CN108850987A - A kind of spice salt production process inhibiting the oxidation of wind goose - Google Patents
A kind of spice salt production process inhibiting the oxidation of wind goose Download PDFInfo
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- CN108850987A CN108850987A CN201810657910.5A CN201810657910A CN108850987A CN 108850987 A CN108850987 A CN 108850987A CN 201810657910 A CN201810657910 A CN 201810657910A CN 108850987 A CN108850987 A CN 108850987A
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- spice
- salt
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- goose
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- 235000013599 spices Nutrition 0.000 title claims abstract description 140
- 150000003839 salts Chemical class 0.000 title claims abstract description 115
- 241000272814 Anser sp. Species 0.000 title claims abstract description 81
- 230000003647 oxidation Effects 0.000 title claims abstract description 27
- 238000007254 oxidation reaction Methods 0.000 title claims abstract description 27
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 21
- 230000002401 inhibitory effect Effects 0.000 title claims abstract description 15
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 35
- 239000000203 mixture Substances 0.000 claims abstract description 25
- 229920002774 Maltodextrin Polymers 0.000 claims abstract description 23
- 239000005913 Maltodextrin Substances 0.000 claims abstract description 23
- 229940035034 maltodextrin Drugs 0.000 claims abstract description 23
- 229920000858 Cyclodextrin Polymers 0.000 claims abstract description 20
- 238000002386 leaching Methods 0.000 claims abstract description 20
- 239000001116 FEMA 4028 Substances 0.000 claims abstract description 19
- WHGYBXFWUBPSRW-FOUAGVGXSA-N beta-cyclodextrin Chemical compound OC[C@H]([C@H]([C@@H]([C@H]1O)O)O[C@H]2O[C@@H]([C@@H](O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O3)[C@H](O)[C@H]2O)CO)O[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@@H]3O[C@@H]1CO WHGYBXFWUBPSRW-FOUAGVGXSA-N 0.000 claims abstract description 19
- 235000011175 beta-cyclodextrine Nutrition 0.000 claims abstract description 19
- 229960004853 betadex Drugs 0.000 claims abstract description 19
- 238000002288 cocrystallisation Methods 0.000 claims abstract description 18
- 235000019441 ethanol Nutrition 0.000 claims abstract description 17
- 235000013409 condiments Nutrition 0.000 claims abstract description 16
- 239000000843 powder Substances 0.000 claims abstract description 15
- 244000062241 Kaempferia galanga Species 0.000 claims abstract description 13
- 235000013421 Kaempferia galanga Nutrition 0.000 claims abstract description 13
- 244000089698 Zanthoxylum simulans Species 0.000 claims abstract description 13
- 235000009421 Myristica fragrans Nutrition 0.000 claims abstract description 12
- 244000223014 Syzygium aromaticum Species 0.000 claims abstract description 12
- 235000016639 Syzygium aromaticum Nutrition 0.000 claims abstract description 12
- 239000000463 material Substances 0.000 claims abstract description 12
- 239000001702 nutmeg Substances 0.000 claims abstract description 12
- 238000010438 heat treatment Methods 0.000 claims abstract description 9
- 238000003756 stirring Methods 0.000 claims abstract description 9
- 238000003825 pressing Methods 0.000 claims abstract description 8
- 244000270834 Myristica fragrans Species 0.000 claims abstract 3
- 239000002893 slag Substances 0.000 claims description 12
- IDGUHHHQCWSQLU-UHFFFAOYSA-N ethanol;hydrate Chemical compound O.CCO IDGUHHHQCWSQLU-UHFFFAOYSA-N 0.000 claims description 8
- 230000002093 peripheral effect Effects 0.000 claims description 8
- 229920001353 Dextrin Polymers 0.000 claims description 2
- 239000004375 Dextrin Substances 0.000 claims description 2
- 235000019425 dextrin Nutrition 0.000 claims description 2
- 230000003078 antioxidant effect Effects 0.000 abstract description 13
- 239000003963 antioxidant agent Substances 0.000 abstract description 12
- 238000004140 cleaning Methods 0.000 abstract description 7
- 240000007232 Illicium verum Species 0.000 abstract description 3
- 235000008227 Illicium verum Nutrition 0.000 abstract description 3
- 238000000227 grinding Methods 0.000 abstract 1
- 238000007873 sieving Methods 0.000 abstract 1
- 235000006708 antioxidants Nutrition 0.000 description 11
- 241000498779 Myristica Species 0.000 description 9
- 239000007788 liquid Substances 0.000 description 8
- -1 Ion radical Chemical class 0.000 description 5
- 239000013078 crystal Substances 0.000 description 5
- HHEAADYXPMHMCT-UHFFFAOYSA-N dpph Chemical compound [O-][N+](=O)C1=CC([N+](=O)[O-])=CC([N+]([O-])=O)=C1[N]N(C=1C=CC=CC=1)C1=CC=CC=C1 HHEAADYXPMHMCT-UHFFFAOYSA-N 0.000 description 5
