CN108931440A - A kind of small sample is uniaxially stretched creep test fixture - Google Patents

A kind of small sample is uniaxially stretched creep test fixture Download PDF

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CN108931440A
CN108931440A CN201710389031.4A CN201710389031A CN108931440A CN 108931440 A CN108931440 A CN 108931440A CN 201710389031 A CN201710389031 A CN 201710389031A CN 108931440 A CN108931440 A CN 108931440A
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fixture
hole
bar
extending
sample
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杨爽
郑鹏飞
魏然
王平怀
许增裕
谌继明
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Southwestern Institute of Physics
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N3/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N3/08Investigating strength properties of solid materials by application of mechanical stress by applying steady tensile or compressive forces
    • G01N3/18Performing tests at high or low temperatures
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N25/00Investigating or analyzing materials by the use of thermal means
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N3/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N3/02Details
    • G01N3/04Chucks
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/20Metals
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2203/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N2203/0014Type of force applied
    • G01N2203/0016Tensile or compressive
    • G01N2203/0017Tensile
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2203/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N2203/0058Kind of property studied
    • G01N2203/0069Fatigue, creep, strain-stress relations or elastic constants
    • G01N2203/0071Creep
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2203/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N2203/02Details not specific for a particular testing method
    • G01N2203/022Environment of the test
    • G01N2203/0222Temperature
    • G01N2203/0226High temperature; Heating means
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2203/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N2203/02Details not specific for a particular testing method
    • G01N2203/04Chucks, fixtures, jaws, holders or anvils
    • G01N2203/0482Chucks, fixtures, jaws, holders or anvils comprising sensing means

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  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Health & Medical Sciences (AREA)
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  • Investigating Strength Of Materials By Application Of Mechanical Stress (AREA)

Abstract

本发明属于拉伸及蠕变力学性能的测试技术领域,具体涉及一种小样品单轴拉伸蠕变测试用夹具。本发明的夹具,包括:上支架、上夹具、通用夹块、夹块销、下支架、下夹具、外引伸杆、下拉杆、内引伸杆、导架、测量脚、螺母、位移测量装置和引伸架。本发明主要解决了现有的小样品测试用夹具,在样品夹持时普遍存在样品拉伸阶段滑移的问题,本发明采用插销定位,并在接触面设置横纹,避免了样品在夹装过程中导致的倾斜歪曲和滑移,同时保证了样品在拉伸过程中不会影响测量的同轴度;将热电偶插入测试样品夹具,能够直接准确的测试样品真实试验温度;采用石英棒连接线性可变差动变压器(LVDT),可适用于最高1200℃环境下的样品高温力学性能测试。

The invention belongs to the technical field of testing tensile and creep mechanical properties, in particular to a fixture for uniaxial tensile creep testing of small samples. The fixture of the present invention comprises: an upper bracket, an upper clamp, a universal clamp block, a clamp pin, a lower bracket, a lower clamp, an outer extension rod, a lower rod, an inner extension rod, a guide frame, a measuring foot, a nut, a displacement measuring device and extension frame. The present invention mainly solves the problem that the existing small sample test fixture generally has the problem of slipping during the sample stretching stage when the sample is clamped. The tilt, distortion and slippage caused by the process ensure that the sample will not affect the coaxiality of the measurement during the stretching process; the thermocouple is inserted into the test sample fixture to directly and accurately test the real test temperature of the sample; the quartz rod is used to connect The linear variable differential transformer (LVDT) can be applied to the high-temperature mechanical performance test of samples in an environment up to 1200°C.

Description

一种小样品单轴拉伸蠕变测试用夹具A Fixture for Uniaxial Tensile Creep Test of Small Samples

技术领域technical field

本发明属于拉伸及蠕变力学性能的测试技术领域,具体涉及一种小样品单轴拉伸蠕变测试用夹具。The invention belongs to the technical field of testing tensile and creep mechanical properties, in particular to a fixture for uniaxial tensile creep testing of small samples.

背景技术Background technique

小样品测试技术是在满足相关测试要求的前提下,极大程度的节约测试材料,并适用尺寸要求严格的实验环境,例如辐照实验中有限的实验空间中,采用小样品进行实验,则能够极大的利用辐照空间,同时对珍惜、薄膜等量小样品也非常适用。同时世界各国也在积极的开展建立小样品的测试标准,各种类型的小样品测试设备也逐渐开始发展起来,但大多数小样品测试设备所用夹具在样品夹持时普遍存在样品拉伸阶段滑移、不能直接准确测量样品部位温度、传感器不能够同时满足拉伸行程及蠕变精度的问题,因此需要提供一种能够克服以上样品测试问题的夹具。The small sample testing technology is to save test materials to a great extent on the premise of meeting the relevant test requirements, and is suitable for the experimental environment with strict size requirements. For example, in the limited experimental space in the irradiation experiment, it can It makes great use of the irradiation space, and is also very suitable for small samples such as treasures and thin films. At the same time, countries around the world are also actively establishing small sample testing standards, and various types of small sample testing equipment have gradually begun to develop. Therefore, it is necessary to provide a fixture that can overcome the above sample testing problems.

发明内容Contents of the invention

本发明需要解决的技术问题为:现有的小样品测试用夹具,在样品夹持时普遍存在样品拉伸阶段滑移的问题。The technical problem to be solved in the present invention is: the existing small sample test fixture generally has the problem of slippage in the sample stretching stage when the sample is clamped.

