CN108902355A - A kind of preparation method and products thereof of compound linseed microcapsules - Google Patents
A kind of preparation method and products thereof of compound linseed microcapsules Download PDFInfo
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- CN108902355A CN108902355A CN201810782873.0A CN201810782873A CN108902355A CN 108902355 A CN108902355 A CN 108902355A CN 201810782873 A CN201810782873 A CN 201810782873A CN 108902355 A CN108902355 A CN 108902355A
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/02—Other edible oils or fats, e.g. shortenings, cooking oils characterised by the production or working-up
- A23D9/04—Working-up
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/06—Preservation of finished products
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23P—SHAPING OR WORKING OF FOODSTUFFS, NOT FULLY COVERED BY A SINGLE OTHER SUBCLASS
- A23P10/00—Shaping or working of foodstuffs characterised by the products
- A23P10/30—Encapsulation of particles, e.g. foodstuff additives
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B5/00—Preserving by using additives, e.g. anti-oxidants
- C11B5/0092—Mixtures
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- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Polymers & Plastics (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Food Science & Technology (AREA)
- Organic Chemistry (AREA)
- Wood Science & Technology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Biochemistry (AREA)
- Medicinal Preparation (AREA)
- Medicines That Contain Protein Lipid Enzymes And Other Medicines (AREA)
- Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
Abstract
The present invention provides a kind of preparation methods of compound linseed microcapsules, include the following steps：(1) water phase is prepared：Wall material is dissolved into water, obtains water phase after being uniformly dissolved；(2) oily phase is prepared：Oily phase is obtained by being uniformly mixed at linseed oil, 50 DEG C of emulsifier；(3) it emulsifies：Oil is mutually poured into water phase, 20-30min is stirred at 40-70 DEG C, then emulsification pretreatment obtains emulsion oil-in-water；(4) homogeneous：Emulsion oil-in-water, stabilizer, antioxidant are subjected to mixing and homogeneous obtains homogenizing fluid.(5) microencapsulation：Homogenizing fluid is spray-dried to obtain compound linseed oil microcapsules.The present invention also provides the products that the preparation method obtains.Compound linseed microcapsules produced by the present invention embedding rate with higher and preferable inoxidizability, thermal stability, water solubility.
Description
Technical field
The present invention relates to a kind of preparation methods and products thereof of compound linseed microcapsules.
Background technique
Linseed oil (linseed oil or siritch), is the drying grease produced from linseed, is in yellow transparent shape,
With pleasant linseed oil fragrance.The oil content of linseed is about 35%-45%, contains a large amount of flax in linseed oil
Acid, it can be converted into the unsaturated fatty acids such as eicosapentaenoic acid (EPA), docosahexaenoic acid (DHA) in animal body,
With high nutritive value and different physiological roles, such as reducing blood lipid, blood pressure lowering, prevention and treatment cardiovascular and cerebrovascular disease, prevention glycosuria
Disease, rheumatism, rheumatoid, antitumor and other effects gradually obtain the concern of people in recent years.But the industrial application degree of linseed oil
It is not directly proportional to its nutritive value, China's linseed oil mainly with the source place of production squeeze it is reversal based on, potential nutritive value
It is not fully utilized.
Traditional grease has not easy to maintain, and oxidizable rotten in air, product quality reduces, and shelf life shortens, makes
The disadvantages of uneven is mixed with inconvenience and in food, linseed oil is also easily oxidized, and uses microcapsules technology can be with
Avoid the above drawback.Emblem capsule technique is one of new technology important in modern food industry technology, answering in the food industry
With mainly have three aspect：(1) solid powdering (edible oil and fat, flavors and fragrances) of liquid product；(2) food additives (tart flavour
Agent, sweetener, preservative, nutrition fortifier and physiological activator etc.)；(3) immobilization of enzyme or cell.Microencapsulation Method
There are physical method, chemical method and physico-chemical process.Wherein, the widest method of the technical application is spray drying process, packet
Include four-stage：Feed liquid atomization；Mist group mixes with heated drying media contact；The evaporation drying of droplet；Dry products and dry Jie
Matter separation.This method have it is easy to operate, easily realization automated production, at low cost, available wall material type is extensive, core material
The advantages that retention rate is high；
In recent years, microcapsules technology is commonly used to oil and fat product, the oil and fat product of high added value.Spray drying is that realization is micro-
Encapsulated important technical, the advantage is that:Dissolubility is high, emulsibility is good, film forming, drying property and low viscosity
Deng；Embedding medium appropriate can increase the oxidation resistance of grease, and the ingredient of thermal sensitivity and light sensitivity is prevented to be destroyed, barrier weight
The destruction of metal ion facilitates addition polyunsaturated fatty acid, improves the trophism and flavor stability of oil product.It is spraying
Seasoning is primarily adapted for use in lipophilic liquid material, and Drying Time of Vertical Spray Dryer is short, can be continuously produced, product from when long by
Heat, thus it is more suitable for many temperature-sensitive materials.
