts are added into reaction kettle
Filler material, after stirring 2-5 minute, then by mass fraction be 15 parts of anise extract, 5 parts of Herba Lysimachiae foenumgraeci extract, 5 parts
Bean dregs extract, 4 parts of Rosmarinus officinalis extract, 3 parts of orange bark extract sequentially add in reaction kettle, then carry out mixing anti-
After answering 2-3 hours, after obtained substance is cooled to room temperature, then it is added in ultrasonic machine and carries out ultrasound after 1-2 hours, it will
It is sealed preservation, which is exactly that plant extracts prepares green preservative.
Embodiment 2
One Plant Extracts prepare the preparation method of green preservative the following steps are included:
(1) preparation of anise extract
In market, the aniseed of purchase is dried, and is then added into pulverizer and is crushed, granular size is
50-100 mesh is carried out refluxing extraction and is reacted 4-6 hour, and wherein reflux solvent is alcohol solvent, and aniseed powder
Mass ratio is 7:3, is filtered after fully reacting, remove filter residue, by obtained solution be added Rotary Evaporators in into
Row revolving, removes alcohol solvent, obtained substance is exactly anise extract.
(2) preparation of bean dregs extract
The bean dregs of collection are crushed, for powder particle diameter size in 10-20 mesh, then weighing its mass fraction is 30 parts
Bean dregs powder and 60 parts ethyl acetate be added reaction kettle in, then under the conditions of 60-70 DEG C, carry out back flow reaction 5-10 it is small
Shi Hou is filtered, and filter residue is removed, and obtained solution is added in Rotary Evaporators and is rotated, and removes ethyl acetate
Solvent, obtained substance are exactly bean dregs extract.
(3) preparation of Herba Lysimachiae foenumgraeci extract
It after the lavender bar of collection is dried, is crushed, powder particle diameter size is in 20-30 mesh, then by it
Refluxing extraction is carried out to react 3-5 hours, wherein reflux solvent is alcohol solvent, and the mass ratio of lavender powder is 7:3,
It is filtered after fully reacting, removes filter residue, obtained solution is added in Rotary Evaporators and is rotated, remove ethyl alcohol
Solvent, obtained substance are exactly Herba Lysimachiae foenumgraeci extract.
(4) preparation of Rosmarinus officinalis extract
It after the rosemary of collection is dried, is crushed, then powder particle diameter size claims in 40-60 mesh
It takes in the powder from rosemary and 50 parts of acetone addition reaction kettle that its mass fraction is 10 parts, then under the conditions of 50-65 DEG C, into
It after row back flow reaction 4-8 hours, is filtered, removes filter residue, obtained solution is added in Rotary Evaporators and is revolved
It steams, removes acetone solvent, obtained substance is exactly Rosmarinus officinalis extract.
(5) prepared by orange bark extract
The orange peel of collection is crushed, in 100-200 mesh, then weigh its mass fraction is powder particle diameter size
10 parts of orange peel powder and 10 parts of distilled water are added in reaction kettle, and then under the conditions of 30-50 DEG C, it is small to carry out reaction 4-5
Shi Hou is carried out after standing 5-10 hours, is carried out being separated off sediment, and obtained substance is exactly that orange peel extracts
Object.
(6) preparation of filler material
20 parts of distilled water and 2 parts of glycerol are carried out mixture prepared.
(7) preparation of antistaling agent
Temperature of reaction kettle is maintained 40-60 DEG C, mechanical agitator revolving speed is 250-350rpm, and nitrogen is passed through into reaction kettle
Gas is protected, and being passed through nitrogen flow rate is 60-100ml/min, and after being passed through nitrogen 10-15 minutes, 30 parts are added into reaction kettle
Filler material, after stirring 2-5 minute, then by mass fraction be 15 parts of anise extract, 5 parts of Herba Lysimachiae foenumgraeci extract, 5 parts
Bean dregs extract, 4 parts of Rosmarinus officinalis extract, 3 parts of orange bark extract sequentially add in reaction kettle, then carry out mixing anti-
After answering 2-3 hours, after obtained substance is cooled to room temperature, then it is added in ultrasonic machine and carries out ultrasound after 1-2 hours, it will
It is sealed preservation, which is exactly that plant extracts prepares green preservative.
