CN108851257A - A kind of moisture absorption heating heat-preserving function panty hose - Google Patents
A kind of moisture absorption heating heat-preserving function panty hose Download PDFInfo
- Publication number
- CN108851257A CN108851257A CN201810923655.4A CN201810923655A CN108851257A CN 108851257 A CN108851257 A CN 108851257A CN 201810923655 A CN201810923655 A CN 201810923655A CN 108851257 A CN108851257 A CN 108851257A
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- CN
- China
- Prior art keywords
- panty hose
- polynosic
- moisture absorption
- weight
- absorption heating
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Links
- 238000010438 heat treatment Methods 0.000 title claims abstract description 31
- 238000010521 absorption reaction Methods 0.000 title claims abstract description 29
- 229920001407 Modal (textile) Polymers 0.000 claims abstract description 50
- 229920002972 Acrylic fiber Polymers 0.000 claims abstract description 23
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims abstract description 22
- 239000002994 raw material Substances 0.000 claims abstract description 19
- 229920002334 Spandex Polymers 0.000 claims abstract description 12
- 239000004759 spandex Substances 0.000 claims abstract description 12
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 110
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 45
- 235000019441 ethanol Nutrition 0.000 claims description 42
- 239000000835 fiber Substances 0.000 claims description 40
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 32
- 238000009987 spinning Methods 0.000 claims description 23
- 238000006243 chemical reaction Methods 0.000 claims description 17
- 238000005406 washing Methods 0.000 claims description 16
- 239000003431 cross linking reagent Substances 0.000 claims description 15
- JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 claims description 14
- FUSNOPLQVRUIIM-UHFFFAOYSA-N 4-amino-2-(4,4-dimethyl-2-oxoimidazolidin-1-yl)-n-[3-(trifluoromethyl)phenyl]pyrimidine-5-carboxamide Chemical compound O=C1NC(C)(C)CN1C(N=C1N)=NC=C1C(=O)NC1=CC=CC(C(F)(F)F)=C1 FUSNOPLQVRUIIM-UHFFFAOYSA-N 0.000 claims description 13
- 239000012493 hydrazine sulfate Substances 0.000 claims description 13
- 229910000377 hydrazine sulfate Inorganic materials 0.000 claims description 13
- 238000000034 method Methods 0.000 claims description 13
- 239000003607 modifier Substances 0.000 claims description 12
- 238000006116 polymerization reaction Methods 0.000 claims description 11
- FDRCDNZGSXJAFP-UHFFFAOYSA-M sodium chloroacetate Chemical compound [Na+].[O-]C(=O)CCl FDRCDNZGSXJAFP-UHFFFAOYSA-M 0.000 claims description 11
- IAZDPXIOMUYVGZ-UHFFFAOYSA-N Dimethylsulphoxide Chemical compound CS(C)=O IAZDPXIOMUYVGZ-UHFFFAOYSA-N 0.000 claims description 10
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 10
- 230000001112 coagulating effect Effects 0.000 claims description 10
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 8
- 229910052799 carbon Inorganic materials 0.000 claims description 8
- 238000004132 cross linking Methods 0.000 claims description 8
- 239000000428 dust Substances 0.000 claims description 8
- HRPVXLWXLXDGHG-UHFFFAOYSA-N Acrylamide Chemical compound NC(=O)C=C HRPVXLWXLXDGHG-UHFFFAOYSA-N 0.000 claims description 7
- 229910026551 ZrC Inorganic materials 0.000 claims description 7
- 238000005119 centrifugation Methods 0.000 claims description 7
- UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 claims description 7
- VVQNEPGJFQJSBK-UHFFFAOYSA-N Methyl methacrylate Chemical compound COC(=O)C(C)=C VVQNEPGJFQJSBK-UHFFFAOYSA-N 0.000 claims description 6
- 239000002202 Polyethylene glycol Substances 0.000 claims description 6
- 229920001223 polyethylene glycol Polymers 0.000 claims description 6
- NLHHRLWOUZZQLW-UHFFFAOYSA-N Acrylonitrile Chemical compound C=CC#N NLHHRLWOUZZQLW-UHFFFAOYSA-N 0.000 claims description 5
- 230000015271 coagulation Effects 0.000 claims description 5
- 238000005345 coagulation Methods 0.000 claims description 5
- 238000007872 degassing Methods 0.000 claims description 5
- 239000002904 solvent Substances 0.000 claims description 5
- 238000001291 vacuum drying Methods 0.000 claims description 5
- 239000003999 initiator Substances 0.000 claims description 4
- NIQCNGHVCWTJSM-UHFFFAOYSA-N dimethyl benzenedicarboxylate Natural products COC(=O)C1=CC=CC=C1C(=O)OC NIQCNGHVCWTJSM-UHFFFAOYSA-N 0.000 claims description 3
- FBSAITBEAPNWJG-UHFFFAOYSA-N dimethyl phthalate Natural products CC(=O)OC1=CC=CC=C1OC(C)=O FBSAITBEAPNWJG-UHFFFAOYSA-N 0.000 claims description 2
- 229960001826 dimethylphthalate Drugs 0.000 claims description 2
- 238000007654 immersion Methods 0.000 claims description 2
- -1 isobutyl dimethyl phthalate Chemical compound 0.000 claims description 2
- 238000012986 modification Methods 0.000 claims description 2
