CN108824736B - Glass mosaic and preparation method and decorative material thereof - Google Patents
Glass mosaic and preparation method and decorative material thereof Download PDFInfo
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- CN108824736B CN108824736B CN201810548584.4A CN201810548584A CN108824736B CN 108824736 B CN108824736 B CN 108824736B CN 201810548584 A CN201810548584 A CN 201810548584A CN 108824736 B CN108824736 B CN 108824736B
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- E—FIXED CONSTRUCTIONS
- E04—BUILDING
- E04F—FINISHING WORK ON BUILDINGS, e.g. STAIRS, FLOORS
- E04F13/00—Coverings or linings, e.g. for walls or ceilings
- E04F13/07—Coverings or linings, e.g. for walls or ceilings composed of covering or lining elements; Sub-structures therefor; Fastening means therefor
- E04F13/08—Coverings or linings, e.g. for walls or ceilings composed of covering or lining elements; Sub-structures therefor; Fastening means therefor composed of a plurality of similar covering or lining elements
- E04F13/14—Coverings or linings, e.g. for walls or ceilings composed of covering or lining elements; Sub-structures therefor; Fastening means therefor composed of a plurality of similar covering or lining elements stone or stone-like materials, e.g. ceramics concrete; of glass or with an outer layer of stone or stone-like materials or glass
- E04F13/145—Coverings or linings, e.g. for walls or ceilings composed of covering or lining elements; Sub-structures therefor; Fastening means therefor composed of a plurality of similar covering or lining elements stone or stone-like materials, e.g. ceramics concrete; of glass or with an outer layer of stone or stone-like materials or glass with an outer layer of glass
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Abstract
The invention discloses a glass mosaic, a preparation method thereof and a decorative material. The preparation method of the glass mosaic comprises the following steps: firstly, pretreating the original glass to obtain a mosaic primary finished product; secondly, firing the primary finished product of the glass mosaic at the firing temperature of more than 800 ℃; thirdly, cooling the sintered glass mosaic primary finished product; fourthly, grinding the cooled primary finished product of the glass mosaic according to the required shape; fifthly, soaking the primary finished product of the glass mosaic with ground bottom in alkaline solution; electroplating the soaked glass mosaic primary finished product, and coloring the ground bottom surface of the product; and (seventhly), painting and sealing the bottom of the colored primary glass mosaic finished product. Correspondingly, the invention also discloses the glass mosaic prepared by the method and a decorative material containing the glass mosaic. The glass mosaic of the invention has the advantages of three-dimensional effect, metallic feeling, high brightness, rich and colorful colors, difficult fading and excellent visual effect.
Description
Technical Field
The invention relates to a building material decorative material, in particular to a glass mosaic, a preparation method of the glass mosaic and a decorative material adopting the glass mosaic.
Background
The glass mosaic is also called glass mosaic brick or glass paper brick. It is a small-sized colored facing glass. The glass mosaic is made of natural mineral substances and glass powder, is the safest building material and is an outstanding environment-friendly material. It is acid and alkali resistant, corrosion resistant and non-fading, and is suitable for fitting wall and floor of bathroom. The glass mosaic generally has the appearance of colorless transparency, colored transparency and translucency. In order to enrich the color of the glass mosaic and increase the diversity of the glass mosaic, the prior art grinds the fired glass mosaic, and then electroplates one surface of the ground glass mosaic to form a layer of electroplated layer. However, the performance of the glass mosaic is changed by polishing the fired glass mosaic, and the adhesion force of the electroplated layer is poor, so that the glass mosaic is easy to fade, the appearance of the glass mosaic is affected, and the product yield is reduced.
Disclosure of Invention
The invention aims to solve the technical problem of providing a glass mosaic which has three-dimensional effect, metal feeling, high brightness, rich and colorful colors, difficult fading and excellent visual effect.
The technical problem to be solved by the invention is to provide a preparation method of the glass mosaic, which has the advantages of simple process, easy operation, strong implementability, low cost and high yield.
The technical problem to be solved by the invention is to provide a decorative material which has three-dimensional effect, metallic feeling, high brightness, rich and colorful colors, difficult fading and excellent visual effect.