- 230000000694 effects Effects 0.000 description 5
- 230000002209 hydrophobic effect Effects 0.000 description 5
- 238000000034 method Methods 0.000 description 5
- 239000002304 perfume Substances 0.000 description 5
- 230000002000 scavenging effect Effects 0.000 description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- OTEKOJQFKOIXMU-UHFFFAOYSA-N 1,4-bis(trichloromethyl)benzene Chemical compound ClC(Cl)(Cl)C1=CC=C(C(Cl)(Cl)Cl)C=C1 OTEKOJQFKOIXMU-UHFFFAOYSA-N 0.000 description 4
- BGNXCDMCOKJUMV-UHFFFAOYSA-N Tert-Butylhydroquinone Chemical compound CC(C)(C)C1=CC(O)=CC=C1O BGNXCDMCOKJUMV-UHFFFAOYSA-N 0.000 description 4
- 235000019658 bitter taste Nutrition 0.000 description 4
- 239000012267 brine Substances 0.000 description 4
- 239000003205 fragrance Substances 0.000 description 4
- 238000002360 preparation method Methods 0.000 description 4
- HPALAKNZSZLMCH-UHFFFAOYSA-M sodium;chloride;hydrate Chemical compound O.[Na+].[Cl-] HPALAKNZSZLMCH-UHFFFAOYSA-M 0.000 description 4
- 239000000243 solution Substances 0.000 description 4
- 238000003860 storage Methods 0.000 description 4
- 239000002699 waste material Substances 0.000 description 4
- 239000000654 additive Substances 0.000 description 3
- 230000000996 additive effect Effects 0.000 description 3
- 230000000844 anti-bacterial effect Effects 0.000 description 3
- 239000000796 flavoring agent Substances 0.000 description 3
- 235000019634 flavors Nutrition 0.000 description 3
- 235000013305 food Nutrition 0.000 description 3
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 3
- 230000005764 inhibitory process Effects 0.000 description 3
- 239000003921 oil Substances 0.000 description 3
- 150000002978 peroxides Chemical class 0.000 description 3
- 241000194032 Enterococcus faecalis Species 0.000 description 2
- UFWIBTONFRDIAS-UHFFFAOYSA-N Naphthalene Chemical compound C1=CC=CC2=CC=CC=C21 UFWIBTONFRDIAS-UHFFFAOYSA-N 0.000 description 2
- 229920002678 cellulose Polymers 0.000 description 2
- 239000001913 cellulose Substances 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 229940032049 enterococcus faecalis Drugs 0.000 description 2
- 239000000284 extract Substances 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- 235000003642 hunger Nutrition 0.000 description 2
- 238000005286 illumination Methods 0.000 description 2
- 229920005610 lignin Polymers 0.000 description 2
- 239000008601 oleoresin Substances 0.000 description 2
- 238000003672 processing method Methods 0.000 description 2
- 150000003254 radicals Chemical class 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 230000037351 starvation Effects 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 235000019640 taste Nutrition 0.000 description 2
- 239000004250 tert-Butylhydroquinone Substances 0.000 description 2
- 235000019281 tert-butylhydroquinone Nutrition 0.000 description 2
- 239000000341 volatile oil Substances 0.000 description 2
- 241000251468 Actinopterygii Species 0.000 description 1
- 244000061520 Angelica archangelica Species 0.000 description 1
- 241000193830 Bacillus <bacterium> Species 0.000 description 1
- 241000193755 Bacillus cereus Species 0.000 description 1
- 244000037364 Cinnamomum aromaticum Species 0.000 description 1
- 235000014489 Cinnamomum aromaticum Nutrition 0.000 description 1
- 235000019542 Cured Meats Nutrition 0.000 description 1
- 240000006927 Foeniculum vulgare Species 0.000 description 1
- 235000004204 Foeniculum vulgare Nutrition 0.000 description 1
- 235000001287 Guettarda speciosa Nutrition 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 241000218394 Magnolia liliiflora Species 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000001476 alcoholic effect Effects 0.000 description 1
- 230000036528 appetite Effects 0.000 description 1
- 235000019789 appetite Nutrition 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 235000011194 food seasoning agent Nutrition 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
- 230000008595 infiltration Effects 0.000 description 1
- 238000001764 infiltration Methods 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 235000013372 meat Nutrition 0.000 description 1
- LPUQAYUQRXPFSQ-DFWYDOINSA-M monosodium L-glutamate Chemical compound [Na+].[O-]C(=O)[C@@H](N)CCC(O)=O LPUQAYUQRXPFSQ-DFWYDOINSA-M 0.000 description 1
- 235000013923 monosodium glutamate Nutrition 0.000 description 1
- 239000004223 monosodium glutamate Substances 0.000 description 1
- 238000005457 optimization Methods 0.000 description 1
- 238000012803 optimization experiment Methods 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 238000004806 packaging method and process Methods 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 235000020995 raw meat Nutrition 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- HFHDHCJBZVLPGP-UHFFFAOYSA-N schardinger α-dextrin Chemical compound O1C(C(C2O)O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC(C(O)C2O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC2C(O)C(O)C1OC2CO HFHDHCJBZVLPGP-UHFFFAOYSA-N 0.000 description 1
