CN108871883A - A kind of static chamber flux observation device and gas production method - Google Patents
A kind of static chamber flux observation device and gas production method Download PDFInfo
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- CN108871883A CN108871883A CN201810836198.5A CN201810836198A CN108871883A CN 108871883 A CN108871883 A CN 108871883A CN 201810836198 A CN201810836198 A CN 201810836198A CN 108871883 A CN108871883 A CN 108871883A
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/02—Devices for withdrawing samples
- G01N1/22—Devices for withdrawing samples in the gaseous state
- G01N1/2273—Atmospheric sampling
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/02—Devices for withdrawing samples
- G01N1/22—Devices for withdrawing samples in the gaseous state
- G01N1/24—Suction devices
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
- G01N33/0004—Gaseous mixtures, e.g. polluted air
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Abstract
The invention belongs to ecological observation technology field, a kind of static chamber flux observation device and gas production method are disclosed.It is made of base ring, top box, gas production external device, temperature sensor and sealing ring.The configuration of the present invention is simple, material is easy to obtain, simple to operate;Specific HO type sealing ring can be realized no water-stop without sealed cistern is arranged;Only needing simple operations air bag and triple valve can be achieved with, gas in cabinet mixes and acquisition gas sample is to gas production bag or gas production bottle, without installing fan, carrying battery and using syringe;Camera bellows and camera-lucida are thermally insulated using (transparent) heat insulation sun paint, can preferably maintain case body temperature, and avoids additionally wrapping up heat-barrier material outside cabinet.The high-efficient effect of gas collecting of the present invention is good, is convenient for carrying, reusable, enormously simplifies gas collecting when carrying out flux observation based on closed chamber method and works, time and labour saving.
Description
Technical field
The invention belongs to flux observation device technical field more particularly to a kind of static chamber flux observation device and gas production sides
Method.
Background technique
Currently, the prior art commonly used in the trade is such:In recent years, due to using climate warming as the whole world of main feature
Variation attracts extensive attention, and China is for CO2、CH4、N2The observational study of O isothermal chamber gas flux is more and more, including
To soil-atmosphere interface greenhouse gases flux observational study.Closed chamber method has equipment letter due to other opposite observation methods
List, flexible operation have pole convenient for carrying out the advantages that repeating and controlling experiment in Soil Trace Gases flux observational study
It is widely applied.The basic principle is that closed cabinet is covered on earth's surface, pass through the change of gas concentration at any time in observation cabinet
Change to calculate Soil Trace Gases discharge or absorption rate.
In order to keep experimental observed data accurate, observation case should completely cut off the gas exchanges inside and outside cabinet, and should be right before gas production
Gas is mixed well to reduce the contingency of gas collecting in cabinet, while should slow down temperature change in cabinet as far as possible.
Presently, there are following defects in static chamber observational study:(1) to realize, gas is sufficiently mixed in cabinet, in research mostly in cabinet
Interior installation fan, and with storage battery power supply.It is individually equipped with battery if each cabinet, then cost increases, while carrying significantly
It is inconvenient;If multiple cabinets share one piece of large-capacity battery, not only field traverse layout is cumbersome, inconvenient to carry, while observation point
The distance between be restricted, be unfavorable for selecting best observation point.Therefore, gas mixing is directly ignored in some observational studies,
To reduce the accuracy of observation to a certain degree.(2) injection is mostly used to be sampled in static chamber observation at present, way is
Gas is extracted with syringe, is then transferred to gas production bag or gas production bottle, during which needs to rotate gas circuit valve repeatedly, is operated more numerous
It is trivial, while large capacity syringe is mostly glassware on the market at present, is easily damaged when field carries.(3) in air-tightness side
Face mostly uses water sealed tank to realize the sealing between top box and base ring, not only increases base ring manufacturing procedure, and because field water intaking is tired
Difficulty, operation difficulty greatly increase.(4) cabinet closed period, since sunlight irradiates, the temperature of confined space is toward up in cabinet
It rises quickly, the temperature especially under summer direct sunlight in 30min internal box will likely be higher by 2~5 DEG C of temperature outside cabinet.And it is warm
Degree is one of main driving factors of greenhouse gases flux, thus, it is larger that temperature rises the result generation that cabinet may be made to observe
Error.Therefore, common way is that there is package the material of reflection and heat insulation effect (it is poly- such as to cover aluminium bubble chamber film, foam outside the enclosure
Styrene etc.).The material is not only easy to damage in the handling process of field, the aesthetics of device entirety is reduced, simultaneously as being wrapped
It is opaque to wrap up in material, observation case selection can only be confined to camera bellows.
