CN108892389A - A kind of high strength glass fiber preparation process - Google Patents
A kind of high strength glass fiber preparation process Download PDFInfo
- Publication number
- CN108892389A CN108892389A CN201811131648.7A CN201811131648A CN108892389A CN 108892389 A CN108892389 A CN 108892389A CN 201811131648 A CN201811131648 A CN 201811131648A CN 108892389 A CN108892389 A CN 108892389A
- Authority
- CN
- China
- Prior art keywords
- glass fibre
- high strength
- preparation process
- glass
- fiber preparation
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C13/00—Fibre or filament compositions
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B37/00—Manufacture or treatment of flakes, fibres, or filaments from softened glass, minerals, or slags
- C03B37/01—Manufacture of glass fibres or filaments
- C03B37/02—Manufacture of glass fibres or filaments by drawing or extruding, e.g. direct drawing of molten glass from nozzles; Cooling fins therefor
- C03B37/022—Manufacture of glass fibres or filaments by drawing or extruding, e.g. direct drawing of molten glass from nozzles; Cooling fins therefor from molten glass in which the resultant product consists of different sorts of glass or is characterised by shape, e.g. hollow fibres, undulated fibres, fibres presenting a rough surface
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C1/00—Ingredients generally applicable to manufacture of glasses, glazes, or vitreous enamels
- C03C1/002—Use of waste materials, e.g. slags
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C1/00—Ingredients generally applicable to manufacture of glasses, glazes, or vitreous enamels
- C03C1/004—Refining agents
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Manufacturing & Machinery (AREA)
- Surface Treatment Of Glass Fibres Or Filaments (AREA)
Abstract
The present invention relates to a kind of fiber more particularly to a kind of glass fibres.A kind of high strength glass fiber preparation process, includes the following steps：1. the weighing feeding equipment system that the raw material that cullet are major ingredient are controlled by computer Weighting and Controlling System is entered mixing machine, above-mentioned material is mixed into batch by the mixing machine；2. wire drawing obtains glass fibre after batch is melted；3. 4. glass fibre, which is soaked into pickling in acid, carries out warm water washing for the glass fibre after immersion, the warm water temperature is between 50 °~60 °；5. carrying out thermal finalization, production is completed.The present invention has produced the similar glass fibre of performance in the case where unexpectedly may be cheap, and post-consumer glass is largely utilized, and turns waste into wealth, and has good economic value and the value of environmental protection.
Description
Technical field
The present invention relates to a kind of fiber more particularly to a kind of glass fibres.
Background technique
Glass fibre is due to characteristics such as its high temperature resistants, and suitable for the various occasions for needing heat-insulation and heat-preservation, dosage is very big, then
How a kind of as far as possible cheap glass fibre is produced, and exactly inventor will solve the problems, such as.
Summary of the invention
The present invention solves the above problem, provides a kind of manufacture craft of most cheap glass fibre, particular technique
Scheme is as follows：
A kind of high strength glass fiber preparation process, includes the following steps：
1. the weighing feeding equipment system that the raw material that cullet are major ingredient are controlled by computer Weighting and Controlling System
Into mixing machine, above-mentioned material is mixed into batch by the mixing machine；
2. wire drawing obtains glass fibre after batch is melted；
3. glass fibre is soaked into pickling in acid；
4. the glass fibre after immersion is carried out warm water washing, the warm water temperature is between 50 °~60 °；
5. carrying out thermal finalization, production is completed.
The thinking set that conventional fiber glass uses pure quartz sand is broken using waste and old cullet, so that more honest and clean
Valence, pickling are to wash away the part contained in post-consumer glass to destroy the substance of fibre property, facilitate thermal finalization.
Preferably, it includes following material that the raw material, which are every 100 kilograms of ingredient,：Cullet 70.53KG, soda ash
13.10KG, feldspar 3.13KG, borax 5.04KG, sodium sulphate 2.67KG, aluminium compound 3.55KG, barium compound 1.33KG, decoloration
The total 0.65KG of agent, the sodium sulphate are clarifying agent, and borax is fluxing agent, and quartz sand can be substituted by cullet fragment.
