CN108825209A - A kind of research oil-well cement ring alters the device and method of slot closure rule - Google Patents

A kind of research oil-well cement ring alters the device and method of slot closure rule Download PDF

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Publication number
CN108825209A
CN108825209A CN201810636720.5A CN201810636720A CN108825209A CN 108825209 A CN108825209 A CN 108825209A CN 201810636720 A CN201810636720 A CN 201810636720A CN 108825209 A CN108825209 A CN 108825209A
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oil
blocking agent
different
oil well
rule
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CN108825209B (en
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傅程
黄斌
宋考平
张宇
赵博文
代亭阁
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Northeast Petroleum University
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    • EFIXED CONSTRUCTIONS
    • E21EARTH OR ROCK DRILLING; MINING
    • E21BEARTH OR ROCK DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
    • E21B47/00Survey of boreholes or wells
    • E21B47/005Monitoring or checking of cementation quality or level

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  • Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Mining & Mineral Resources (AREA)
  • Quality & Reliability (AREA)
  • Geophysics (AREA)
  • Environmental & Geological Engineering (AREA)
  • Fluid Mechanics (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Consolidation Of Soil By Introduction Of Solidifying Substances Into Soil (AREA)

Abstract

The present invention relates to a kind of research oil-well cement rings to alter the device and method that slot blocks rule, wherein it includes blocking agent injection device, oil well model, multiple groups bismuth terne metal thin slice, steel column that research oil-well cement ring, which alters slot to block the device of rule,;The intermediate receptacle of blocking agent injection device is connect with oil well model, and the perforation of oil well model is separately connected the core of a different permeabilities;The outer tube of oil well model is formed by two semi-circular tube make-ups, and inner and outer tubes are coaxially twisted admittedly between top cover and pedestal, and steel column is for blocking perforation;Multiple groups width 25mm bismuth terne metal thin slice, one group is thickness is identical, length is identical, bending shape is different multiple bismuth terne metal pieces;One group identical for length, the bismuth terne metal piece that shape is identical, thickness is different;One group identical for thickness, the bismuth terne metal piece that shape is identical, length is different.The plastic situation of various blocking agents in the crack of observable various forms of the present invention, migration rule of the blocking agent in core and cement sheath in interstitial space.

