CN108913051A - A kind of expansion solution adhesive tape and production method - Google Patents
A kind of expansion solution adhesive tape and production method Download PDFInfo
- Publication number
- CN108913051A CN108913051A CN201811031101.XA CN201811031101A CN108913051A CN 108913051 A CN108913051 A CN 108913051A CN 201811031101 A CN201811031101 A CN 201811031101A CN 108913051 A CN108913051 A CN 108913051A
- Authority
- CN
- China
- Prior art keywords
- glue
- parts
- adhesive tape
- line
- layer
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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- 239000002390 adhesive tape Substances 0.000 title claims abstract description 32
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 24
- 239000010410 layer Substances 0.000 claims abstract description 64
- 239000000758 substrate Substances 0.000 claims abstract description 42
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims abstract description 31
- 239000003292 glue Substances 0.000 claims abstract description 25
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 22
- 230000008961 swelling Effects 0.000 claims abstract description 16
- 239000003999 initiator Substances 0.000 claims abstract description 15
- 239000002346 layers by function Substances 0.000 claims abstract description 11
- 239000006185 dispersion Substances 0.000 claims abstract description 6
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 claims description 18
- 239000000243 solution Substances 0.000 claims description 18
- BAPJBEWLBFYGME-UHFFFAOYSA-N Methyl acrylate Chemical compound COC(=O)C=C BAPJBEWLBFYGME-UHFFFAOYSA-N 0.000 claims description 16
- -1 polyoxyethylene Polymers 0.000 claims description 11
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 claims description 10
- 235000000126 Styrax benzoin Nutrition 0.000 claims description 10
- CQEYYJKEWSMYFG-UHFFFAOYSA-N butyl acrylate Chemical compound CCCCOC(=O)C=C CQEYYJKEWSMYFG-UHFFFAOYSA-N 0.000 claims description 10
- ISAOCJYIOMOJEB-UHFFFAOYSA-N benzoin Chemical compound C=1C=CC=CC=1C(O)C(=O)C1=CC=CC=C1 ISAOCJYIOMOJEB-UHFFFAOYSA-N 0.000 claims description 9
- 239000003995 emulsifying agent Substances 0.000 claims description 9
- 239000003863 metallic catalyst Substances 0.000 claims description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 9
- LCGLNKUTAGEVQW-UHFFFAOYSA-N Dimethyl ether Chemical compound COC LCGLNKUTAGEVQW-UHFFFAOYSA-N 0.000 claims description 8
- 229920003171 Poly (ethylene oxide) Polymers 0.000 claims description 8
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 claims description 8
- 125000002524 organometallic group Chemical group 0.000 claims description 8
- 238000010792 warming Methods 0.000 claims description 8
- 239000011248 coating agent Substances 0.000 claims description 7
- 238000000576 coating method Methods 0.000 claims description 7
- OMIGHNLMNHATMP-UHFFFAOYSA-N 2-hydroxyethyl prop-2-enoate Chemical compound OCCOC(=O)C=C OMIGHNLMNHATMP-UHFFFAOYSA-N 0.000 claims description 6
- 244000028419 Styrax benzoin Species 0.000 claims description 6
- ZLNAFSPCNATQPQ-UHFFFAOYSA-N ethenyl-dimethoxy-methylsilane Chemical compound CO[Si](C)(OC)C=C ZLNAFSPCNATQPQ-UHFFFAOYSA-N 0.000 claims description 6
- OZAIFHULBGXAKX-UHFFFAOYSA-N 2-(2-cyanopropan-2-yldiazenyl)-2-methylpropanenitrile Chemical compound N#CC(C)(C)N=NC(C)(C)C#N OZAIFHULBGXAKX-UHFFFAOYSA-N 0.000 claims description 5
- 235000015511 Liquidambar orientalis Nutrition 0.000 claims description 5
- 239000004870 Styrax Substances 0.000 claims description 5
- 235000008411 Sumatra benzointree Nutrition 0.000 claims description 5
- 229960002130 benzoin Drugs 0.000 claims description 5
- NKSJNEHGWDZZQF-UHFFFAOYSA-N ethenyl(trimethoxy)silane Chemical compound CO[Si](OC)(OC)C=C NKSJNEHGWDZZQF-UHFFFAOYSA-N 0.000 claims description 5
- 238000004108 freeze drying Methods 0.000 claims description 5
- 235000019382 gum benzoic Nutrition 0.000 claims description 5
- XFRVVPUIAFSTFO-UHFFFAOYSA-N 1-Tridecanol Chemical compound CCCCCCCCCCCCCO XFRVVPUIAFSTFO-UHFFFAOYSA-N 0.000 claims description 4
- KMNCBSZOIQAUFX-UHFFFAOYSA-N 2-ethoxy-1,2-diphenylethanone Chemical compound C=1C=CC=CC=1C(OCC)C(=O)C1=CC=CC=C1 KMNCBSZOIQAUFX-UHFFFAOYSA-N 0.000 claims description 4
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims description 4