本发明的技术方案如下所述:Technical scheme of the present invention is as follows:

一种小样品单轴拉伸蠕变测试用夹具,包括:上支架、上夹具、通用夹块、夹块销、下支架、下夹具、外引伸杆、下拉杆、内引伸杆、导架、测量脚、螺母、位移测量装置和引伸架;其中,所述上夹具为长方体形状,其下端设置有用于定位的夹块销;一个所述通用夹块通过螺钉固定设置于上夹具的下端,通用夹块上设置有夹块销孔,夹块销孔的设置位置与设置于上夹具下端的夹块销的空间位置相匹配,夹块销孔与夹块销配合定位通用夹块在上夹具下端的安装位置;通用夹块通过螺钉固定安装于上夹具的下端;在该通用夹块和上夹具下端的两个相接触的面上,还均设置有若干横纹,用于增加对试样的夹持力;A fixture for uniaxial tensile creep test of small samples, including: upper bracket, upper clamp, universal clamp block, clamp pin, lower bracket, lower clamp, outer extension rod, lower rod, inner extension rod, guide frame, Measuring feet, nuts, displacement measuring devices and extension frames; wherein, the upper fixture is in the shape of a cuboid, and its lower end is provided with clamp pins for positioning; one of the universal clamps is fixed on the lower end of the upper fixture by screws. The clamping block is provided with a clamping pin hole, and the setting position of the clamping pin hole matches the spatial position of the clamping pin arranged at the lower end of the upper fixture, and the clamping pin hole and the clamping pin cooperate to position the universal clamping block at the lower end of the upper fixture The installation position of the universal clamp block is fixed on the lower end of the upper fixture by screws; on the two contacting surfaces of the universal clamp block and the lower end of the upper fixture, there are also several horizontal lines, which are used to increase the stability of the sample. clamping force;

所述下夹具为长方体形状,其上端也设置有用于定位的夹块销;在下夹具的上端通过螺钉固定设置有另一个通用夹块,通用夹块上设置有夹块销孔,夹块销孔的设置位置与设置于下夹具上端的夹块销的空间位置相匹配,夹块销孔与夹块销配合定位通用夹块在上夹具下端的安装位置;在该通用夹块和下夹具上端的两个相接触的面上,还均设置有若干横纹,用于增加对试样的夹持力;The lower clamp is in the shape of a cuboid, and its upper end is also provided with a clamp pin for positioning; another universal clamp is fixed on the upper end of the lower clamp by screws, and the universal clamp is provided with a clamp pin hole and a clamp pin hole. The setting position of the clamping block matches the spatial position of the clamping block pin arranged at the upper end of the lower fixture, and the clamping block pin hole and the clamping block pin cooperate to locate the installation position of the universal clamping block at the lower end of the upper clamping fixture; the upper end of the universal clamping block and the lower clamping There are also several horizontal lines on the two contacting surfaces, which are used to increase the clamping force of the sample;

所述上支架和下支架均为条状形状,上夹具通过螺钉固定安装于所述上支架之上,下夹具通过螺钉固定安装于所述下支架之上;Both the upper bracket and the lower bracket are strip-shaped, the upper clamp is fixed on the upper bracket by screws, and the lower clamp is fixed on the lower bracket by screws;

所述外引伸杆和内引伸杆各有一对;两根外引伸杆的上端分别固定安装于上支架的两端,两根外引伸杆沿竖直方向设置,并且两根外引伸杆平行;两根内引伸杆的上端分别固定安装于下支架的两端,两根内引伸杆沿竖直方向设置,并且两根内引伸杆平行,两根内引伸杆位于两根外引伸杆之间;There is a pair of outer extension rods and inner extension rods; the upper ends of the two outer extension rods are fixedly installed on the two ends of the upper bracket respectively, and the two outer extension rods are arranged along the vertical direction, and the two outer extension rods are parallel; The upper ends of the inner extension rods are respectively fixedly installed on the two ends of the lower bracket, the two inner extension rods are arranged along the vertical direction, and the two inner extension rods are parallel, and the two inner extension rods are located between the two outer extension rods;

所述下拉杆为圆柱状杆,下夹具通过插销固定安装于下拉杆的顶端;在下拉杆的中下部位置处,还固定有导架;导架的中部设置有大通孔,下拉杆从大通孔中穿过;导架的两侧还各有两个小通孔,两根外引伸杆分别从位置相对靠外侧的两个小通孔中穿出,两根内引伸杆分别从位置相对靠内侧的两个小通孔中穿出;其中两根外引伸杆与导架位置相对固定,两根内引伸杆能够在其穿过的小通孔中沿轴向来回滑动;The pull-down rod is a cylindrical rod, and the lower fixture is fixedly installed on the top of the pull-down rod through a bolt; at the middle and lower part of the pull-down rod, a guide frame is also fixed; the middle part of the guide frame is provided with a large through-hole, and the pull-down rod passes through the large through-hole. There are two small through-holes on both sides of the guide frame, the two outer extension rods pass through the two small through-holes relatively to the outer side, and the two inner extension rods pass through the two relatively inner through-holes respectively. Two small through holes are pierced; the two outer extension rods are relatively fixed to the guide frame, and the two inner extension rods can slide back and forth axially in the small through holes through which they pass;