Description

A kind of research oil-well cement ring alters the device and method of slot closure rule
Technical field
The present invention relates to technical field of oil production engineering, and in particular to a kind of research oil-well cement ring alters the dress of slot closure rule It sets and method.
Background technique
In oil extraction operation, oil well produces water, influences on economic benefit very big, in some instances it may even be possible to certain barrelers be caused to turn Become uncommercial oil well.Well water is likely to occur the region of bypassed oil that hydrosphere closes, infuses as taken measures not in time in stratum Enter water to detour and mistake, to reduce recovery ratio, causes greatly to waste.Well water is made it is also possible to destroy reservoir structure At sand production;Also it will increase relative density of fluid after well water, increase shaft bottom oil pressure, flowing well is made to switch to pumpingh well;Separately Outside, well water can corrode underground equipment, may cause accident when serious, increase simultaneously as producing water, will necessarily make ground Dehydration expense increases.And well water takes increase lifting rate, the method with water band oil be it is uneconomical, worthless, it is water detection, stifled Water be must be solved the problems, such as in time in oil field development and oilfield chemistry research important topic.
With the extension of oil field development time and secondary, Tertiary infilling recovery scheme implementation, oil field subsurface picture is more next It is more complicated, discovery to alter slot well also more and more.Since that alters slot, especially multi-section multi-layer alters slot, straticulate exploration is upset, has caused Serious interlayer interference.Both at home and abroad at present oilwell water shutoff practical activity prove, water-blocking operation fail the reason of, more than half Be due to that cannot recognize and determine all kinds of differences for altering slot and its property, in Correct Analysis oil well difference alter groove shape, Size is particularly significant, because the different shape for altering slot directly determines to alter in slot blocking agent plugging effect and quality and blocking agent in difference State, directly affect the development effectiveness in oil field.
Currently, existing chemical water shutoff method is mainly general injection blocking agent, different blocking agents are not distinguished in difference The injection situation in slot is altered, due to having very big difference in parameters such as different crack inner capillary tube power, pressure-bearings, general injection is stifled Agent will cause great waste, and plugging effect is difficult to accurately estimate, so, it is real that simulation oil well crack is carried out in laboratory Test it is particularly important, by injecting blocking agent in the crack to different shape, blocking agent envelope metric rule and suitable in overall merit crack Injection parameter.
Summary of the invention
It is an object of the present invention to provide a kind of research oil-well cement rings to alter the device that slot blocks rule, and this method is used Solve the problems, such as that present oilwell water shutoff can not consider that slot property is altered in underground, it is a further object to provide this researchs Oil-well cement ring alters slot and blocks the method that the device of rule carries out experimental study.
The technical solution adopted by the present invention to solve the technical problems is:This research oil-well cement ring alters slot and blocks rule Device include blocking agent injection device, oil well model, multiple groups bismuth terne metal thin slice, steel column;Blocking agent injection device by constant-flux pump, Intermediate receptacle, pressure gauge, six-way valve composition, constant-flux pump connect intermediate receptacle, and intermediate receptacle is connected by six-way valve and oil well model It connects, pressure gauge is mounted on six-way valve, and the perforation of oil well model is separately connected the core of a different permeabilities;Oil well model packet Inner tube, outer tube, top cover, pedestal are included, outer tube is formed by two semi-circular tube make-ups, and inner tube, outer tube upper and lower end both ends all have spiral shell Line has a circular protrusions among pedestal, and circular protrusions have external screw thread, and pedestal outer has internal screw thread, and inner and outer tubes are coaxial It twists admittedly between top cover and pedestal, there is blocking agent injection hole among top cover, one-to-one perforation is arranged in inner and outer tubes, and steel column is used Vaseline is used to block perforation after smearing;Multiple groups width 25mm bismuth terne metal thin slice, one group for thickness is identical, length is identical, The different multiple bismuth terne metal pieces of bending shape;One group identical for length, the bismuth terne metal that shape is identical, thickness is different Piece;One group identical for thickness, the bismuth terne metal piece that shape is identical, length is different.
It is provided with sealing at the docking that two semi-circular tube make-ups are formed in above scheme, prevents cement from leaking.
In above scheme there are two oil well models, the inner tube high 600mm of one of oil well model, internal diameter 140mm, wall thickness 5mm;Outer tube high 600mm, internal diameter 200mm, wall thickness 5mm;The inner tube of another oil well model high 300mm, internal diameter 140mm, wall thickness 5mm, outer tube high 300mm, internal diameter 200mm, wall thickness 5mm, with the closure rule in the crack for comparing different length.