- 238000003307 slaughter Methods 0.000 description 1
- 238000002791 soaking Methods 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 238000009461 vacuum packaging Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
- A23L27/10—Natural spices, flavouring agents or condiments; Extracts thereof
- A23L27/11—Natural spices, flavouring agents or condiments; Extracts thereof obtained by solvent extraction
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23B—PRESERVING, e.g. BY CANNING, MEAT, FISH, EGGS, FRUIT, VEGETABLES, EDIBLE SEEDS; CHEMICAL RIPENING OF FRUIT OR VEGETABLES; THE PRESERVED, RIPENED, OR CANNED PRODUCTS
- A23B4/00—General methods for preserving meat, sausages, fish or fish products
- A23B4/14—Preserving with chemicals not covered by groups A23B4/02 or A23B4/12
- A23B4/18—Preserving with chemicals not covered by groups A23B4/02 or A23B4/12 in the form of liquids or solids
- A23B4/20—Organic compounds; Microorganisms; Enzymes
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23B—PRESERVING, e.g. BY CANNING, MEAT, FISH, EGGS, FRUIT, VEGETABLES, EDIBLE SEEDS; CHEMICAL RIPENING OF FRUIT OR VEGETABLES; THE PRESERVED, RIPENED, OR CANNED PRODUCTS
- A23B4/00—General methods for preserving meat, sausages, fish or fish products
- A23B4/14—Preserving with chemicals not covered by groups A23B4/02 or A23B4/12
- A23B4/18—Preserving with chemicals not covered by groups A23B4/02 or A23B4/12 in the form of liquids or solids
- A23B4/24—Inorganic compounds
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L13/00—Meat products; Meat meal; Preparation or treatment thereof
- A23L13/40—Meat products; Meat meal; Preparation or treatment thereof containing additives
- A23L13/42—Additives other than enzymes or microorganisms in meat products or meat meals
- A23L13/428—Addition of flavours, spices, colours, amino acids or their salts, peptides, vitamins, yeast extract or autolysate, nucleic acid or derivatives, organic acidifying agents or their salts or acidogens, sweeteners, e.g. sugars or sugar alcohols; Addition of alcohol-containing products
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L13/00—Meat products; Meat meal; Preparation or treatment thereof
- A23L13/40—Meat products; Meat meal; Preparation or treatment thereof containing additives
- A23L13/42—Additives other than enzymes or microorganisms in meat products or meat meals
- A23L13/432—Addition of inorganic compounds, e.g. minerals; oligo-elements
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
- A23L27/40—Table salts; Dietetic salt substitutes
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
- A23L27/70—Fixation, conservation, or encapsulation of flavouring agents
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
- A23L27/70—Fixation, conservation, or encapsulation of flavouring agents
- A23L27/72—Encapsulation
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
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- Chemical & Material Sciences (AREA)
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- Food Science & Technology (AREA)
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- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
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- Chemical Kinetics & Catalysis (AREA)
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- Seasonings (AREA)
Abstract
A kind of spice salt production process inhibiting the oxidation of wind goose, includes the following steps：1）By the spice mix grinding and sieving of cloves, galanga, Chinese prickly ash, nutmeg and illiciumverum, the ethanol solution that 10-30 times of condiment powder weight is added impregnates 2-5h at 30-80 DEG C, after filters pressing, obtains spice leaching liquor；2）The spice leaching liquor of 1-6 times of salt weight is added into salt, and is separately added into the beta-cyclodextrin of salt weight 2-10% and the maltodextrin of 2-10%, heating concentration, ethyl alcohol is recycled, is heated while stirring, is done until moisture is received, material is fully crystallized, and obtains spice salt cocrystallization embedded object；3）It crushes, crosses 30 meshes.The present invention can effectively prevent the loss of antioxidant content in spice, and effective component can be evenly distributed on goose body surface face with salt, and it is fast to penetrate into goose body speed, and goose body surface face is without spice fines, without cleaning, it is easy to accomplish the standardization green production of wind goose.