- 230000004048 modification Effects 0.000 claims description 2
- 229920002239 polyacrylonitrile Polymers 0.000 claims description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims 2
- 239000004743 Polypropylene Substances 0.000 claims 1
- 239000007788 liquid Substances 0.000 claims 1
- 150000002825 nitriles Chemical class 0.000 claims 1
- 229910052757 nitrogen Inorganic materials 0.000 claims 1
- 229920001155 polypropylene Polymers 0.000 claims 1
- 230000006870 function Effects 0.000 abstract description 18
- 230000000844 anti-bacterial effect Effects 0.000 abstract description 5
- 239000004753 textile Substances 0.000 description 7
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 6
- 239000004744 fabric Substances 0.000 description 6
- KQNPFQTWMSNSAP-UHFFFAOYSA-N isobutyric acid Chemical compound CC(C)C(O)=O KQNPFQTWMSNSAP-UHFFFAOYSA-N 0.000 description 4
- 238000009940 knitting Methods 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 4
- KMOZMCXISHYPFO-UHFFFAOYSA-N C(C)O.S(=O)(=O)(O)O.NN Chemical compound C(C)O.S(=O)(=O)(O)O.NN KMOZMCXISHYPFO-UHFFFAOYSA-N 0.000 description 3
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 3
- 206010037660 Pyrexia Diseases 0.000 description 3
- 238000004821 distillation Methods 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- RDRCCJPEJDWSRJ-UHFFFAOYSA-N pyridine;1h-pyrrole Chemical compound C=1C=CNC=1.C1=CC=NC=C1 RDRCCJPEJDWSRJ-UHFFFAOYSA-N 0.000 description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- 229920000742 Cotton Polymers 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 238000011161 development Methods 0.000 description 2
- 230000004069 differentiation Effects 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000002657 fibrous material Substances 0.000 description 2
- 230000014759 maintenance of location Effects 0.000 description 2
- OJURWUUOVGOHJZ-UHFFFAOYSA-N methyl 2-[(2-acetyloxyphenyl)methyl-[2-[(2-acetyloxyphenyl)methyl-(2-methoxy-2-oxoethyl)amino]ethyl]amino]acetate Chemical compound C=1C=CC=C(OC(C)=O)C=1CN(CC(=O)OC)CCN(CC(=O)OC)CC1=CC=CC=C1OC(C)=O OJURWUUOVGOHJZ-UHFFFAOYSA-N 0.000 description 2
- 238000004321 preservation Methods 0.000 description 2
- 238000010792 warming Methods 0.000 description 2
- 238000009941 weaving Methods 0.000 description 2
- 241000255789 Bombyx mori Species 0.000 description 1
- 229920002101 Chitin Polymers 0.000 description 1
- 229920000433 Lyocell Polymers 0.000 description 1
- 229920001131 Pulp (paper) Polymers 0.000 description 1
- 229920002125 Sokalan® Polymers 0.000 description 1
- 229920002472 Starch Polymers 0.000 description 1
- 230000006750 UV protection Effects 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 238000005054 agglomeration Methods 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 238000004378 air conditioning Methods 0.000 description 1
- 230000001476 alcoholic effect Effects 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- 150000001450 anions Chemical class 0.000 description 1
- 238000010923 batch production Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 125000002057 carboxymethyl group Chemical group [H]OC(=O)C([H])([H])[*] 0.000 description 1
- 229920002678 cellulose Polymers 0.000 description 1
- 239000001913 cellulose Substances 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 230000003750 conditioning effect Effects 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000004332 deodorization Methods 0.000 description 1
- 235000012489 doughnuts Nutrition 0.000 description 1
- 238000004043 dyeing Methods 0.000 description 1
- 210000003746 feather Anatomy 0.000 description 1
- 238000005338 heat storage Methods 0.000 description 1
- ZGCHATBSUIJLRL-UHFFFAOYSA-N hydrazine sulfate Chemical compound NN.OS(O)(=O)=O ZGCHATBSUIJLRL-UHFFFAOYSA-N 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 238000011065 in-situ storage Methods 0.000 description 1
- 239000011810 insulating material Substances 0.000 description 1
- 125000000959 isobutyl group Chemical group [H]C([H])([H])C([H])(C([H])([H])[H])C([H])([H])* 0.000 description 1
- 239000000178 monomer Substances 0.000 description 1
- 239000004584 polyacrylic acid Substances 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000012827 research and development Methods 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 230000002269 spontaneous effect Effects 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
- 210000004243 sweat Anatomy 0.000 description 1
- 230000028016 temperature homeostasis Effects 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 230000007704 transition Effects 0.000 description 1
- 230000032258 transport Effects 0.000 description 1
- 210000002268 wool Anatomy 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A41—WEARING APPAREL
- A41B—SHIRTS; UNDERWEAR; BABY LINEN; HANDKERCHIEFS
- A41B11/00—Hosiery; Panti-hose