所述引伸架设置于下拉杆的下部位置处;引伸架为条状形状,在引伸架的中部也设置有大通孔,下拉杆从引伸架的大通孔中穿出,并且能够在引伸架的大通孔中沿自身轴向来回滑动;在引伸架上,位于大通孔两侧的位置处,还各设置有一个小通孔,两根内引伸杆的下端分别插入引伸架上的此两个小通孔中并固定;在引伸架的两端,也分别设置有通孔,位移测量装置固定安装在于引伸架两端的通孔中;The extension frame is arranged at the lower part of the extension frame; the extension frame is a strip shape, and a large through hole is also arranged in the middle of the extension frame, and the pull rod passes through the large through hole of the extension frame, and can be inserted into the large through hole of the extension frame. The hole slides back and forth along its own axial direction; on the extension frame, at the positions on both sides of the large through hole, there is also a small through hole, and the lower ends of the two inner extension rods are respectively inserted into the two small holes on the extension frame. and fixed in the hole; at both ends of the extension frame, there are also through holes respectively, and the displacement measuring device is fixedly installed in the through holes at both ends of the extension frame;

所述位移测量装置具有壳体和探针,壳体固定安装在于引伸架两端的通孔中;The displacement measuring device has a housing and a probe, and the housing is fixedly installed in the through holes at both ends of the extension frame;

所述测量脚有两个,测量脚为片状结构,分别设置于下拉杆两侧;两个测量脚的一端分别固定连接至两个外引伸杆下端,两个测量脚的另一端上均设置有通孔,位移测量装置的探针从测量脚的通孔向上穿出,并通过螺母锁紧连接;所述螺母为滚花薄螺母,具有大的外径,能够阻止探针向下的位移。There are two measuring feet, the measuring feet are sheet-like structures, which are respectively arranged on both sides of the pull-down rod; one end of the two measuring feet is respectively fixedly connected to the lower ends of the two external extension rods, and the other ends of the two measuring feet are all set There is a through hole, the probe of the displacement measuring device passes through the through hole of the measuring foot upwards, and is connected by nut locking; the nut is a knurled thin nut with a large outer diameter, which can prevent the downward displacement of the probe .

优选的,本发明的家具还包括热电偶探头,在上夹具的侧边还设置有孔,孔内安装有热电偶探头,在夹持有试样时,热电偶探头直接与试样相接触,能够在保证夹具强度的同时,最大可能测量试样的真实温度。Preferably, the furniture of the present invention also includes a thermocouple probe, and a hole is arranged on the side of the upper clamp, and a thermocouple probe is installed in the hole. When the sample is clamped, the thermocouple probe directly contacts the sample. It can measure the true temperature of the sample to the greatest extent possible while ensuring the strength of the fixture.

优选的,设置于上夹具下端的所述夹块销有三个,在空间中呈倒三角形排布,且所呈倒三角形的高线位于竖直方向上。Preferably, there are three clamping pins arranged at the lower end of the upper fixture, arranged in an inverted triangle in space, and the height line of the inverted triangle is located in the vertical direction.

优选的,在上夹具上,还设置有穿销,用于将整个夹具系统与测试设备拉伸系统相连,进行拉伸蠕变测试。Preferably, pins are also provided on the upper clamp for connecting the entire clamp system with the tensile system of the test equipment for tensile creep testing.

优选的,设置于下夹具上端的夹块销有三个,在空间中呈三角形排布,且所呈三角形的高线位于竖直方向上。Preferably, there are three clamping pins arranged at the upper end of the lower fixture, arranged in a triangle in space, and the height line of the triangle is located in the vertical direction.

优选的,所述外引伸杆和内引伸杆均由石英材质制成,以保证高温下的刚性。Preferably, both the outer extension rod and the inner extension rod are made of quartz material to ensure rigidity at high temperature.

优选的,所述两根外引伸杆的上端分别通过两个耐热螺钉固定安装于上支架的两端。Preferably, the upper ends of the two outer extension rods are respectively fixed and installed on the two ends of the upper bracket by two heat-resistant screws.

优选的,所述两根内引伸杆的上端分别通过两个耐热螺钉固定安装于下支架的两端。Preferably, the upper ends of the two inner extension rods are respectively fixed and installed on the two ends of the lower bracket by two heat-resistant screws.

优选的,本发明的夹具还包括开口套,两个开口套分别安装于引伸架两端的这两个通孔中;每个开口套内均夹持有位移测量装置;在引伸架每端的侧面,均安装有调节螺栓,旋转调节螺栓能够调整开口套对位移测量装置的夹持力。Preferably, the fixture of the present invention also includes split sleeves, and the two split sleeves are respectively installed in the two through holes at both ends of the extension frame; each split sleeve is clamped with a displacement measuring device; on the side of each end of the extension frame, Both are equipped with adjusting bolts, and rotating the adjusting bolts can adjust the clamping force of the split sleeve on the displacement measuring device.

优选的,所述位移测量装置为线性可变差动变压器。Preferably, the displacement measuring device is a linear variable differential transformer.