Description
Technical field
The invention belongs to food processing technology field, it is related to inhibiting the spice salt preparation of wind goose oxidation.
Background technique
Wind goose is one of famous traditional native article in China, is cured meat and fish good merchantable brand.Although various regions processing technology is different,
It but is formed marinated through salt, air-dried after goose slaughter.Traditional wind goose is to produce in winter, and salt dosage is up to 10%, storage period
It is 3-6 months, with the raising of temperature, grease can be aoxidized quickly, cause wind goose rotten.It can suitably delay to produce using vacuum packaging
Product oxidation, but cannot be from solving the problems, such as at all, effect is limited.Some producers are by adding chemically synthesized antioxidant, such as：
TBHQ, sodium iso-vc etc., the antioxidant to inhibit wind goose to aoxidize, but add chemistry are just receiving more and more consumers conflict.
Therefore, a kind of Natural Antioxidants that can efficiently inhibit wind goose to aoxidize are badly in need of in the production of wind goose.
Spice is common seasoning, has the function of that flavouring is dispelled raw meat, the effect of improving a poor appetite.Research also indicates that spice
Have the function of anti-oxidant and antibacterial.But it is used to inhibiting the oxidation of wind goose there are following main problem spice, first, can have
Effect, which inhibits the spice composition of wind goose Oxidation of Fat and Oils to be screened and optimized, just can determine that；Second, graininess spice, perfume (or spice)
Pungent material essential oil or oleoresin are difficult to be uniformly mixed with raw material goose when marinated；Third, the spice of powdery still contain more
It is slow to have that effective component penetrates into goose body when marinated for cellulose, lignin；4th, the spice fines of powdery can stick
Invest goose body surface face, the time-consuming water wasting of when cleaning, and be difficult to clean up, influence wind goose product appearance.
Summary of the invention
The purpose of the present invention is in view of the deficiencies of the prior art, propose a kind of spice salt preparation side of inhibition wind goose oxidation
Method, is effectively retained the ingredients such as the flavors such as fragrance and antioxidant in spice, and product is easy to use without slag, is easy to mix, enter
Taste is fast, significantly inhibits wind goose Oxidation of Fat and Oils, substantially reduces the discharge of salt dosage and brine waste, extend the shelf life, helps realization
The standardization green production of wind goose.
The present invention is achieved by the following technical solutions.
A kind of spice salt production process inhibiting the oxidation of wind goose of the present invention, includes the following steps.
（1）The preparation of spice leaching liquor：It is 20-30% cloves, 10-30% galanga, 10-30% Chinese prickly ash, 10- by weight ratio
The spice mix of 30% nutmeg and 10-20% illiciumverum smashes it through 10-60 mesh, and the second of 10-30 times of condiment powder weight is added
Alcoholic solution impregnates 2-5h at 30-80 DEG C, after filters pressing, obtains spice leaching liquor.
（2）The preparation of spice salt cocrystallization embedded object：The spice extraction of 1-6 times of salt weight is added into salt
Liquid, and it is separately added into the beta-cyclodextrin of salt weight 2-10% and the maltodextrin of 2-10%, heating concentration is boiled, ethyl alcohol is recycled,
It heats while stirring, the peripheral speed of anchor agitator blade outer rim is 0.2-1.5m/s, is done until moisture is received, material is tied completely
Crystalline substance obtains spice salt cocrystallization embedded object.