- 125000005233 alkylalcohol group Chemical group 0.000 claims description 4
- 239000007864 aqueous solution Substances 0.000 claims description 4
- 238000006243 chemical reaction Methods 0.000 claims description 4
- 238000001816 cooling Methods 0.000 claims description 4
- 239000004744 fabric Substances 0.000 claims description 4
- 229910052710 silicon Inorganic materials 0.000 claims description 4
- 239000010703 silicon Substances 0.000 claims description 4
- 229910000030 sodium bicarbonate Inorganic materials 0.000 claims description 4
- 235000017557 sodium bicarbonate Nutrition 0.000 claims description 4
- 239000010936 titanium Substances 0.000 claims description 4
- 229910052719 titanium Inorganic materials 0.000 claims description 4
- MSAHTMIQULFMRG-UHFFFAOYSA-N 1,2-diphenyl-2-propan-2-yloxyethanone Chemical compound C=1C=CC=CC=1C(OC(C)C)C(=O)C1=CC=CC=C1 MSAHTMIQULFMRG-UHFFFAOYSA-N 0.000 claims description 3
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims description 3
- 239000000839 emulsion Substances 0.000 claims description 3
- 238000010422 painting Methods 0.000 claims description 3
- PUNSEDFDYHKBHO-IPEZHVIRSA-N [Na].C(\C=C/C(=O)OC1CCCCC1)(=O)OC1CCCCC1.S(=O)(=O)(O)C(C(=O)O)CC(=O)O Chemical compound [Na].C(\C=C/C(=O)OC1CCCCC1)(=O)OC1CCCCC1.S(=O)(=O)(O)C(C(=O)O)CC(=O)O PUNSEDFDYHKBHO-IPEZHVIRSA-N 0.000 claims 1
- 239000003054 catalyst Substances 0.000 claims 1
- 229910052751 metal Inorganic materials 0.000 claims 1
- 239000002184 metal Substances 0.000 claims 1
- 239000003522 acrylic cement Substances 0.000 abstract 1
- 238000000034 method Methods 0.000 description 8
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 6
- 239000000463 material Substances 0.000 description 5
- 241000736148 Styrax Species 0.000 description 4
- YKUBBPKBQQFDLW-AFEZEDKISA-N [Na].C(\C=C/C(=O)OC1CCCCC1)(=O)OC1CCCCC1 Chemical compound [Na].C(\C=C/C(=O)OC1CCCCC1)(=O)OC1CCCCC1 YKUBBPKBQQFDLW-AFEZEDKISA-N 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 239000003792 electrolyte Substances 0.000 description 3
- 230000001681 protective effect Effects 0.000 description 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- ULUAUXLGCMPNKK-UHFFFAOYSA-N Sulfobutanedioic acid Chemical compound OC(=O)CC(C(O)=O)S(O)(=O)=O ULUAUXLGCMPNKK-UHFFFAOYSA-N 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 238000003786 synthesis reaction Methods 0.000 description 2
- OZAIFHULBGXAKX-VAWYXSNFSA-N AIBN Substances N#CC(C)(C)\N=N\C(C)(C)C#N OZAIFHULBGXAKX-VAWYXSNFSA-N 0.000 description 1
- WXQDFOGZIYLEGP-UHFFFAOYSA-N C(C(C)C)#N.C(C(C)C)#N.[N] Chemical compound C(C(C)C)#N.C(C(C)C)#N.[N] WXQDFOGZIYLEGP-UHFFFAOYSA-N 0.000 description 1
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 1
- 239000005977 Ethylene Substances 0.000 description 1
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 239000004820 Pressure-sensitive adhesive Substances 0.000 description 1
- 229920000297 Rayon Polymers 0.000 description 1
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000005253 cladding Methods 0.000 description 1
- 229920001577 copolymer Polymers 0.000 description 1
- 239000006071 cream Substances 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000004945 emulsification Methods 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 125000004435 hydrogen atom Chemical class [H]* 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 229920002521 macromolecule Polymers 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 239000002985 plastic film Substances 0.000 description 1
- 229920006255 plastic film Polymers 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 238000000197 pyrolysis Methods 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- KDYFGRWQOYBRFD-UHFFFAOYSA-N succinic acid Chemical compound OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 description 1
- 230000002194 synthesizing effect Effects 0.000 description 1
- YUYCVXFAYWRXLS-UHFFFAOYSA-N trimethoxysilane Chemical compound CO[SiH](OC)OC YUYCVXFAYWRXLS-UHFFFAOYSA-N 0.000 description 1
- 238000009281 ultraviolet germicidal irradiation Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J7/00—Adhesives in the form of films or foils
- C09J7/20—Adhesives in the form of films or foils characterised by their carriers
- C09J7/22—Plastics; Metallised plastics
