CN108843377A - A kind of coal seam high pressure hydrothermal solution resistanceization method - Google Patents

A kind of coal seam high pressure hydrothermal solution resistanceization method Download PDF

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Publication number
CN108843377A
CN108843377A CN201810505188.3A CN201810505188A CN108843377A CN 108843377 A CN108843377 A CN 108843377A CN 201810505188 A CN201810505188 A CN 201810505188A CN 108843377 A CN108843377 A CN 108843377A
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steel pipe
solution
pressure
retardant
coal
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CN108843377B (en
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亓冠圣
陆伟
程卫民
李金亮
胡相明
路遥
谢军
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Shandong University of Science and Technology
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Shandong University of Science and Technology
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    • EFIXED CONSTRUCTIONS
    • E21EARTH OR ROCK DRILLING; MINING
    • E21FSAFETY DEVICES, TRANSPORT, FILLING-UP, RESCUE, VENTILATION, OR DRAINING IN OR OF MINES OR TUNNELS
    • E21F5/00Means or methods for preventing, binding, depositing, or removing dust; Preventing explosions or fires
    • EFIXED CONSTRUCTIONS
    • E21EARTH OR ROCK DRILLING; MINING
    • E21CMINING OR QUARRYING
    • E21C35/00Details of, or accessories for, machines for slitting or completely freeing the mineral from the seam, not provided for in groups E21C25/00 - E21C33/00, E21C37/00 or E21C39/00
    • E21C35/04Safety devices
    • EFIXED CONSTRUCTIONS
    • E21EARTH OR ROCK DRILLING; MINING
    • E21FSAFETY DEVICES, TRANSPORT, FILLING-UP, RESCUE, VENTILATION, OR DRAINING IN OR OF MINES OR TUNNELS
    • E21F5/00Means or methods for preventing, binding, depositing, or removing dust; Preventing explosions or fires
    • E21F5/02Means or methods for preventing, binding, depositing, or removing dust; Preventing explosions or fires by wetting or spraying
    • E21F5/06Fluids used for spraying

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  • Engineering & Computer Science (AREA)
  • Mining & Mineral Resources (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Geology (AREA)
  • Mechanical Engineering (AREA)
  • Consolidation Of Soil By Introduction Of Solidifying Substances Into Soil (AREA)

Abstract

The invention discloses a kind of coal seam high pressure hydrothermal solution resistanceization methods, belong to preventing and extinguishing fire of coal mine technical field.It plays concordant drilling in coal seam first, certain density high temperature retardant solution is prepared using high temperature slot, it will be in the concordant drilling in retardant solution high pressure injection coal seam using high-pressure pump, after retardant solution is sufficiently reacted with coal, by concordant drill in retardant solution extraction be discharged into high temperature slot, then to concordant drilling in circulation water filling with draw water, by concordant drill in heat discharge.By the high pressure pressure injection high temperature retardant solution into coal bed drilling, active group of the retardant in high temperature and high pressure environment with coal surface is reacted.The present invention can significantly reduce the quantity of the active group on coal surface, further increase the resistance efficiency of retardant, effectively prevent the generation of coal spontaneous combustion disaster, have wide applicability in the art.