本发明的有益效果为:The beneficial effects of the present invention are:

(1)本发明采用插销定位,使用上下四个螺栓锁紧样品,并在接触面设置横纹,避免了样品在夹装过程中导致的倾斜歪曲和滑移,同时保证了样品在拉伸过程中不会影响样品测量的同轴度;(1) The present invention adopts pin positioning, uses four upper and lower bolts to lock the sample, and sets horizontal lines on the contact surface, which avoids the inclination, distortion and slippage of the sample during the clamping process, and at the same time ensures that the sample is stretched during the stretching process. It will not affect the coaxiality of the sample measurement;

(2)将热电偶插入测试样品夹具,能够直接准确的测试样品真实试验温度;(2) Insert the thermocouple into the test sample fixture to directly and accurately test the real test temperature of the sample;

(3)采用石英棒连接线性可变差动变压器(LVDT),可适用于最高1200℃环境下的样品高温力学性能测试。(3) The linear variable differential transformer (LVDT) is connected by quartz rods, which can be applied to the high-temperature mechanical performance test of samples under the environment of up to 1200°C.

附图说明Description of drawings

图1为本发明的夹具整体组成示意图;Fig. 1 is a schematic diagram of the overall composition of the fixture of the present invention;

图2为本发明的夹具上部放大示意图;Fig. 2 is an enlarged schematic view of the upper part of the fixture of the present invention;

图3为本发明夹具的侧视图;Fig. 3 is the side view of fixture of the present invention;

其中,1-上支架,2-穿销,3-上夹具,4-耐热螺钉,5-试样,6-通用夹块,7-夹块销,8-下支架,9-下夹具,10-插销,11-外引伸杆,12-下拉杆,13-内引伸杆,14-导架,15-测量脚,16-螺母,17-位移测量装置,18-开口套,19-引伸架,20-调节螺栓,21-热电偶探头。Among them, 1-upper bracket, 2-piercing pin, 3-upper clamp, 4-heat-resistant screw, 5-sample, 6-general clamp block, 7-clamp pin, 8-lower bracket, 9-lower clamp, 10-pin, 11-outer extension rod, 12-down rod, 13-inner extension rod, 14-guide frame, 15-measuring foot, 16-nut, 17-displacement measuring device, 18-split sleeve, 19-extension frame , 20-adjusting bolt, 21-thermocouple probe.

具体实施方式Detailed ways

下面结合附图和实施例对本发明的小样品单轴拉伸蠕变测试用夹具进行详细说明。The jig for uniaxial tensile creep test of small samples of the present invention will be described in detail below with reference to the accompanying drawings and examples.

如图1和2所示,本发明的夹具包括上夹具3和下夹具9。上夹具3为长方体形状,其下端设置有用于定位的夹块销7,设置在上夹具3下端的夹块销7有三个,在空间中呈倒三角形排布,且所呈倒三角形的高线位于竖直方向上。在上夹具3的下端还设置有通用夹块6,该通用夹块6上设置有夹块销孔,夹块销孔的设置位置与设置于上夹具3下端的夹块销7的空间位置相匹配,夹块销孔与夹块销7配合定位通用夹块6在上夹具3下端的安装位置。该通用夹块6通过螺钉固定安装于上夹具3的下端。在该通用夹块6和上夹具3下端的两个相接触的面上,还均设置有若干横纹,用于增加对试样5的夹持力。As shown in FIGS. 1 and 2 , the jig of the present invention includes an upper jig 3 and a lower jig 9 . The upper fixture 3 is in the shape of a cuboid, and its lower end is provided with a clamp pin 7 for positioning. There are three clamp pins 7 arranged at the lower end of the upper fixture 3, which are arranged in an inverted triangle in space, and the height line of the inverted triangle in the vertical direction. The lower end of the upper clamp 3 is also provided with a universal clamp 6, the universal clamp 6 is provided with a clamp pin hole, and the location of the clamp pin hole is the same as the spatial position of the clamp pin 7 arranged at the lower end of the upper clamp 3. Matching, the clip pin hole cooperates with the clip pin 7 to locate the installation position of the universal clip 6 at the lower end of the upper fixture 3 . The universal clamping block 6 is fixedly mounted on the lower end of the upper clamp 3 by screws. On the two contacting surfaces of the universal clamp block 6 and the lower end of the upper clamp 3 , there are also several horizontal lines, which are used to increase the clamping force on the sample 5 .

在上夹具3上,还设置有穿销2,用于将整个夹具系统与测试设备拉伸系统相连,进行拉伸蠕变测试。On the upper clamp 3, there is also a pin 2, which is used to connect the entire clamp system with the tensile system of the test equipment for tensile creep testing.

下夹具9为长方体形状,其上端设置有用于定位的夹块销7,设置在下夹具9上端的夹块销7有三个,在空间中呈三角形排布,且所呈三角形的高线位于竖直方向上。在下夹具9的上端设置有另一个通用夹块6,该通用夹块6上设置有夹块销孔,夹块销孔的设置位置与设置于下夹具9上端的夹块销7的空间位置相匹配,夹块销孔与夹块销7配合定位通用夹块6在上夹具3下端的安装位置。该通用夹块6通过螺钉固定安装于上夹具3的下端。在该通用夹块6和下夹具9上端的两个相接触的面上,还均设置有若干横纹,用于增加对试样5的夹持力。The lower clamp 9 is in the shape of a cuboid, and its upper end is provided with a clamp pin 7 for positioning. There are three clamp pins 7 arranged at the upper end of the lower clamp 9, which are arranged in a triangle in space, and the triangular high line is located in the vertical position. direction. The upper end of lower fixture 9 is provided with another universal clamping block 6, and this universal clamping block 6 is provided with clamping block pin hole, and the setting position of clamping block pin hole is arranged on the space position of clamping block pin 7 that is arranged on lower clamp 9 upper ends. Matching, the clip pin hole cooperates with the clip pin 7 to locate the installation position of the universal clip 6 at the lower end of the upper fixture 3 . The universal clamping block 6 is fixedly mounted on the lower end of the upper clamp 3 by screws. On the two contacting surfaces of the upper end of the universal clamp block 6 and the lower clamp 9 , there are also several horizontal lines for increasing the clamping force on the sample 5 .

