CN108911932A - A kind of emulsifying liquid gunpowder for the production of micro- cigarette lead wet process - Google Patents
A kind of emulsifying liquid gunpowder for the production of micro- cigarette lead wet process Download PDFInfo
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- CN108911932A CN108911932A CN201811000685.4A CN201811000685A CN108911932A CN 108911932 A CN108911932 A CN 108911932A CN 201811000685 A CN201811000685 A CN 201811000685A CN 108911932 A CN108911932 A CN 108911932A
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- nitrostarch
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- C—CHEMISTRY; METALLURGY
- C06—EXPLOSIVES; MATCHES
- C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
- C06B29/00—Compositions containing an inorganic oxygen-halogen salt, e.g. chlorate, perchlorate
- C06B29/22—Compositions containing an inorganic oxygen-halogen salt, e.g. chlorate, perchlorate the salt being ammonium perchlorate
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- Inorganic Chemistry (AREA)
- Organic Chemistry (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
The invention discloses a kind of emulsifying liquid gunpowder for the production of micro- cigarette lead wet process.Feature is:Including potassium bichromate, ammonium perchlorate, ammonium dichromate, potassium chlorate, sibilant rale agent, nitrostarch, powdered carbon, glutinous rice flour, the weight fraction ratio of above-mentioned component is:Potassium bichromate 10-15 parts by weight;Ammonium perchlorate 15-30 parts by weight;Ammonium dichromate 20-40 parts by weight;Potassium chlorate 15-30 parts by weight;Sibilant rale agent 10-20 parts by weight;Nitrostarch 30-40 parts by weight;Powdered carbon 10-20 parts by weight;Glutinous rice flour 10-15 parts by weight.The advantages that there is the present invention system to draw simple process, and the dry powder system that changes draws method, and medicine-feeding uniform continuity is good, safe and reliable.
Description
Technical field
The invention belongs to pyrotechnics lead technology fields, more particularly, to a kind of emulsion for the production of micro- cigarette lead wet process
Body gunpowder.
Background technique
Fireworks, which is seted off too busy to get away lead and lighted, leads fire, so the quality of lead quality is directly linked making for firework display
With effect and economic benefit.There are many fireworks leads classification at present, mainly classify from using effect, lead fire draw, enclose draw, point
Fire draws, safety is drawn, commonly draw, micro- cigarette draws, draws slowly, drawing fastly etc., and lead processing method has Manual Wire and machining lead
Two kinds.And in the prior art, lead production is typically all to pass through flour/rice flour/paste after wrapping powder train by paper strip winding
It impregnates cementing, airing to be made, lead is linear in flexibility.But the powder train of existing processing lead is all using the dry of traditional handicraft
Powder production method, this lead production have the following defects:First is that make risk big for lead itself, it is easy to happen safe thing
Therefore dry mash is easy explosion of igniting of catching fire, and injures personal safety and property loss;Second is that dry powder production ignition charge loss is big, draw
Line is easy to fall or loose wire;Third is that during lead medicine-feeding pasting(Especially mechanical system is drawn)Medicine-feeding is difficult to uniformly, be easy to appear
Off-drug falls medicine, dissipates the problems such as paper, lead folding;Fourth is that traditional handicraft dry powder legal system is drawn, system draws workshop dirt dye greatly, pollution
Surrounding enviroment.Such as factors above, not only influence fireworks sets off using effect, but also also adds being produced into for enterprise
Originally and cost is seted off.
Summary of the invention
The purpose of the present invention is to provide a kind of emulsifying liquid gunpowder for the production of micro- cigarette lead wet process, by powder train tune
Emulsification colloidal liquid is made, not only can be convenient bar-shaped lead paper medicine-feeding bonding, avoid production lead during off-drug, fall
Medicine dissipates paper and during setting off the problem of intermediate cutoff, also reduces slurry and draws production process, saves cost, effectively improve
The safety of lead manufacturing process and dirt dye.
Realizing the technical solution of the object of the invention is:
A kind of emulsifying liquid gunpowder for the production of micro- cigarette lead wet process, it is characterised in that:Including potassium bichromate, ammonium perchlorate,
Ammonium dichromate, potassium chlorate, sibilant rale agent, nitrostarch, powdered carbon, glutinous rice flour, the weight fraction ratio of above-mentioned component are:Potassium bichromate
10-15 parts by weight;Ammonium perchlorate 15-30 parts by weight;Ammonium dichromate 20-40 parts by weight;Potassium chlorate 15-30 parts by weight;Sibilant rale agent
10-20 parts by weight;Nitrostarch 30-40 parts by weight;Powdered carbon 10-20 parts by weight;Glutinous rice flour 10-15 parts by weight.
