CN108914165A - A kind of novel powder electrolysis unit - Google Patents
A kind of novel powder electrolysis unit Download PDFInfo
- Publication number
- CN108914165A CN108914165A CN201810983452.4A CN201810983452A CN108914165A CN 108914165 A CN108914165 A CN 108914165A CN 201810983452 A CN201810983452 A CN 201810983452A CN 108914165 A CN108914165 A CN 108914165A
- Authority
- CN
- China
- Prior art keywords
- anode
- connecting base
- electrolysis unit
- novel powder
- hole
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000000843 powder Substances 0.000 title claims abstract description 36
- 238000005868 electrolysis reaction Methods 0.000 title claims abstract description 33
- 210000005056 cell body Anatomy 0.000 claims abstract description 20
- 239000007788 liquid Substances 0.000 claims abstract description 5
- 210000000481 breast Anatomy 0.000 claims abstract description 4
- 238000007789 sealing Methods 0.000 claims description 4
- 230000001681 protective effect Effects 0.000 claims 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 abstract description 8
- 238000012423 maintenance Methods 0.000 abstract description 4
- 238000009825 accumulation Methods 0.000 abstract description 3
- 238000005137 deposition process Methods 0.000 abstract description 3
- 238000009434 installation Methods 0.000 description 4
- 238000004070 electrodeposition Methods 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- 210000004027 cell Anatomy 0.000 description 2
- 238000010276 construction Methods 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 230000005611 electricity Effects 0.000 description 2
- LULLIKNODDLMDQ-UHFFFAOYSA-N arsenic(3+) Chemical compound [As+3] LULLIKNODDLMDQ-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000003792 electrolyte Substances 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000013011 mating Effects 0.000 description 1
- 238000003466 welding Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25C—PROCESSES FOR THE ELECTROLYTIC PRODUCTION, RECOVERY OR REFINING OF METALS; APPARATUS THEREFOR
- C25C5/00—Electrolytic production, recovery or refining of metal powders or porous metal masses
- C25C5/02—Electrolytic production, recovery or refining of metal powders or porous metal masses from solutions
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25C—PROCESSES FOR THE ELECTROLYTIC PRODUCTION, RECOVERY OR REFINING OF METALS; APPARATUS THEREFOR
- C25C7/00—Constructional parts, or assemblies thereof, of cells; Servicing or operating of cells
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Electrolytic Production Of Metals (AREA)
Abstract
The invention discloses a kind of novel powder electrolysis units, it includes cell body and locating rod, and cell body top is equipped with upper connecting base, and lower part is equipped with connection and is shorted, and bosom is equipped with anode；Connection is shorted side and offers first through hole, and lower part is equipped with lower connecting base；Anode upper end is fixedly connected with locating rod lower end, and lower end is equipped with power part；Anode lower end passes through first through hole and is fixedly connected by anode positioning sleeve with short circuit is connect；Upper connecting base top is equipped with upper end cover；Liquid outlet and inlet are respectively equipped on upper connecting base and lower connecting base.Power receiving section position not windrow, reduces period and the workload of sorting, period cost, workload and maintenance cost after reduction in the electrolysis unit electrolytic deposition process；Solve the problems, such as that powder causes its to burn leakage in lower connecting base accumulation, at the same when also very good solution powder train backlash is washed black copper powder scour rate, reduce the cost and workload of subsequent powder electrolysis system maintenance.
Description
The invention belongs to electrolysis unit technical fields, and in particular to a kind of novel powder electrolysis unit.