- A41B11/14—Panti-hose; Body-stockings
-
- A—HUMAN NECESSITIES
- A41—WEARING APPAREL
- A41B—SHIRTS; UNDERWEAR; BABY LINEN; HANDKERCHIEFS
- A41B17/00—Selection of special materials for underwear
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F6/00—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof
- D01F6/44—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polymers obtained by reactions only involving carbon-to-carbon unsaturated bonds as major constituent with other polymers or low-molecular-weight compounds
- D01F6/54—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polymers obtained by reactions only involving carbon-to-carbon unsaturated bonds as major constituent with other polymers or low-molecular-weight compounds of polymers of unsaturated nitriles
-
- D—TEXTILES; PAPER
- D02—YARNS; MECHANICAL FINISHING OF YARNS OR ROPES; WARPING OR BEAMING
- D02G—CRIMPING OR CURLING FIBRES, FILAMENTS, THREADS, OR YARNS; YARNS OR THREADS
- D02G3/00—Yarns or threads, e.g. fancy yarns; Processes or apparatus for the production thereof, not otherwise provided for
- D02G3/02—Yarns or threads characterised by the material or by the materials from which they are made
- D02G3/04—Blended or other yarns or threads containing components made from different materials
- D02G3/045—Blended or other yarns or threads containing components made from different materials all components being made from artificial or synthetic material
-
- D—TEXTILES; PAPER
- D02—YARNS; MECHANICAL FINISHING OF YARNS OR ROPES; WARPING OR BEAMING
- D02G—CRIMPING OR CURLING FIBRES, FILAMENTS, THREADS, OR YARNS; YARNS OR THREADS
- D02G3/00—Yarns or threads, e.g. fancy yarns; Processes or apparatus for the production thereof, not otherwise provided for
- D02G3/22—Yarns or threads characterised by constructional features, e.g. blending, filament/fibre
- D02G3/32—Elastic yarns or threads ; Production of plied or cored yarns, one of which is elastic
- D02G3/328—Elastic yarns or threads ; Production of plied or cored yarns, one of which is elastic containing elastane
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
- D06B3/00—Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating
- D06B3/02—Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating of fibres, slivers or rovings
-
- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2201/00—Cellulose-based fibres, e.g. vegetable fibres
- D10B2201/20—Cellulose-derived artificial fibres
- D10B2201/22—Cellulose-derived artificial fibres made from cellulose solutions
-
- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2321/00—Fibres made from polymers obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D10B2321/10—Fibres made from polymers obtained by reactions only involving carbon-to-carbon unsaturated bonds polymers of unsaturated nitriles, e.g. polyacrylonitrile, polyvinylidene cyanide
-
- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2331/00—Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products
- D10B2331/10—Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products polyurethanes
Abstract
The invention discloses a kind of moisture absorption heating heat-preserving function panty hose, including panty hose ontology, the panty hose ontology is interwoven by inner yarn and table yarn, the inner yarn is by modified acrylic fibre and modified polynosic is blended forms, the table yarn is spandex, by weight percentage, the group of each fibrous raw material of panty hose ontology becomes：Spandex 7 ~ 8%, modified polynosic 75 ~ 78%, modified acrylic fibre 14 ~ 17%.The present invention has excellent moisture absorption heating performance, has both the functions such as wash resistant, antibacterial deodourizing, uvioresistant.
Description
Technical field
The present invention relates to a kind of panty hose, in particular to a kind of moisture absorption heating heat-preserving function panty hose.
Background technique
In recent years, continuing to bring out for new fiber materials provides new development space for textile, and textile is taken
Performance is continuously improved, this is greatly enriched the material and cultural life of people, while also meeting people and using valence to textile
The fashion requirement of value innovation, high-quality and Individuation.Currently, the functional fiber in new fiber materials is quickly grown,
The production scale of the new varieties fiber such as sea-island fibre, profiled fibre is expanded；Biofunctional fiber, chitin fiber
Deng also starting to move towards the marketization；In addition, silkworm protein fiber, a batch such as acid fiber by polylactic based on starch exploitation have originality
It is researched and developed successfully with the fibre new species of independent intellectual property right, and puts into batch production, enrich the kind of fibrous raw material.