Embodiment 3
One Plant Extracts prepare the preparation method of green preservative the following steps are included:
(1) preparation of anise extract
In market, the aniseed of purchase is dried, and is then added into pulverizer and is crushed, granular size is
50-100 mesh is carried out refluxing extraction and is reacted 4-6 hour, and wherein reflux solvent is alcohol solvent, and aniseed powder
Mass ratio is 7:3, is filtered after fully reacting, remove filter residue, by obtained solution be added Rotary Evaporators in into
Row revolving, removes alcohol solvent, obtained substance is exactly anise extract.
(2) preparation of bean dregs extract
The bean dregs of collection are crushed, for powder particle diameter size in 10-20 mesh, then weighing its mass fraction is 25 parts
Bean dregs powder and 50 parts ethyl acetate be added reaction kettle in, then under the conditions of 60-70 DEG C, carry out back flow reaction 5-10 it is small
Shi Hou is filtered, and filter residue is removed, and obtained solution is added in Rotary Evaporators and is rotated, and removes ethyl acetate
Solvent, obtained substance are exactly bean dregs extract.
(3) preparation of Herba Lysimachiae foenumgraeci extract
It after the lavender bar of collection is dried, is crushed, powder particle diameter size is in 20-30 mesh, then by it
Refluxing extraction is carried out to react 3-5 hours, wherein reflux solvent is alcohol solvent, and the mass ratio of lavender powder is 7:3,
It is filtered after fully reacting, removes filter residue, obtained solution is added in Rotary Evaporators and is rotated, remove ethyl alcohol
Solvent, obtained substance are exactly Herba Lysimachiae foenumgraeci extract.
(4) preparation of Rosmarinus officinalis extract
It after the rosemary of collection is dried, is crushed, then powder particle diameter size claims in 40-60 mesh
It takes in the powder from rosemary and 60 parts of acetone addition reaction kettle that its mass fraction is 15 parts, then under the conditions of 50-65 DEG C, into
It after row back flow reaction 4-8 hours, is filtered, removes filter residue, obtained solution is added in Rotary Evaporators and is revolved
It steams, removes acetone solvent, obtained substance is exactly Rosmarinus officinalis extract.
(5) prepared by orange bark extract
The orange peel of collection is crushed, in 100-200 mesh, then weigh its mass fraction is powder particle diameter size
20 parts of orange peel powder and 20 parts of distilled water are added in reaction kettle, and then under the conditions of 30-50 DEG C, it is small to carry out reaction 4-5
Shi Hou is carried out after standing 5-10 hours, is carried out being separated off sediment, and obtained substance is exactly that orange peel extracts
Object.
(6) preparation of filler material
20 parts of distilled water and 2 parts of glycerol are carried out mixture prepared.
(7) preparation of antistaling agent
Temperature of reaction kettle is maintained 40-60 DEG C, mechanical agitator revolving speed is 250-350rpm, and nitrogen is passed through into reaction kettle
Gas is protected, and being passed through nitrogen flow rate is 60-100ml/min, and after being passed through nitrogen 10-15 minutes, 30 parts are added into reaction kettle
Filler material, after stirring 2-5 minute, then by mass fraction be 10 parts of anise extract, 2 parts of Herba Lysimachiae foenumgraeci extract, 5 parts
Bean dregs extract, 4 parts of Rosmarinus officinalis extract, 3 parts of orange bark extract sequentially add in reaction kettle, then carry out mixing anti-
After answering 2-3 hours, after obtained substance is cooled to room temperature, then it is added in ultrasonic machine and carries out ultrasound after 1-2 hours, it will
It is sealed preservation, which is exactly that plant extracts prepares green preservative.
Embodiment 4
One Plant Extracts prepare the preparation method of green preservative the following steps are included:
(1) preparation of anise extract
In market, the aniseed of purchase is dried, and is then added into pulverizer and is crushed, granular size is
50-100 mesh is carried out refluxing extraction and is reacted 4-6 hour, and wherein reflux solvent is alcohol solvent, and aniseed powder
Mass ratio is 7:3, is filtered after fully reacting, remove filter residue, by obtained solution be added Rotary Evaporators in into
Row revolving, removes alcohol solvent, obtained substance is exactly anise extract.
(2) preparation of bean dregs extract
The bean dregs of collection are crushed, for powder particle diameter size in 10-20 mesh, then weighing its mass fraction is 25 parts
Bean dregs powder and 60 parts ethyl acetate be added reaction kettle in, then under the conditions of 60-70 DEG C, carry out back flow reaction 5-10 it is small
Shi Hou is filtered, and filter residue is removed, and obtained solution is added in Rotary Evaporators and is rotated, and removes ethyl acetate
Solvent, obtained substance are exactly bean dregs extract.
