CN108911096A - A kind of cleanser and preparation method thereof of metallic pollution water body - Google Patents
A kind of cleanser and preparation method thereof of metallic pollution water body Download PDFInfo
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- CN108911096A CN108911096A CN201810883109.2A CN201810883109A CN108911096A CN 108911096 A CN108911096 A CN 108911096A CN 201810883109 A CN201810883109 A CN 201810883109A CN 108911096 A CN108911096 A CN 108911096A
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/58—Treatment of water, waste water, or sewage by removing specified dissolved compounds
- C02F1/62—Heavy metal compounds
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Abstract
The invention discloses a kind of cleansers of metallic pollution water body, including below according to the raw material of parts by weight:36-48 parts of jasmine flower extract, 23-30 parts of Radix Glycyrrhizae, 17-26 parts of garlic, reaches 11-19 parts of logical sequence wood, 11-19 parts of sepiolite, 6-10 parts of olibanum, 3-7 parts of caramel, recessed 1-5 parts of soil at silver-colored 24-31 parts of queen.Cleanser of the invention has significant removal effect to the beavy metal impurity in heavy metal-polluted water, especially for Cu2+、Hg2+、Cd2、+Ni2+Removal rate be even more to reach 98% or more;Formula is invented simultaneously rationally, has excellent purifying property under each component synergistic effect.
Description
Technical field
The present invention relates to environment protection field, the cleanser and preparation method thereof of specifically a kind of metallic pollution water body.
Background technique
Water pollution refers to that five major class such as raw water sensory properties, inorganic pollution, organic pollutant, microorganism, radioactivity refers to
Mark is abnormal, causes water-producing process control and effluent water quality control to be influenced to different extents, to water supply quality and people
The far water water quality condition that body health causes damages.
Wherein heavy metal-containing polluted water is to the very harmful of human body, heavy metal (mercury, lead, cadmium, nickel, selenium, arsenic, chromium, bismuth, vanadium,
Gold, platinum, silver etc.) pollution, they be mainly derived from mining and smelting process, trade waste, leather-making waste water, textile mills' waste water,
House refuse (such as battery, cosmetics).These heavy metals have direct physiological-toxicity to people, animal.
How treatment of heavy metal polluted water body has become a significant problem of human society.
Summary of the invention
The purpose of the present invention is to provide a kind of cleansers of metallic pollution water body, to solve to propose in above-mentioned background technique
The problem of.
To achieve the above object, the present invention provides the following technical solutions:
A kind of cleanser of metallic pollution water body, including below according to the raw material of parts by weight:Jasmine flower extract 36-48
Part, 23-30 parts of Radix Glycyrrhizae, 17-26 parts of garlic, reaches 11-19 parts of logical sequence wood, 11-19 parts of sepiolite, olibanum 6-10 at silver-colored 24-31 parts of queen
Part, 3-7 parts of caramel, recessed 1-5 parts of soil.
As a further solution of the present invention:Including below according to the raw material of parts by weight:39-40 parts of jasmine flower extract,
Silver-colored queen 26-29 parts, 25-28 parts of Radix Glycyrrhizae, 19-24 parts of garlic, up to 13-17 parts of logical sequence wood, 13-17 parts of sepiolite, 7-9 parts of olibanum,
4-6 parts of caramel, recessed 2-4 parts of soil.
As further scheme of the invention:Including below according to the raw material of parts by weight:42 parts of jasmine flower extract, silver
28 parts of queen, 26 parts of Radix Glycyrrhizae, 21 parts of garlic, up to 15 parts of logical sequence wood, 15 parts of sepiolite, 8 parts of olibanum, 5 parts of caramel, native 3 parts recessed.