（3）The packaging of spice salt：Spice salt cocrystallization embedded object is crushed, and 30 meshes are crossed, and the inhibition without slag is made
The spice salt finished product of wind goose oxidation.
Step of the present invention（1）Middle preferred weight ratio is that 25% cloves, 20% galanga, 20% Chinese prickly ash, 20% nutmeg and 15% are octagonal
Spice mix.
Step of the present invention（1）In spice mix is preferably smashed it through into 30 meshes.
Step of the present invention（1）In be preferably added to 20 times of condiment powder weight of ethanol solution and impregnate 3 h at 50 DEG C.
Step of the present invention（1）Middle preferred alcohol solution is 50%（v/v）Ethanol water.
Step of the present invention（2）In 2 times of salt weight of spice leaching liquor is added preferably into salt.
Step of the present invention（2）In be preferably separately added into the beta-cyclodextrin of salt weight 5% and 5% maltodextrin.
Step of the present invention（2）In the peripheral speed of preferably blade outer rim be 0.6m/s.
It is comparative studies illiciumverum, cassia bark, Chinese prickly ash, spiceleaf, cloves, meat bandit, tsaoko, fennel seeds, the root of Dahurain angelica, careless button, mountain naphthalene, old
Skin, Radix Glycyrrhizae, the flower bud of lily magnolia, galanga, fructus amomi etc. more than 20 commonly uses the oxidation resistance of spice, it is found that different spices remove super oxygen yin
Ion radical (O2 -), hydroxy radical (OH) it is different for the ability of bitter taste diazanyl free radical (DPPH) with hexichol, it is same
The ability that the water extract and alcohol extract of spice remove three kinds of free radicals is also different, chooses remove three kinds of free radical abilities by force five
Kind spice is combined optimization experiment, and spice salt is made for wind goose processing experiment, as a result, it has been found that weight ratio is 25% fourth
The octagonal spice mix object of perfume, 20% galanga, 20% Chinese prickly ash, 20% nutmeg and 15% can effectively inhibit wind goose Oxidation of Fat and Oils, and use is fresh
The peroxide value < 1.1g/100g that the wind goose product that the spice salt that goose weighs 2.7% is pickled is placed at room temperature for 9 months（With buttermeter）,
Meet wind goose national standard≤1.5g/100g requirement, and suitable with the addition effect of chemical antioxidants TBHQ, and tradition is pure
The peroxide value that the marinated wind goose product of salt method is placed at room temperature for 6 months is as high as 2.0g/100g, and the results are shown in attached figure 1.Cause
This, the composition of spice mix determined by the present invention can effectively inhibit wind goose to aoxidize, and achieve in wind goose production application imaginary
Less than remarkable result.
It is difficult to be uniformly mixed with raw material goose when marinated for graininess spice, aromatic condiment essential oil or oleoresin, and
The spice of powdery still contains more cellulose, lignin, there is a problem of that effective component infiltration goose body is slow when marinated,
The present invention is removed by the way that the effective component in cloves, galanga, Chinese prickly ash, nutmeg and octagonal five kinds of spice mix to be leached out
After bits, then with salt hybrid process at instant spice salt without slag.Effective component in spice can be uniformly distributed with salt
In goose body surface face, it is fast to penetrate into goose body speed, and goose body surface face is without spice fines, without cleaning, it is easy to accomplish the standard of wind goose
Change green production.
The present invention cloves, galanga, Chinese prickly ash, nutmeg and octagonal five kinds of spice mix are crushed after with 50%（v/v）Ethyl alcohol
The molten and water-soluble fragrance matter of alcohol in spice, antibacterial and antioxidant content can be sufficiently leached out by aqueous solution soaking,
It effectively prevents extracting insufficient, the larger problem of loss of effective components in spice when being extracted with ethyl alcohol or water merely.
By adding beta-cyclodextrin into spice leaching liquor, the hydrophobic combination in spice can be made to include to β-ring paste
In the cavity of essence, maltodextrin, which is added, can sufficiently embed the beta-cyclodextrin containing the hydrophobic combination in spice, make β-ring paste
Smart cavity is closed at both ends, effectively prevent the volatilization and oxidational losses of the hydrophobic combination in spice, to significantly extend product
Stability and the shelf-life.