Bismuth terne metal sheet thickness >=0.5mm in above scheme, for being bent into various shape.
Bismuth terne metal sheet thickness is 0.5mm, 0.8mm, 1mm in above scheme, is selected among 2mm, 3mm.
The research oil-well cement ring alters slot and blocks the method that the device of rule researches:
After steel column is smeared with vaseline, it is inserted into perforation respectively, for blocking perforation;To annular space between inner tube and outer tube Cement is injected, the bismuth terne metal thin slice of multiple and different thickness, different shape, different length is against into steel column insertion cement respectively In, each bismuth terne metal piece endpoint is stayed in respectively at two perforations, and after cement solidification, being heated to 50 DEG C applies steel column outer wall The vaseline smeared melts, and extracts steel column out, then the oil well model with cementing concrete ring is warming up to 100 DEG C, makes bismuth terne metal Piece is melted in cement, is flowed out to outside oil well model by perforation, and is gone out remaining liquid alloy with 100 DEG C of boiled water, is made Make the cement sheath with different shape, different length crack;Then by oil well model and blocking agent note with cementing concrete ring Enter device connection, and a core will be connected at each perforation, blocking agent is injected into cement sheath, after blocking agent is fully cured, takes out Cement sheath and core carry out slice axially and radially, under the microscope observe various forms crack in various blocking agents at Migration rule of the blocking agent retentate blocking agent in core and cement sheath in gluey condition, distribution, shape characteristic and interstitial space Rule, to sum up closure rule of the different blocking agents in different cracks.
The invention has the advantages that:
Current water shutoff in oil well is only to inject blocking agent according to blocking agent property and geological condition roughly come rough selection, Not only plugging effect is bad, and closure success rate is low, is also easy to appearance and blocks duration short situation.Sum up its reason, mainly It is to understand very little to altering slot property in oil well and alter the match condition information of slot and blocking agent, underground address situation is complicated, alters slot Form, size are even more to be difficult to survey.The present invention is low using bismuth terne metal fusing point and can make very thin, is easy to be converted into each Kind this feature of shape, simulation underground are difficult to the form in the various cracks measured, melt bismuth terne metal thin slice by heating, Crack is formed in cement sheath, then injects different blocking agents into model, can be very good various in the crack of observation various forms The plastic situation of blocking agent, distribution, shape characteristic, fortune of the blocking agent retentate blocking agent in core and cement sheath in interstitial space Rule is moved, so that closure rule of the different blocking agents in different cracks is summed up, by rule application and practical oil field, it will greatly Ground improves the utilization rate and plugging effect of blocking agent, greatly reduces the loss in oil field development, improves oil well output.
Detailed description of the invention
Fig. 1 is that present invention research oil-well cement ring alters the structural schematic diagram that slot blocks the device of rule;
Fig. 2 is outer tube and inner tube main view in the present invention;
Fig. 3 is outer tube and inner tube top view in the present invention;
Fig. 4 is the schematic diagram of pedestal of the present invention;
Bismuth terne metal thin slice side view in Fig. 5 step 2 of the present invention;
Bismuth terne metal thin slice side view in Fig. 6 step 7 of the present invention;
Fig. 7 present invention is Step 8: bismuth slicker solder closes thin gold wafer side view in nine;
Fig. 8 present invention is Step 10: bismuth terne metal thin slice side view in 11.
In figure:1 constant-flux pump, 2 intermediate receptacles, 3 pressure gauges, 4 six-way valves, 5 oil well models, 6 graduated cylinders, 7 cores.
Specific embodiment
The present invention will be further described below with reference to the drawings:
As shown in Figure 1, it is this research oil-well cement ring alter slot block rule device include blocking agent injection device, oil well model 5, Core 7, bismuth terne metal thin slice, steel column, blocking agent injection device is by constant-flux pump 1, intermediate receptacle 2, pressure gauge 3,4 groups of six-way valve At constant-flux pump 1 connects intermediate receptacle 2, and intermediate receptacle 2 is connect by six-way valve 4 with oil well model 5, and it is logical that pressure gauge 3 is mounted on six On valve 4, there are two cores 7, and the permeability of two cores 7 is different, and each core 7 is respectively used to the perforation phase with oil well model 5 Connection, core 7 can be used to simulate the strata condition of different permeabilities.As shown in Figure 2 and Figure 3, oil well model 5 include inner tube, it is outer Pipe, top cover, pedestal, outer tube are formed by two semi-circular tube make-ups, and inner tube, outer tube upper and lower end both ends all have screw thread, such as Fig. 4 institute Show there are a circular protrusions among pedestal, circular protrusions have external screw thread, and pedestal outer has internal screw thread, and inner and outer tubes are coaxial It twists admittedly between top cover and pedestal, two semicanals, at a detachable oil-pipe external wall, can be repeated real by pedestal fixed-analog It tests;There is blocking agent injection hole among top cover, for connecting blocking agent injection device, blocking agent injects bore dia 10mm in present embodiment, One-to-one perforation is arranged in inner and outer tubes, and perforation is used to simulation oil well perforation, and perforation diameter is 12mm in present embodiment, When being tested into inner and outer tubes Process of Cementing, two steel columns are respectively used to block perforation after being smeared with vaseline;Ginseng Read Fig. 5, multiple groups width 25mm bismuth terne metal thin slice, one group is thickness is identical, length is identical, bending shape is different multiple bismuths Terne metal piece;One group identical for length, the different bismuth terne metal piece of shape same thickness;One group identical for thickness, shape The different bismuth terne metal piece of equal length.