The preparation method of the cleanser of the metallic pollution water body, includes the following steps:
1) silver-colored queen and Da Lun wood are weighed, is crushed, is sieved with 100 mesh sieve, put into pyroreaction kettle, quality times 4-6 is added
Distilled water, 56-78min is reacted in the environment of 105 DEG C -126 DEG C, obtains reaction solution after centrifuge separation;
2) merge jasmine flower extract and reaction solution, stirring is sufficiently mixed under normal temperature environment, obtains mixed liquor;
3) Radix Glycyrrhizae, garlic and olibanum are weighed, is crushed, 300 meshes are crossed, the water that quality is 2-4 times of three again is added, 220
It is distilled at a temperature of DEG C -270 DEG C, then water-oil separating obtains essential oil;
4) sepiolite and recessed soil are weighed, in 100 DEG C -120 DEG C of at a temperature of frying 13-18min, is then crushed the two,
200 meshes are crossed, mixed-powder is obtained;
5) merge mixed liquor and essential oil, be sufficiently mixed stirring and be added in processor for ultrasonic wave later, at 67 DEG C -74 DEG C
At a temperature of be ultrasonically treated 1-2h, during which addition mixed-powder in batches, ultrasonic treatment is stood under normal temperature environment after terminating
Semi-finished product liquid is made after filter residue by 36-42min;
6) weigh caramel, be added in semi-finished product liquid, be thoroughly mixed so that caramel dissolution to get.
As further scheme of the invention:Mixed-powder at least divides in the step 4) is added several times.
As further scheme of the invention:Mixed-powder point is at least added three times in the step 4).
Compared with prior art, the beneficial effects of the invention are as follows:
Cleanser of the invention has significant removal effect to the beavy metal impurity in heavy metal-polluted water, especially
For Cu2+、Hg2+、Cd2、+Ni2+Removal rate be even more to reach 98% or more;Formula is invented simultaneously rationally, is cooperateed with and is made in each component
Has excellent purifying property under.
Specific embodiment
The technical solution of the patent is explained in further detail With reference to embodiment.
Embodiment 1
A kind of cleanser of metallic pollution water body, including below according to the raw material of parts by weight:42 parts of jasmine flower extract, silver
28 parts of queen, 26 parts of Radix Glycyrrhizae, 21 parts of garlic, up to 15 parts of logical sequence wood, 15 parts of sepiolite, 8 parts of olibanum, 3 parts of caramel, native 3 parts recessed.
Wherein the preparation method of the jasmine flower extract is:Jasmine calyx is obtained into Jasmine after being dried
Dried flower calyx crushes, obtains Jasmine powder;Then ethanol solution is added in Jasmine powder to extract under normal temperature environment repeatedly,
Merge multiple extracting solution, is concentrated to give jasmine flower extract.
The preparation method of the cleanser of metallic pollution water body, includes the following steps in the present embodiment:
1) silver-colored queen and Da Lun wood are weighed, is crushed, is sieved with 100 mesh sieve, put into pyroreaction kettle, quality times 4 is added
Distilled water reacts 5min in the environment of 105 DEG C, obtains reaction solution after centrifuge separation;
2) merge jasmine flower extract and reaction solution, stirring is sufficiently mixed under normal temperature environment, obtains mixed liquor;
3) Radix Glycyrrhizae, garlic and olibanum are weighed, is crushed, 300 meshes are crossed, the water that quality is 3 times of three again is added, at 240 DEG C
At a temperature of distilled, then water-oil separating obtains essential oil;
4) sepiolite and recessed soil are weighed, in 110 DEG C of at a temperature of frying 15min, is then crushed the two, 200 meshes are crossed,
Obtain mixed-powder;
5) merge mixed liquor and essential oil, be sufficiently mixed stirring and be added in processor for ultrasonic wave later, in 70 DEG C of temperature
Lower ultrasonic treatment 1.5h, during which addition mixed-powder in four times, ultrasonic treatment are stood under normal temperature environment after terminating
Semi-finished product liquid is made after filter residue by 40min;
6) weigh caramel, be added in semi-finished product liquid, be thoroughly mixed so that caramel dissolution to get.
Embodiment 2
A kind of cleanser of metallic pollution water body, including below according to the raw material of parts by weight:36 parts of jasmine flower extract, silver
24 parts of queen, 23 parts of Radix Glycyrrhizae, 17 parts of garlic, up to 11 parts of logical sequence wood, 11 parts of sepiolite, 6 parts of olibanum, 4 parts of caramel, native 1 part recessed.
Wherein the preparation method of the jasmine flower extract is:Jasmine calyx is obtained into Jasmine after being dried
Dried flower calyx crushes, obtains Jasmine powder;Then ethanol solution is added in Jasmine powder to extract under normal temperature environment repeatedly,
Merge multiple extracting solution, is concentrated to give jasmine flower extract.