Background technique
It is copper powder containing arsenic black that electrodeposition, which comes out, in powder swirl-flow electrorefining, in electrolytic deposition process, slowly from being electrolysed liquation
Out, on the inner wall for being adsorbed on cell body under the action of charge.After an electrolysing period, backwashed with wind liquid feeding, still
Manually sorting, black copper powder can all be deposited in bottom of electrolytic tank.Native copper powder electrolysis unit anode directly fills, and anode locating flange is straight
It connects and is contacted with lower connecting base, copper powder is caused to be accumulated at anode connecting flange, with the progress of electrodeposition, copper powder is periodically electric
Product, electrolysis, in the process can continuous heat release, melt so as to cause lower connecting base is heated, cause in electrolytic process constantly
There is electrolyte to flow to outside system.In order to solve above-mentioned problem, need to design a kind of novel powder electrolysis unit to avoid electrodeposition mistake
Accumulation of the black copper powder of journey in power receiving section position.
Summary of the invention
For powder electrolysis system in the above problem present on industrial production, the purpose of the present invention is to provide one kind to make
With the powder swirl-flow electrolytic cell dedicated unit convenient, structure is simple, operating efficiency is high.
To achieve the above object, the present invention uses following technical scheme：
A kind of novel powder electrolysis unit, including cell body and locating rod, cell body top are equipped with upper connecting base, and lower part is set
There is connection to be shorted, bosom is equipped with anode；Connection is shorted side and offers first through hole, and lower part is equipped with lower connecting base；Anode
Upper end is fixedly connected with locating rod lower end, and lower end is equipped with power part；Anode lower end passes through first through hole and passes through anode positioning sleeve
It is fixedly connected with connecting to be shorted；Upper connecting base top is equipped with upper end cover；Liquid outlet is respectively equipped on upper connecting base and lower connecting base
And inlet.
A kind of novel powder electrolysis unit, it is characterised in that connection be shorted side be also provided with the second through-hole and
Third through-hole corresponding with the second through-hole, anode-supported bar passes through the second through-hole and third through-hole, and passes through anode-supported set
It is fixedly connected with anode lower end, anode-supported bar both ends pass through the second nut and O-ring respectively and connect with short circuit fixing seal is connect
It connects.
A kind of novel powder electrolysis unit, it is characterised in that be equipped with groove among upper end cover lower part, groove and fixed
Position bar upper end cooperates.
A kind of novel powder electrolysis unit, it is characterised in that anodic protection set is equipped with outside power part.
A kind of novel powder electrolysis unit, it is characterised in that further include the first nut, the first nut locks anode
Positioning sleeve.
A kind of novel powder electrolysis unit, it is characterised in that set between cell body upper end periphery and upper connecting base
There is housing.
A kind of novel powder electrolysis unit, it is characterised in that upper connecting base, cell body, connection short circuit, lower company
Joint chair is bolted to connection between each other, and squeezes sealing by O-ring and plane rubber mat.
A kind of novel powder electrolysis unit, it is characterised in that cell body is cylinder-like structure, and both ends are equipped with
Flange.
A kind of novel powder electrolysis unit, it is characterised in that anode is round tube shape structure, outer diameter 50-130mm；
Anode positioning sleeve internal diameter is 31-33mm, preferably 32mm, outer diameter 73-75mm, preferably 74mm；Positioning pole length is 289-
291mm, preferably 290mm, outer diameter 31-33mm, preferably 32mm；Cell body is cylindric, outer diameter 215-222mm,
Preferably 219mm, wall thickness 4-5mm, preferably 4.5mm, length 1580-1585mm, preferably 1583mm, tubular tube body two
End welding DN200 standard flange.
A kind of novel powder electrolysis unit, it is characterised in that the lower connecting base nominal diameter is 150mm.
Beneficial effects of the present invention：Apparatus of the present invention structure is simple, easy to operate, power receiving section position not heap in electrolytic deposition process
Material, compared to original powder cell construction, reduces period and the workload of sorting, period cost after reduction, workload and
Maintenance cost；Solve the problems, such as that powder causes its to burn leakage in lower connecting base accumulation, while also very good solution powder
The scour rate of black copper powder when train backlash is washed reduces the cost and workload of subsequent powder electrolysis system maintenance.