In order to solve the technical problem, the invention provides a preparation method of a glass mosaic, which comprises the following steps:
firstly, pretreating the original glass to obtain a mosaic primary finished product;
secondly, firing the primary finished product of the glass mosaic at the firing temperature of more than 800 ℃;
thirdly, cooling the sintered glass mosaic primary finished product;
fourthly, grinding the cooled primary finished product of the glass mosaic according to the required shape;
fifthly, soaking the primary finished product of the glass mosaic with ground bottom in alkaline solution;
electroplating the soaked glass mosaic primary finished product, and coloring the ground bottom surface of the product;
and (seventhly), painting and sealing the bottom of the colored primary glass mosaic finished product.
As a modification of the above, the alkaline solution includes: one or more of sodium hydroxide, sodium carbonate, potassium hydroxide and potassium carbonate.
As a modification of the above, the alkaline solution includes:
80-97% of sodium hydroxide;
3-20% of sodium carbonate.
As a modification of the above, the alkaline solution includes:
50-80% of sodium hydroxide;
30-50% of potassium hydroxide.
As an improvement of the scheme, the step (V) comprises the following steps:
soaking the primary finished product of the glass mosaic with ground bottom in alkaline solution for 10-300 minutes;
and cleaning the primary mosaic finished product soaked in the alkaline solution with clear water.
As an improvement of the scheme, the step (V) comprises the following steps:
and soaking the primary finished product of the glass mosaic with ground bottom in an alkaline solution at the temperature of 40-80 ℃.
In the third step, the reacted glass mosaic primary product is cooled by a quenching fan.
As an improvement of the above scheme, in the step (one), the pretreatment comprises:
cutting the original glass sheet into a required shape and size to obtain a glass sheet;
preparing glaze;
printing the prepared glaze on the surface of the glass sheet, and drying to finish printing treatment;
and (5) opening the printed glass sheets for classification to obtain a mosaic primary finished product.
Correspondingly, the invention also provides a glass mosaic which is prepared by the preparation method.
Correspondingly, the invention also provides a decorative material comprising the glass mosaic.
The implementation of the invention has the following beneficial effects:
according to the invention, 3 processes are combined together, namely, steps S104, S105 and S106, the primary glass mosaic finished product is ground according to a required shape, then the primary glass mosaic finished product which is ground is soaked in an alkaline solution, then the primary soaked glass mosaic finished product is electroplated, the ground bottom surface of the product is colored, and the finished glass mosaic is three-dimensional, metallic and high in brightness, rich and colorful in color, difficult to fade, excellent in visual effect and high in yield through the synergistic effect of the 3 processes.
And secondly, the adhesion and the wear resistance of the electroplated layer are improved through the synergistic effect of the 3 processes.
In addition, the preparation method has the advantages of simple process, easy operation, strong implementability, short time, low cost and high yield; the decorative material adopting the glass mosaic has the advantages of three-dimensional effect, metallic effect, high brightness, rich and colorful colors, difficult fading and excellent visual effect.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention more apparent, the present invention will be described in further detail below.
The invention provides a preparation method of a glass mosaic, which comprises the following steps:
s101, pretreating the original piece of glass to obtain a mosaic primary finished product;
the pretreatment comprises the following steps:
cutting the original glass sheet into a required shape and size to obtain a glass sheet;
preparing glaze;
printing the prepared glaze on the surface of the glass sheet, and drying to finish printing treatment;
and (5) opening the printed glass sheets for classification to obtain a mosaic primary finished product.
The glaze material should be prepared according to the requirements of the color and style of the finished product, and the preparation method is just the prior art.
S102, firing the primary glass mosaic finished product at the firing temperature of more than 800 ℃;
specifically, the glass mosaic primary finished product is placed on a high-temperature backing plate to be cleaned and then enters a kiln to be fired, wherein the firing temperature is preferably 800-850 ℃, and the firing time is preferably 30-50 min. More preferably, the sintering temperature is 800-.
The firing is the first key step of the invention, which needs to be performed at a temperature range of 800-. If the sintering temperature is too high, the shrinkage rate of the product is too high, and the good strength of the finished product cannot be ensured.