- C09J7/25—Plastics; Metallised plastics based on macromolecular compounds obtained otherwise than by reactions involving only carbon-to-carbon unsaturated bonds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F220/00—Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical or a salt, anhydride ester, amide, imide or nitrile thereof
- C08F220/02—Monocarboxylic acids having less than ten carbon atoms; Derivatives thereof
- C08F220/04—Acids; Metal salts or ammonium salts thereof
- C08F220/06—Acrylic acid; Methacrylic acid; Metal salts or ammonium salts thereof
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F220/00—Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical or a salt, anhydride ester, amide, imide or nitrile thereof
- C08F220/02—Monocarboxylic acids having less than ten carbon atoms; Derivatives thereof
- C08F220/10—Esters
- C08F220/12—Esters of monohydric alcohols or phenols
- C08F220/14—Methyl esters, e.g. methyl (meth)acrylate
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F220/00—Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical or a salt, anhydride ester, amide, imide or nitrile thereof
- C08F220/02—Monocarboxylic acids having less than ten carbon atoms; Derivatives thereof
- C08F220/10—Esters
- C08F220/12—Esters of monohydric alcohols or phenols
- C08F220/16—Esters of monohydric alcohols or phenols of phenols or of alcohols containing two or more carbon atoms
- C08F220/18—Esters of monohydric alcohols or phenols of phenols or of alcohols containing two or more carbon atoms with acrylic or methacrylic acids
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J133/00—Adhesives based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Adhesives based on derivatives of such polymers
- C09J133/02—Homopolymers or copolymers of acids; Metal or ammonium salts thereof
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J133/00—Adhesives based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Adhesives based on derivatives of such polymers
- C09J133/04—Homopolymers or copolymers of esters
- C09J133/06—Homopolymers or copolymers of esters of esters containing only carbon, hydrogen and oxygen, the oxygen atom being present only as part of the carboxyl radical
- C09J133/08—Homopolymers or copolymers of acrylic acid esters
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J133/00—Adhesives based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Adhesives based on derivatives of such polymers
- C09J133/04—Homopolymers or copolymers of esters
- C09J133/14—Homopolymers or copolymers of esters of esters containing halogen, nitrogen, sulfur or oxygen atoms in addition to the carboxy oxygen
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J7/00—Adhesives in the form of films or foils
- C09J7/20—Adhesives in the form of films or foils characterised by their carriers
- C09J7/22—Plastics; Metallised plastics
- C09J7/24—Plastics; Metallised plastics based on macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F220/00—Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical or a salt, anhydride ester, amide, imide or nitrile thereof
- C08F220/02—Monocarboxylic acids having less than ten carbon atoms; Derivatives thereof
- C08F220/10—Esters
- C08F220/12—Esters of monohydric alcohols or phenols
- C08F220/16—Esters of monohydric alcohols or phenols of phenols or of alcohols containing two or more carbon atoms
- C08F220/18—Esters of monohydric alcohols or phenols of phenols or of alcohols containing two or more carbon atoms with acrylic or methacrylic acids
- C08F220/1804—C4-(meth)acrylate, e.g. butyl (meth)acrylate, isobutyl (meth)acrylate or tert-butyl (meth)acrylate
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J2301/00—Additional features of adhesives in the form of films or foils
- C09J2301/10—Additional features of adhesives in the form of films or foils characterized by the structural features of the adhesive tape or sheet
- C09J2301/12—Additional features of adhesives in the form of films or foils characterized by the structural features of the adhesive tape or sheet by the arrangement of layers
- C09J2301/122—Additional features of adhesives in the form of films or foils characterized by the structural features of the adhesive tape or sheet by the arrangement of layers the adhesive layer being present only on one side of the carrier, e.g. single-sided adhesive tape
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J2301/00—Additional features of adhesives in the form of films or foils