In conclusion problem of the existing technology is:Existing technology in gas mixing, take gas, sealing, cabinet heat-insulated
Etc. existing defects, concentrate on operation convenience and observation accuracy in terms of there are larger contradictions.
Solve the difficulty and meaning of above-mentioned technical problem:The configuration of the present invention is simple, material are easy to obtain, side easy to operate
Just;The increased simple gas production external device of institute of the invention, integrates gas mixing and gas sample acquisition function, only needs simple operations
Air bag and triple valve can be achieved in cabinet that gas mixes and acquisition gas sample is to gas production bag or gas production bottle, without install fan,
It carries battery and uses syringe, enormously simplify the mixing of field gas and acquisition device;Designed specific sealing ring energy
It is enough to realize without water-stop without sealed cistern is arranged and carries sealing water;Using (transparent) heat insulation sun paint to camera bellows and bright
Case is thermally insulated, and can preferably maintain case body temperature, and avoids additionally wrapping up thermal isolation film outside cabinet, makes to open using glass box
Exhibition flux observation is possibly realized.The high-efficient effect of gas collecting of the present invention is good, is convenient for carrying, reusable, enormously simplifies
Gas collecting works when carrying out flux observation based on closed chamber method, time and labour saving, and improves the accuracy of observation.
Summary of the invention
In view of the problems of the existing technology, the present invention provides a kind of static chamber flux observation device and gas production methods.
The invention is realized in this way a kind of static chamber flux observation device, the static chamber flux observation device setting
Have:
Top box, sealing ring, base ring, thermometer and gas production external device;
Gas production external device and thermometer are fixed on top box;
It places between top box and base ring and is connected and sealed with specific HO type sealing ring;
Top box outer surface is coated with waterproof and heat-insulating paint.
Further, the gas production external device includes:Air-intake filter, inlet end threading quick connector, inlet end are inverse
Only valve, air bag, outlet side non-return valve, triple valve, outlet side threading quick connector, gas outlet aeration head, gas production adapter tube (or connect
Head), each element is connected by polyfluortetraethylene pipe, and threading quick connector is fixed on top box.
Each element connection method of gas production external device is specially:The inlet end threading quick connector is fixed on top box side
(or bottom end), inlet end threading quick connector protrude into top box one end and connect inlet filter by polyfluortetraethylene pipe;Air inlet
End bulkhead filter stays in the outer one end of top box, and by polyfluortetraethylene pipe to be sequentially connected inlet end non-return valve, air bag, outlet side inverse
Only valve, triple valve first interface, triple valve second interface, outlet side threading quick connector;Outlet side threading quick connector is fixed
In the top box other side (or top), protrudes into one end polyfluortetraethylene pipe in top box and connect gas outlet aeration head;Triple valve third
Interface connects gas production adapter tube (or connector);(or connector) connection gas production bag or gas production bottle are taken in gas production.
Specific HO type sealing ring upper end is U-lag, and groove width is slightly less than top box wall thickness, after top box low side is inserted into upper U-lag
It is fixed with glue;Lower end is inverted U-channel, and groove width is wide compared with base ring thickness, and to increase the convenience of installation, while lower end U-lag is perpendicular
Straight inner wall is provided with one or more pairs of elongated dentations to enhance the leakproofness of sealing ring Yu base ring wall surface.
Top box outer surface applies waterproof and heat-insulating paint, and to slow down, the temperature rises in cabinet.When top box material be transparent material make and
Cheng Shi, the applied waterproof and heat-insulating paint in outer surface are transparent type waterproof and heat-insulating paint;When top box material is that nontransparent material is made
When, the applied waterproof and heat-insulating paint in outer surface is transparent type or universal waterproof and heat-insulating paint.