S103, cooling the sintered glass mosaic primary product.
The cooling treatment is quenching treatment, and specifically, the reacted glass mosaic primary product can be cooled by a quenching fan.
And S104, performing bottom grinding processing on the cooled primary glass mosaic finished product according to the required shape.
Specifically, the cooled glass mosaic primary finished product is edged by an edging machine, so that a required shape is formed. According to the invention, the cooled primary glass mosaic finished product is ground to form mosaics of different shapes, so that the diversity of the mosaics is increased, and the requirements of different customers are met. In addition, the primary finished product of the glass mosaic is ground to form a rough surface, so that alkaline solution can enter the primary finished product of the glass mosaic conveniently.
And further, polishing the ground surface of the primary finished product of the glass mosaic.
And S105, soaking the primary finished product of the glass mosaic with the ground bottom in alkaline solution.
Wherein the alkaline solution comprises: one or more of sodium hydroxide, sodium carbonate, potassium hydroxide and potassium carbonate.
According to the invention, the glass mosaic primary finished product after bottom grinding is cleaned by the alkaline solution, and the alkaline solution permeates into the glass mosaic primary finished product through one surface of the ground bottom, so that a porous structure is formed in the glass mosaic primary finished product, an electroplated layer is convenient to attach to the glass mosaic primary finished product, and fading is prevented.
Preferably, the alkaline solution comprises:
80-97% of sodium hydroxide;
3-20% of sodium carbonate.
Preferably, the alkaline solution comprises:
50-80% of sodium hydroxide;
1-10% of sodium carbonate;
5-10% of potassium carbonate.
Preferably, the alkaline solution comprises:
50-80% of sodium hydroxide;
30-50% of potassium hydroxide.
It should be noted that the alkaline solution contains sodium hydroxide and potassium hydroxide simultaneously, which can effectively improve the cleaning effect of the glass mosaic primary finished product after bottom grinding, enhance the adhesive force of the electroplated layer and improve the coloring effect.
Step S105 includes:
soaking the primary finished product of the glass mosaic with ground bottom in alkaline solution for 10-300 minutes;
and cleaning the primary mosaic finished product soaked in the alkaline solution with clear water.
In order to save time and improve the cleaning effect, the glass mosaic primary finished product with ground bottom is soaked in an alkaline solution with the temperature of 40-80 ℃. The temperature of the alkaline solution plays a crucial role in cleaning the glass mosaic primary finished product, and when the temperature of the alkaline solution is less than 40 ℃, the glass mosaic primary finished product needs to be soaked in the alkaline solution for 300 minutes; when the temperature of the alkaline solution is within the range of 40-80 ℃, the primary finished product of the glass mosaic with ground bottom only needs to be soaked in the alkaline solution for 10-60 minutes, so that the cleaning time can be effectively shortened, and the production efficiency is improved. When the temperature of the alkaline solution is higher than 80 ℃, cracks appear in the primary finished glass mosaic solution after being ground, and the diameter of the holes in the primary finished glass mosaic is too large, so that the subsequent electroplating and coloring are not facilitated, and the hardness and the quality of the finished glass mosaic are reduced. Preferably, the primary finished product of the glass mosaic with ground bottom is soaked in an alkaline solution with the temperature of 40-60 ℃.
In addition, the mosaic primary finished product after being soaked in the alkaline solution is cleaned by clear water and used for removing the alkaline solution in the mosaic primary finished product, so that subsequent electroplating and coloring are prevented from being influenced.
After the primary mosaic finished product is cleaned by clear water, the primary mosaic finished product is dried, or wiped off by using a dust-free cloth, or naturally dried.
And S106, electroplating the soaked glass mosaic primary finished product, and coloring the ground bottom surface of the product.
Specifically, the primary soaked glass mosaic finished product is electroplated by an electroplating process, so that the finished glass mosaic is stereoscopic, metallic and high in brightness. In addition, the product ground bottom surface is colored, the colors of the finished product glass mosaic are enriched, and the visual effect is excellent.
Grind the bottom surface to the product and color the processing, include: and (3) printing a glass pigment and printing oil on the ground bottom surface by adopting a screen printing process, and printing and coloring pattern lines.