Chinese patent application CN201510362595.X discloses a kind of linseed oil microscapsule powder and preparation method thereof.
Contain emulsifier, wall material, antioxidant, filler etc. in the linseed oil microscapsule powder.The linseed oil microscapsule powder
Be using linseed oil as core material, with wall material, antioxidant, filler etc. by emulsifier it is fully emulsified, high-pressure homogeneous after, through spraying
The microscapsule powder that mist is dry and is formed.The embedding rate of linseed oil microscapsule powder made from the invention is not high, inoxidizability,
Thermal stability, water solubility are bad.
Summary of the invention
It is obtained compound the technical problem to be solved in the present invention is to provide a kind of preparation method of compound linseed microcapsules
Flaxseed gum microcapsules embedding rate with higher and preferable inoxidizability, thermal stability, water solubility.
In order to solve the above technical problems, the technical scheme is that：
A kind of compound linseed microcapsules, include the following steps：
(1) water phase is prepared：Wall material is dissolved into water, obtains water phase after being uniformly dissolved；
(2) oily phase is prepared：Oily phase is obtained by being uniformly mixed at linseed oil, 50 DEG C of emulsifier；
(3) it emulsifies：Oil is mutually poured into water phase, 20-30min is stirred at 40-70 DEG C, then emulsification pretreatment obtains water packet
Water emulsion；
(4) homogeneous：Emulsion oil-in-water, stabilizer, antioxidant are subjected to mixing and homogeneous obtains homogenizing fluid.
(5) microencapsulation：Homogenizing fluid is spray-dried to obtain compound linseed oil microcapsules.
Further, according to parts by weight, linseed oil 20-30 parts, 60-75 parts of wall material, 0.25-0.35 parts of stabilizer,
Emulsifier 0.01-0.3%, antioxidant 0.15-0.25%.
Further, wall material of the present invention is the mixture of soybean protein isolate, maltodextrin, oligomeric maltose.
Further, soybean protein isolate of the present invention, maltodextrin, oligomeric maltose weight ratio be 1:(6-7):
1。
Further, stabilizer of the present invention is the mixture of maltodextrin and polydextrose.
Further, emulsifier of the present invention be casein sodium, single diglycerine fatty acid ester, soybean lecithin it is mixed
Close object.
Further, antioxidant of the present invention is the mixture of multi-vitamins and folic acid.
Further, multi-vitamins of the present invention include vitamin E, vitamin C, niacinamide, vitamin E, pantothenic acid
Calcium, vitamin B1, vitamin B2, vitamin B6, vitamin B12, vitamin A, vitamine D3.
Further, the emulsification pretreatment in the step (3) carries out in emulsification pretreatment machine, and the time of emulsification pretreatment is
5min, the speed of emulsification pretreatment are 6000-10000r/min；Homogeneous in the step (4) carries out in homogenizer, homogeneous
Time is 30min, and the pressure of homogeneous is 35-40MPa；The inlet air temperature of spray drying in the step (5) is 175-185
DEG C, leaving air temp is 65-75 DEG C.
The present invention also provides the products that above-mentioned preparation method obtains.
Compared with prior art, the invention has the advantages that：
1) present invention is using casein sodium, single diglycerine fatty acid ester, soybean lecithin as emulsifier, with the life of compound dimension
Element, folic acid as antioxidant, using soybean protein isolate, maltodextrin and oligoisomaltose as wall material, with maltodextrin,
Polydextrose is stabilizer, successfully converts the powdered microcapsules of solid grease for the linseed oil of liquid, effectively prevents
Linseed oil is oxidized, and extends storage period and the shelf life of linseed oil, and without trans-fatty acid, will not cause to hurt to human body
Evil, microcapsules obtained embedding rate with higher and preferable inoxidizability, thermal stability, water solubility.