Another object of the present invention is to provide a kind of static chamber gas production sides using the static chamber flux observation device
Method, the static chamber gas production method include:
2~5cm of earth's surface is exposed in step 1, the good soil base ring of pre-plugged before gas production, upper end;
Assembled top box when observation, is placed on base ring and is compressed, be connected to HO sealing ring with base ring by step 2
Position, and triple valve is rotated to the first and second orifice;
Step 3 when gas production, connects gas production bag or gas production bottle;It is more in the state of the first and second orifice of triple valve
Secondary extruding sacculus keeps gas mixing in cabinet and pipeline uniform;
Step 4 rotates triple valve to the first and third orifice, and repeatedly squeezing sacculus makes gas enter airbag or gas
Bottle.
Step 5, gas production bag or adopt cylinder gas it is sufficient after, triple valve is rotated to the first and second orifice, closing is simultaneously
It removes gas production bag or gas production bottle, gas production finishes;
Step 6 requires according to gas production number, repeats step 3 to step 5.
In conclusion advantages of the present invention and good effect are:The high-efficient effect of gas collecting of the present invention is good, conveniently takes
Band, it is reusable, it enormously simplifies gas collecting when carrying out flux observation based on closed chamber method and works, time and labour saving, and mention
The accuracy of height observation.It is embodied in:(1) the configuration of the present invention is simple, material is easy to obtain, simple to operate;(2) this hair
The increased simple gas production external device of bright institute, integrates gas mixing and gas sample acquisition function, only need simple operations air bag and
Triple valve can be achieved with gas in cabinet and mix and acquire gas sample to gas production bag or gas production bottle, avoids installation fan, carries storage
Battery and use syringe, enormously simplify field gas mix and acquisition device;(3) the specific HO type sealing ring energy designed by
It is enough effectively to realize without water-stop, it avoids setting sealed cistern and field carries sealing water;(4) (transparent) waterproof and heat-insulating is used
Paint is thermally insulated camera bellows and camera-lucida, and case body temperature can be maintained not rise substantially, avoid outside cabinet additional package every
Hot material, meanwhile, make it possible to carry out flux observation using glass box.
Detailed description of the invention
Fig. 1 is static chamber agent structure schematic diagram provided in an embodiment of the present invention;
Fig. 2 is static chamber thermometer provided in an embodiment of the present invention and gas production external device connection schematic diagram;
Fig. 3 is static chamber HO sealing ring cross section structure schematic diagram provided in an embodiment of the present invention;
In figure:1, top box;2, HO type sealing ring;3, base ring;4, thermometer;5, air-intake filter;6, inlet end threading
Quick connector;7, inlet end non-return valve;8, air bag;9, outlet side non-return valve;10, triple valve;11, the fast grafting of outlet side threading
Head;12, gas outlet aeration head;13, polytetrafluoroethylene (PTFE) tracheae;14, gas production adapter tube (or connector).
Specific embodiment
In order to make the objectives, technical solutions, and advantages of the present invention clearer, with reference to embodiments, to the present invention
It is further elaborated.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, it is not used to
Limit the present invention.
The present invention provides a kind of soil and atmosphere interface gas collecting device and acquisition method, it is intended to solve presently, there are
The sealing of gas collecting equipment and gas evenly mixing device be complicated, the technologies such as gas production is cumbersome, the temperature rises in cabinet amplitude is big
Problem.
Application principle of the invention is explained in detail with reference to the accompanying drawing.
As shown in Figure 1-Figure 3, static chamber flux observation device provided in an embodiment of the present invention includes:Top box 1, the sealing of HO type
Circle 2, base ring 3, thermometer 4 and gas production external device.Wherein gas production external device includes:Air-intake filter 5, inlet end threading
Quick connector 6, air bag 8, outlet side non-return valve 9, triple valve 10, outlet side threading quick connector 11, goes out inlet end non-return valve 7
(or connector) 14 is taken in port aeration head 12, polytetrafluoroethylene (PTFE) tracheae 13, gas production.