In order to which the closure for comparing the crack of different length is regular, two oil well models, one of oil well mould are made respectively 5 inner tube of type high 600mm, internal diameter 140mm, wall thickness 5mm;Outer tube high 600mm, internal diameter 200mm, wall thickness 5mm;Another oil well model 5 inner tube high 300mm, internal diameter 140mm, wall thickness 5mm, outer tube high 300mm, internal diameter 200mm, wall thickness 5mm.
Research oil-well cement ring alter slot block rule method the specific steps are:
Research oil-well cement ring is connected by Fig. 1 and alters the device that slot blocks rule, blocking agent is put into intermediate receptacle 2, is opened flat Stream pump 1 injects blocking agent with the constant-velocity of 0.3ml/min, and blocking agent is injected into oil well model 5 by six-way valve 4, passes through bottom Perforation is injected into cement and core 7, the external graduated cylinder 6 of core 7, when core 7 corresponding with perforation begins with blocking agent exudation, is stopped Inject blocking agent.
Step 1:One combination of oil well model 5 is installed, after two steel columns are smeared with vaseline, insertion is penetrated respectively Kong Zhong injects cementing concrete into the annular space between inner tube and outer tube for blocking two perforations.
Step 2:Prepare with a thickness of 0.5mm, the straight bismuth terne metal thin slice of a length of 600mm(Refering to Fig. 5)Against steel column It is inserted into cement.
Step 3:After theing cement solidifies, melts vaseline for 50 DEG C the heating of oil well model 5, extract the steel column in perforation out.
Step 4:Oil well model 5 is put into high/low temperature experimental box, 100 DEG C is heated to, melts alloy sheet, then use 100 DEG C of boiling water rinse, and alloy sheet fusing Liquid Residue is prolonged perforation and is developed.
Step 5:The oil well model 5 that step 4 obtains is connect with blocking agent injection device, and ready two kinds are permeated Rate core 7 is mounted on perforation, core 7 is connected with graduated cylinder 6, downwards injection of polymer gel-like blocking agent in perforation, until Corresponding core 7 has blocking agent outflow.After blocking agent plastic, core 7 is removed, opens oil well model outer tube, is taken out after blocking Cementing concrete.
Step 6:By two pieces of cores 7 and cement sheath axial slices and the radial section up and down after the closure of taking-up, it is placed on aobvious Micro- microscopic observation, observes distribution of the blocking agent in core 7 and cement sheath, shape characteristic, blocking agent retentate in interstitial space Migration rule research of the blocking agent in core 7 and cement sheath.
Step 7:Oil well model is cleaned up, with a thickness of 0.8mm, 1mm, 2mm, 3mm, length is the flat of 600mm for replacement Straight alloy sheet(Refering to Fig. 6)It is tested, repeats step 1 to step 6.
Step 8:Oil well model is cleaned up, replacement is with a thickness of 0.5mm, the alloy sheet of length 600mm and by alloy sheet It is converted into Fig. 7 shape, is tested, repeats step 1 to step 6.
Step 9:Oil well model is cleaned up, is replaced with a thickness of 0.8mm, 1mm, 2mm, the alloy sheet of 3mm is simultaneously converted into figure 7 shapes, and tested respectively, step 1 is repeated to six.
Step 10:Oil well model is cleaned up, replacement with a thickness of 0.5mm alloy sheet and is converted into Fig. 8 shape, and respectively into Row experiment repeats step 1 to step 6.
Step 11:Oil well model is cleaned up, is replaced with a thickness of 0.8mm, 1mm, 2mm, the alloy sheet of 3mm is simultaneously converted into Fig. 8 shape is tested respectively, repeats step 1 to step 6.
Step 12:The combination of another oil well model is installed, the alloy sheet that replacement length is 300mm repeats step Two are tested to step 11.
Step 13:Oil well model 5 is cleaned up, the polypropylene cyanogen Gelling Plugging Agent in step 5 be changed to The speed of 0.3ml/min injects gelled plugging agent, repeats step 1 to step 12, is tested.
Step 14:Oil well model 5 is cleaned up, the polypropylene cyanogen Gelling Plugging Agent in step 5 be changed to The speed of 0.3ml/min injects waterglass class blocking agent, repeats step 1 to step 12, is tested.
Step 15:Oil well model 5 is cleaned up, the polypropylene cyanogen Gelling Plugging Agent in step 5 be changed to The speed of 0.3ml/min injects phenol formaldehyde resin class blocking agent, repeats step 1 to step 12, is tested.
It can be very good the plastic situation of various blocking agents in the crack of observation various forms with the experimental method, be distributed shape State, shape characteristic, migration rule of the blocking agent retentate blocking agent in core 7 and cement sheath in interstitial space, to sum up not With closure rule of the blocking agent in different cracks, rule is applied to practical oil field, it will greatly improve the utilization rate of blocking agent And plugging effect, the loss in oil field development is greatly reduced, oil well output is improved.