Preferably, the batch puts into the melting furnaces that thermal autocontrol system controls by feeding apparatus, melting furnaces are produced
Raw glass melts enter work pool by dog-hole, and the work pool is controlled by fuel gas temperature automatic control system；Its temperature
Control is between 1460 °~1467 °, then by the glass precursor solution of melting by being controlled by electrical heating temperature automatic control system
Feeder channel is sent into wire drawing machine and carries out wire drawing.
Preferably, the pickling is：The phosphorus molybdenum acid solution of 0.6mol/L and glass fibre are added to polytetrafluoroethyl-ne
It in alkene reaction kettle, is kept stirring 1 hour with 180 ° of temperature, then cleans glass fibre, 2 hours are stood at a temperature of 100 ° and is done
It is dry.
Preferably, the thermal finalization, by carrying out in continuous heat-treating drier, the heat setting temperature is 850~900
DEG C, setting time is 1.5 hours.
The present invention has produced the similar glass fibre of performance in the case where unexpectedly may be cheap, and is largely utilized useless
Old glass, turns waste into wealth, and has good economic value and the value of environmental protection.
Specific embodiment
Embodiment 1
The embodiment of the present invention 1 is described in further detail below：
A kind of high strength glass fiber preparation process, includes the following steps：
1. the weighing feeding equipment system that the raw material that cullet are major ingredient are controlled by computer Weighting and Controlling System
Into mixing machine, above-mentioned material is mixed into batch by the mixing machine；
2. wire drawing obtains glass fibre after batch is melted；
3. glass fibre is soaked into pickling in acid；
4. the glass fibre after immersion is carried out warm water washing, the warm water temperature is between 50 °~60 °；
5. carrying out thermal finalization, production is completed.
The raw material are that every 100 kilograms of ingredient includes following material：Cullet 70.53KG, soda ash 13.10KG, length
Stone 3.13KG, borax 5.04KG, sodium sulphate 2.67KG, aluminium compound 3.55KG, barium compound 1.33KG, decolorising agent are total
0.65KG, the sodium sulphate are clarifying agent, and borax is fluxing agent, and quartz sand can be substituted by cullet fragment.The batch is logical
The melting furnaces of feeding apparatus investment thermal autocontrol system control are crossed, the glass melts that melting furnaces generate enter work by dog-hole
Pond, the work pool are controlled by fuel gas temperature automatic control system；Its temperature controls between 1460 °~1467 °, then will melt
The glass precursor solution melted is sent into wire drawing machine by the feeder channel controlled by electrical heating temperature automatic control system and carries out wire drawing.It is described
Pickling is：The phosphorus molybdenum acid solution of 0.6mol/L and glass fibre are added in ptfe autoclave, with 180 ° of temperature
It keeps stirring 1 hour, then cleans glass fibre, drying in 2 hours is stood at a temperature of 100 °.The thermal finalization passes through continuous
It is carried out in formula heat-treatment furnace, the heat setting temperature is 850~900 DEG C, and setting time is 1.5 hours.
It is emphasized that:The above is only presently preferred embodiments of the present invention, not do in any form to the present invention
Limitation, any simple modification, equivalent change and modification that above embodiments are done according to the technical essence of the invention,
It still falls within protection category of the present invention.
Claims (5)
1. a kind of high strength glass fiber preparation process, which is characterized in that include the following steps：
1. the raw material that cullet are major ingredient are entered by the weighing feeding equipment system that computer Weighting and Controlling System controls
Above-mentioned material is mixed into batch by mixing machine, the mixing machine；
2. wire drawing obtains glass fibre after batch is melted；
3. glass fibre is soaked into pickling in acid；
4. the glass fibre after immersion is carried out warm water washing, the warm water temperature is between 50 °~60 °；
5. carrying out thermal finalization, production is completed.
2. a kind of high strength glass fiber preparation process according to claim 1, which is characterized in that the raw material are every
100 kilograms of ingredient includes following material：Cullet 70.53KG, soda ash 13.10KG, feldspar 3.13KG, borax 5.04KG, sulphur
Sour sodium 2.67KG, aluminium compound 3.55KG, barium compound 1.33KG, the total 0.65KG of decolorising agent, the sodium sulphate are clarifying agent, boron
Sand is fluxing agent, and quartz sand can be substituted by cullet fragment.
