CN108863070A - The preparation method of clear frit - Google Patents
The preparation method of clear frit Download PDFInfo
- Publication number
- CN108863070A CN108863070A CN201810952353.XA CN201810952353A CN108863070A CN 108863070 A CN108863070 A CN 108863070A CN 201810952353 A CN201810952353 A CN 201810952353A CN 108863070 A CN108863070 A CN 108863070A
- Authority
- CN
- China
- Prior art keywords
- preparation
- glaze
- clear frit
- fluorite
- feldspar
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
- C04B41/5022—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/85—Coating or impregnation with inorganic materials
- C04B41/86—Glazes; Cold glazes
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Structural Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Glass Compositions (AREA)
Abstract
The present invention relates to ceramic glaze fields, in particular to a kind of preparation method of clear frit comprising following steps：The first step weighs the raw material of following parts by weight, kaolin 10-15%, quartzy 5-10%, feldspar 45-55%, fluorite 10-20%, zinc oxide 1-3%；Second step is added ball mill and carries out ball milling；Third step, 500 mesh of spheroidal graphite material through screens；4th step is aged 3-6 days, obtains glaze slip；5th step, glazing, using leaching glaze gimmick；6th step, firing, sintering temperature are 1200 ° -1220 °.It is not in sagging phenomenon in preparation process, and glaze paint glossiness is good using the preparation method of clear frit of the invention, the transparency is high.
Description
Technical field
The present invention relates to ceramic glaze fields, in particular to a kind of preparation method of clear frit.
Background technique
Glaze is the colorless or colored glassy thin layer for being covered on ceramic surface, is with raw mineral materials and industrial chemicals
Glaze slip is made by grinding in cooperation by a certain percentage, imposes on billet surface, calcines through certain temperature.Glaze can increase product
Mechanical strength, thermal stability and dielectric strength, there are also beautify implements, convenient for wipe wash, not erosion dirty by dust raw meat the features such as.
Clear frit refers to can see that the glaze of the color of green body and various engravings and illuminated under glaze by glaze layer.It is making
It often will appear that transparency is inadequate and non-uniform problem when standby.
Summary of the invention
It is a primary object of the present invention to provide a kind of transparent glaze formula and preparation method regarding to the issue above.
To achieve the goals above, the preparation method of clear frit of the invention, includes the following steps：
The first step weighs the raw material of following parts by weight, kaolin 10-15%, quartzy 5-10%, feldspar 45-55%, fluorite
10-20%, zinc oxide 1-3%；
Second step is added ball mill and carries out ball milling；
Third step, 500 mesh of spheroidal graphite material through screens；
4th step is aged 3-6 days, obtains glaze slip；
5th step, glazing, using leaching glaze gimmick；
6th step, firing, sintering temperature are 1200 ° -1220 °.
Further, in the first step, raw material proportioning is kaolin 14%, quartz 10%, feldspar 55%, fluorite 20%, oxygen
Change zinc 1%；
Further, in second step, the spheroidal graphite time be 1 hour, material, ball, water ratio be 1:1.5:0.6.
Further, in the 6th step, the test piece for having applied glaze is put into baking oven before firing and is dried, by test piece surrounding after drying
Glaze strike off.
Further, in the 6th step, soaking time is 30-45 minutes.
The invention has the advantages that：Using the preparation method of clear frit of the invention, will not go out in preparation process
Existing sagging phenomenon, and glaze paint glossiness is good, the transparency is high.
Specific embodiment
The preparation method of clear frit of the invention, includes the following steps：
The first step weighs the raw material of following parts by weight, kaolin 14%, quartz 10%, feldspar 55%, fluorite 20%, oxygen
Change zinc 1%；
Second step, be added ball mill carry out ball milling, the spheroidal graphite time be 1 hour, material, ball, water ratio be 1:1.5:0.6；
Third step, 500 mesh of spheroidal graphite material through screens；
4th step is aged 3-6 days, obtains glaze slip；
5th step, glazing, using leaching glaze gimmick, glaze layer will reach certain thickness when glazing and glaze layer will be uniformly without gas
Bubble；
The test piece for having applied glaze is put into baking oven before firing and dries, by the glaze of test piece surrounding after drying by the 6th step, firing
It strikes off, sintering temperature is 1200 ° -1220 °, and soaking time is 30-45 minutes.
The foregoing is only a preferred embodiment of the present invention, is not intended to restrict the invention, for the skill of this field
For art personnel, the invention may be variously modified and varied.All within the spirits and principles of the present invention, made any to repair
Change, equivalent replacement, improvement etc., should all be included in the protection scope of the present invention.
Claims (5)
1. a kind of preparation method of clear frit, which is characterized in that include the following steps：
The first step weighs the raw material of following parts by weight, kaolin 10-15%, quartzy 5-10%, feldspar 45-55%, fluorite 10-
20%, zinc oxide 1-3%；
Second step is added ball mill and carries out ball milling；
Third step, 500 mesh of spheroidal graphite material through screens；
4th step is aged 3-6 days, obtains glaze slip；
5th step, glazing, using leaching glaze gimmick；
6th step, firing, sintering temperature are 1200 ° -1220 °.
2. the preparation method of clear frit according to claim 1, which is characterized in that in the first step, raw material proportioning is kaolinite
Soil 14%, quartz 10%, feldspar 55%, fluorite 20%, zinc oxide 1%.
3. the preparation method of clear frit according to claim 1, which is characterized in that in second step, the spheroidal graphite time is 1 small
When, material, ball, water ratio be 1:1.5:0.6.
4. the preparation method of clear frit according to claim 1, which is characterized in that in the 6th step, glaze will have been applied before firing
Test piece be put into baking oven and dry, the glaze of test piece surrounding is struck off after drying.
5. the preparation method of clear frit according to claim 1, which is characterized in that in the 6th step, soaking time 30-45
Minute.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810952353.XA CN108863070A (en) | 2018-08-21 | 2018-08-21 | The preparation method of clear frit |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810952353.XA CN108863070A (en) | 2018-08-21 | 2018-08-21 | The preparation method of clear frit |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108863070A true CN108863070A (en) | 2018-11-23 |
Family
ID=64321122
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810952353.XA Withdrawn CN108863070A (en) | 2018-08-21 | 2018-08-21 | The preparation method of clear frit |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108863070A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109942190A (en) * | 2019-03-14 | 2019-06-28 | 江西和美陶瓷有限公司 | Anti-skidding matt ceramic brick |
| CN113305994A (en) * | 2021-06-11 | 2021-08-27 | 黑龙江微雕科技有限公司 | Method for micro-carving artistic picture on ceramic product surface |
-
2018
- 2018-08-21 CN CN201810952353.XA patent/CN108863070A/en not_active Withdrawn
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109942190A (en) * | 2019-03-14 | 2019-06-28 | 江西和美陶瓷有限公司 | Anti-skidding matt ceramic brick |
| CN109942190B (en) * | 2019-03-14 | 2022-05-17 | 江西和美陶瓷有限公司 | Anti-skid matte ceramic tile |
| CN113305994A (en) * | 2021-06-11 | 2021-08-27 | 黑龙江微雕科技有限公司 | Method for micro-carving artistic picture on ceramic product surface |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20181123 |
|
| WW01 | Invention patent application withdrawn after publication |