本发明的夹具还包括上支架1和下支架8,上支架1和下支架8均为条状形状,上夹具3通过螺钉固定安装于上支架1之上,下夹具9通过螺钉固定安装于下支架8之上。The fixture of the present invention also includes an upper bracket 1 and a lower bracket 8, the upper bracket 1 and the lower bracket 8 are strip-shaped, the upper clamp 3 is fixed on the upper bracket 1 by screws, and the lower clamp 9 is fixed on the lower bracket by screws. on the bracket 8.

本发明的夹具还包括外引伸杆11和内引伸杆13。外引伸杆11和内引伸杆13各有一对,且由石英材质制成,以保证高温下的刚性。两根外引伸杆11的上端分别通过两个耐热螺钉4固定安装于上支架1的两端,两根外引伸杆11沿竖直方向设置,并且两根外引伸杆11平行。两根内引伸杆13的上端也分别通过两个耐热螺钉4固定安装于下支架8的两端,两根内引伸杆13沿竖直方向设置,并且两根内引伸杆13平行,两根内引伸杆13位于两根外引伸杆11之间。The clamp of the present invention also includes an outer extension rod 11 and an inner extension rod 13 . Each of the outer extension rods 11 and the inner extension rods 13 has a pair, and is made of quartz material to ensure rigidity under high temperature. The upper ends of the two outer extension rods 11 are fixedly installed on the two ends of the upper bracket 1 by two heat-resistant screws 4 respectively, and the two outer extension rods 11 are arranged vertically, and the two outer extension rods 11 are parallel. The upper ends of the two inner extension rods 13 are also fixedly installed on the two ends of the lower bracket 8 by two heat-resistant screws 4 respectively. The two inner extension rods 13 are arranged in the vertical direction, and the two inner extension rods 13 are parallel. The inner extension rod 13 is located between the two outer extension rods 11 .

本发明的夹具还包括下拉杆12,下拉杆12为圆柱状杆。下夹具9通过插销10固定安装于下拉杆12的顶端。在下拉杆12的中下部位置处,还固定有导架14。导架14的中部设置有大通孔,下拉杆12从大通孔中穿过。导架14的两侧还各有两个小通孔,两根外引伸杆11分别从位置相对靠外侧的两个小通孔中穿出,两根内引伸杆13分别从位置相对靠内侧的两个小通孔中穿出。其中两根外引伸杆11与导架14位置相对固定,两根内引伸杆13能够在其穿过的小通孔中沿轴向来回滑动。The clamp of the present invention also includes a pull-down rod 12, which is a cylindrical rod. The lower clamp 9 is fixedly installed on the top of the pull-down rod 12 through the latch 10 . A guide frame 14 is also fixed at the middle and lower part of the pull down rod 12 . The middle part of the guide frame 14 is provided with a large through hole, and the lower rod 12 passes through the large through hole. There are also two small through-holes on both sides of the guide frame 14, two outer extension rods 11 pass through the two small through-holes at positions relatively on the outside respectively, and two inner extension rods 13 pass from the positions relatively on the inside respectively. through two small through-holes. The positions of the two outer extension rods 11 and the guide frame 14 are relatively fixed, and the two inner extension rods 13 can slide back and forth axially in the small through holes through which they pass.

在下拉杆12的下部位置处,设置有引伸架19。引伸架19为条状形状,在引伸架19的中部也设置有大通孔,下拉杆12从引伸架19的大通孔中穿出,并且能够在引伸架19的大通孔中沿自身轴向来回滑动。在引伸架19上,位于大通孔两侧的位置处,还各设置有一个小通孔,两根内引伸杆13的下端分别插入引伸架19上的此两个小通孔中并固定。在引伸架19的两端,也分别设置有通孔,两个开口套18分别安装于引伸架19两端的这两个通孔中。每个开口套18内还均夹持有位移测量装置17,所述位移测量装置为线性可变差动变压器。在引伸架19每端的侧面,均安装有调节螺栓20,旋转调节螺栓20能够调整开口套18对移测量装置17的夹持力。At the lower position of the pull down rod 12, an extension frame 19 is provided. The extension frame 19 is strip-shaped, and a large through hole is also arranged in the middle of the extension frame 19. The pull-down rod 12 passes through the large through hole of the extension frame 19, and can slide back and forth in the large through hole of the extension frame 19 along its own axis. . On the extension frame 19, a small through hole is respectively arranged at the positions on both sides of the large through hole, and the lower ends of the two inner extension rods 13 are respectively inserted into the two small through holes on the extension frame 19 and fixed. The two ends of the extension frame 19 are respectively provided with through holes, and the two open sleeves 18 are respectively installed in the two through holes at the two ends of the extension frame 19 . Each split sleeve 18 also clamps a displacement measuring device 17, and the displacement measuring device is a linear variable differential transformer. On the side of each end of the extension frame 19 , an adjusting bolt 20 is installed, and the rotating adjusting bolt 20 can adjust the clamping force of the open sleeve 18 on the movement measuring device 17 .