Detailed description of the invention
Fig. 1 is the structural diagram of the present invention；
Fig. 2 is the left view of Fig. 1；
Fig. 3 is anode construction schematic diagram；
In figure：1- upper end cover, 2- upper connecting base, 3- cell body, 4- anode, 5- locating rod, 6- housing, 7- lower connecting base,
8- anodic protection set, 9- connection are shorted, 10- anode positioning sleeve, 11- anode-supported bar, 12- anode-supported set, the first spiral shell of 13-
Cap, the second nut of 14-, 101- groove, 401- power part, 901- first through hole, the second through-hole of 902-, 903- third through-hole.
Specific embodiment
Below in conjunction with Figure of description, the invention will be further described：
As shown in Figure 1, Figure 2 and Figure 3, a kind of novel powder electrolysis unit of the invention, including upper end cover 1, upper connecting base 2, electricity
Solve groove body 3, anode 4, locating rod 5, housing 6, lower connecting base 7, anodic protection set 8, connection short circuit 9, anode positioning sleeve 10, sun
Pole support rod 11, anode-supported cover the 12, first nut 13, the second nut 14.3 top of cell body is equipped with upper connecting base 2, lower part
9 are shorted equipped with connection, bosom is equipped with anode 4；Connection is shorted 9 sides and offers first through hole 901, and lower part is equipped with lower connection
Seat 7；4 upper end of anode is fixedly connected with 5 lower end of locating rod, and lower end is equipped with power part 401；4 lower end of anode passes through first through hole 901
And it is fixedly connected by anode positioning sleeve 10 with short circuit 9 is connect；2 top of upper connecting base is equipped with upper end cover 1；Upper connecting base 2 is under
Liquid outlet and inlet are respectively equipped on attachment base 7.Connection is shorted 9 sides and is also provided with the second through-hole 902 and leads to second
The corresponding third through-hole 903 in hole 902, anode-supported bar 11 passes through the second through-hole 902 and third through-hole 903, and passes through anode
Support sleeve 12 is fixedly connected with 4 lower end of anode, 11 both ends of anode-supported bar pass through respectively the second nut 14 and O-ring with connect it is short
Connect 9 fixed seal connections.Groove 101 is equipped among 1 lower part of upper end cover, groove 101 and 5 upper end of locating rod cooperate.Connect electricity
Anodic protection set 8 is equipped with outside portion 401.First nut 13 locks anode positioning sleeve 10.3 upper end periphery of cell body and upper connection
Housing 6 is equipped between seat 2.Upper connecting base 2, cell body 3, connection are shorted 9, lower connecting base 7 and are consolidated between each other by bolt
Fixed connection, and sealing is squeezed by O-ring and plane rubber mat.Cell body 3 is cylinder-like structure, and outer diameter is φ 219mm, wall thickness
4.5mm, length 1583mm, both ends are equipped with DN200 flange.Anode 4 is round tube shape structure, and outer diameter 50-130mm, anode is fixed
Position 10 internal diameters of set are 32mm, and outer diameter 74mm, 5 length of locating rod is 290mm, outer diameter 32mm.7 nominal diameter of lower connecting base is
150mm。
Since anode 4 connects electric position in device side, it is installed as unconventional installation.It is logical to pass through first for 4 lower end of anode first
Hole 901 is simultaneously installed on connection short circuit 9 by anode positioning sleeve 10；Secondly, passing through the second through-hole 902, third through-hole 903, sun
Pole support rod 11 and anode-supported cover 12 mating reactions, and fixed anode 4 topples over anode 4 not in center；Then, it will be electrolysed
Groove body 3 is installed to be shorted on 9 in succession, is sealed by plane rubber mat and bolt compresses；Again from upper installation upper connecting base 2, by flat
Face rubber mat is sealed in bolt compresses, from lower installation lower connecting base 7, is sealed by plane rubber mat and bolt compresses；Pass through on anode 4
Locating rod 5 is loaded onto threaded connection, is finally installed upper end cover 1, is placed in locating rod 5 in 1 groove of upper end cover, keeps anode 4 complete
Positioning；Finally, installation thinks matched first nut 13, the second nut 14 with short circuit 9 is connect, passes through O-ring and squeeze sealing, complete
Assembly.