And S107, performing paint bottom sealing on the colored primary glass mosaic finished product.
The colored primary glass mosaic product is finally painted and sealed, and the electroplated layer and the ground glass pigment and the printing oil are protected to further prevent fading.
The preparation method has the advantages of simple process, easy operation, strong implementability, short time, low cost and high yield.
Correspondingly, the invention also provides a glass mosaic which is prepared by the preparation method. The glass mosaic has the advantages of three-dimensional effect, metallic feeling, high brightness, rich and colorful colors, difficult fading and excellent visual effect.
Correspondingly, the invention also provides a decorative material comprising the glass mosaic. The decorative material can be a decorative brick, and a glass mosaic is pasted on the decorative brick; or a decorative plate on which a glass mosaic is stuck. It should be noted that the decorative material including the glass mosaic described above should be included in the scope of the present invention. The invention has the advantages of three-dimensional effect, metallic feeling, high brightness, rich and colorful colors, difficult fading and excellent visual effect.
The implementation of the invention has the following beneficial effects:
according to the invention, 3 processes are combined together, namely, steps S104, S105 and S106, the primary glass mosaic finished product is ground according to a required shape, then the primary glass mosaic finished product which is ground is soaked in an alkaline solution, then the primary soaked glass mosaic finished product is electroplated, the ground bottom surface of the product is colored, and the finished glass mosaic is three-dimensional, metallic and high in brightness, rich and colorful in color, difficult to fade, excellent in visual effect and high in yield through the synergistic effect of the 3 processes.
And secondly, the adhesion and the wear resistance of the electroplated layer are improved through the synergistic effect of the 3 processes.
In addition, the preparation method has the advantages of simple process, easy operation, strong implementability, short time, low cost and high yield; the decorative material adopting the glass mosaic has the advantages of three-dimensional effect, metallic effect, high brightness, rich and colorful colors, difficult fading and excellent visual effect.
The invention is further illustrated by the following specific examples
Example 1
Preparing a glass mosaic, comprising:
1. cutting the original glass sheet into a required shape and size to obtain a glass sheet;
2. preparing glaze;
3. printing the prepared glaze on the surface of the glass sheet, and drying to finish printing treatment;
4. carrying out dielectric separation and classification on the printed glass sheets to obtain a mosaic primary finished product;
5. sintering the glass mosaic primary product at 850 ℃ for 40 min;
6. cooling the fired primary glass mosaic finished product;
7. carrying out bottom grinding processing on the cooled primary glass mosaic finished product according to the required shape;
8. soaking the primary finished product of the glass mosaic with ground bottom in a sodium hydroxide solution at the temperature of 26 ℃ for 300 minutes;
9. cleaning the primary mosaic finished product soaked in the alkaline solution with clear water;
10. electroplating the cleaned glass mosaic primary finished product, and coloring the ground bottom surface of the product;
11. and (4) performing paint bottom sealing on the colored primary glass mosaic finished product, detecting and packaging to obtain a finished product.
Example 2
1. Cutting the original glass sheet into a required shape and size to obtain a glass sheet;
2. preparing glaze;
3. printing the prepared glaze on the surface of the glass sheet, and drying to finish printing treatment;
4. carrying out dielectric separation and classification on the printed glass sheets to obtain a mosaic primary finished product;
5. sintering the glass mosaic primary product at 830 ℃ for 42 min;
6. cooling the fired primary glass mosaic finished product;
7. carrying out bottom grinding processing on the cooled primary glass mosaic finished product according to the required shape;
8. soaking the primary finished product of the glass mosaic with ground bottom in a sodium hydroxide and sodium carbonate solution at the temperature of 40 ℃ for 60 minutes;
9. cleaning the primary mosaic finished product soaked in the alkaline solution with clear water;
10. electroplating the cleaned glass mosaic primary finished product, and coloring the ground bottom surface of the product;
11. and (4) performing paint bottom sealing on the colored primary glass mosaic finished product, detecting and packaging to obtain a finished product.