- C09J2301/40—Additional features of adhesives in the form of films or foils characterized by the presence of essential components
- C09J2301/412—Additional features of adhesives in the form of films or foils characterized by the presence of essential components presence of microspheres
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J2301/00—Additional features of adhesives in the form of films or foils
- C09J2301/50—Additional features of adhesives in the form of films or foils characterized by process specific features
- C09J2301/502—Additional features of adhesives in the form of films or foils characterized by process specific features process for debonding adherents
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J2423/00—Presence of polyolefin
- C09J2423/04—Presence of homo or copolymers of ethene
- C09J2423/046—Presence of homo or copolymers of ethene in the substrate
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J2467/00—Presence of polyester
- C09J2467/006—Presence of polyester in the substrate
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Adhesive Tapes (AREA)
Abstract
The invention discloses a kind of expansions to solve adhesive tape production method, and expansion solution adhesive tape production method includes the following steps：S1. acrylic glue is synthesized, S2. synthesizes swelling agent, and the step S2 and step S3 swelling agent synthesized and acrylic glue are uniformly mixed, are added initiator 0.1-0.5 parts and are coated on substrate by S3., and add release layer, are fabricated to adhesive tape；A kind of expansion solves adhesive tape, including release layer 1, glue-line 2, substrate layer 3 and functional layer 4, glue-line described in substrate layer coated on one side, substrate layer another side is connected with functional layer, and glue-line another side is connected with the release layer, and expanded granular is set in glue-line, glue-line is acrylic glue-line, and substrate layer is pet layer；Relatively traditional adhesive tape, one aspect of the present invention use acrylic glue, and expanded granular is equipped in acrylic glue-line.On the other hand, because dispersibility of the expanded granular in acrylic adhesive, solves dispersion problem.So that application range of the present invention is wider.
Description
Technical field
The present invention relates to adhesive tape production fields, and in particular to a kind of expansion solution adhesive tape and production method.
Background technique
In modern manufacturing industry, making technology process can undergo the manufacturing process such as more high temperature, high humidity, soda acid, salt fog,
It is required that it is extremely stringent, non-process part or cracky region are needed to carry out protection processing.The main function of surface protection film is just
It is that certain protection is played to the surface of commodity, also known as protective glue band or sensitive film generally use macromolecule plastic film
Perhaps special paper as substrate rubber or acrylate copolymer as pressure-sensitive adhesive agent, by sides such as coating drying
Method is process.Surface protection film at this stage oneself through largely for building, machinery production, in terms of automobile production, instrument instrument
Table, wrist-watch and other production aspects, in addition, can also be used to protection steel, plastics, organic glass, various oil ?plates, woodwork etc.
The surface of material.
But protective glue band at present on the market, mostly exist in the production process：Rubber polymer shipwreck, expanded granular system
Feel embarrassed, the dispersion problem between glue and expanded granular.And then causing protective film manufacturing quality low, the scope of application is low, cannot
It meets the requirements.
Summary of the invention
The technical problem to be solved by the present invention is to provide a kind of expansion solution adhesive tapes and production method, the present invention to solve synthesis
Glue is difficult, expanded granular production is difficult, dispersibility between glue and expanded granular the problems such as.The quality of adhesive tape is improved, is made
It is wider model must to be applicable in.