2) addition of antioxidant, emulsifier and stabilizer has promotion fetal brain, visual acuity, control in the present invention
Pregnancy period weight processed, balanced nutrients enhance the healthcare functions such as pregnant and lying-in women and infant immunity, resistance, add different antioxygens
Agent, emulsifier and stabilizer can also play different effects, can be applied in different crowds.
Specific embodiment
Below in conjunction with specific embodiment, the present invention will be described in detail, herein illustrative embodiments and their description of the invention
For explaining the present invention, but it is not as a limitation of the invention.
Embodiment 1-4
Compound linseed microcapsules are prepared according to the parts by weight listed in table 1：
| Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | |
| Linseed oil | 20 | 30 | 25 | 26 |
| Wall material | 60 | 75 | 70 | 65 |
| Stabilizer | 0.3 | 0.25 | 0.35 | 0.28 |
| Emulsifier | 0.2 | 0.01 | 0.3 | 0.1 |
| Antioxidant | 0.2 | 0.15 | 0.25 | 0.24 |
Table 1
Wherein, it is 1 that the wall material in embodiment 1 and embodiment 3, which is weight ratio,:7:1 soybean protein isolate, maltodextrin,
The mixture of oligomeric maltose, it is 1 that the wall material in embodiment 2 and embodiment 4, which is weight ratio,:6:1 soybean protein isolate, malt
The mixture of dextrin, oligomeric maltose；Stabilizer in embodiment 1-4 is the mixture of maltodextrin and polydextrose；Implement
Emulsifier in example 1-4 is the mixture of casein sodium, single diglycerine fatty acid ester, soybean lecithin；In embodiment 1-4
Antioxidant is the mixture of multi-vitamins and folic acid, and multi-vitamins include vitamin E, vitamin C, niacinamide, dimension life
Plain E, calcium pantothenate, vitamin B1, vitamin B2, vitamin B6, vitamin B12, vitamin A, vitamine D3.
The preparation method of embodiment 1 includes the following steps：
(1) water phase is prepared：Wall material is dissolved into water, obtains water phase after being uniformly dissolved；
(2) oily phase is prepared：Oily phase is obtained by being uniformly mixed at linseed oil, 50 DEG C of emulsifier；
(3) it emulsifies：Oil is mutually poured into water phase, 30min is stirred at 50 DEG C, then the 10000r/ in emulsification pretreatment machine
Emulsification pretreatment 30min obtains emulsion oil-in-water under min speed, and solid concentration is 25% or so；
(4) homogeneous：It will be mixed simultaneously under emulsion oil-in-water, stabilizer, antioxidant 40MPa pressure in homogenizer
Homogeneous 30min obtains homogenizing fluid.
(5) microencapsulation：Homogenizing fluid is spray-dried to obtain compound linseed oil microcapsules, the air inlet of spray drying
Temperature is 175 DEG C, and leaving air temp is 70 DEG C.
The preparation method of embodiment 2 is unlike the first embodiment：The temperature stirred in step (3) is 60 DEG C, stirring when
Between be 25min；The speed of emulsification pretreatment is 10000r/min；The pressure of homogeneous is 40MPa in the step (4)；The step
(5) inlet air temperature of the spray drying in is 180 DEG C, and leaving air temp is 65 DEG C.
The preparation method of embodiment 3 is unlike the first embodiment：The temperature stirred in step (3) is 70 DEG C, stirring when
Between be 20min；The speed of emulsification pretreatment is 6000r/min；The pressure of homogeneous is 35MPa in the step (4)；The step
(5) inlet air temperature of the spray drying in is 185 DEG C, and leaving air temp is 75 DEG C.
The preparation method of embodiment 4 is unlike the first embodiment：The temperature stirred in step (3) is 40 DEG C, stirring when
Between be 28min；The speed of emulsification pretreatment is 9000r/min；The pressure of homogeneous is 36MPa in the step (4)；The step
(5) inlet air temperature of the spray drying in is 183 DEG C, and leaving air temp is 72 DEG C.
Comparative Examples 1
It does not include maltodextrin in wall material, other components and preparation method are same as Example 1.