Description

A kind of coal seam high pressure hydrothermal solution resistanceization method
Technical field
The invention belongs to preventing and extinguishing fire of coal mine technical fields, are specifically related to a kind of resistance of the high pressure pressure injection high temperature into coal bed drilling Method of the agent solution to prevent spontaneous combustion of coal seam.
Background technique
Coal spontaneous combustion is one of the major natural disasters that coal mine faces.Coal spontaneous combustion can not only generate toxic and harmful gas, can also Cause gas explosion, causes huge casualties and economic loss.Retardant fire prevention is conventional one of fire prevention means, chemistry Retardant can be reacted with the active group in coal, and the quantity of the active group by reducing coal surface reaches prevention coal spontaneous combustion Effect.
Currently, using retardant prevent coal spontaneous combustion when mainly use room temperature retardant, at a temperature of room temperature, retardant with The chemical reaction that coal occurs is extremely limited, and the active group on coal surface can not effectively eliminate, and the Inhibition of retardant is simultaneously It cannot give full play to.It is anti-by improving retardant and coal generation according to Chemical Kinetics and chemical reaction thermodynamic argument The temperature of environment, is aided with hyperbaric environment where seasonable, can be improved the response intensity of retardant and coal, can strength removal coal surface Active group, significantly reduce coal from thermal hazard, can effectively prevent the generation of coal spontaneous combustion disaster.
Summary of the invention
In order to solve above-mentioned defect existing in the prior art, the invention proposes a kind of coal seam high pressure hydrothermal solution resistanceization sides Method, by the high pressure pressure injection high temperature retardant solution into coal bed drilling, enable retardant in high temperature and high pressure environment with The active group on coal surface reacts, and significantly reduces the quantity of the active group on coal surface, improves the resistance efficiency of retardant.
Its technical solution includes:
A kind of coal seam high pressure hydrothermal solution resistanceization method, which is characterized in that successively include the following steps:
A constructs concordant drilling in coal seam, and insertion hole packer carries out sealing of hole in the described concordant drilling;
Hardware needed for b prepares comprising solution tank, control temperature unit, rabbling mechanism, drawing liquid pump, high-pressure pump and process pipeline, The control temperature unit and rabbling mechanism is installed in the solution tank, and the control temperature unit is used for in solution tank Liquid is heated up and maintains constant temperature, and the rabbling mechanism is for being stirred the liquid in solution tank;The technique Pipeline includes sebific duct, intermediate steel pipe, water supplying pipe, drainpipe, the first steel pipe, the second steel pipe, third steel pipe and the 4th steel pipe, by institute The intermediate penstock installation stated is connect with the solution tank by sebific duct at the middle part of the hole packer, by the intermediate steel pipe, and It is sequentially connected high-pressure pump, pressure gauge and flow valve on the sebific duct close to solution tank one end, by the water supplying pipe and the solution Slot is connected by the first steel pipe, the drainpipe, the drawing liquid pump and the intermediate steel pipe is connected by third steel pipe, by institute It states water supplying pipe and is connect with the high-pressure pump by the second steel pipe, the drawing liquid pump and the solution tank are passed through into the 4th steel pipe connecting It connects;
Retardant of the c into coal seam after injection heating,
A certain amount of water is injected into solution tank by the water supplying pipe, and a certain amount of resistanceization is added into the solution tank Control temperature unit and rabbling mechanism are opened in agent, after the fluid temperature in solution tank reaches 50 DEG C -80 DEG C, starting high-pressure pump and stream Measure valve and be perfused retardant solution into the described concordant drilling, continuous pressure injection retardant solution for a period of time after, close temperature control list Member, rabbling mechanism, high-pressure pump and flow valve;
D drawing liquid, meets step c, opens drawing liquid pump, by concordant drill in retardant solution extract and passes through the 4th steel pipe and arrange Into solution tank;