The preparation method of the cleanser of metallic pollution water body, includes the following steps in the present embodiment:
1) silver-colored queen and Da Lun wood are weighed, is crushed, is sieved with 100 mesh sieve, put into pyroreaction kettle, quality times 4 is added
Distilled water reacts 70min in the environment of 116 DEG C, obtains reaction solution after centrifuge separation;
2) merge jasmine flower extract and reaction solution, stirring is sufficiently mixed under normal temperature environment, obtains mixed liquor;
3) Radix Glycyrrhizae, garlic and olibanum are weighed, is crushed, 300 meshes are crossed, the water that quality is 2 times of three again is added, at 220 DEG C
At a temperature of distilled, then water-oil separating obtains essential oil;
4) sepiolite and recessed soil are weighed, in 100 DEG C of at a temperature of frying 13min, is then crushed the two, 200 meshes are crossed,
Obtain mixed-powder;
5) merge mixed liquor and essential oil, be sufficiently mixed stirring and be added in processor for ultrasonic wave later, in 67 DEG C of temperature
Lower ultrasonic treatment 1h, during which addition mixed-powder in three times, ultrasonic treatment stand 36min under normal temperature environment after terminating,
Semi-finished product liquid is made after filter residue;
6) weigh caramel, be added in semi-finished product liquid, be thoroughly mixed so that caramel dissolution to get.
Embodiment 3
A kind of cleanser of metallic pollution water body, including below according to the raw material of parts by weight:39 parts of jasmine flower extract, silver
26 parts of queen, 25 parts of Radix Glycyrrhizae, 19 parts of garlic, up to 13 parts of logical sequence wood, 13 parts of sepiolite, 7 parts of olibanum, 5 parts of caramel, native 2 parts recessed.
Wherein the preparation method of the jasmine flower extract is:Jasmine calyx is obtained into Jasmine after being dried
Dried flower calyx crushes, obtains Jasmine powder;Then ethanol solution is added in Jasmine powder to extract under normal temperature environment repeatedly,
Merge multiple extracting solution, is concentrated to give jasmine flower extract.
The preparation method of the cleanser of metallic pollution water body, includes the following steps in the present embodiment:
1) silver-colored queen and Da Lun wood are weighed, is crushed, is sieved with 100 mesh sieve, put into pyroreaction kettle, quality times 5 is added
Distilled water reacts 60min in the environment of 118 DEG C, obtains reaction solution after centrifuge separation;
2) merge jasmine flower extract and reaction solution, stirring is sufficiently mixed under normal temperature environment, obtains mixed liquor;
3) Radix Glycyrrhizae, garlic and olibanum are weighed, is crushed, 300 meshes are crossed, the water that quality is 3 times of three again is added, at 240 DEG C
At a temperature of distilled, then water-oil separating obtains essential oil;
4) sepiolite and recessed soil are weighed, in 110 DEG C of at a temperature of frying 15min, is then crushed the two, 200 meshes are crossed,
Obtain mixed-powder;
5) merge mixed liquor and essential oil, be sufficiently mixed stirring and be added in processor for ultrasonic wave later, in 70 DEG C of temperature
Lower ultrasonic treatment 1.5h, during which addition mixed-powder in five times, ultrasonic treatment are stood under normal temperature environment after terminating
Semi-finished product liquid is made after filter residue by 40min;
6) weigh caramel, be added in semi-finished product liquid, be thoroughly mixed so that caramel dissolution to get.
Embodiment 4
A kind of cleanser of metallic pollution water body, including below according to the raw material of parts by weight:44 parts of jasmine flower extract, silver
29 parts of queen, 28 parts of Radix Glycyrrhizae, 24 parts of garlic, up to 17 parts of logical sequence wood, 17 parts of sepiolite, 9 parts of olibanum, 6 parts of caramel, native 4 parts recessed.
Wherein the preparation method of the jasmine flower extract is:Jasmine calyx is obtained into Jasmine after being dried
Dried flower calyx crushes, obtains Jasmine powder;Then ethanol solution is added in Jasmine powder to extract under normal temperature environment repeatedly,
Merge multiple extracting solution, is concentrated to give jasmine flower extract.