" 13 " textile industry tackling of key scientific and technical problems and Industrialization Projects（Knitting）It proposes, develops fibre in differentiation, high-performance
Application of the novel materials such as fiber in high-grade knitted fabric.Using have the function of the natural fiber of specific function or it is differential,
Property fiber（Such as there are antibacterial, moisture absorbing and sweat releasing, warming, anion, far infrared, UV resistance, doughnut and anisotropic cross-section fibers
Deng）, the development of knitted fabric technology of knitting product function is realized in conjunction with knitting and weaving technology.
Trend with clothes fashion and the pursuit to comfort property, fabric heat insulating material is increasingly by people
Favor, with society advance and the improvement of people's living standards, only by plus-minus clothes thickness have been unable to meet people couple
The requirement of comfort, the fabric that can adjust temperature become higher pursuit, and a series of dress ornament class product of heat preservation heat-preserving functions is answered
It transports and gives birth to, panty hose of the exploitation with highly hygroscopic heat generating and retention function have extraordinary economic benefit and market prospects.
Currently, the domestic research about heat preservation Thermal textile product is concentrated mainly on spinning process and is knitted the exploitation side of fabric
Face, for example, then hygroscopic heating fibers and modal fiber blended are developed as raw material and given birth to using the mixed yarn and bright and beautiful ammonia covering yarn
Knitting thermal underwear has been produced, and has explored the production technology of a set of spinning, weaving, dyeing and finishing.
A kind of American invention phase change heat-storage thermoregulation material --- Outlust air-conditioning fiber, it is by adding in county Party committee
Add certain medium（Consider that its phase transition temperature is in a certain range）, using the phase-change characteristic of medium, guarantee that it is absorbing or is dissipating
Maintain textile temperature constant when calorific value.The novel touch functional fiber of toray company exploitation --- Softwarm is fine
The advantages of tieing up, combining special artificial wood pulp cellulose and differentiation acrylic fibers has the characteristics that fever, warming, flexible touch,
Softwarm fiber absorbs the moisture that human skin distributes, and is converted to thermal energy by chemical reaction and realizes fever.Dongyang spinning company
The EKS fiber of exploitation has the function of conditioning, it is by the way that the hydrophilings group such as amino, carboxyl is introduced polyacrylic acid point
Son, and carry out crosslinking Treatment and obtain, this county is 3.5 times that wettability power is cotton, and moisture absorption heating amount is approximately the 2 of wool and natural feather
Quilt is widely used in lingerie, bedding cotton for wadding, gym suit, ski-wear etc..
To sum up, moisture absorption heating tencel and its dress and personal adornment application product are developed, is had to textile added value is promoted
Significance is that a period of time domestic and foreign scholars and enterprise will try to be the first one of the important topics of research and development from now on.
Summary of the invention
The purpose of the present invention is to provide a kind of moisture absorption heating heat-preserving function panty hose, have excellent moisture absorption heating performance,
Have both the functions such as wash resistant, antibacterial deodourizing, uvioresistant.
The technical solution adopted by the present invention to solve the technical problems is：
A kind of moisture absorption heating heat-preserving function panty hose, including panty hose ontology, the panty hose ontology are interweaved by inner yarn and table yarn
Form, the inner yarn by modified acrylic fibre and it is modified polynosic is blended forms, the table yarn is spandex, by weight hundred
Divide than meter, the group of each fibrous raw material of panty hose ontology becomes：Spandex 7 ~ 8%, modified polynosic 75 ~ 78%, modified polyacrylonitrile
Fiber 14 ~ 17%.
In the present invention yarn by modified acrylic fibre and it is modified polynosic is blended forms, there is excellent moisture absorption heating
Can, have both the functions such as wash resistant, antibacterial deodourizing, uvioresistant.The proportion of modified polynosic and modified acrylic fibre is controlled,
It can be effectively controlled production cost, and obtain excellent moisture absorption heating performance.
Preferably, the modified polynosic is prepared by the following method and obtains：
（1）Polynosic, sodium hydroxide solution and ethyl alcohol are added in kneader simultaneously, 38 ~ 42 DEG C of temperature of control, alkalization 20 ~
25min；
（2）By the monoxone ethanol solution and step of mass concentration 70 ~ 75%（1）Polynosic after alkalization is uniformly mixed, etherificate
The temperature of reaction is controlled at 72 ~ 75 DEG C, is reacted 40 ~ 60 minutes, and polynosic, which is adopted, after etherificate is neutralized with hydrochloric acid, and distills water washing,
Centrifugation, and be dried in vacuo；
（3）By step（2）The polynosic handled is soaked in 25 ~ 30min in 30 ~ 35 DEG C of temperature of crosslinking agent, is subsequently added into
The ethanol solution of pyridine, hydrazine sulfate controls 40 ~ 45 DEG C of temperature cross-linking reaction 12 ~ 14 hours, distills water washing after reaction,
Centrifugation, and be dried in vacuo, it is then placed in 30 ~ 60s of immersion in 35 ~ 40 DEG C of polyethylene glycol, is finally dried in vacuo.