In order to solve the above technical problems, the technical scheme is that：A kind of expansion solution adhesive tape production method, including with
Lower step：
S1. acrylic glue is synthesized：0-100 parts of butanone are added in flask, is warming up to 60-80 DEG C, butyl acrylate is added
0-30 parts, 0-30 parts of methyl acrylate, 0-30 parts of hydroxy-ethyl acrylate, 0-30 parts of 2- butanone, 0-30 parts of acrylic acid are added and cause
It 0.1-3 parts of agent azodiisobutyronitrile, reacts 120-360 minutes, is then slowly added to the initiator of equal quality part, the reaction was continued
120-240 minutes, etc. glue colos it is transparent after, cooling discharge；
S2. swelling agent is synthesized：By 0-10 parts of vinyltrimethoxysilane, 50-100 parts of vinyl methyl dimethoxysilane,
0-10 parts of phenyltrimethoxysila,e, 50-100 parts of water, emulsifier, are emulsified with high speed disperser, spare；In sodium bicarbonate
5% aqueous solution in be added organo-metallic catalyst 0.1-1 parts, be warming up to 60 DEG C, spare organic silicon emulsion be slowly added dropwise, instead
It answers 2 hours, then the solution of acquisition is removed water with freeze-drying, obtains powdered swelling agent；
S3. the step S2 and step S3 swelling agent synthesized and acrylic glue are uniformly mixed, initiator 0.1-0.5 parts of painting is added
Cloth adds release layer on substrate, is fabricated to adhesive tape.
Preferably, emulsifier described in step S2 is alkyl alcohol ethoxylates, isomerous tridecanol polyoxyethylene, sulfo group amber
The one or more of amber acid dicyclohexyl maleate sodium, alkylol polyoxyethylene.
Preferably, high speed disperser speed described in step S2 is 2500rpm, and jitter time is 30 minutes.
Preferably, organo-metallic catalyst described in step S2 is organotin or organic titanium.
Preferably, initiator described in step S3 is styrax, benzoin dimethylether, benzoin ethyl ether, benzoin isopropyl
The one or more of ether.
Preferably, substrate described in step S3 is PET, and 20-30 microns of coating thickness.
The present invention also provides：A kind of expansion solution adhesive tape, including release layer, glue-line, substrate layer and functional layer, the base
The laminated coating glue-line of material, the substrate layer another side are connected with functional layer, the glue-line another side and the release layer
Connection sets expanded granular in the glue-line, and the glue-line is acrylic glue-line, and the substrate layer is pet layer.
Preferably, the glue-line with a thickness of 20 μm -30 μm.
Preferably, it is room temperature that the glue-line, which is coated on temperature when on the substrate layer,.
Preferably, the two sides of the substrate layer is equipped with frosted layer.
The beneficial effect that the present invention realizes：
1. the present invention prepares swelling agent in such a way that organosilicon wraps up inorganic foamed material, while it can satisfy UV or pyrolysis is viscous
Mode.Using the method for freeze-drying in preparation process, it can both guarantee that grain shape was not destroyed, it is also ensured that preparation
Inorganic foamed material is complete in the process, reduces the presence of invalid particle.When expanded granular is heated again, sodium bicarbonate release
Gas breaks film surface is out to realize that solution is viscous；In the case where UV irradiation again, the double bond of organosilicon shell is cross-linked to form largely
Free silica segment so that film surface is free organosilicon entirely, glue-line can also lose viscosity, to realize the viscous effect of solution.
2. compared with prior art, the present invention first synthesis can be with the acrylic glue of low-temperature setting, then with unique technique
The expanded granular of synthesizing organo-silicon cladding, the two is in combination with being coated into suitable thickness, can be realized simultaneously different solutions
Viscous mode.
Detailed description of the invention
Fig. 1 is sectional drawing of the invention.
The title or process name for the corresponding component that number or letter in figure represent：1. release layer, 2. glue-lines, 3. substrates
Layer, 4. functional layers.
The attached figures are only used for illustrative purposes and cannot be understood as limitating the patent；In order to better illustrate this embodiment, attached
Scheme certain components to have omission, zoom in or out, does not represent the size of actual product；To those skilled in the art,
The omitting of some known structures and their instructions in the attached drawings are understandable；The same or similar label corresponds to same or similar
Component；The terms describing the positional relationship in the drawings are only for illustration, should not be understood as the limitation to this patent.
Specific embodiment
In order to facilitate the understanding of those skilled in the art, being carried out below in conjunction with attached drawing and embodiment to the present invention further
Detailed description.