Claims (6)

1. a kind of research oil-well cement ring alters the device that slot blocks rule, it is characterised in that:This research oil-well cement ring alters slot The device for blocking rule includes blocking agent injection device, oil well model(5), multiple groups bismuth terne metal thin slice, steel column, blocking agent injection dress It sets by constant-flux pump(1), intermediate receptacle(2), pressure gauge(3), six-way valve(4)Composition, constant-flux pump(1)Connect intermediate receptacle(2), in Between container(2)Pass through six-way valve(4)With oil well model(5)Connection, pressure gauge(3)It is mounted on six-way valve(4)On, oil well model (5)Perforation be separately connected the cores of a different permeabilities(7);Oil well model(5)Including inner tube, outer tube, top cover, pedestal, Outer tube is formed by two semi-circular tube make-ups, and inner tube, outer tube upper and lower end both ends all have screw thread, there is a circular protrusions among pedestal, Circular protrusions have external screw thread, and pedestal outer has internal screw thread, and inner and outer tubes coaxially twist solid between top cover and pedestal, top cover There is blocking agent injection hole in centre, and one-to-one perforation is arranged in inner and outer tubes, and steel column is used to block perforation after being smeared with vaseline; Multiple groups width 25mm bismuth terne metal thin slice, one group is closed for multiple bismuth slicker solders that thickness is identical, length is identical, bending shape is different Gold plaque;One group identical for length, the different bismuth terne metal piece of shape same thickness;One group identical for thickness, the identical length of shape Spend different bismuth terne metal pieces.
2. research oil-well cement ring according to claim 1 alters the device that slot blocks rule, it is characterised in that:Described two Sealing is provided at the docking that a semi-circular tube make-up is formed.
3. research oil-well cement ring according to claim 2 alters the device that slot blocks rule, it is characterised in that:The oil Well model(5)There are two, one of oil well model(5)Inner tube high 600mm, internal diameter 140mm, wall thickness 5mm;Outer tube is high 600mm, internal diameter 200mm, wall thickness 5mm;Another oil well model(5)Inner tube high 300mm, internal diameter 140mm, wall thickness 5mm, outer tube High 300mm, internal diameter 200mm, wall thickness 5mm.
4. research oil-well cement ring according to claim 3 alters the device that slot blocks rule, it is characterised in that:The bismuth Terne metal sheet thickness >=0.5mm.
5. research oil-well cement ring according to claim 4 alters the device that slot blocks rule, it is characterised in that:The bismuth Terne metal sheet thickness is 0.5mm, 0.8mm, 1mm, is selected among 2mm, 3mm.
6. a kind of research oil-well cement ring as claimed in claim 3 alters slot and blocks the method that the device of rule researches, It is characterized by comprising following steps:
One, it after smearing steel column with vaseline, is inserted into perforation respectively, for blocking perforation;To annular between inner tube and outer tube Cement is injected in space, and the bismuth terne metal thin slice of multiple and different thickness, different shape, different length is against steel column insertion respectively In cement, each bismuth terne metal piece endpoint is stayed in respectively at two perforations, and after cement solidification, being heated to 50 DEG C makes outside steel column The vaseline that wall is smeared melts, and extracts steel column out, then by the oil well model with cementing concrete ring(5)100 DEG C are warming up to, bismuth lead is made Tin alloy piece is melted in cement, flows out to oil well model by perforation(5)Outside, and with 100 DEG C of boiled water by remaining liquid it closes Gold is gone out, and the cement sheath with different shape, different length crack is produced;By the oil well model with cementing concrete ring(5) It is connect with blocking agent injection device, and a core will be connected at each perforation(7), blocking agent is injected into cement sheath, it is complete to blocking agent After solidification, cement sheath and core are taken out(7), carry out slice axially and radially;The crack of various forms is observed under the microscope In the plastic situations of various blocking agents, distribution, in shape characteristic and interstitial space blocking agent retentate blocking agent in core(7) With the migration rule in cement sheath, thus sum up different blocking agents in different cracks closure rule.
CN201810636720.5A 2018-06-20 2018-06-20 A kind of research oil-well cement ring alters the device and method of slot closure rule Active CN108825209B (en)

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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104131803A (en) * 2013-05-10 2014-11-05 中国石油大学(北京) Experiment method for evaluating shale fracturing crack mesh forming capability
CN104314514A (en) * 2014-10-10 2015-01-28 中国石油大学(华东) Visualization experiment device and method for profile control performance evaluation of weak gel of fractured reservoir
CN104500034A (en) * 2014-12-29 2015-04-08 西南石油大学 Device and method for evaluating influence of pressure change on completeness of cement sheath
CN205538625U (en) * 2016-02-17 2016-08-31 中国石油天然气股份有限公司 Experimental device for it scurries glued intensity of agent to be used for detecting sealing
CN106869895A (en) * 2017-04-07 2017-06-20 中国石油大学(华东) A kind of thing mould preparation method of indoor coal petrography hydraulic fracturing cement sheath destruction

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104131803A (en) * 2013-05-10 2014-11-05 中国石油大学(北京) Experiment method for evaluating shale fracturing crack mesh forming capability
CN104314514A (en) * 2014-10-10 2015-01-28 中国石油大学(华东) Visualization experiment device and method for profile control performance evaluation of weak gel of fractured reservoir
CN104500034A (en) * 2014-12-29 2015-04-08 西南石油大学 Device and method for evaluating influence of pressure change on completeness of cement sheath
CN205538625U (en) * 2016-02-17 2016-08-31 中国石油天然气股份有限公司 Experimental device for it scurries glued intensity of agent to be used for detecting sealing
CN106869895A (en) * 2017-04-07 2017-06-20 中国石油大学(华东) A kind of thing mould preparation method of indoor coal petrography hydraulic fracturing cement sheath destruction

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