Example 3
1. Cutting the original glass sheet into a required shape and size to obtain a glass sheet;
2. preparing glaze;
3. printing the prepared glaze on the surface of the glass sheet, and drying to finish printing treatment;
4. carrying out dielectric separation and classification on the printed glass sheets to obtain a mosaic primary finished product;
5. sintering the glass mosaic primary product at 800 ℃ for 40 min;
6. cooling the fired primary glass mosaic finished product;
7. carrying out bottom grinding processing on the cooled primary glass mosaic finished product according to the required shape;
8. soaking the primary finished product of the glass mosaic with ground bottom in a sodium hydroxide and potassium hydroxide solution at the temperature of 50 ℃ for 30 minutes;
9. cleaning the primary mosaic finished product soaked in the alkaline solution with clear water;
10. electroplating the cleaned glass mosaic primary finished product, and coloring the ground bottom surface of the product;
11. and (4) performing paint bottom sealing on the colored primary glass mosaic finished product, detecting and packaging to obtain a finished product.
Example 4
1. Cutting the original glass sheet into a required shape and size to obtain a glass sheet;
2. preparing glaze;
3. printing the prepared glaze on the surface of the glass sheet, and drying to finish printing treatment;
4. carrying out dielectric separation and classification on the printed glass sheets to obtain a mosaic primary finished product;
5. sintering the glass mosaic primary product at 800 ℃ for 45 min;
6. cooling the fired primary glass mosaic finished product;
7. carrying out bottom grinding processing on the cooled primary glass mosaic finished product according to the required shape;
8. soaking the primary finished product of the glass mosaic with ground bottom in a sodium hydroxide and potassium hydroxide solution at the temperature of 60 ℃ for 15 minutes;
9. cleaning the primary mosaic finished product soaked in the alkaline solution with clear water;
10. electroplating the cleaned glass mosaic primary finished product, and coloring the ground bottom surface of the product;
11. and (4) performing paint bottom sealing on the colored primary glass mosaic finished product, detecting and packaging to obtain a finished product.
Example 5
1. Cutting the original glass sheet into a required shape and size to obtain a glass sheet;
2. preparing glaze;
3. printing the prepared glaze on the surface of the glass sheet, and drying to finish printing treatment;
4. carrying out dielectric separation and classification on the printed glass sheets to obtain a mosaic primary finished product;
5. sintering the glass mosaic primary product at 800 ℃ for 50 min;
6. cooling the fired primary glass mosaic finished product;
7. carrying out bottom grinding processing on the cooled primary glass mosaic finished product according to the required shape;
8. soaking the primary finished product of the glass mosaic with ground bottom in a mixed solution of sodium hydroxide, sodium carbonate and potassium hydroxide at the temperature of 80 ℃ for 10 minutes;
9. cleaning the primary mosaic finished product soaked in the alkaline solution with clear water;
10. electroplating the cleaned glass mosaic primary finished product, and coloring the ground bottom surface of the product;
11. and (4) performing paint bottom sealing on the colored primary glass mosaic finished product, detecting and packaging to obtain a finished product.
Comparative example 1
1. Cutting the original glass sheet into a required shape and size to obtain a glass sheet;
2. preparing glaze;
3. printing the prepared glaze on the surface of the glass sheet, and drying to finish printing treatment;
4. carrying out dielectric separation and classification on the printed glass sheets to obtain a mosaic primary finished product;
5. sintering the glass mosaic primary product at 800 ℃ for 40 min;
6. cooling the fired primary glass mosaic finished product;
7. carrying out bottom grinding processing on the cooled primary glass mosaic finished product according to the required shape;
8. electroplating the primary finished product of the glass mosaic with ground bottom, and coloring the ground bottom surface of the product;
9. and (4) performing paint bottom sealing on the colored primary glass mosaic finished product, detecting and packaging to obtain a finished product.
Comparative example 2
1. Cutting the original glass sheet into a required shape and size to obtain a glass sheet;
2. preparing glaze;
3. printing the prepared glaze on the surface of the glass sheet, and drying to finish printing treatment;
4. carrying out dielectric separation and classification on the printed glass sheets to obtain a mosaic primary finished product;
5. sintering the glass mosaic primary product at 800 ℃ for 50 min;
6. cooling the fired primary glass mosaic finished product;
7. carrying out bottom grinding processing on the cooled primary glass mosaic finished product according to the required shape;
8. cleaning the primary finished mosaic product with clear water;
9. electroplating the cleaned glass mosaic primary finished product, and coloring the ground bottom surface of the product;
10. and (4) performing paint bottom sealing on the colored primary glass mosaic finished product, detecting and packaging to obtain a finished product.