Claims (10)
1. a kind of novel powder electrolysis unit, it is characterised in that including cell body（3）And locating rod（5）, cell body（3）On
Portion is equipped with upper connecting base（2）, lower part is equipped with connection and is shorted（9）, bosom is equipped with anode（4）；Connection is shorted（9）Side opens up
There is first through hole（901）, lower part is equipped with lower connecting base（7）；Anode（4）Upper end and locating rod（5）Lower end is fixedly connected, and lower end is set
There is power part（401）；Anode（4）Lower end passes through first through hole（901）And pass through anode positioning sleeve（10）It is shorted with connecting（9）Gu
Fixed connection；Upper connecting base（2）Top is equipped with upper end cover（1）；Upper connecting base（2）And lower connecting base（7）On be respectively equipped with liquid outlet
And inlet.
2. a kind of novel powder electrolysis unit according to claim 1, it is characterised in that connection is shorted（9）Side also opens up
There is the second through-hole（902）And with the second through-hole（902）Corresponding third through-hole（903）, anode-supported bar（11）Across
Two through-holes（902）And third through-hole（903）, and pass through anode-supported set（12）With anode（4）Lower end is fixedly connected, anode-supported
Bar（11）Both ends pass through the second nut respectively（14）With O-ring with connect be shorted（9）Fixed seal connection.
3. a kind of novel powder electrolysis unit according to claim 1, it is characterised in that upper end cover（1）It is equipped among lower part
Groove（101）, groove（101）With locating rod（5）Upper end cooperates.
4. a kind of novel powder electrolysis unit according to claim 1, it is characterised in that power part（401）Outside is equipped with sun
Pole protective case（8）.
5. a kind of novel powder electrolysis unit according to claim 1, it is characterised in that further include the first nut（13）, the
One nut（13）Lock anode positioning sleeve（10）.
6. a kind of novel powder electrolysis unit according to claim 1, it is characterised in that cell body（3）Upper end periphery with
Upper connecting base（2）Between be equipped with housing（6）.
7. a kind of novel powder electrolysis unit according to claim 1, it is characterised in that upper connecting base（2）, cell body
（3）, connection be shorted（9）, lower connecting base（7）It is bolted to connection, and is squeezed by O-ring and plane rubber mat between each other
Sealing.
8. a kind of novel powder electrolysis unit according to claim 1, it is characterised in that cell body（3）For cylindrical shape knot
Structure, both ends are equipped with flange.
9. a kind of novel powder electrolysis unit according to claim 1, it is characterised in that anode（4）For round tube shape structure,
Outer diameter is 50-130mm；Anode positioning sleeve（10）Internal diameter is 31-33mm, preferably 32mm, outer diameter 73-75mm, preferably
74mm；Locating rod（5）Length is 289-291mm, preferably 290mm, outer diameter 31-33mm, preferably 32mm；Cell body
（3）For cylindrical shape, outer diameter 215-222mm, preferably 219mm, wall thickness 4-5mm, preferably 4.5mm, length 1580-
DN200 standard flange is welded at 1585mm, preferably 1583mm, tubular tube body both ends.