Top box 1 and base ring 3 are process with stainless steel, wall thickness 2mm, internal diameter 250mm.Top box 1 is bottom opening, top
The trapezoidal rotary table of sealing, total height 200mm.Base ring 3 is the cylinder of bottom and top opening, high 100mm.Top box 1 and base ring 3 it
Between be connected and sealed with the specific HO type sealing ring 2 of silica gel material.1 top surface of top box is embedded with handle.1 outer surface of top box is coated with
Universal waterproof and heat-insulating paint.
Gas production external device and thermometer 4 are fixed on top box 1.
The connection of gas production external device and fixed form are as follows:Inlet end threading quick connector 6 is fixed on top box bottom end, air inlet
End threading quick connector 6 protrudes into one end in top box 1 and passes through the connection inlet filter 5 of polyfluortetraethylene pipe 13;Inlet end threading is fast
Connection-peg 6 stays in the outer one end of top box 1, and by polyfluortetraethylene pipe 13 to be sequentially connected inlet end non-return valve 7, air bag 8, outlet side inverse
Only valve 9,10 first interface of triple valve, 10 second interface of triple valve, outlet side threading quick connector 11;The fast grafting of outlet side threading
First 11 are fixed on top box top, protrude into one end polyfluortetraethylene pipe 13 in top box and connect gas outlet aeration head 12;Triple valve 10
Third interface connects gas production adapter tube 14;Gas production adapter tube 14 connects gas production bag.
The installation direction of non-return valve 7 and 9 is consistent, to ensure air-flow one-way flow in pipeline.
13 internal diameter 4mm of polyfluortetraethylene pipe, outer diameter 6mm, other elements connection size selects matched.
Static chamber gas production method provided in an embodiment of the present invention includes the following steps:
Step 1,48 hours before gas production, 2~3cm of earth's surface is exposed in the good soil base ring of pre-plugged, upper end;
Assembled top box when observation, is placed on base ring and is compressed, be connected to HO sealing ring with base ring by step 2
Position, and triple valve is rotated to the first and second orifice;
Step 3 when gas production, connects the gas production bag of 50ml;In the state of the first and second orifice of triple valve, squeeze
Sacculus 10~15 times, keep gas mixing in cabinet and pipeline uniform;
Step 4 rotates triple valve to the first and third orifice, and repeatedly squeezing sacculus makes gas enter gas production bag and fill
It is full of.
Step 5 rotates triple valve to the first and second orifice, closes and removes gas production bag, gas production finishes;
Step 6 requires according to gas production number, repeats step 3 to step 5.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all in essence of the invention
Made any modifications, equivalent replacements, and improvements etc., should all be included in the protection scope of the present invention within mind and principle.
Claims (7)
1. a kind of static chamber flux observation device, which is characterized in that the static chamber flux observation device is provided with:
Top box, sealing ring, base ring, thermometer and gas production external device;
Gas production external device and thermometer are fixed on top box;
It is connected and sealed between top box and base ring with specific HO type sealing ring;
Top box outer surface is coated with waterproof and heat-insulating paint.
2. static chamber flux observation device as described in claim 1, which is characterized in that the gas production external device is by air inlet
Filter, inlet end threading quick connector, inlet end non-return valve, air bag, outlet side non-return valve, triple valve, outlet side threading are fast
Connection-peg, gas outlet aeration head, gas production adapter tube or connector composition, each element are connected by polyfluortetraethylene pipe, the fast grafting of threading
Head is fixed on top box.
3. static chamber flux observation device as described in claim 1, which is characterized in that the inlet end threading quick connector is solid
Due to top box side or bottom end, inlet end threading quick connector protrudes into top box one end and connects air inlet by polyfluortetraethylene pipe
Filter;The outer one end of inlet end threading quick connector top box by polyfluortetraethylene pipe be sequentially connected inlet end non-return valve, air bag,
Outlet side non-return valve, triple valve first interface, triple valve second interface, outlet side threading quick connector;Outlet side threading is inserted fastly
Connector is fixed on the top box other side or top, protrudes into one end polyfluortetraethylene pipe in top box and connects gas outlet aeration head;Threeway
Valve third interface connects gas production adapter tube or connector;Gas production adapter tube or connector connection gas production bag or gas production bottle.