A kind of expansion solution adhesive tape production method, includes the following steps：
S1. acrylic glue is synthesized：0-100 parts of butanone are added in flask, is warming up to 60-80 DEG C, butyl acrylate is added
0-30 parts, 0-30 parts of methyl acrylate, 0-30 parts of hydroxy-ethyl acrylate, 0-30 parts of 2- butanone, 0-30 parts of acrylic acid are added and cause
It 0.1-3 parts of agent azodiisobutyronitrile, reacts 120-360 minutes, is then slowly added to the initiator of equal quality part, the reaction was continued
120-240 minutes, etc. glue colos it is transparent after, cooling discharge；
S2. swelling agent is synthesized：By 0-10 parts of vinyltrimethoxysilane, 50-100 parts of vinyl methyl dimethoxysilane,
0-10 parts of phenyltrimethoxysila,e, 50-100 parts of water, emulsifier, are emulsified with high speed disperser, spare；In sodium bicarbonate
5% aqueous solution in be added organo-metallic catalyst 0.1-1 parts, be warming up to 60 DEG C, spare organic silicon emulsion be slowly added dropwise, instead
It answers 2 hours, then the solution of acquisition is removed water with freeze-drying, obtains powdered swelling agent；
S3. the step S2 and step S3 swelling agent synthesized and acrylic glue are uniformly mixed, initiator 0.1-0.5 parts of painting is added
Cloth adds release layer on substrate, is fabricated to adhesive tape.
Specifically, emulsifier is alkyl alcohol ethoxylates, isomerous tridecanol polyoxyethylene, sulfosuccinic acid in step S2
The one or more of dicyclohexyl maleate sodium, alkylol polyoxyethylene.
Specifically, step S2 high speed dispersion machine speed is 2500rpm, jitter time is 30 minutes.
Specifically, organo-metallic catalyst is organotin or organic titanium in step S2.
Specifically, initiator is styrax, benzoin dimethylether, benzoin ethyl ether, benzoin isopropyl ether in step S3
It is one or more of.
Specifically, substrate is PET in step S3, and 20-30 microns of coating thickness.
The present invention also provides：A kind of expansion solution adhesive tape, including release layer 1, glue-line 2, substrate layer 3 and functional layer 4, base
The laminated coating glue-line of material, substrate layer another side are connected with functional layer, and glue-line another side is connected with the release layer, in glue
Expanded granular is set in layer, glue-line is acrylic glue-line, and substrate layer is pet layer.
Specifically, glue-line with a thickness of 20 μm -30 μm.
Specifically, it is room temperature that glue-line, which is coated on temperature when on the substrate layer,.
Specifically, the two sides of substrate layer is equipped with frosted layer.The effect that substrate layer setting frosted layer can allow glue-line to be pasted is more
It is good.
Embodiment one
Expansion above-mentioned solution adhesive tape is combined into specific way in reality, does corresponding elaboration, it is specific as follows：Expansion solution viscose glue
Band production method, includes the following steps：
S1. acrylic glue is synthesized：0-100 parts of butanone are added in flask, is warming up to 60-80 DEG C, butyl acrylate is added
0-30 parts, 0-30 parts of methyl acrylate, 0-30 parts of hydroxy-ethyl acrylate, 0-30 parts of 2- butanone, 0-30 parts of acrylic acid are added and cause
It 0.1-3 parts of agent azodiisobutyronitrile, reacts 120-360 minutes, is then slowly added to the initiator of equal quality part, the reaction was continued
120-240 minutes, etc. glue colos it is transparent after, cooling discharge；By 50 parts of butanone, butyl acrylate (BA) 15 in the present embodiment
Part, 15 parts of methyl acrylate (MA), 15 parts of hydroxy-ethyl acrylate (HEA), 15 parts of 2- butanone (MEK), 15 parts of acrylic acid (AA), idol
1 part of nitrogen bis-isobutyronitrile (AIBN).
S2. swelling agent is synthesized：By 0-10 parts of vinyltrimethoxysilane, vinyl methyl dimethoxysilane 50-100
Part, 0-10 parts of phenyltrimethoxysila,e, 50-100 parts of water, emulsifier, are emulsified with high speed disperser, spare；In carbonic acid
Organo-metallic catalyst 0.1-1 parts is added in 5% aqueous solution of hydrogen sodium, is warming up to 60 DEG C, spare organosilicon cream is slowly added dropwise
Liquid reacts 2 hours, then the solution of acquisition is removed water with freeze-drying, obtains powdered swelling agent；Ethylene in the present embodiment
5 parts of base trimethoxy silane, 60 parts of vinyl methyl dimethoxysilane, 5 parts of phenyltrimethoxysila,e, 80 parts of water, emulsification
1 part, 0.5 part of organo-metallic catalyst of agent alkylol polyoxyethylene (25) ether.