10. a kind of novel powder electrolysis unit according to claim 1, it is characterised in that the lower connecting base（7）It is public
Diameter is referred to as 150mm.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810983452.4A CN108914165B (en) | 2018-08-27 | 2018-08-27 | Novel powder electrolysis device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810983452.4A CN108914165B (en) | 2018-08-27 | 2018-08-27 | Novel powder electrolysis device |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN108914165A true CN108914165A (en) | 2018-11-30 |
| CN108914165B CN108914165B (en) | 2023-11-21 |
Family
ID=64407079
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810983452.4A Active CN108914165B (en) | 2018-08-27 | 2018-08-27 | Novel powder electrolysis device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108914165B (en) |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2007071713A1 (en) * | 2005-12-20 | 2007-06-28 | Industrie De Nora S.P.A. | Electrolytic cell for metal deposition |
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| CN202430302U (en) * | 2012-01-10 | 2012-09-12 | 西安瑞凯电力科技有限公司 | Barrel-shaped selective electrolyzing device |
| CN102758215A (en) * | 2012-07-24 | 2012-10-31 | 嘉兴科菲冶金科技股份有限公司 | Special anode in cyclone electrolyzer |
| CN102959134A (en) * | 2010-07-07 | 2013-03-06 | 田中贵金属工业株式会社 | Precious metal recovery device and recovery method |
| CN102965693A (en) * | 2012-11-21 | 2013-03-13 | 淮阴工学院 | Ultrasonic cyclone electrolyzer |
| CN103103581A (en) * | 2012-12-10 | 2013-05-15 | 重庆智锐德科技有限公司 | Automatic impurity removing device for waste copper sulfate electrolyte |
| CN104726901A (en) * | 2015-03-31 | 2015-06-24 | 浙江科菲科技股份有限公司 | Diaphragm swirl-flow electrolyzer |
| CN204530000U (en) * | 2015-03-31 | 2015-08-05 | 浙江科菲科技股份有限公司 | A kind of barrier film swirl electrolysis device |
| CN205313682U (en) * | 2015-11-30 | 2016-06-15 | 金川集团股份有限公司 | A electric installation for whirl electrolysis trough |
| CN205382217U (en) * | 2015-12-29 | 2016-07-13 | 无锡市瑞思科环保科技有限公司 | Electrolysis equipment is flowed in centrifugation |
| CN209338671U (en) * | 2018-08-27 | 2019-09-03 | 浙江科菲科技股份有限公司 | A kind of novel powder electrolysis unit |
-
2018
- 2018-08-27 CN CN201810983452.4A patent/CN108914165B/en active Active
Patent Citations (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2007071713A1 (en) * | 2005-12-20 | 2007-06-28 | Industrie De Nora S.P.A. | Electrolytic cell for metal deposition |
| CN101886271A (en) * | 2009-05-15 | 2010-11-17 | 邓涛 | Rotational-flow electrolysis method and device thereof |
| CN102959134A (en) * | 2010-07-07 | 2013-03-06 | 田中贵金属工业株式会社 | Precious metal recovery device and recovery method |
| CN202430302U (en) * | 2012-01-10 | 2012-09-12 | 西安瑞凯电力科技有限公司 | Barrel-shaped selective electrolyzing device |
| CN102758215A (en) * | 2012-07-24 | 2012-10-31 | 嘉兴科菲冶金科技股份有限公司 | Special anode in cyclone electrolyzer |
| CN102965693A (en) * | 2012-11-21 | 2013-03-13 | 淮阴工学院 | Ultrasonic cyclone electrolyzer |
| CN103103581A (en) * | 2012-12-10 | 2013-05-15 | 重庆智锐德科技有限公司 | Automatic impurity removing device for waste copper sulfate electrolyte |
| CN104726901A (en) * | 2015-03-31 | 2015-06-24 | 浙江科菲科技股份有限公司 | Diaphragm swirl-flow electrolyzer |
| CN204530000U (en) * | 2015-03-31 | 2015-08-05 | 浙江科菲科技股份有限公司 | A kind of barrier film swirl electrolysis device |
| CN205313682U (en) * | 2015-11-30 | 2016-06-15 | 金川集团股份有限公司 | A electric installation for whirl electrolysis trough |
| CN205382217U (en) * | 2015-12-29 | 2016-07-13 | 无锡市瑞思科环保科技有限公司 | Electrolysis equipment is flowed in centrifugation |
| CN209338671U (en) * | 2018-08-27 | 2019-09-03 | 浙江科菲科技股份有限公司 | A kind of novel powder electrolysis unit |
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| Publication number | Publication date |
|---|---|
| CN108914165B (en) | 2023-11-21 |
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