The present invention first uses monoxone ethanol solution etherificate to introduce carboxymethyl, provides basis for the crosslinking of subsequent sulphuric acid hydrazine, so
Its moisture absorption heating performance, the temperature of fever can also be improved while improving polynosic intensity with hydrazine sulfate cross-linking reaction again afterwards
Highest can promote 1.8 DEG C or so, hydroscopicity 15% or so；Polyethylene glycol processing can be improved washing resistance performance.
Preferably, the polynosic：Sodium hydroxide solution：Mass ratio=1 of ethyl alcohol：6~9：3~5.
Preferably, the mass concentration of the sodium hydroxide solution is 10 ~ 15%, the mass concentration of ethyl alcohol is 85 ~ 90%；It is rich
The mass ratio of strong fiber and monoxone ethanol solution is 1:0.8~1.2.
Preferably, the crosslinking agent is the N that concentration is 0.01 ~ 0.012moL/L, the second of N- dicyclohexylcarbodiimide
Alcoholic solution；The concentration of the ethanol solution of hydrazine sulfate is 0.008 ~ 0.009moL/L.
Preferably, the polynosic：Crosslinking agent：Pyridine：Mass ratio=1 of the ethanol solution of hydrazine sulfate:6 0~70：
0.3~0.5:60~70。
Preferably, the modified acrylic fibre is prepared by the following method and obtains：
(1) prepared by spinning solution：The polymerization reaction raw material of 20 ~ 25 parts by weight is added to the solvent dimethyl sulfoxide of 100 parts by weight
Middle mixing reacts 12 ~ 16 hours at 40 ~ 45 DEG C, spinning solution is obtained after discontinuous degassing；The polymerization reaction raw material group becomes：
100 parts by weight of acrylonitrile, 10 ~ 15 parts by weight of acrylamide, 5 ~ 10 parts by weight of methyl methacrylate, 3 ~ 6 weight of nano modifier
Measure part, 0.2 ~ 0.3 parts by weight of initiator；
(2) coagulation forming：After the spinning solution is measured, filtered, is extruded into coagulating bath and coagulated by filament spinning component
Gu obtaining as-spun fibre；
(3) as-spun fibre obtains modified acrylic fibre after superheated water drawing-off, washing, vacuum drying.
Acrylamide is mainly used for introducing hydrophilic radical, improves the hygroscopicity energy, methyl methacrylate is for improving fiber
Intensity overcomes acrylamide to introduce the defect that hydrophilic radical brings fibre strength to decline；The present invention by nano modifier with polymerize
Monomer in situ polymerization reaction, nano modifier disperse that more evenly, secondary agglomeration, Nanometer coffee carbon dust and nano-zirconium carbide can be prevented
With far-infrared functional, heating property can be improved, Nanometer coffee carbon dust can assign fiber surface hole abundant, to improve suction
The addition of wet performance, Nanometer coffee carbon dust can also bacteriostasis, and deodorization, uvioresistant.Nano-zirconium carbide can improve the wearability of fabric
Energy.
Preferably, the initiator is azo-bis-iso-dimethyl.
Preferably, the nano modifier is by Nanometer coffee carbon dust and nano-zirconium carbide according to 1:2 ~ 3 weight ratio is mixed
It closes.
Preferably, the coagulating bath is the liquor zinci chloridi of mass concentration 20 ~ 25%, setting temperature is 1 ~ 5 DEG C；It is described
The hot water temperature of hot water drawing-off is 100 DEG C, and hot water drafting multiple is 3 ~ 5 times.
The beneficial effects of the invention are as follows：
The present invention has excellent moisture pick-up properties, and water absorption rate is up to 28%, and the present invention has spontaneous well when meeting steam
Thermal effect, good warmth retention effect.In addition, the present invention has both the functions such as wash resistant, antibacterial deodourizing, uvioresistant.
Specific embodiment
Below by specific embodiment, technical scheme of the present invention will be further explained in detail.
In the present invention, if not refering in particular to, used raw material and equipment etc. are commercially available or commonly used in the art.
Method in following embodiments is unless otherwise instructed the conventional method of this field.
Embodiment 1：
A kind of moisture absorption heating heat-preserving function panty hose, including panty hose ontology, the panty hose ontology are interweaved by inner yarn and table yarn
Form, the inner yarn by modified acrylic fibre and it is modified polynosic is blended forms, the table yarn is spandex, by weight hundred
Divide than meter, the group of each fibrous raw material of panty hose ontology becomes：Spandex 8%, modified polynosic 75%, modified acrylic fibre
17%。
The modified polynosic is prepared by the following method and obtains：
（1）Polynosic, sodium hydroxide solution and ethyl alcohol are added in kneader simultaneously, control 38 DEG C of temperature, alkalize 25min；
Polynosic：Sodium hydroxide solution：Mass ratio=1 of ethyl alcohol：6：3；The mass concentration of the sodium hydroxide solution is 15%, ethyl alcohol
Mass concentration be 90%.