Comparative Examples 2
It does not include oligomeric maltose in wall material, other components and preparation method are same as Example 1.
Comparative Examples 3
It does not include soybean protein isolate in wall material, other components and preparation method are same as Example 1.
Comparative Examples 4
It does not include polydextrose in stabilizer, other components and preparation method are same as Example 1.
Comparative Examples 5
It does not include multi-vitamins in antioxidant, other components and preparation method are same as Example 1.
Comparative example
Comparative example is the embodiment 1 of the Chinese invention application No. is CN201510362595.X.
Experimental example one：Inoxidizability test
Test method is：It will be stored 30 days at 60 DEG C of linseed oil capsule, measure linseed oil in linseed oil microcapsules
Peroxide value difference, peroxide value before peroxide value-storage, the smaller table of peroxide value difference after peroxide value difference=storage
Bright inoxidizability is better.Test result is as shown in table 2：
| Peroxide value difference (meq/kg) | |
| Embodiment 1 | 4.32 |
| Embodiment 2 | 4.43 |
| Embodiment 3 | 4.38 |
| Embodiment 4 | 4.46 |
| Comparative Examples 1 | 4.85 |
| Comparative Examples 2 | 4.40 |
| Comparative Examples 3 | 4.39 |
| Comparative Examples 4 | 4.45 |
| Comparative Examples 5 | 10.61 |
| Comparative example | 10.27 |
Table 2
As can be seen from Table 2, the peroxide value difference of 1-4 of the embodiment of the present invention is significantly less than comparative example, shows this hair
Bright to have preferable inoxidizability, wherein the inoxidizability of embodiment 1 is best.The constituent part of Comparative Examples 1-5 and implementation
Example 1 is different, and wherein the peroxide value difference of Comparative Examples 1 is increased, and illustrates the maltodextrin in wall material to inoxidizability
It can play the role of certain raising；The peroxide value difference of Comparative Examples 5 increases very much, illustrates multi-vitamins to antioxygen
Change performance and plays the role of very big raising；The peroxide value difference and embodiment 1-4 of remaining Comparative Examples maintain an equal level, and illustrate remaining
Component does not influence inoxidizability substantially.
Experimental example two：Heat stability testing
Test method is：Using TGA/SDTA851 type thermogravimetric analyzer, nitrogen flow 20ml/min, heating rate is
15 DEG C/min, 680 DEG C are heated to from room temperature, the thermogravimetric curve of linseed oil microcapsules is measured, obtains linseed oil microcapsules
Initial temperature is thermally decomposed, initial temperature is higher shows that thermal stability is better for thermal decomposition.Test result is as shown in table 3：
| It thermally decomposes initial temperature (DEG C) | |
| Embodiment 1 | 190.9 |
| Embodiment 2 | 190.5 |
| Embodiment 3 | 190.1 |
| Embodiment 4 | 190.6 |
| Comparative Examples 1 | 182.8 |
| Comparative Examples 2 | 183.5 |
| Comparative Examples 3 | 190.7 |
| Comparative Examples 4 | 186.4 |
| Comparative Examples 5 | 190.3 |
| Comparative example | 181.0 |
Table 3
As can be seen from Table 3, the thermal decomposition initial temperature of 1-4 of the embodiment of the present invention shows this obviously higher than comparative example
Invention has preferable thermal stability, and wherein the thermal stability of embodiment 1 is best.The constituent part and reality of Comparative Examples 1-5
Apply that example 1 is different, wherein the thermal decomposition initial temperature of Comparative Examples 1,2 reduces many, illustrates maltodextrin in wall material, oligomeric
Maltose plays the role of good raising to thermal stability；The thermal decomposition initial temperature of Comparative Examples 4 reduces, and says
Bright polydextrose can also play the role of certain raising to thermal stability；The thermal decomposition initial temperature and reality of remaining Comparative Examples
It applies a 1-4 to maintain an equal level, illustrates that remaining component does not influence thermal stability substantially.