4. static chamber flux observation device as described in claim 1, which is characterized in that the specific HO type sealing ring upper end is
U-lag, groove width are slightly less than top box wall thickness, and top box bottom end is fixed after being inserted into upper U-lag with glue;Lower end is inverted U-channel, groove width
Wide compared with base ring thickness, to increase the convenience of installation, while lower end U-lag vertical inner wall is provided with one or more pairs of elongated teeth
Shape protrusion is to enhance the leakproofness of sealing ring Yu base ring wall surface.
5. static chamber flux observation device as described in claim 1, which is characterized in that when top box material is transparent material production
Into when, the applied waterproof and heat-insulating paint in outer surface be transparent type waterproof and heat-insulating paint;When top box material be nontransparent material make and
Cheng Shi, the applied waterproof and heat-insulating paint in outer surface are transparent type or universal waterproof and heat-insulating paint.
6. a kind of observation and gas production method using static chamber flux observation device described in claim 1, which is characterized in that described
Static chamber observation and gas production method include:
2~5cm of earth's surface is exposed in step 1, the good soil base ring of pre-plugged before gas production, upper end;
Assembled top box when observation, is placed on base ring and is compressed, connect HO type sealing ring with base ring in place by step 2,
And triple valve is rotated to the first and second orifice;
Step 3 when gas production, connects gas production bag or gas production bottle;In the state of the first and second orifice of triple valve, repeatedly squeeze
Pressure ball capsule keeps gas mixing in cabinet and pipeline uniform;
Step 4 rotates triple valve to the first and third orifice, and repeatedly squeezing sacculus makes gas enter airbag or gas cylinder.
Step 5, gas production bag or adopt cylinder gas it is sufficient after, triple valve is rotated to the first and second orifice, closes and removes
Gas production bag or gas production bottle, gas production finish;
Step 6 requires according to gas production number, repeats step 3 to step 5.
7. a kind of Soil Trace Gases flux using static chamber flux observation device described in claim 1~6 any one is supervised
Examining system.
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CN201810836198.5A CN108871883A (en) | 2018-07-26 | 2018-07-26 | A kind of static chamber flux observation device and gas production method |
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Cited By (6)
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CN110926887A (en) * | 2019-11-25 | 2020-03-27 | 陈洁 | Portable sampling device for detecting atmospheric pollution degree |
CN112798346A (en) * | 2020-12-30 | 2021-05-14 | 农业部沼气科学研究所 | Gas-liquid co-sampling experimental method and system for biogas fermentation batch test |
CN113340678A (en) * | 2021-07-21 | 2021-09-03 | 中国农业大学 | Method for collecting greenhouse gas of high-stalk crop farmland |
CN113358426A (en) * | 2021-06-11 | 2021-09-07 | 重庆师范大学 | Acquisition device and method for measuring emission contribution of endogenous greenhouse gases in shallow water body |
CN114354290A (en) * | 2021-12-16 | 2022-04-15 | 中国科学院生态环境研究中心 | Device and method for dynamically measuring greenhouse gas emission flux of water body |
CN116591668A (en) * | 2023-07-19 | 2023-08-15 | 大庆鑫得丰石油技术有限公司 | Flow data acquisition device of gas production wellhead |
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CN113340678A (en) * | 2021-07-21 | 2021-09-03 | 中国农业大学 | Method for collecting greenhouse gas of high-stalk crop farmland |
CN114354290A (en) * | 2021-12-16 | 2022-04-15 | 中国科学院生态环境研究中心 | Device and method for dynamically measuring greenhouse gas emission flux of water body |
CN114354290B (en) * | 2021-12-16 | 2023-11-24 | 中国科学院生态环境研究中心 | Device and method for dynamically measuring water body greenhouse gas emission flux |
CN116591668A (en) * | 2023-07-19 | 2023-08-15 | 大庆鑫得丰石油技术有限公司 | Flow data acquisition device of gas production wellhead |
CN116591668B (en) * | 2023-07-19 | 2023-09-22 | 大庆鑫得丰石油技术有限公司 | Flow data acquisition device of gas production wellhead |
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