3. a kind of high strength glass fiber preparation process according to claim 1, which is characterized in that the batch passes through
Feeding apparatus puts into the melting furnaces of thermal autocontrol system control, and the glass melts that melting furnaces generate enter work by dog-hole
Pond, the work pool are controlled by fuel gas temperature automatic control system；Its temperature controls between 1460 °~1467 °, then will melt
The glass precursor solution melted is sent into wire drawing machine by the feeder channel controlled by electrical heating temperature automatic control system and carries out wire drawing.
4. a kind of high strength glass fiber preparation process according to claim 1, which is characterized in that the pickling is：It will
The phosphorus molybdenum acid solution and glass fibre of 0.6mol/L is added in ptfe autoclave, keeps stirring 1 with 180 ° of temperature
Hour, then glass fibre is cleaned, drying in 2 hours is stood at a temperature of 100 °.
5. a kind of high strength glass fiber preparation process according to claim 1, which is characterized in that the thermal finalization passes through
It is carried out in continuous heat-treating drier, the heat setting temperature is 850~900 DEG C, and setting time is 1.5 hours.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811131648.7A CN108892389A (en) | 2018-09-27 | 2018-09-27 | A kind of high strength glass fiber preparation process |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811131648.7A CN108892389A (en) | 2018-09-27 | 2018-09-27 | A kind of high strength glass fiber preparation process |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108892389A true CN108892389A (en) | 2018-11-27 |
Family
ID=64360396
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811131648.7A Withdrawn CN108892389A (en) | 2018-09-27 | 2018-09-27 | A kind of high strength glass fiber preparation process |
Country Status (1)
| Country | Link |
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| CN (1) | CN108892389A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112094056A (en) * | 2020-09-04 | 2020-12-18 | 五河县永兴复合材料有限公司 | Preparation process of high-strength glass fiber |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101811824A (en) * | 2010-05-11 | 2010-08-25 | 太仓宏大方圆电气有限公司 | Method for producting superfine glass wool |
| CN101979354A (en) * | 2010-09-09 | 2011-02-23 | 太仓宏大方圆电气有限公司 | Heat preserving cotton and production method thereof |
| CN102351413A (en) * | 2011-07-13 | 2012-02-15 | 苏州维艾普新材料有限公司 | Manufacturing method of grade A fireproof and flame retardant energy saving ultrafine glass wool |
| CN105060726A (en) * | 2015-07-28 | 2015-11-18 | 安徽丹凤集团桐城玻璃纤维有限公司 | High performance glass fiber |
| CN107956041A (en) * | 2017-11-18 | 2018-04-24 | 安徽玉然经编科技有限公司 | A kind of glass fabric with high tenacity |
-
2018
- 2018-09-27 CN CN201811131648.7A patent/CN108892389A/en not_active Withdrawn
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101811824A (en) * | 2010-05-11 | 2010-08-25 | 太仓宏大方圆电气有限公司 | Method for producting superfine glass wool |
| CN101979354A (en) * | 2010-09-09 | 2011-02-23 | 太仓宏大方圆电气有限公司 | Heat preserving cotton and production method thereof |
| CN102351413A (en) * | 2011-07-13 | 2012-02-15 | 苏州维艾普新材料有限公司 | Manufacturing method of grade A fireproof and flame retardant energy saving ultrafine glass wool |
| CN105060726A (en) * | 2015-07-28 | 2015-11-18 | 安徽丹凤集团桐城玻璃纤维有限公司 | High performance glass fiber |
| CN107956041A (en) * | 2017-11-18 | 2018-04-24 | 安徽玉然经编科技有限公司 | A kind of glass fabric with high tenacity |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112094056A (en) * | 2020-09-04 | 2020-12-18 | 五河县永兴复合材料有限公司 | Preparation process of high-strength glass fiber |
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Application publication date: 20181127 |