位移测量装置17具有壳体和探针,壳体夹持于开口套18之内。The displacement measuring device 17 has a housing and a probe, and the housing is clamped in the open sleeve 18 .

本发明的夹具还包括两个测量脚15,测量脚15为片状结构,分别设置于下拉杆12两侧。两个测量脚15的一端分别固定连接至两个外引伸杆11下端,两个测量脚15的另一端上均设置有通孔,位移测量装置17的探针从测量脚15的通孔向上穿出,并通过螺母16锁紧连接。所述螺母16为滚花薄螺母,具有大的外径,能够阻止探针向下的位移。The fixture of the present invention also includes two measuring feet 15 , the measuring feet 15 are sheet-like structures and are respectively arranged on both sides of the pull-down rod 12 . One end of the two measuring feet 15 is respectively fixedly connected to the lower ends of the two outer extension rods 11, the other ends of the two measuring feet 15 are provided with through holes, and the probe of the displacement measuring device 17 passes through the through holes of the measuring feet 15 upwards. Out, and through the nut 16 locking connection. The nut 16 is a knurled thin nut with a large outer diameter, which can prevent the downward displacement of the probe.

如图3所示,在上夹具3的侧边还设置有孔,孔内安装有热电偶探头21,在夹持有试样5时,热电偶探头21直接与试样5相接触,能够在保证夹具强度的同时,最大可能测量试样5的真实温度。As shown in Figure 3, a hole is also provided on the side of the upper clamp 3, and a thermocouple probe 21 is installed in the hole. When the sample 5 is clamped, the thermocouple probe 21 is directly in contact with the sample 5, which can be While ensuring the strength of the fixture, measure the real temperature of sample 5 to the greatest possible extent.

本发明的小样品单轴拉伸蠕变测试用夹具,在使用时将所需要测试的材料按照小样品尺寸要求加工制取后,装入适用于小样品力学性能测试相关设备,即可进行拉伸蠕变等力学性能测试。The jig for uniaxial tensile creep test of small samples of the present invention, when in use, the materials to be tested are processed and prepared according to the size requirements of small samples, and then loaded into relevant equipment suitable for testing the mechanical properties of small samples, then the tensile test can be carried out. Mechanical performance tests such as elongation and creep.

以聚变堆结构材料钒合金为室温拉伸实验为例,本发明的夹具使用过程如下:Taking the vanadium alloy, the structural material of the fusion reactor, as the room temperature tensile test as an example, the use process of the fixture of the present invention is as follows:

1)按照小样品标准加工好钒合金小样品,并在小样品的两端穿孔。将小样品穿在上夹具3和下夹具9上位置位于中部的夹块销7上。通过预加载一定小力值,调整连杆的同轴度,让样品与夹具连杆成一条直线,分别通过上夹具3和下夹具9上另外两个夹块销7在上夹具3和下夹具9定位安装上通用夹块6,使得通用夹块6贴紧样品表面,并通过螺钉固定,使得夹块表面横纹咬紧样品表面;1) Process a small vanadium alloy sample according to the small sample standard, and perforate both ends of the small sample. Put the small sample on the upper clamp 3 and the lower clamp 9 on the clamp block pin 7 located in the middle. By preloading a certain small force value, adjust the coaxiality of the connecting rod, so that the sample and the connecting rod of the fixture are in a straight line, and pass the other two clamp pins 7 on the upper fixture 3 and the lower fixture 9 respectively. 9 Position and install the universal clamp 6, so that the universal clamp 6 is close to the surface of the sample, and fixed by screws, so that the horizontal lines on the surface of the clamp bite the surface of the sample;

2)调节拉伸测试设备加载力,预夹紧样品,使整个夹具系统间隙消除,之后卸载力值为零,同时将变形和位移数据归零;2) Adjust the loading force of the tensile testing equipment, pre-clamp the sample, eliminate the gap of the entire fixture system, and then unload the force value to zero, and return the deformation and displacement data to zero at the same time;

3)软件端设定样品及拉伸数据参数,开始拉伸试验直至样品断裂,试验结束后,利用力值与变形数据可绘制材料应力应变曲线,可以分析得到材料的抗拉强度、屈服强度及延伸率等数据参数。3) Set the sample and tensile data parameters on the software side, and start the tensile test until the sample breaks. After the test, the stress-strain curve of the material can be drawn using the force value and deformation data, and the tensile strength, yield strength and elongation and other data parameters.

以聚变堆结构材料钒合金的高温拉伸实验为例,本发明的夹具使用过程如下:Taking the high-temperature tensile experiment of vanadium alloy, the structural material of the fusion reactor, as an example, the use process of the fixture of the present invention is as follows:

1)小样品加工安装夹持如上例步骤1和2所述;1) Small sample processing, installation and clamping are as described in steps 1 and 2 of the above example;

2)将热电偶插入夹具设计位置,同时在小样品外部加入锆箔包围一周,用于高温条件下吸收氧气,在测试样品及夹具周围设置加热装置,将夹持好样品的夹具整体放入抽真空装置内;2) Insert the thermocouple into the design position of the fixture, and at the same time add zirconium foil to the outside of the small sample to surround it for a week to absorb oxygen under high temperature conditions. in a vacuum device;