（2）By the monoxone ethanol solution and step of mass concentration 70%（1）Polynosic after alkalization is uniformly mixed, ether
The temperature for changing reaction is controlled at 72 DEG C, is reacted 60 minutes, and polynosic, which is adopted, after etherificate is neutralized with hydrochloric acid, distillation water washing, centrifugation,
And it is dried in vacuo；The mass ratio of polynosic and monoxone ethanol solution is 1: 1.2.
（3）By step（2）The polynosic handled is soaked in 30min in 30 DEG C of temperature of crosslinking agent, is subsequently added into pyrrole
Pyridine, hydrazine sulfate ethanol solution, control 40 DEG C of temperature cross-linking reaction 14 hours, distill water washing after reaction, be centrifuged, and true
Sky is dry, is then placed in 35 DEG C of polyethylene glycol and impregnates 60s, is finally dried in vacuo.The crosslinking agent is that concentration is 0.01moL/L
N, the ethanol solution of N- dicyclohexylcarbodiimide；The concentration of the ethanol solution of hydrazine sulfate is 0.008moL/L.It is described rich and powerful
Fiber：Crosslinking agent：Pyridine：Mass ratio=1 of the ethanol solution of hydrazine sulfate:6 0：0.3:60.
The modified acrylic fibre is prepared by the following method and obtains：
(1) prepared by spinning solution：The polymerization reaction raw material of 20 parts by weight is added in the solvent dimethyl sulfoxide of 100 parts by weight
It mixes, is reacted 16 hours at 40 DEG C, spinning solution is obtained after discontinuous degassing；The polymerization reaction raw material group becomes：Acrylonitrile 100
Parts by weight, 10 parts by weight of acrylamide, 10 parts by weight of methyl methacrylate, 3 parts by weight of nano modifier, two isobutyric acid of azo
0.2 parts by weight of dimethyl ester；
(2) coagulation forming：After the spinning solution is measured, filtered, is extruded into coagulating bath and coagulated by filament spinning component
Gu obtaining as-spun fibre；The nano modifier is by Nanometer coffee carbon dust and nano-zirconium carbide according to 1:2 weight ratio mixing and
At.The coagulating bath is the liquor zinci chloridi of mass concentration 20%, and setting temperature is 1 DEG C；The hot water temperature of the hot water drawing-off is
100 DEG C, hot water drafting multiple is 3 times.
(3) as-spun fibre obtains modified acrylic fibre after superheated water drawing-off, washing, vacuum drying.
Embodiment 2：
A kind of moisture absorption heating heat-preserving function panty hose, including panty hose ontology, the panty hose ontology are interweaved by inner yarn and table yarn
Form, the inner yarn by modified acrylic fibre and it is modified polynosic is blended forms, the table yarn is spandex, by weight hundred
Divide than meter, the group of each fibrous raw material of panty hose ontology becomes：Spandex 7%, modified polynosic 78%, modified acrylic fibre
15%。
The modified polynosic is prepared by the following method and obtains：
（1）Polynosic, sodium hydroxide solution and ethyl alcohol are added in kneader simultaneously, control 42 DEG C of temperature, alkalize 20min；
Polynosic：Sodium hydroxide solution：Mass ratio=1 of ethyl alcohol： 9： 5；The mass concentration of the sodium hydroxide solution is 10%, second
The mass concentration of alcohol is 85%.
（2）By the monoxone ethanol solution and step of mass concentration 75%（1）Polynosic after alkalization is uniformly mixed, ether
The temperature for changing reaction is controlled at 75 DEG C, is reacted 40 minutes, and polynosic, which is adopted, after etherificate is neutralized with hydrochloric acid, distillation water washing, centrifugation,
And it is dried in vacuo；The mass ratio of polynosic and monoxone ethanol solution is 1:0.8.
（3）By step（2）The polynosic handled is soaked in 25min in 35 DEG C of temperature of crosslinking agent, is subsequently added into pyrrole
Pyridine, hydrazine sulfate ethanol solution, control temperature 45 C cross-linking reaction 12 hours, distill water washing after reaction, be centrifuged, and true
Sky is dry, is then placed in 40 DEG C of polyethylene glycol and impregnates 30s, is finally dried in vacuo.The crosslinking agent is that concentration is 0.012moL/
The ethanol solution of the N of L, N- dicyclohexylcarbodiimide；The concentration of the ethanol solution of hydrazine sulfate is 0.009moL/L.It is described rich and powerful
Fiber：Crosslinking agent：Pyridine：Mass ratio=1 of the ethanol solution of hydrazine sulfate: 70： 0.5: 70.