S3. the step S2 and step S3 swelling agent synthesized and acrylic glue are uniformly mixed, initiator 0.1-0.5 is added
Part is coated on substrate, and adds release layer, is fabricated to adhesive tape.Initiator is 0.5 part in the present embodiment.
Specifically, emulsifier is alkyl alcohol ethoxylates, isomerous tridecanol polyoxyethylene, sulfosuccinic acid in step S2
The one or more of dicyclohexyl maleate sodium, alkylol polyoxyethylene；Step S2 high speed dispersion machine speed is 2500rpm, when dispersion
Between be 30 minutes；Organo-metallic catalyst is organotin or organic titanium in step S2.Emulsifier is poly- for alkylol in the present embodiment
Ethylene oxide ether, organo-metallic catalyst use organotin.
Specifically, initiator is styrax, benzoin dimethylether, benzoin ethyl ether, benzoin isopropyl ether in step S3
It is one or more of；Substrate is PET in step S3, and 20-30 microns of coating thickness.Initiator is styrax in the present embodiment, is applied
Cloth is with a thickness of 25 microns.
The test data of the present embodiment is：It is just viscous：2#；Peeling force（N/25mm）：8.5；100 DEG C, 2 hours heatproofs：OK；It is resistance to
Electrolyte（85 DEG C, 24 hours）：OK；UV, after irradiation in 30 seconds, peeling force（N/25mm）：0.2；After 120 DEG C of bakings（N/25mm）：
0.09。
Embodiment two
As embodiment two with two basic setup of embodiment is, primary difference is that：Butyl acrylate (BA) in the present embodiment
20 parts, 20 parts of acrylic acid (AA), 7 parts of vinyltrimethoxysilane, 65 parts of vinyl methyl dimethoxysilane, phenyl front three
7 parts of oxysilane.The test data of the present embodiment is：It is just viscous：2#；Peeling force（N/25mm）：7.3；100 DEG C, 2 hours heatproofs：
OK；Electrolyte resistance（85 DEG C, 24 hours）：OK；UV, after irradiation in 30 seconds, peeling force（N/25mm）：0.15；After 120 DEG C of bakings（N/
25mm）：0.06.
Embodiment three
As embodiment three with one basic setup of embodiment is, primary difference is that：Butyl acrylate (BA) in the present embodiment
20 parts, 5 parts of methyl acrylate (MA), 20 parts of 2- butanone (MEK), 20 parts of acrylic acid (AA).The test data of the present embodiment is：Just
It is viscous：2#；Peeling force（N/25mm）：7.4；100 DEG C, 2 hours heatproofs：OK；Electrolyte resistance（85 DEG C, 24 hours）：OK；UV, 30 seconds
After irradiation, peeling force（N/25mm）：0.15；After 120 DEG C of bakings（N/25mm）：0.05.
Example IV
Expansion above-mentioned solution adhesive tape is combined into specific way in reality, does corresponding elaboration, it is specific as follows：As shown in Figure 1,
Expansion solution adhesive tape, including release layer 1, glue-line 2, substrate layer 3 and functional layer 4, substrate layer coated on one side glue-line, substrate layer are another
Face is connected with functional layer, and glue-line another side is connected with the release layer, and expanded granular is set in glue-line, and glue-line is acrylic glue
Layer, certain glue-line are also not necessarily limited to acrylic glue-line, and substrate layer is pet layer, and substrate layer is also not necessarily limited to PET.It is used in the present embodiment
Acrylic glue-line and expanded granular are acrylic glue and swelling agent made by embodiment one.
Specifically, glue-line with a thickness of 20 μm -30 μm.The present embodiment mesoglea with a thickness of 25 μm.
Specifically, temperature is room temperature when glue-line is coated on substrate layer.
Specifically, the two sides of substrate layer is equipped with frosted layer.The effect that substrate layer setting frosted layer can allow glue-line to be pasted is more
It is good.Not set frosted layer in the present embodiment.
Embodiment five
As embodiment five with example IV basic setup is, primary difference is that：Substrate layer uses PE layers in the present embodiment,
Glue-line with a thickness of 20 μm.