The preparation method of the cleanser of metallic pollution water body, includes the following steps in the present embodiment:
1) silver-colored queen and Da Lun wood are weighed, is crushed, is sieved with 100 mesh sieve, put into pyroreaction kettle, quality times 6 is added
Distilled water reacts 75min in the environment of 120 DEG C, obtains reaction solution after centrifuge separation;
2) merge jasmine flower extract and reaction solution, stirring is sufficiently mixed under normal temperature environment, obtains mixed liquor;
3) Radix Glycyrrhizae, garlic and olibanum are weighed, is crushed, 300 meshes are crossed, the water that quality is 3 times of three again is added, at 240 DEG C
At a temperature of distilled, then water-oil separating obtains essential oil;
4) sepiolite and recessed soil are weighed, in 110 DEG C of at a temperature of frying 15min, is then crushed the two, 200 meshes are crossed,
Obtain mixed-powder;
5) merge mixed liquor and essential oil, be sufficiently mixed stirring and be added in processor for ultrasonic wave later, in 68 DEG C of temperature
Lower ultrasonic treatment 1.5h, during which addition mixed-powder in three times, ultrasonic treatment are stood under normal temperature environment after terminating
Semi-finished product liquid is made after filter residue by 40min;
6) weigh caramel, be added in semi-finished product liquid, be thoroughly mixed so that caramel dissolution to get.
Embodiment 5
A kind of cleanser of metallic pollution water body, including below according to the raw material of parts by weight:48 parts of jasmine flower extract, silver
31 parts of queen, 30 parts of Radix Glycyrrhizae, 26 parts of garlic, up to 19 parts of logical sequence wood, 19 parts of sepiolite, 10 parts of olibanum, 7 parts of caramel, native 5 parts recessed.
Wherein the preparation method of the jasmine flower extract is:Jasmine calyx is obtained into Jasmine after being dried
Dried flower calyx crushes, obtains Jasmine powder;Then ethanol solution is added in Jasmine powder to extract under normal temperature environment repeatedly,
Merge multiple extracting solution, is concentrated to give jasmine flower extract.
The preparation method of the cleanser of metallic pollution water body, includes the following steps in the present embodiment:
1) silver-colored queen and Da Lun wood are weighed, is crushed, is sieved with 100 mesh sieve, put into pyroreaction kettle, quality times 6 is added
Distilled water reacts 78min in the environment of 126 DEG C, obtains reaction solution after centrifuge separation;
2) merge jasmine flower extract and reaction solution, stirring is sufficiently mixed under normal temperature environment, obtains mixed liquor;
3) Radix Glycyrrhizae, garlic and olibanum are weighed, is crushed, 300 meshes are crossed, the water that quality is 4 times of three again is added, at 270 DEG C
At a temperature of distilled, then water-oil separating obtains essential oil;
4) sepiolite and recessed soil are weighed, in 120 DEG C of at a temperature of frying 18min, is then crushed the two, 200 meshes are crossed,
Obtain mixed-powder;
5) merge mixed liquor and essential oil, be sufficiently mixed stirring and be added in processor for ultrasonic wave later, in 74 DEG C of temperature
Lower ultrasonic treatment 2h, during which addition mixed-powder in four times, ultrasonic treatment stand 42min under normal temperature environment after terminating,
Semi-finished product liquid is made after filter residue;
6) weigh caramel, be added in semi-finished product liquid, be thoroughly mixed so that caramel dissolution to get.
Comparative example 1:Compared with Example 3, not argentiferous queen, other are same as Example 3.
Comparative example 2:Compared with Example 3, without up to logical sequence wood, other are same as Example 3.
Comparative example 3:Compared with Example 3, argentiferous queen and Da Lun be not wooden, other are same as Example 3.
Performance test
Cleanser corresponding to embodiment 3 and comparative example 1-3 is added separately to take from same heavy metal pollution water source
In four parts of polluted-waters out, the additional amount of cleanser is 50mg/l, will treated sewage, by filtration system or device,
Pressure filtration, heavy metal precipitation are retained by filter membrane or strainer, are then detected to heavy metal in filtrate, testing result such as following table
It is shown.