The modified acrylic fibre is prepared by the following method and obtains：
(1) prepared by spinning solution：The polymerization reaction raw material of 25 parts by weight is added in the solvent dimethyl sulfoxide of 100 parts by weight
It mixes, is reacted 12 hours at 45 DEG C, spinning solution is obtained after discontinuous degassing；The polymerization reaction raw material group becomes：Acrylonitrile
100 parts by weight, 15 parts by weight of acrylamide, 5 parts by weight of methyl methacrylate, 6 parts by weight of nano modifier, two isobutyl of azo
0.3 parts by weight of dimethyl phthalate；
(2) coagulation forming：After the spinning solution is measured, filtered, is extruded into coagulating bath and coagulated by filament spinning component
Gu obtaining as-spun fibre；The nano modifier is by Nanometer coffee carbon dust and nano-zirconium carbide according to 1:3 weight ratio mixing
It forms.The coagulating bath is the liquor zinci chloridi of mass concentration 25%, and setting temperature is 5 DEG C；The hot water temperature of the hot water drawing-off
It is 100 DEG C, hot water drafting multiple is 5 times.
(3) as-spun fibre obtains modified acrylic fibre after superheated water drawing-off, washing, vacuum drying.
Embodiment 3：
A kind of moisture absorption heating heat-preserving function panty hose, including panty hose ontology, the panty hose ontology are interweaved by inner yarn and table yarn
Form, the inner yarn by modified acrylic fibre and it is modified polynosic is blended forms, the table yarn is spandex, by weight hundred
Divide than meter, the group of each fibrous raw material of panty hose ontology becomes：Spandex 8%, modified polynosic 78%, modified acrylic fibre
14%。
The modified polynosic is prepared by the following method and obtains：
（1）Polynosic, sodium hydroxide solution and ethyl alcohol are added in kneader simultaneously, control 40 DEG C of temperature, alkalize 25min；
Polynosic：Sodium hydroxide solution：Mass ratio=1 of ethyl alcohol：7：4；The mass concentration of the sodium hydroxide solution is 12%, ethyl alcohol
Mass concentration be 90%.
（2）By the monoxone ethanol solution and step of mass concentration 72%（1）Polynosic after alkalization is uniformly mixed, ether
The temperature for changing reaction is controlled at 74 DEG C, is reacted 50 minutes, and polynosic, which is adopted, after etherificate is neutralized with hydrochloric acid, distillation water washing, centrifugation,
And it is dried in vacuo；The mass ratio of polynosic and monoxone ethanol solution is 1:1.
（3）By step（2）The polynosic handled is soaked in 28min in 32 DEG C of temperature of crosslinking agent, is subsequently added into pyrrole
Pyridine, hydrazine sulfate ethanol solution, control 42 DEG C of temperature cross-linking reaction 13 hours, distill water washing after reaction, be centrifuged, and true
Sky is dry, is then placed in 38 DEG C of polyethylene glycol and impregnates 50s, is finally dried in vacuo.The crosslinking agent is that concentration is 0.01moL/L
N, the ethanol solution of N- dicyclohexylcarbodiimide；The concentration of the ethanol solution of hydrazine sulfate is 0.0085moL/L.It is described rich and powerful
Fiber：Crosslinking agent：Pyridine：Mass ratio=1 of the ethanol solution of hydrazine sulfate:65：0.4:65.
The modified acrylic fibre is prepared by the following method and obtains：
(1) prepared by spinning solution：The polymerization reaction raw material of 22 parts by weight is added in the solvent dimethyl sulfoxide of 100 parts by weight
It mixes, is reacted 14 hours at 42 DEG C, spinning solution is obtained after discontinuous degassing；The polymerization reaction raw material group becomes：Acrylonitrile 100
Parts by weight, 12 parts by weight of acrylamide, 7 parts by weight of methyl methacrylate, 5 parts by weight of nano modifier, two isobutyric acid of azo
0.25 parts by weight of dimethyl ester；
(2) coagulation forming：After the spinning solution is measured, filtered, is extruded into coagulating bath and coagulated by filament spinning component
Gu obtaining as-spun fibre；The nano modifier is by Nanometer coffee carbon dust and nano-zirconium carbide according to 1:3 weight ratio mixing
It forms.The coagulating bath is the liquor zinci chloridi of mass concentration 20%, and setting temperature is 2 DEG C；The hot water temperature of the hot water drawing-off
It is 100 DEG C, hot water drafting multiple is 4 times.
(3) as-spun fibre obtains modified acrylic fibre after superheated water drawing-off, washing, vacuum drying.
The manufacturing of panty hose is carried out according to existing common process.
Properties of product Testing index of the invention is as follows：
（1）Safety indexes：
Content of formaldehyde/（mg/kg）：It is not detected；
PH value=8.0.
（2）Color fastness index：
The color fastness of resistance to dry friction/grade：4-5；
Moisture-proof colorfastness to rubbing/grade：4-5.
（3）Moisture absorption heating functional parameter：
Highest heating value/DEG C：9.7；
Average heating value in 30min/DEG C：3.4；
Water absorption rate >=25%.
Above-mentioned embodiment is only a preferred solution of the present invention, not the present invention is made in any form
Limitation, there are also other variations and modifications on the premise of not exceeding the technical scheme recorded in the claims.