Embodiment six
As embodiment six with example IV basic setup is, primary difference is that：Substrate layer has frosted layer in the present embodiment；
Glue-line with a thickness of 30 μm.
Obviously, the above embodiment of the present invention be only to clearly illustrate example of the present invention, and not be pair
The restriction of embodiments of the present invention.For those of ordinary skill in the art, may be used also on the basis of the above description
To make other variations or changes in different ways.There is no necessity and possibility to exhaust all the enbodiments.It is all this
Made any modifications, equivalent replacements, and improvements etc., should be included in the claims in the present invention within the spirit and principle of invention
Protection scope within.
Claims (10)
1. a kind of expansion solves adhesive tape production method, which is characterized in that include the following steps：
S1. acrylic glue is synthesized：0-100 parts of butanone are added in flask, is warming up to 60-80 DEG C, butyl acrylate is added
0-30 parts, 0-30 parts of methyl acrylate, 0-30 parts of hydroxy-ethyl acrylate, 0-30 parts of 2- butanone, 0-30 parts of acrylic acid are added and cause
It 0.1-3 parts of agent azodiisobutyronitrile, reacts 120-360 minutes, is then slowly added to the initiator of equal quality part, the reaction was continued
120-240 minutes, etc. glue colos it is transparent after, cooling discharge；
S2. swelling agent is synthesized：By 0-10 parts of vinyltrimethoxysilane, 50-100 parts of vinyl methyl dimethoxysilane,
0-10 parts of phenyltrimethoxysila,e, 50-100 parts of water, emulsifier, are emulsified with high speed disperser, spare；In sodium bicarbonate
5% aqueous solution in be added organo-metallic catalyst 0.1-1 parts, be warming up to 60 DEG C, spare organic silicon emulsion be slowly added dropwise, instead
It answers 2 hours, then the solution of acquisition is removed water with freeze-drying, obtains powdered swelling agent；
S3. the step S2 and step S3 swelling agent synthesized and acrylic glue are uniformly mixed, initiator 0.1-0.5 parts of painting is added
Cloth adds release layer on substrate, is fabricated to adhesive tape.
2. expansion according to claim 1 solves adhesive tape production method, it is characterised in that：Emulsifier described in step S2 is
Alkyl alcohol ethoxylates, isomerous tridecanol polyoxyethylene, sulfosuccinic acid dicyclohexyl maleate sodium, alkylol polyoxyethylene one kind
Or it is several.
3. expansion according to claim 1 solves adhesive tape production method, it is characterised in that：High speed dispersion described in step S2
Machine speed is 2500rpm, and jitter time is 30 minutes.
4. expansion according to claim 1 solves adhesive tape production method, it is characterised in that：Organic metal described in step S2
Catalyst is organotin or organic titanium.
5. expansion according to claim 1-4 solves adhesive tape production method, it is characterised in that：Described in step S3
Initiator is the one or more of styrax, benzoin dimethylether, benzoin ethyl ether, benzoin isopropyl ether.
6. expansion according to claim 5 solves adhesive tape production method, it is characterised in that：Substrate described in step S3 is
PET, and 20-30 microns of coating thickness.
7. a kind of expansion solves adhesive tape, which is characterized in that including release layer, glue-line, substrate layer and functional layer, the substrate layer one
Face is coated with the glue-line, and the substrate layer another side is connected with functional layer, and the glue-line another side is connected with the release layer,
Expanded granular is set in the glue-line, the glue-line is acrylic glue-line, and the substrate layer is pet layer.
8. expansion according to claim 7 solves adhesive tape, it is characterised in that：The glue-line with a thickness of 20 μm -30 μm.
9. expansion according to claim 7 solves adhesive tape, it is characterised in that：When the glue-line is coated on the substrate layer
Temperature is room temperature.
10. solving adhesive tape according to the described in any item expansions of claim 7-9, it is characterised in that：The two sides of the substrate layer is equal
Equipped with frosted layer.
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| CN112175542A (en) * | 2020-10-15 | 2021-01-05 | 天津市中运国际工贸有限公司 | Low-temperature hot melt adhesive expansion adhesive tape and preparation method thereof |
| CN117720861A (en) * | 2023-12-21 | 2024-03-19 | 东莞帝亿特电子胶带有限公司 | Electronic adhesive tape and preparation method thereof |
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