3)开启机械泵进行初步抽真空,同时开启冷却装置,待真空腔室压力低于20Pa时,开启分子泵,待整个腔室真空度达到1×10-4Pa级时,开启加热,加热前通过程序设定5-10牛顿预紧力加载并进行保持,防止加热过程中夹具膨胀时样品压缩变形;3) Turn on the mechanical pump for preliminary vacuuming, and at the same time turn on the cooling device. When the pressure in the vacuum chamber is lower than 20Pa, turn on the molecular pump. When the vacuum degree of the entire chamber reaches 1×10 -4 Pa level, turn on the heating. Set the 5-10 Newton pre-tightening force to load and maintain it through the program to prevent the sample from compressing and deforming when the fixture expands during the heating process;

4)加热过程通过调节加热丝功率的方式控制加热,保证整个加热过程中真空度优于1×10-3Pa;4) The heating process is controlled by adjusting the power of the heating wire to ensure that the vacuum degree is better than 1×10 -3 Pa during the entire heating process;

5)待温度达到750℃,保温15分钟,之后设定拉伸速率为0.2mm/min,开始拉伸实验直到试样断裂,软件系统将实时记录整个实验过程中的温度、真空度及应力应变等实验参数;5) When the temperature reaches 750°C, keep it warm for 15 minutes, then set the tensile rate to 0.2mm/min, start the tensile test until the sample breaks, and the software system will record the temperature, vacuum degree and stress and strain during the whole experiment in real time and other experimental parameters;

6)实验结束后数据将自动保存以供分析,关闭加热系统,待温度降至300℃以下关闭挡板阀隔断分子泵一侧,同时关闭分子泵,待分子泵完全停下来之后,同时温度降至100℃以下再关闭机械泵。待真空腔室温度降至80℃以下时,可松开螺栓,开启密封法兰,取出测试样品,实验完成。6) After the experiment is over, the data will be automatically saved for analysis. Turn off the heating system. When the temperature drops below 300°C, close the baffle valve to isolate the side of the molecular pump. At the same time, turn off the molecular pump. After the molecular pump stops completely, the temperature drops simultaneously. Turn off the mechanical pump when the temperature is below 100°C. When the temperature of the vacuum chamber drops below 80°C, the bolts can be loosened, the sealing flange can be opened, and the test sample can be taken out to complete the experiment.

以聚变堆结构材料钒合金的高温蠕变实验为例,本发明的夹具使用过程如下:Taking the high-temperature creep experiment of vanadium alloy, the structural material of fusion reactor, as an example, the use process of the fixture of the present invention is as follows:

1)样品安装、抽真空及加热步骤如上例步骤1-4所述;1) The steps of sample installation, vacuuming and heating are as described in steps 1-4 of the above example;

2)待温度达到750℃,保温6小时以完全释放夹具及样品高温膨胀变形,该过程中保持预紧力至变形数据曲线趋于完全平稳后,调整加载应力至蠕变试验目标值并保持,开始蠕变实验。2) When the temperature reaches 750°C, keep it warm for 6 hours to completely release the clamp and the high-temperature expansion deformation of the sample. During the process, maintain the pre-tightening force until the deformation data curve tends to be completely stable, adjust the loading stress to the target value of the creep test and maintain it. Start the creep experiment.

3)试验结束后,利用变形数据及试验时间数据进行蠕变试验曲线绘制,可以分析得到材料的最低蠕变速率等数据参数。3) After the test, use the deformation data and test time data to draw the creep test curve, and then analyze and obtain data parameters such as the minimum creep rate of the material.

Claims (10)