A kind of emulsifying liquid gunpowder for the production of micro- cigarette lead wet process, it is characterised in that:The emulsifying liquid
The preferred weight fraction ratio of each component is in gunpowder:10 parts by weight of potassium bichromate;25 parts by weight of ammonium perchlorate;30 weight of ammonium dichromate
Measure part;20 parts by weight of potassium chlorate;15 parts by weight of sibilant rale agent;25 parts by weight of nitrostarch;15 parts by weight of powdered carbon;12 weight of glutinous rice flour
Part.
Compared with prior art, the present invention the remarkable advantage and beneficial effect that have are:
1, since the emulsifying liquid gunpowder wet process for using present composition preparation makes micro- cigarette lead, use is revolutionized
Traditional Method dry powder gunpowder makes the technique of lead, by the way that emulsifying liquid shape is made in the powder train of lead, during drawing system on
Prescription just, uniformly, cementing drying quickly, without intermediate off-drug circuit fire phenomenon, be conducive to firework display igniting, lead fire string combustion consistency
Raising and set off the improvement of safety;
2, using the wet process technique of emulsifying liquid gunpowder, dirt dye is to environment during thoroughly solving the medicine-feeding of lead powder train
The problem of pollution and harmful worker's health, reduces lead slurry and draws process, saves cost, reached lead manufacture craft
Environmental requirement, reduce lead production production process in security risk, improve firework product quality and firework display effect;
3, due to the micro- cigarette lead gunpowder of emulsifying liquid made of component compatibility of the present invention, lead is realized when setting off fireworks
The environmental protection standard of fire only a small amount of micro- cigarette after igniting, to reach the goal of the invention of the micro- cigarette of whole firework display.
The present invention is as the emulsifying liquid gunpowder for the production of micro- cigarette lead wet process, through inspection country fireworks and firecrackers product matter
Amount Supervision Test Center testing result see the table below 1:
According to GB 10631-2013《Fireworks and crackers safety and quality》,GB 11652-2012《Fireworks and firecrackers operation safety technology
Regulation》,GB/T16814.1-2010《The qualitative formulation of fireworks and firecrackers medicament component》,GB/T 21241-2007《Fireworks and firecrackers is prohibited
Limit the use of medicament qualitative checking method》,AQ 4104-2008《Fireworks and firecrackers pyrotechnic composition security performance and formulating method》, nonstandard side
Method 201703《Pyrotechnic composition smog percent of pass detection method》, associated specifications
Table 1:The report of national fireworks and firecrackers product quality supervision and inspection center fireworks safety performance detection.
NO:WJ20183058 client or individual:Pictograph fine work fireworks Manufacturing Co., Ltd of Liuyang City
。
Specific embodiment
Below in conjunction with specific embodiment, the present invention is described in further detail.
A kind of emulsifying liquid gunpowder for the production of micro- cigarette lead wet process of the invention, including potassium bichromate, ammonium perchlorate,
Ammonium dichromate, potassium chlorate, sibilant rale agent, nitrostarch, powdered carbon, glutinous rice flour, the weight fraction ratio of above-mentioned component are:Potassium bichromate
10-15 parts by weight;Ammonium perchlorate 15-30 parts by weight;Ammonium dichromate 20-40 parts by weight;Potassium chlorate 15-30 parts by weight;Sibilant rale agent
10-20 parts by weight;Nitrostarch 30-40 parts by weight;Powdered carbon 10-20 parts by weight;Glutinous rice flour 10-15 parts by weight.
A kind of emulsifying liquid gunpowder for the production of micro- cigarette lead wet process, it is characterised in that:The emulsifying liquid
The preferred weight fraction ratio of each component is in gunpowder:10 parts by weight of potassium bichromate;25 parts by weight of ammonium perchlorate;30 weight of ammonium dichromate
Measure part;20 parts by weight of potassium chlorate;15 parts by weight of sibilant rale agent;25 parts by weight of nitrostarch;15 parts by weight of powdered carbon;12 weight of glutinous rice flour
Part.
The preferred embodiment of emulsifying liquid gunpowder each component is in embodiment of the present invention:
Potassium bichromate K in the component of the present invention2CR2O7, ammonium perchlorate NH4CIO4, ammonium dichromate NH4CR2O7, potassium chlorate
KCIO3It is strong oxidizer, is synthesized for cordite, be alternatively arranged as smokeless reducing agent.