The effective components such as the fragrance matter in smashed condiment powder are volatile or aoxidize, and the easy moisture absorption, unsuitable long-term
Storage.Spice leaching liquor is added in salt by the present invention, boils heating concentration, in salt crystallization, spice leaching liquor
In hydrophilic composition can enter salt crystals, with salt cocrystallization.Maltodextrin, which is added, sufficiently to be embedded containing in spice
The salt cocrystallization object of hydrophilic composition, effective starvation and illumination prevent the oxidation of the hydrophilic composition in spice from damaging
It loses, to significantly extend stability and the shelf-life of product.
The present invention heats while stirring in heating crystalline, so that the crystal of salt and beta-cyclodextrin is smaller, and with stirring
The crystal of the increase of speed, salt and beta-cyclodextrin can become very tiny, and the specific surface area of the salt of Unit Weight sharply increases
Add, the amount of hydrophilic composition also dramatically increases in spice leaching liquor entrained by cocrystallization.
To compare different processing methods to the preservation effect of flavor in spice and antioxidant content, in optimization of the invention
Under the conditions of, it is that 25% cloves, 20% galanga, 20% Chinese prickly ash, 20% nutmeg and 15% octagonal spice mix smash it through by weight ratio
The 50% of 20 times of spice weight is added in 30 meshes（v/v）Ethanol water impregnate 3h at 50 DEG C, after filters pressing, obtain perfume (or spice)
Pungent material leaching liquor, the spice leaching liquor of 2 times of its weight is added into salt, and is separately added into the beta-cyclodextrin of salt weight 5%
Maltodextrin with 5%, boils heating concentration, heats while stirring, and the peripheral speed of anchor agitator blade outer rim is 0.6m/
S is crushed spice salt cocrystallization embedded object until material is fully crystallized, and after crossing 30 meshes, is weighed, and pack is made without slag
Inhibit wind goose oxidation spice salt finished product（Labeled as spice liquid+salt+beta-cyclodextrin+maltodextrin）；In same item
Under part, the spice salt finished product that maltodextrin is not added is prepared respectively（Labeled as spice liquid+salt+beta-cyclodextrin）, β-is not added
The spice salt finished product of cyclodextrin（Labeled as spice liquid+salt+maltodextrin）, the spice salt finished product of salt is not added（Mark
It is denoted as spice liquid+beta-cyclodextrin+maltodextrin）, the spice salt finished product of beta-cyclodextrin and maltodextrin is not added（Labeled as perfume (or spice)
Pungent feed liquid+salt）, the spice salt finished product of salt and maltodextrin is not added（Labeled as spice liquid+beta-cyclodextrin）, food is not added
The spice salt finished product of salt and beta-cyclodextrin（Labeled as spice liquid+maltodextrin）, and traditionally prepare fragrant pungent
Expect salt finished product（Labeled as condiment powder+salt）.After all samples are stored 12 months, their scavenging hydroxyls are measured respectively
(OH) and hexichol is for the ability of bitter taste diazanyl free radical (DPPH), and the results are shown in attached figure 2 and 3.
From attached drawing 2 and 3 as can be seen that being removed after spice salt products storage 12 months using made from the method for the present invention
The ability highest of OH and DPPH, traditional product remove the ability of the two not as good as its one third, show that the present invention can be protected effectively
Deposit the flavor and antioxidant content in spice.The Scavenging activity of maltodextrin group is not added than adding maltodextrin group low, table
Bright maltodextrin can not only sufficiently embed beta-cyclodextrin, keep beta-cyclodextrin cavity closed at both ends, moreover it is possible to it is total to embed spice salt
Crystal；The Scavenging activity of salt group is not added than adding the low of salt group, shows that salt can be with the water-soluble wind in spice
Taste and antioxidant content form cocrystallization object, to significantly extend stability and the shelf-life of product.
The present invention has the following advantages that compared with prior art.
The composition of spice mix determined by the present invention can effectively inhibit wind goose to aoxidize, and wind goose product is guaranteed the quality in room temperature storage
Phase up to 9 months or more, wind goose salt content≤4.5%.The present invention spice mix is crushed after with 50%（v/v）Ethanol water
It impregnates, the molten and water-soluble fragrance matter of the alcohol in spice, antibacterial and antioxidant content is sufficiently leached out, remove bits
Afterwards, with salt cocrystallization at instant spice salt without slag.Spice salt is easy to use, and the effective component in spice can be with
Salt is evenly distributed on goose body surface face, and it is fast to penetrate into goose body speed, and goose body surface face is without spice fines, without cleaning, it is easy to accomplish
The standardization green production of wind goose.