Claims (10)
1. a kind of moisture absorption heating heat-preserving function panty hose, including panty hose ontology, the panty hose ontology is handed over by inner yarn and table yarn
Knit, which is characterized in that the inner yarn by modified acrylic fibre and it is modified polynosic is blended forms, the table yarn is
Spandex, by weight percentage, the group of each fibrous raw material of panty hose ontology become：Spandex 7 ~ 8%, modified polynosic 75 ~ 78%,
Modified acrylic fibre 14 ~ 17%.
2. a kind of moisture absorption heating heat-preserving function panty hose according to claim 1, which is characterized in that the rich and powerful fibre of modification
Dimension is prepared by the following method and obtains：
（1）Polynosic, sodium hydroxide solution and ethyl alcohol are added in kneader simultaneously, 38 ~ 42 DEG C of temperature of control, alkalization 20 ~
25min；
（2）By the monoxone ethanol solution and step of mass concentration 70 ~ 75%（1）Polynosic after alkalization is uniformly mixed, etherificate
The temperature of reaction is controlled at 72 ~ 75 DEG C, is reacted 40 ~ 60 minutes, and polynosic, which is adopted, after etherificate is neutralized with hydrochloric acid, and distills water washing,
Centrifugation, and be dried in vacuo；
（3）By step（2）The polynosic handled is soaked in 25 ~ 30min in 30 ~ 35 DEG C of temperature of crosslinking agent, is subsequently added into
The ethanol solution of pyridine, hydrazine sulfate controls 40 ~ 45 DEG C of temperature cross-linking reaction 12 ~ 14 hours, distills water washing after reaction,
Centrifugation, and be dried in vacuo, it is then placed in 30 ~ 60s of immersion in 35 ~ 40 DEG C of polyethylene glycol, is finally dried in vacuo.
3. a kind of moisture absorption heating heat-preserving function panty hose according to claim 2, which is characterized in that the polynosic：
Sodium hydroxide solution：Mass ratio=1 of ethyl alcohol：6~9：3~5.
4. a kind of moisture absorption heating heat-preserving function panty hose according to claim 2, which is characterized in that the sodium hydroxide is molten
The mass concentration of liquid is 10 ~ 15%, and the mass concentration of ethyl alcohol is 85 ~ 90%；The mass ratio of polynosic and monoxone ethanol solution
It is 1:0.8~1.2.
5. a kind of moisture absorption heating heat-preserving function panty hose according to claim 2, which is characterized in that the crosslinking agent is dense
Degree is the N of 0.01 ~ 0.012moL/L, the ethanol solution of N- dicyclohexylcarbodiimide；The concentration of the ethanol solution of hydrazine sulfate is
0.008~0.009moL/L。
6. a kind of modified polyacrylonitrile moisture absorption heating heat-preserving function panty hose according to claim 2, which is characterized in that institute
State polynosic：Crosslinking agent：Pyridine：Mass ratio=1 of the ethanol solution of hydrazine sulfate:6 0~70：0.3~0.5:60~70.
7. a kind of moisture absorption heating heat-preserving function panty hose according to claim 1, which is characterized in that the modified polypropene
Nitrile fiber is prepared by the following method and obtains：
(1) prepared by spinning solution：The polymerization reaction raw material of 20 ~ 25 parts by weight is added to the solvent dimethyl sulfoxide of 100 parts by weight
Middle mixing reacts 12 ~ 16 hours at 40 ~ 45 DEG C, spinning solution is obtained after discontinuous degassing；The polymerization reaction raw material group becomes：
100 parts by weight of acrylonitrile, 10 ~ 15 parts by weight of acrylamide, 5 ~ 10 parts by weight of methyl methacrylate, 3 ~ 6 weight of nano modifier
Measure part, 0.2 ~ 0.3 parts by weight of initiator；
(2) coagulation forming：After the spinning solution is measured, filtered, is extruded into coagulating bath and coagulated by filament spinning component
Gu obtaining as-spun fibre；
(3) as-spun fibre obtains modified acrylic fibre after superheated water drawing-off, washing, vacuum drying.
8. a kind of moisture absorption heating heat-preserving function panty hose according to claim 7, which is characterized in that the nano modifier
By Nanometer coffee carbon dust and nano-zirconium carbide according to 1:2 ~ 3 weight ratio mixes.
9. a kind of moisture absorption heating heat-preserving function panty hose according to claim 7, which is characterized in that the initiator is even
Two isobutyl dimethyl phthalate of nitrogen.
10. a kind of moisture absorption heating heat-preserving function panty hose according to claim 7, which is characterized in that the coagulating bath is
The liquor zinci chloridi of mass concentration 20 ~ 25%, setting temperature are 1 ~ 5 DEG C；The hot water temperature of the hot water drawing-off is 100 DEG C, hot water
Drafting multiple is 3 ~ 5 times.
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