Experimental example three：Embedding rate test
Test method is：Oil content is measured according to GB/T 5512-2008 using soxhlet extraction methods, is calculated according to the following formula
Embedding rate：Embedding rate=(oil content-surface oil content)/oil content × 100%.Test result is as shown in table 4：
Table 4
As can be seen from Table 4, the embedding rate of 1-4 of the embodiment of the present invention is obviously higher than comparative example, wherein the packet of embodiment 1
Bury rate highest.The constituent part of Comparative Examples 1-5 is different from embodiment 1, and wherein the embedding rate of Comparative Examples 1,3 reduces
Much, illustrate that the maltodextrin in wall material, soybean protein isolate can play the role of good raising to embedding rate；Remaining reference is real
The embedding rate and embodiment 1-4 for applying example maintain an equal level, and illustrate that remaining component does not influence embedding rate substantially.
Experimental example four：Water solubility test
Test method is：Microcapsules are weighed in beaker, dissolve microcapsules with distilled water at 30 DEG C, are moved into centrifuge tube,
It is centrifuged 10min under 4000r/min speed, precipitating is placed in evaporating dish, drying to constant weight at 100 DEG C, calculates solubility, molten
Xie Du=[1- (W2-W1)/(1-X) W] × 100%, wherein W2For evaporating dish and precipitating gross mass, W1For evaporating dish quality, X
For the moisture content of microcapsules, W is the quality of microcapsules, and solubility shows more greatly water-soluble better.Test result is as shown in table 5：
| Solubility (%) | |
| Embodiment 1 | 57.09 |
| Embodiment 2 | 57.05 |
| Embodiment 3 | 57.00 |
| Embodiment 4 | 57.04 |
| Comparative Examples 1 | 50.26 |
| Comparative Examples 2 | 57.03 |
| Comparative Examples 3 | 50.18 |
| Comparative Examples 4 | 57.07 |
| Comparative Examples 5 | 57.02 |
| Comparative example | 43.51 |
Table 5
As can be seen from Table 5, the solubility of 1-4 of the embodiment of the present invention shows that the present invention has obviously higher than comparative example
Preferable water-soluble, wherein the water solubility of embodiment 1 is best.The constituent part of Comparative Examples 1-5 is different from embodiment 1,
The solubility of middle Comparative Examples 1,3 reduces the maltodextrin much illustrated in wall material, soybean protein isolate to water soluble characteristic
Play the role of good raising；The solubility and embodiment 1-4 of remaining Comparative Examples maintain an equal level, and illustrate remaining component to water solubility
Substantially it does not influence.
The above-described embodiments merely illustrate the principles and effects of the present invention, and is not intended to limit the present invention.It is any ripe
The personage for knowing this technology all without departing from the spirit and scope of the present invention, carries out modifications and changes to above-described embodiment.Cause
This, institute is complete without departing from the spirit and technical ideas disclosed in the present invention by those of ordinary skill in the art such as
At all equivalent modifications or change, should be covered by the claims of the present invention.
Claims (10)
1. a kind of preparation method of compound linseed microcapsules, it is characterised in that：Include the following steps：
(1) water phase is prepared：Wall material is dissolved into water, obtains water phase after being uniformly dissolved；
(2) oily phase is prepared：Oily phase is obtained by being uniformly mixed at linseed oil, 50 DEG C of emulsifier；
(3) it emulsifies：Oil is mutually poured into water phase, 20-30min is stirred at 40-70 DEG C, then emulsification pretreatment obtains oil-in-water type
Lotion；
(4) homogeneous：Emulsion oil-in-water, stabilizer, antioxidant are subjected to mixing and homogeneous obtains homogenizing fluid.
(5) microencapsulation：Homogenizing fluid is spray-dried to obtain compound linseed oil microcapsules.
2. a kind of compound linseed microcapsules according to claim 1, it is characterised in that：According to parts by weight, linseed
It is 20-30 parts oily, 60-75 parts of wall material, 0.25-0.35 parts of stabilizer, emulsifier 0.01-0.3%, antioxidant 0.15-0.25%.
3. a kind of compound linseed microcapsules according to claim 2, it is characterised in that：The wall material is soybean separation protein
The mixture of white, maltodextrin, oligomeric maltose.
4. a kind of compound linseed microcapsules according to claim 3, it is characterised in that：The soybean protein isolate, wheat
Bud dextrin, oligomeric maltose weight ratio be 1:(6-7):1.
5. a kind of compound linseed microcapsules according to claim 4, it is characterised in that：The stabilizer is maltodextrin
With the mixture of polydextrose.