E water filling is drawn water, and step d is met, and is infused high pressure water into concordant drilling by water supplying pipe, the second steel pipe, high-pressure pump, is infused Water extracts the water in concordant drilling by third steel pipe, drawing liquid pump afterwards for a period of time and is discharged into drainpipe;
F by water filling described in step e, draw water circuit sequentially execute 12h stop, complete concordant drilling high pressure hydrothermal solution resistance Change.
As a preferred solution of the present invention, in step a, the length of the concordant drilling is 80~120m, described Hole packer length be 8m~10m, the hole packer be resistant to maximum pressure be 12MPa.
As another preferred embodiment of the invention, in step c, starts high-pressure pump and flow valve and drill to the concordant When in interior perfusion retardant solution, the outlet pressure that high-pressure pump is arranged makes the reading of pressure gauge reach 6MPa.
Further, in step e, into crossheading drilling in the injecting process, the outlet pressure that high-pressure pump is arranged makes pressure The reading of table reaches 6MPa.
Advantageous effects brought by the present invention are:
Compared with prior art, the present invention passes through high pressure pressure injection high temperature retardant solution, retardant energy in drilling to concordant Enough active groups in the environment of high pressure-temperature with coal surface react, and can be effectively reduced the active group on coal surface Quantity further increases the resistance efficiency of retardant, effectively prevents the generation of coal spontaneous combustion disaster, coal seam high pressure proposed by the present invention Hydrothermal solution resistanceization method has wide applicability and promotional value in the art.
Detailed description of the invention
The present invention will be further described with reference to the accompanying drawing:
Fig. 1 is a kind of coal seam high pressure hydrothermal solution resistanceization method schematic diagram of the invention.
In figure, the coal seam 1-, the drilling of 2- concordant, 3- hole packer, 4- sebific duct, the centre 5- steel pipe, 6- flow valve, 7- pressure gauge, 8- high-pressure pump, 9- solution tank, 10- control temperature unit, 11- rabbling mechanism, the first steel pipe of 12-, 13- water supplying pipe, the second steel pipe of 14-, 15- third steel pipe, 16- drawing liquid pump, 17- drainpipe, the 4th steel pipe of 18-.
Specific embodiment
The invention discloses a kind of coal seam high pressure hydrothermal solution resistanceization methods, in order to make advantages of the present invention, technical solution more It is clear, clear, it elaborates combined with specific embodiments below to the present invention.
As shown in Figure 1, a kind of coal seam high pressure hydrothermal solution resistanceization method of the invention, includes the following steps:
A, concordant of constructing in coal seam 1 drilling 2, insertion hole packer 3 completes the sealing of hole of concordant drilling 2 in concordant drilling 2, The length of concordant drilling 2 is 80-120m, and the length of hole packer 3 is 8m-10m, and the maximum pressure that is resistant to of hole packer 3 is 12MPa;
B, intermediate steel pipe 5, flow valve 6, pressure gauge 7, the high-pressure pump 8, solution tank of hole packer 3 are sequentially connected using sebific duct 4 9, sebific duct 4 is high pressure resistant high temperature sebific duct, there is control temperature unit 10 and rabbling mechanism 11 in solution tank 9, and control temperature unit 10 can incite somebody to action Liquid in solution tank 9 is rapidly heated to specified temperature and maintains constant temperature, and rabbling mechanism 11 can at the uniform velocity be turned with constant rate of speed It is dynamic;
C, it using the first steel pipe 12 connection underground water supplying pipe 13 and solution tank 9, is supplied water using the second steel pipe 14 connection underground Pipe 13 and high-pressure pump 8 are sequentially connected the intermediate steel pipe 5, drawing liquid pump 16 and drainage underground pipe of hole packer 3 using third steel pipe 15 17, using the 4th steel pipe 18 connection drawing liquid pump 16 and solution tank 9;
D, it is filled the water by underground water supplying pipe 13 and the first steel pipe 12 to 9 quantification of solution tank, is added to 9 quantification of solution tank Retardant starts the control temperature unit 10 and rabbling mechanism 11 of solution tank 9;