(3) preparation of Herba Lysimachiae foenumgraeci extract
It after the lavender bar of collection is dried, is crushed, powder particle diameter size is in 20-30 mesh, then by it
Refluxing extraction is carried out to react 3-5 hours, wherein reflux solvent is alcohol solvent, and the mass ratio of lavender powder is 7:3,
It is filtered after fully reacting, removes filter residue, obtained solution is added in Rotary Evaporators and is rotated, remove ethyl alcohol
Solvent, obtained substance are exactly Herba Lysimachiae foenumgraeci extract.
(4) preparation of Rosmarinus officinalis extract
It after the rosemary of collection is dried, is crushed, then powder particle diameter size claims in 40-60 mesh
It takes in the powder from rosemary and 50 parts of acetone addition reaction kettle that its mass fraction is 15 parts, then under the conditions of 50-65 DEG C, into
It after row back flow reaction 4-8 hours, is filtered, removes filter residue, obtained solution is added in Rotary Evaporators and is revolved
It steams, removes acetone solvent, obtained substance is exactly Rosmarinus officinalis extract.
(5) prepared by orange bark extract
The orange peel of collection is crushed, in 100-200 mesh, then weigh its mass fraction is powder particle diameter size
20 parts of orange peel powder and 15 parts of distilled water are added in reaction kettle, and then under the conditions of 30-50 DEG C, it is small to carry out reaction 4-5
Shi Hou is carried out after standing 5-10 hours, is carried out being separated off sediment, and obtained substance is exactly that orange peel extracts
Object.
(6) preparation of filler material
20 parts of distilled water and 2 parts of glycerol are carried out mixture prepared.
(7) preparation of antistaling agent
Temperature of reaction kettle is maintained 40-60 DEG C, mechanical agitator revolving speed is 250-350rpm, and nitrogen is passed through into reaction kettle
Gas is protected, and being passed through nitrogen flow rate is 60-100ml/min, and after being passed through nitrogen 10-15 minutes, 30 parts are added into reaction kettle
Filler material, after stirring 2-5 minute, then by mass fraction be 15 parts of anise extract, 5 parts of Herba Lysimachiae foenumgraeci extract, 3 parts
Bean dregs extract, 4 parts of Rosmarinus officinalis extract, 3 parts of orange bark extract sequentially add in reaction kettle, then carry out mixing anti-
After answering 2-3 hours, after obtained substance is cooled to room temperature, then it is added in ultrasonic machine and carries out ultrasound after 1-2 hours, it will
It is sealed preservation, which is exactly that plant extracts prepares green preservative.
Experimental analysis:
1. fresh keeping time is tested
Guarantor of the antistaling agent that the antistaling agent for preparing embodiment 1-4 of embodiment 1-4 and market are bought to fruit beverage
Fresh time test tests fruit beverage deteriorating time, as a result as shown in the table.
Above-mentioned test result is it is found that its fresh keeping time of antistaling agent prepared by the present invention is longer.
Finally, it is stated that preferred embodiment above is only used to illustrate the technical scheme of the present invention rather than limits, although logical
It crosses above preferred embodiment the present invention is described in detail, however, those skilled in the art should understand that, can be
Various changes are made to it in form and in details, without departing from defined by claims of the present invention.
Claims (8)
1. the preparation method that a Plant Extracts prepare green preservative, it is characterised in that a Plant Extracts system
The composition of standby green preservative are as follows: mass fraction is 10-15 parts of anise extract, 2-5 parts of Herba Lysimachiae foenumgraeci extract, 3-5 parts
Bean dregs extract, 2-4 parts of Rosmarinus officinalis extract, 1-3 parts of orange bark extract, 20-30 parts of filler material.