The present invention pastes β-ring by the hydrophobic combination in beta-cyclodextrin inclusion compound spice, and by maltodextrin embedding
Smart cavity is closed at both ends, effectively prevent the volatilization and oxidational losses of the hydrophobic combination in spice.Meanwhile the parent in spice
Water composition and salt cocrystallization, sufficiently embed, effective starvation and illumination into salt crystals, and by maltodextrin, prevent
The only oxidational losses of the hydrophilic composition in spice.Compared with traditional condiment powder, the present invention no slag spice produced
Product salt has the advantages that stability is good and long shelf-life.
Detailed description of the invention
Fig. 1 is influence diagram of the different processing methods to wind goose peroxide value.
Fig. 2 is capable of trying hard to for different sample scavenging hydroxyls (OH).
Fig. 3 is that different samples removing hexichol can try hard to for bitter taste diazanyl free radical (DPPH).
Specific embodiment
The present invention is further described by following embodiment.
Embodiment 1.
It is after 25% cloves, 20% galanga, 20% Chinese prickly ash, 20% nutmeg and 15% octagonal spice mix crush by weight ratio
30 meshes are crossed, the 50% of 20 times of condiment powder weight is added（v/v）Ethanol water impregnate 3h at 50 DEG C, after filters pressing, obtain
To spice leaching liquor, the spice leaching liquor of 2 times of its weight is added into salt, and is separately added into β-ring of salt weight 5%
Dextrin and 5% maltodextrin, boiled through high steam, heating concentration, recycle ethyl alcohol, heat while stirring, anchor agitator paddle
The peripheral speed of leaf outer rim is 0.6m/s, is done until moisture is received, and material is fully crystallized, and obtains spice salt cocrystallization embedded object,
Spice salt cocrystallization embedded object is crushed, after crossing 30 meshes, is weighed, the perfume (or spice) for inhibiting the oxidation of wind goose without slag is made in pack
Pungent material salt finished product.
For obtained spice product salt in marinated Xingguo Grey Geese, additive amount is the 3% of fresh smooth goose weight, easy to use, fragrant
Effective component in pungent material can be evenly distributed on goose body surface face with salt, it is fast penetrate into goose body speed, and goose body surface face is thin without spice
Bits, without cleaning, substantially reduce the discharge of brine waste, it can be achieved that wind goose standardization green production, antioxidant effect is significant,
Shelf life of products can significantly reduce the salt content of wind goose up to 9 months（≤5%）.Obtained spice product salt is deposited in bag
After putting 12 months, scavenging hydroxyl (OH) and hexichol are all remarkably higher than for the ability of bitter taste diazanyl free radical (DPPH)
Traditional condiment powder product inhibits spoilage organisms enterococcus faecalis in food（Enterococcus faecalis）CGMCC1.2135
And Bacillus cercus（Bacillus cereus）The ability of CGMCC1.260 is also significantly stronger than traditional condiment powder product, table
The bright present invention no slag spice product salt produced has stability good and the distinguishing feature of long shelf-life.
Embodiment 2.
It is after 25% cloves, 20% galanga, 20% Chinese prickly ash, 20% nutmeg and 15% octagonal spice mix crush by weight ratio
30 meshes are crossed, the 50% of 20 times of condiment powder weight is added（v/v）Ethanol water impregnate 2h at 65 DEG C, after filters pressing, obtain
To spice leaching liquor, the spice leaching liquor of 3 times of its weight is added into salt, and β-ring paste of salt weight 5% is added
Essence, 7.5% maltodextrin and 5% monosodium glutamate, boil through high steam, and heating concentration recycles ethyl alcohol, heats while stirring, anchor
The peripheral speed of formula propeller-blade outer rim is 0.7m/s, is done until moisture is received, material is fully crystallized, and is obtained spice salt and is tied altogether
Brilliant embedded object is crushed spice salt cocrystallization embedded object, after crossing 30 meshes, is weighed, and the inhibition wind goose without slag is made in pack
The spice salt finished product of oxidation.
For obtained spice product salt in marinated Yangzhou white goose, additive amount is the 2.7% of fresh smooth goose weight, easy to use,
Effective component in spice can be evenly distributed on goose body surface face with salt, it is fast penetrate into goose body speed, and goose body surface face is without spice
Fines, without cleaning, substantially reduce the discharge of brine waste, it can be achieved that wind goose standardization green production, antioxidant effect is aobvious
It writes, shelf life of products can significantly reduce the salt content of wind goose up to 9 months（≤4.5%）.