The nitrostarch is one kind of high nitrogen-containing, is both the medicament containing energy and smokeless fuel agent, to replace nitre
Sour fiber, alias are starch nitrate, the similar [C of chemical formula6H7O2(ONO2)r(OH)3-r] n, it is seen that its element composition very class
It is similar to cellulose nitrate, only the two molecular structure is different.It is not soluble in water, it is dissolved in acetone.It is yellowish(It is produced with reagent and is
Pure white)White powder or the small granule that is easy to crumb.There is no aroma and flavor.As NC, nitrostarch also has nitrogenous
Measure point of height.Nitrogen content is higher, and explosions are stronger.Nitrogen content reaches as high as 14.4%.Nitrogenous 12.2% nitrostarch is quick-fried
Speed is 4970m/s(ρ=1.6g/cm3);Power is greater than TNT, is 120%;Bursting point(Heat 5 seconds temperature exploded)183
℃.Prominent advantage is that sensitivity is low, and use is safe.Bulk gas, and smokeless, environmental protection can be generated after burning.Present invention selection
The high nitrogen type nitrostarch that the nitrogen content of nitrostarch is 13.4% ~ 14.4% makees compatibility component.
But above embodiment described in the invention is merely illustrative of the technical solution of the present invention and should not be understood as pair
The present invention imposes any restrictions.Those skilled in the art should understand that there is the present invention well known multiple material to substitute/replace
Change, without departing from essential meaning of the invention under the premise of, should all cover within the protection scope of the present invention.
Claims (2)
1. a kind of emulsifying liquid gunpowder for the production of micro- cigarette lead wet process, it is characterised in that:Including potassium bichromate, perchloric acid
Ammonium, ammonium dichromate, potassium chlorate, sibilant rale agent, nitrostarch, powdered carbon, glutinous rice flour, the weight fraction ratio of above-mentioned component are:
Potassium bichromate 10-15 parts by weight;Ammonium perchlorate 15-30 parts by weight;
Ammonium dichromate 20-40 parts by weight;Potassium chlorate 15-30 parts by weight;
Sibilant rale agent 10-20 parts by weight;Nitrostarch 30-40 parts by weight;
Powdered carbon 10-20 parts by weight;Glutinous rice flour 10-15 parts by weight.
2. a kind of emulsifying liquid gunpowder for the production of micro- cigarette lead wet process according to claim 1, it is characterised in that:Institute
Stating the preferred weight fraction ratio of each component in emulsifying liquid gunpowder is:
10 parts by weight of potassium bichromate;25 parts by weight of ammonium perchlorate;
30 parts by weight of ammonium dichromate;20 parts by weight of potassium chlorate;
15 parts by weight of sibilant rale agent;25 parts by weight of nitrostarch;
15 parts by weight of powdered carbon;12 parts by weight of glutinous rice flour.
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CN201811000685.4A CN108911932A (en) | 2018-08-30 | 2018-08-30 | A kind of emulsifying liquid gunpowder for the production of micro- cigarette lead wet process |
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CN201811000685.4A CN108911932A (en) | 2018-08-30 | 2018-08-30 | A kind of emulsifying liquid gunpowder for the production of micro- cigarette lead wet process |
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Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN87100780A (en) * | 1987-02-18 | 1988-10-05 | 萍乡市排上乡花炮厂 | A kind of preparation method of gluey powder train |
CN104058906A (en) * | 2014-06-27 | 2014-09-24 | 湖南飞宇新材料有限公司 | Sulfur-free ring stabilizing agent propellant powder |
CN105085128A (en) * | 2015-08-14 | 2015-11-25 | 苏飞 | Flying disc guiding line |
CN106397075A (en) * | 2016-08-31 | 2017-02-15 | 万载县建坤化工有限公司 | Safe blasting-fuse composition for firecracker |
-
2018
- 2018-08-30 CN CN201811000685.4A patent/CN108911932A/en active Pending
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN87100780A (en) * | 1987-02-18 | 1988-10-05 | 萍乡市排上乡花炮厂 | A kind of preparation method of gluey powder train |
CN104058906A (en) * | 2014-06-27 | 2014-09-24 | 湖南飞宇新材料有限公司 | Sulfur-free ring stabilizing agent propellant powder |
CN105085128A (en) * | 2015-08-14 | 2015-11-25 | 苏飞 | Flying disc guiding line |
CN106397075A (en) * | 2016-08-31 | 2017-02-15 | 万载县建坤化工有限公司 | Safe blasting-fuse composition for firecracker |
Non-Patent Citations (1)
Title |
---|
欧育湘: "《炸药学》", 31 January 2006, 北京理工大学出版社 * |
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