1. a kind of small sample is uniaxially stretched creep test fixture, including:Upper bracket (1), upper fixture (3), general fixture block (6), Fixture block pin (7), lower bracket (8), lower fixture (9), bar (11) of extending outside, lower pull rod (12), interior bar of extending (13), saddle (14), Measure foot (15), nut (16), displacement measuring device (17) and frame of extending (19);It is characterized in that:
The upper fixture (3) is rectangular shape, and lower end is provided with fixture block pin (7) used for positioning;One universal clamp Block (6) is fixedly installed on the lower end of upper fixture (3) by screw, is provided with fixture block pin hole on general fixture block (6), fixture block pin hole Position and the spatial position for the fixture block pin (7) for being set to upper fixture (3) lower end is arranged to match, fixture block pin hole and fixture block pin (7) Cooperation positions general fixture block (6) in the installation site of upper fixture (3) lower end;General fixture block (6) is fixedly installed in by screw The lower end of fixture (3);On two faces being in contact of the general fixture block (6) and upper fixture (3) lower end, also it is provided with several Band, for increasing the chucking power to sample (5);
The lower fixture (9) is rectangular shape, and the upper end is also equipped with fixture block pin (7) used for positioning;In lower fixture (9) Upper end is fixedly installed another general fixture block (6) by screw, is provided with fixture block pin hole, fixture block pin hole on general fixture block (6) Setting position and the spatial position of the fixture block pin (7) for being set to lower fixture (9) upper end match, fixture block pin hole and fixture block pin (7) cooperation positions general fixture block (6) in the installation site of upper fixture (3) lower end;On the general fixture block (6) and lower fixture (9) On two faces being in contact at end, several bands are also provided with, for increasing the chucking power to sample (5);
The upper bracket (1) and lower bracket (8) are streaky shape, and upper fixture (3) is fixedly installed in the upper branch by screw On frame (1), lower fixture (9) is fixedly installed on the lower bracket (8) by screw;
It is described outer to extend bar (11) and interior bar of extending (13) respectively has a pair;The upper end of two bars (11) of extending outside is fixedly mounted respectively It is arranged along the vertical direction in bar (11) of extending outside the both ends of upper bracket (1), two, and bar (11) of extending outside two is parallel;Two Extend in the root upper end of bar (13) is fixedly installed in the both ends of lower bracket (8) respectively, extends bar (13) along the vertical direction in two Setting, and extends bar (13) in parallel in two, extend in two bar (13) extended between bar (11) outside two;
The lower pull rod (12) is cylindric bar, and lower fixture (9) is fixedly installed in the top of lower pull rod (12) by bolt (10); At the middle and lower part position of lower pull rod (12), it is further fixed on saddle (14);Large through-hole, lower pull rod are provided in the middle part of saddle (14) (12) it is passed through from large through-hole;The two sides of saddle (14) are also each there are two small through hole, and two are extended bar (11) respectively from position outside It is pierced by two small through hole relatively in the outer part, two small through hole of the bar (13) respectively from position relatively in the inner part of extending in two In be pierced by;Wherein extend outside two bar (11) and saddle (14) position it is relatively fixed, bar (13) of extending in two can be worn at it It slidably reciprocates in the small through hole crossed along axial direction;
The frame of extending (19) is set to the lower position of lower pull rod (12);Frame (19) are extended for streaky shape, in frame of extending (19) large through-hole is also equipped in the middle part of, lower pull rod (12) is pierced by from the large through-hole of frame of extending (19), and can extend It axially slidably reciprocates in the large through-hole of frame (19) along itself;It is also each at the position of large through-hole two sides on frame of extending (19) It is provided with a small through hole, the lower end for bar (13) of extending in two is inserted into this two small through hole on frame of extending (19) simultaneously respectively It is fixed;At the both ends of frame of extending (19), it is also respectively arranged with through-hole, displacement measuring device (17) fixed installation is frame of extending (19) in the through-hole at both ends;
Institute's displacement measurement device (17) has shell and probe, and the through-hole at frame (19) both ends that are to extend is fixedly mounted in shell In;
There are two the measurement feet (15), and measurement foot (15) is laminated structure, is respectively arranged at lower pull rod (12) two sides;Two surveys One end of foot-measuring (15) is respectively fixedly connected with to two bar (11) lower ends of extending outside, is all provided on the other end of two measurements foot (15) It is equipped with through-hole, the probe of displacement measuring device (17) is pierced by upwards from the through-hole of measurement foot (15), and is locked by nut (16) Connection;The nut (16) is annular knurl thin nut, has big outer diameter, the displacement that probe can be prevented downward.
2. small sample as described in claim 1 is uniaxially stretched creep test fixture, it is characterised in that:Furniture of the invention is also Including thermocouple probe (21), it is additionally provided with hole in the side of upper fixture (3), thermocouple probe (21) are installed in hole, are being pressed from both sides When holding sample (5), thermocouple probe (21) is directly in contact with sample (5), can be maximum while guaranteeing fixture intensity The true temperature of sample (5) can be capable of measuring.
3. small sample as claimed in claim 2 is uniaxially stretched creep test fixture, it is characterised in that:It is set to upper fixture (3) it there are three the fixture block pins (7) of lower end, arranges in space in up-side down triangle, and the high line of be in up-side down triangle is located at On vertical direction.
4. small sample as claimed in claim 3 is uniaxially stretched creep test fixture, it is characterised in that:On upper fixture (3), It is additionally provided with and wears pin (2), for entire chucking appliance system to be connected with test equipment tensioning system, carry out tensile creep test.
5. small sample as claimed in claim 4 is uniaxially stretched creep test fixture, it is characterised in that:It is set to lower fixture (9) there are three the fixture block pins (7) of upper end, arrangement triangular in shape in space, and high line triangular in shape is located at vertical direction On.
6. small sample as claimed in claim 5 is uniaxially stretched creep test fixture, it is characterised in that:The outer bar of extending (11) it is made with interior bar of extending (13) of quartz material, to guarantee the rigidity under high temperature.
7. small sample as claimed in claim 6 is uniaxially stretched creep test fixture, it is characterised in that:It extends outside described two The upper end of bar (11) passes through the both ends that two resistance to thermal screws (4) are fixedly installed in upper bracket (1) respectively.
8. small sample as claimed in claim 7 is uniaxially stretched creep test fixture, it is characterised in that:It extends in described two The upper end of bar (13) passes through the both ends that two resistance to thermal screws (4) are fixedly installed in lower bracket (8) respectively.
9. small sample as claimed in claim 8 is uniaxially stretched creep test fixture, it is characterised in that:Fixture of the invention is also Including opening sleeve (18), two opening sleeves (18) are respectively arranged in the two through-holes at frame of extending (19) both ends;Each opening Displacement measuring device (17) are clamped in set (18);In the side at frame of extending (19) every end, it is mounted on and adjusts bolt (20), Rotation, which adjusts bolt (20), can adjust opening sleeve (18) to the chucking power of displacement measuring device (17).
10. small sample as claimed in claim 9 is uniaxially stretched creep test fixture, it is characterised in that:Institute's displacement measurement Device (17) is linear variable difference transformer.
CN201710389031.4A 2017-05-27 2017-05-27 A kind of small sample is uniaxially stretched creep test fixture Pending CN108931440A (en)

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CN112649278A (en) * 2020-11-27 2021-04-13 宁夏大学 Method for testing metal creep property
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