It can be seen that cleanser of the invention from the data in upper table embodiment 3 and have removal effect to beavy metal impurity,
Especially for Cu2+、Hg2+、Cd2、+Ni2+Removal rate be even more to reach 98% or more;It can in combination with the data of comparative example 1-3
To find out, the present invention is to play effect under each component synergistic effect.
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie
In the case where without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power
Benefit requires rather than above description limits, it is intended that all by what is fallen within the meaning and scope of the equivalent elements of the claims
Variation is included within the present invention.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped
Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should
It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
The other embodiments being understood that.
Claims (7)
1. a kind of cleanser of metallic pollution water body, which is characterized in that including below according to the raw material of parts by weight:Jasmine is extracted
36-48 parts of object, silver-colored 24-31 part of queen, 23-30 parts of Radix Glycyrrhizae, 17-26 parts of garlic, reach 11-19 parts of logical sequence wood, 11-19 parts of sepiolite,
6-10 parts of olibanum, 3-7 parts of caramel, recessed 1-5 parts of soil.
2. the cleanser of metallic pollution water body according to claim 1, which is characterized in that including below according to parts by weight
Raw material:39-44 parts of jasmine flower extract, silver-colored 26-29 part of queen, 25-28 parts of Radix Glycyrrhizae, 19-24 parts of garlic, reach 13-17 parts of logical sequence wood,
13-17 parts of sepiolite, 7-9 parts of olibanum, 4-6 parts of caramel, recessed 2-4 parts of soil.
3. the cleanser of metallic pollution water body according to claim 2, which is characterized in that including below according to parts by weight
Raw material:42 parts of jasmine flower extract, 26 parts of Radix Glycyrrhizae, 21 parts of garlic, reaches logical sequence wooden 15 parts, 15 parts of sepiolite, olibanum at silver-colored 28 parts of queen
8 parts, it is 5 parts of caramel, native 3 parts recessed.
4. the cleanser of metallic pollution water body according to claim 3, which is characterized in that the system of the jasmine flower extract
Preparation Method is:Jasmine calyx is obtained into dry jasmine flower calyx after being dried, crushes, obtains Jasmine powder;Then exist
Ethanol solution is added in Jasmine powder to extract under normal temperature environment repeatedly, merges multiple extracting solution, is concentrated to give Jasmine extraction
Object.
5. a kind of preparation method of the cleanser of the metallic pollution water body as described in claim 1-4 is any, which is characterized in that packet
Include following steps:
Silver-colored queen and Da Lun wood are weighed, is crushed, is sieved with 100 mesh sieve, put into pyroreaction kettle, the distillation of quality times 4-6 is added
Water reacts 56-78min in the environment of 105 DEG C -126 DEG C, obtains reaction solution after centrifuge separation;
Merge jasmine flower extract and reaction solution, stirring is sufficiently mixed under normal temperature environment, obtains mixed liquor;
3)Weigh Radix Glycyrrhizae, garlic and olibanum, crush, cross 300 meshes, it is 2-4 times of three of water again that quality, which is added, 220 DEG C-
It is distilled at a temperature of 270 DEG C, then water-oil separating obtains essential oil;
4)Sepiolite and recessed soil are weighed, in 100 DEG C -120 DEG C of at a temperature of frying 13-18min, is then crushed the two, crosses 200
Mesh obtains mixed-powder;
5)Merge mixed liquor and essential oil, is sufficiently mixed stirring and is added in processor for ultrasonic wave later, in 67 DEG C -74 DEG C of temperature
Lower ultrasonic treatment 1-2h, during which addition mixed-powder in batches, ultrasonic treatment stand 36- under normal temperature environment after terminating
Semi-finished product liquid is made after filter residue by 42min;
6)Weigh caramel, be added in semi-finished product liquid, be thoroughly mixed so that caramel dissolution to get.
6. the preparation method of the cleanser of metallic pollution water body according to claim 5, which is characterized in that the step 4)
Middle mixed-powder is added several times.
7. the preparation method of the cleanser of metallic pollution water body according to claim 5, which is characterized in that the step 4)
Middle mixed-powder point is at least added three times.
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Cited By (1)
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CN112108124A (en) * | 2020-09-26 | 2020-12-22 | 江西师范大学 | Water body iron and manganese efficient adsorbent and optimization method thereof |
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