E, after the retardant solution in solution tank 9 reaches 50 DEG C -80 DEG C, starting high-pressure pump 8 and flow valve 6 are to described High temperature retardant solution is perfused in concordant drilling 2, and the outlet pressure that high-pressure pump 8 is arranged reaches the reading of pressure gauge 7 6MPa;
F, after pressure injection high temperature retardant solution 20 hours, the control temperature unit 10 closed in solution tank 9 and solution tank with stir Mechanism 11 is mixed, extracted out the retardant solution in concordant drilling 2 by drawing liquid pump 16 and is discharged to solution by the 4th steel pipe 18 In slot 9, then by underground water supplying pipe 13, the second steel pipe 14, the high pressure water injection into concordant drilling 2 of high-pressure pump 8, high-pressure pump is set 8 outlet pressure makes the reading of pressure gauge 7 reach 6MPa, and water injection time passes through third steel pipe 15, drawing liquid pump after reaching 2 hours 16 extract the water in concordants drilling 2 and are discharged into drainage underground pipe 17;
G, water filling described in step f stops after recycling execution 12h with pump process, completes the hot high pressure of concordant drilling 2 Liquid resistanceization.
Embodiment 1:
Coal seam high pressure hydrothermal solution resistanceization method, the specific steps are:
Firstly, the concordant drilling 2 that an aperture is 113mm, length is 120m of constructing in coal seam, is then with length 10m, the hole packer for being resistant to 12MPa carry out sealing of hole to concordant drilling 2.Then, successively connected using the sebific duct of resistance to 120 DEG C and 12MPa Intermediate steel pipe 5, flow valve 6, pressure gauge 7, high-pressure pump 8, the solution tank 9 for connecing hole packer 3 are supplied using the first steel pipe 12 connection underground Water pipe 13 and solution tank 9 are successively connected using the second steel pipe 14 connection underground water supplying pipe 13 and high-pressure pump 8 using third steel pipe 15 The intermediate steel pipe 5, drawing liquid pump 16 and drainage underground pipe 17 for connecing hole packer 3 connect drawing liquid pump 16 and solution using the 4th steel pipe 18 Slot 9.
It is filled the water later by underground water supplying pipe 13 and the first steel pipe 12 to 9 quantification of solution tank, simultaneous quantitative adds resistanceization Agent, in the present embodiment, retardant used is sodium chlorate, is configured to 30% sodium chlorate solution.In the present embodiment, high temperature resistanceization Agent solution will not generate corrosion to entire high pressure hydrothermal solution resistanceization system.Start the control temperature unit 10 and rabbling mechanism of solution tank 9 11, the solution in solution tank 9 is rapidly heated to 60 DEG C and maintains constant temperature by control temperature unit 10, and rabbling mechanism 11 is with 30 turns per minute Rate at the uniform velocity stir.After the retardant solution in solution tank 9 reaches 60 DEG C, starting high-pressure pump 8 and flow valve 6 are to described High temperature retardant solution is perfused in concordant drilling 2, and the outlet pressure that high-pressure pump 8 is arranged reaches the reading of pressure gauge 7 6MPa。
After high temperature retardant infusion, the temperature in drilling can be higher, in order to which the heat extraction in drilling is come out, After pressure injection high temperature retardant solution 20 hours, the control temperature unit 10 and rabbling mechanism 11 in solution tank 9 and solution tank are closed, is led to It crosses drawing liquid pump 16 to extract the retardant solution in concordant drilling 2 out and be discharged in solution tank 9 by the 4th steel pipe 18, then lead to Underground water supplying pipe 13, the second steel pipe 14, the high pressure water injection into concordant drilling 2 of high-pressure pump 8 are crossed, the outlet pressure of high-pressure pump 8 is set So that the reading of pressure gauge 7 reaches 6MPa, water injection time passes through third steel pipe 15 after reaching 2 hours, drawing liquid pump 16 extracts concordant Drilling 2 in water and be discharged into drainage underground pipe 17.Water filling stops after recycling execution 12h with pump process, completes concordant The high pressure hydrothermal solution resistanceization of drilling 2.
It uses for reference the prior art and can be realized in the part that do not addressed in the present invention.
It should be noted that:Any equivalent way that those skilled in the art are made under the introduction of this specification, or Obvious variant should all be within the scope of the present invention.