Embodiment 3.
It is after 25% cloves, 20% galanga, 20% Chinese prickly ash, 20% nutmeg and 15% octagonal spice mix crush by weight ratio
20 meshes are crossed, the 50% of 10 times of condiment powder weight is added（v/v）Ethanol water impregnate 2h at 70 DEG C, after filters pressing, to
The 50% of 10 times of condiment powder weight is added in spice slag（v/v）Ethanol water 2 h are impregnated at 70 DEG C, through filters pressing
Afterwards, merge the spice leaching liquor extracted twice, after extracting twice, the effective component extraction in spice is more filled
Point, the spice leaching liquor of 2 times of its weight is added into salt, and the beta-cyclodextrin and salt weight 5% of salt weight 5% is added
Maltodextrin, boiled through high steam, heating concentration, recycle ethyl alcohol, heat while stirring, anchor agitator blade outer rim
Peripheral speed is 0.6 m/s, is done until moisture is received, material is fully crystallized, and spice salt cocrystallization embedded object is obtained, by spice
Salt cocrystallization embedded object is crushed, cross 30 meshes after, weigh, pack, be made without slag inhibit wind goose oxidation spice salt at
Product.
For obtained spice product salt in marinated Yangzhou white goose, additive amount is the 3% of fresh smooth goose weight, easy to use, fragrant
Effective component in pungent material can be evenly distributed on goose body surface face with salt, it is fast penetrate into goose body speed, and goose body surface face is thin without spice
Bits, without cleaning, substantially reduce the discharge of brine waste, it can be achieved that wind goose standardization green production, antioxidant effect is significant,
And the salt content of wind goose can be significantly reduced（≤5%）.
Claims (8)
1. a kind of spice salt production process for inhibiting the oxidation of wind goose, it is characterized in that including the following steps：
（1）It is that 20-30% cloves, 10-30% galanga, 10-30% Chinese prickly ash, 10-30% nutmeg and 10-20% are octagonal by weight ratio to mix
10-60 mesh is crossed after conjunction condiment powder is broken, the ethanol solution that 10-30 times of condiment powder weight is added impregnates 2- at 30-80 DEG C
5h obtains spice leaching liquor after filters pressing；
（2）The spice leaching liquor of 1-6 times of salt weight is added into salt, and is separately added into β-ring of salt weight 2-10%
The maltodextrin of dextrin and 2-10% boils heating concentration, recycles ethyl alcohol, heat while stirring, anchor agitator blade outer rim
Peripheral speed is 0.2-1.5m/s, is done until moisture is received, material is fully crystallized, and obtains spice salt cocrystallization embedded object；
（3）Spice salt cocrystallization embedded object is crushed, cross 30 meshes, be made without slag inhibit wind goose oxidation spice salt at
Product.
2. a kind of spice salt production process for inhibiting the oxidation of wind goose according to claim 1, it is characterized in that step（1）In
Weight ratio is 25% cloves, 20% galanga, 20% Chinese prickly ash, 20% nutmeg and 15% octagonal spice mix.
3. a kind of spice salt production process for inhibiting the oxidation of wind goose according to claim 1, it is characterized in that step（1）In
Spice mix is smashed it through into 30 meshes.
4. a kind of spice salt production process for inhibiting the oxidation of wind goose according to claim 1, it is characterized in that step（1）In
20 times of condiment powder weight of ethanol solution is added and impregnates 3 h at 50 DEG C.
5. a kind of spice salt production process for inhibiting the oxidation of wind goose according to claim 1, it is characterized in that step（1）In
Ethanol solution is 50%（v/v）Ethanol water.
6. a kind of spice salt production process for inhibiting the oxidation of wind goose according to claim 1, it is characterized in that step（2）In
2 times of salt weight of spice leaching liquor is added into salt.
7. a kind of spice salt production process for inhibiting the oxidation of wind goose according to claim 1, it is characterized in that step（2）In
It is separately added into the beta-cyclodextrin of salt weight 5% and 5% maltodextrin.
8. a kind of spice salt production process for inhibiting the oxidation of wind goose according to claim 1, it is characterized in that step（2）In
The peripheral speed of blade outer rim is 0.6m/s.
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