6. a kind of compound linseed microcapsules according to claim 5, it is characterised in that：The emulsifier is caseinic acid
Sodium, single diglycerine fatty acid ester, soybean lecithin mixture.
7. a kind of compound linseed microcapsules according to claim 6, it is characterised in that：The antioxidant is compound dimension
The mixture of raw element and folic acid.
8. a kind of preparation method of compound linseed microcapsules according to claim 7 any one, it is characterised in that：Institute
Stating multi-vitamins includes vitamin E, vitamin C, niacinamide, vitamin E, calcium pantothenate, vitamin B1, vitamin B2, dimension life
Plain B6, vitamin B12, vitamin A, vitamine D3.
9. a kind of preparation method of compound linseed microcapsules according to claim 8, it is characterised in that：The step
(2) emulsification pretreatment in carries out in emulsification pretreatment machine, and the time of emulsification pretreatment is 5min, and the speed of emulsification pretreatment is 6000-
10000r/min；Homogeneous in the step (3) carries out in homogenizer, and the time of homogeneous is 30min, and the pressure of homogeneous is
35-40MPa；The inlet air temperature of spray drying in the step (4) is 175-185 DEG C, and leaving air temp is 65-75 DEG C.
10. the product that preparation method described in -9 any one obtains according to claim 1.
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109805337A (en) * | 2018-12-24 | 2019-05-28 | 中国农业科学院农产品加工研究所 | A kind of citrus flavors additive and preparation method thereof containing polymethoxyflavone |
| CN111466448A (en) * | 2020-04-14 | 2020-07-31 | 劲牌持正堂药业有限公司 | Preparation method of high-water-solubility fructus cannabis extract |
| CN113142548A (en) * | 2021-03-31 | 2021-07-23 | 广州金酮特殊医用食品有限公司 | Microcapsule powder and lactating mothers nutritional composition containing same |
| CN113598397A (en) * | 2021-08-05 | 2021-11-05 | 仙乐健康科技股份有限公司 | Microencapsulated encapsulated particles and method for their preparation |
| CN114947043A (en) * | 2022-06-18 | 2022-08-30 | 海南舒普生物科技有限公司 | Preparation method of thermostable and photostable phycocyanin |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104322712A (en) * | 2014-09-22 | 2015-02-04 | 杭州卡侬生物科技有限公司 | Linseed oil stabilization emulsion and preparation method thereof |
| CN104544092A (en) * | 2015-01-29 | 2015-04-29 | 王维义 | Linseed oil microcapsule powder and preparation process thereof |
| CN105029409A (en) * | 2015-06-24 | 2015-11-11 | 芦冰 | Flaxseed oil microcapsule powder and preparation method thereof |
| US20160175432A1 (en) * | 2014-06-18 | 2016-06-23 | Institute Of Process Engineering, Chinese Academy Of Sciences | An oil-in-water emulsion containing no surfactant and use thereof |
-
2018
- 2018-07-17 CN CN201810782873.0A patent/CN108902355A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20160175432A1 (en) * | 2014-06-18 | 2016-06-23 | Institute Of Process Engineering, Chinese Academy Of Sciences | An oil-in-water emulsion containing no surfactant and use thereof |
| CN104322712A (en) * | 2014-09-22 | 2015-02-04 | 杭州卡侬生物科技有限公司 | Linseed oil stabilization emulsion and preparation method thereof |
| CN104544092A (en) * | 2015-01-29 | 2015-04-29 | 王维义 | Linseed oil microcapsule powder and preparation process thereof |
| CN105029409A (en) * | 2015-06-24 | 2015-11-11 | 芦冰 | Flaxseed oil microcapsule powder and preparation method thereof |
Non-Patent Citations (5)
| Title |
|---|
| 吉鹤立: "《中国食品添加剂及配料使用手册》", 30 June 2016, 中国质检出版社 * |
| 张志明，等: "不同填充剂对虾青素微囊粉品质影响的研究", 《食品工业》 * |
| 王明锋，等: "《烟用香料控制释放技术及其应用》", 31 May 2016, 西南交通大学出版社 * |
| 董增，等: "茶油微胶囊化制备及其特性研究", 《宿州学院学报》 * |
| 陈智斌，等: "《食品加工学》", 31 August 2012, 哈尔滨工业大学出版社 * |
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