Claims (4)

1. a kind of coal seam high pressure hydrothermal solution resistanceization method, which is characterized in that successively include the following steps:
A constructs concordant drilling in coal seam, and insertion hole packer carries out sealing of hole in the described concordant drilling;
Hardware needed for b prepares comprising solution tank, control temperature unit, rabbling mechanism, drawing liquid pump, high-pressure pump and process pipeline, it is described Control temperature unit and rabbling mechanism be installed in the solution tank, the control temperature unit is used for the liquid in solution tank It is heated up and maintains constant temperature, the rabbling mechanism is for being stirred the liquid in solution tank;The process pipeline It, will be described including sebific duct, intermediate steel pipe, water supplying pipe, drainpipe, the first steel pipe, the second steel pipe, third steel pipe and the 4th steel pipe Intermediate penstock installation is connect with the solution tank by sebific duct at the middle part of the hole packer, by the intermediate steel pipe, and is being leaned on It is sequentially connected high-pressure pump, pressure gauge and flow valve on the sebific duct of nearly solution tank one end, the water supplying pipe and the solution tank are led to The connection of the first steel pipe is crossed, the drainpipe, the drawing liquid pump and the intermediate steel pipe are connected by third steel pipe, by the confession Water pipe is connect with the high-pressure pump by the second steel pipe, and the drawing liquid pump is connect with the solution tank by the 4th steel pipe;
Retardant of the c into coal seam after injection heating,
A certain amount of water is injected into solution tank by the water supplying pipe, and a certain amount of retardant is added into the solution tank, opens Open control temperature unit and rabbling mechanism, after the fluid temperature in solution tank reaches 50 DEG C -80 DEG C, start high-pressure pump and flow valve to Be perfused retardant solution in the described concordant drilling, continuous pressure injection retardant solution for a period of time after, close control temperature unit, stirring Mechanism, high-pressure pump and flow valve;
D drawing liquid, meets step c, opens drawing liquid pump, by concordant drill in retardant solution extract out and pass through the 4th steel pipe be discharged to it is molten In liquid bath;
E water filling is drawn water, and step d is met, and is filled the water by water supplying pipe, the second steel pipe, high-pressure pump into concordant drilling, when filling the water one section Between after by third steel pipe, drawing liquid pump extract concordant drilling in water and be discharged into drainpipe;
F by water filling described in step e, draw water circuit sequentially execute 12h stop, complete concordant drilling high pressure hydrothermal solution resistanceization.
2. a kind of coal seam high pressure hydrothermal solution resistanceization method according to claim 1, it is characterised in that:In step a, described is suitable The length of layer drilling is 80~120m, and the length of the hole packer is 8m~10m, and the hole packer is resistant to maximum pressure and is 12MPa。
3. a kind of coal seam high pressure hydrothermal solution resistanceization method according to claim 1, it is characterised in that:In step c, start high pressure When pump and flow valve are perfused in retardant solution into the concordant drilling, the outlet pressure that high-pressure pump is arranged makes pressure gauge Reading reach 6MPa.
4. a kind of coal seam high pressure hydrothermal solution resistanceization method according to claim 1, it is characterised in that:In step e, bored to crossheading In hole in the injecting process, the outlet pressure that high-pressure pump is arranged makes the reading of pressure gauge reach 6MPa.
CN201810505188.3A 2018-05-24 2018-05-24 A kind of coal seam high pressure hydrothermal solution resistanceization method Active CN108843377B (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110819417A (en) * 2019-11-26 2020-02-21 辽宁大学 Method for treating coal-fired atmospheric pollution by coal seam water injection

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101092879A (en) * 2007-07-26 2007-12-26 康怀宇 Method for injecting retarder to coal body
CN202578751U (en) * 2012-04-06 2012-12-05 中国矿业大学 Fire extinguishing and cooling system used in coal empty and loose areas of coal field fire zone
CN106121711A (en) * 2016-06-22 2016-11-16 陈舸 A kind of high fire-retardance pliable and tough artesian water glass combined casting material and preparation method
CN108005706A (en) * 2017-10-16 2018-05-08 山东科技大学 A kind of gas for preventing spontaneous combustion in goaf helps formula spraying device
CN108301862A (en) * 2018-04-23 2018-07-20 华北科技学院 A kind of new method preventing spontaneous combustion of remaining coal to goaf pressure injection retardant

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101092879A (en) * 2007-07-26 2007-12-26 康怀宇 Method for injecting retarder to coal body
CN202578751U (en) * 2012-04-06 2012-12-05 中国矿业大学 Fire extinguishing and cooling system used in coal empty and loose areas of coal field fire zone
CN106121711A (en) * 2016-06-22 2016-11-16 陈舸 A kind of high fire-retardance pliable and tough artesian water glass combined casting material and preparation method
CN108005706A (en) * 2017-10-16 2018-05-08 山东科技大学 A kind of gas for preventing spontaneous combustion in goaf helps formula spraying device
CN108301862A (en) * 2018-04-23 2018-07-20 华北科技学院 A kind of new method preventing spontaneous combustion of remaining coal to goaf pressure injection retardant

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110819417A (en) * 2019-11-26 2020-02-21 辽宁大学 Method for treating coal-fired atmospheric pollution by coal seam water injection

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