2. the preparation method that a Plant Extracts according to claim 1 prepare green preservative, which is characterized in that institute
The Plant Extracts stated prepare green preservative the preparation method comprises the following steps: temperature of reaction kettle is maintained 40-60 DEG C, machinery stirs
Mixing device revolving speed is 250-350rpm, is passed through nitrogen into reaction kettle and is protected, and being passed through nitrogen flow rate is 60-100ml/min, is led to
After entering nitrogen 10-15 minutes, 20-30 part of filler material is added into reaction kettle, after stirring 2-5 minutes, then by mass fraction is
10-15 parts of anise extract, 2-5 parts of Herba Lysimachiae foenumgraeci extract, 3-5 parts of bean dregs extract, 2-4 parts of rosemary extract
Object, 1-3 parts of orange bark extract sequentially adds in reaction kettle, after then carrying out hybrid reaction 2-3 hours, the substance that will obtain
After being cooled to room temperature, then it is added in ultrasonic machine and carries out ultrasound after 1-2 hours, be sealed preservation, the substance is just
It is that plant extracts prepares green preservative.
3. the preparation method that a Plant Extracts according to claim 1 prepare green preservative, which is characterized in that institute
The anise extract stated are as follows: in market, the aniseed of purchase is dried, and is then added into pulverizer and is crushed,
Grain size is 50-100 mesh, is carried out refluxing extraction and reacted 4-6 hours, wherein reflux solvent is alcohol solvent, and fennel
The mass ratio of sub- powder is 7:3, is filtered after fully reacting, and filter residue is removed, and rotation is added in obtained solution and is steamed
It is rotated in hair instrument, removes alcohol solvent, obtained substance is exactly anise extract.
4. the preparation method that a Plant Extracts according to claim 1 prepare green preservative, which is characterized in that institute
The Herba Lysimachiae foenumgraeci extract stated are as follows: after being dried the lavender bar of collection, crushed, powder particle diameter size is in 20-30
Then mesh is carried out refluxing extraction and is reacted 3-5 hours, wherein reflux solvent is alcohol solvent, and the matter of lavender powder
Amount ratio is 7:3, is filtered after fully reacting, and filter residue is removed, and obtained solution is added in Rotary Evaporators and is carried out
Revolving removes alcohol solvent, and obtained substance is exactly Herba Lysimachiae foenumgraeci extract.
5. the preparation method that a Plant Extracts according to claim 1 prepare green preservative, which is characterized in that institute
The bean dregs extract stated are as follows: crush the bean dregs of collection, then powder particle diameter size weighs its quality in 10-20 mesh
The bean dregs powder and 50-60 parts of ethyl acetate that number is 20-30 parts are added in reaction kettle, then under the conditions of 60-70 DEG C, into
It after row back flow reaction 5-10 hours, is filtered, removes filter residue, obtained solution is added in Rotary Evaporators and is revolved
It steams, removes ethyl acetate solvent, obtained substance is exactly bean dregs extract.
6. a Plant Extracts according to claim 1 prepare the preparation method of green preservative, which is characterized in that institute
The Rosmarinus officinalis extract stated are as follows: after being dried the rosemary of collection, crushed, powder particle diameter size is in 40-
Then 60 mesh weigh in the powder from rosemary and 50-60 parts of acetone addition reaction kettle that its mass fraction is 10-15 parts, then
It under the conditions of 50-65 DEG C, after carrying out back flow reaction 4-8 hours, is filtered, removes filter residue, obtained solution is added
It is rotated in Rotary Evaporators, removes acetone solvent, obtained substance is exactly Rosmarinus officinalis extract.
7. the preparation method that a Plant Extracts according to claim 1 prepare green preservative, which is characterized in that institute
The orange bark extract stated are as follows: crush the orange peel of collection, then powder particle diameter size is weighed in 100-200 mesh
The orange peel powder and 10-30 parts of distilled water that its mass fraction is 10-30 parts are added in reaction kettle, then in 30-50 DEG C of item
Under part, after carrying out reaction 4-5 hours, is carried out after standing 5-10 hours, carried out being separated off sediment, obtained object
Matter is exactly orange bark extract.
8. the preparation method that a Plant Extracts according to claim 1 prepare green preservative, which is characterized in that institute
The filler material stated are as follows: 10-20 parts of distilled water and 1-2 parts of glycerol are subjected to the objects such as mixture prepared or flour
One of matter.
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| CN201810863403.7A CN108936198A (en) | 2018-08-01 | 2018-08-01 | One Plant Extracts prepare the preparation method of green preservative |
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| CN110100991A (en) * | 2019-05-30 | 2019-08-09 | 周江尚 | A kind of preparation method of long-acting food preservative |
| CN110789850A (en) * | 2019-10-12 | 2020-02-14 | 宝应县永佳米业有限公司 | Germ rice fresh-keeping packaging storage method |
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Application publication date: 20181207 |