The technical examination of the glass mosaic obtained in examples 1 to 5 and comparative examples 1 to 2 was carried out as follows:
the abrasion resistance test method is as follows: the weight is 1kg, 0000# steel wool, and the contact area is 20mm by 20 mm.
As can be seen from the above table, the finished products of examples 1 to 5 of the present invention have low discoloration rate and high yield, and the finished products of examples 1 to 5 of the present invention can be kept intact in a general collision (100N), which proves that they have high hardness and good wear resistance.
In conclusion, the glass mosaic disclosed by the invention has the advantages of three-dimensional effect, metallic feeling, high brightness, rich and colorful colors, difficulty in fading, excellent visual effect and high yield; the preparation method has the advantages of simple process, easy operation, strong feasibility and low cost; the decorative material of the invention has the advantages of three-dimensional effect, metallic feeling, high brightness, rich and colorful colors, difficult fading and excellent visual effect.
While the invention has been described in connection with what is presently considered to be the most practical and preferred embodiment, it is to be understood that the invention is not to be limited to the disclosed embodiment, but on the contrary, is intended to cover various modifications and equivalent arrangements included within the spirit and scope of the appended claims.
Claims (9)
1. A preparation method of a glass mosaic is characterized by comprising the following steps:
firstly, pretreating the original glass to obtain a mosaic primary finished product;
secondly, firing the primary glass mosaic finished product at 800-850 ℃;
thirdly, cooling the sintered glass mosaic primary finished product;
fourthly, carrying out bottom grinding processing on the cooled primary glass mosaic finished product according to a required shape to form a rough surface;
soaking the primary finished glass mosaic product subjected to bottom grinding in an alkaline solution, wherein the alkaline solution permeates into the primary finished glass mosaic product through a rough surface to enable the interior of the primary finished glass mosaic product to form a porous structure, and the alkaline solution comprises two or more of sodium hydroxide, sodium carbonate, potassium hydroxide and potassium carbonate;
electroplating the soaked glass mosaic primary finished product, and coloring the ground bottom surface of the product;
and (seventhly), painting and sealing the bottom of the colored primary glass mosaic finished product.
2. The method for preparing glass mosaic according to claim 1, wherein said alkaline solution comprises:
80-97% of sodium hydroxide;
3-20% of sodium carbonate.
3. The method for preparing glass mosaic according to claim 1, wherein said alkaline solution comprises:
50-80% of sodium hydroxide;
30-50% of potassium hydroxide.
4. The method for preparing a glass mosaic as claimed in claim 1, wherein the step (five) comprises:
soaking the primary finished product of the glass mosaic with ground bottom in alkaline solution for 10-300 minutes;
and cleaning the primary mosaic finished product soaked in the alkaline solution with clear water.
5. The method for preparing glass mosaic according to claim 4, wherein the step (five) comprises:
and soaking the primary finished product of the glass mosaic with ground bottom in an alkaline solution at the temperature of 40-80 ℃.
6. The method for preparing glass mosaic according to claim 1, wherein in the third step, the reacted glass mosaic primary product is cooled by a quenching fan.
7. The method for preparing glass mosaic according to claim 1, wherein in step (one), said pretreatment comprises:
cutting the original glass sheet into a required shape and size to obtain a glass sheet;
preparing glaze;
printing the prepared glaze on the surface of the glass sheet, and drying to finish printing treatment;
and (5) opening the printed glass sheets for classification to obtain a mosaic primary finished product.
8. A glass mosaic, characterized in that it is obtained by the process according to any one of claims 1 to 7.
9. A decorative material comprising the glass mosaic according to claim 8.
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| CN106186654B (en) * | 2016-07-11 | 2019-01-11 | 佛山市爱歌装饰材料有限公司 | Three-dimensional glass Mosaic process flow is electroplated |
| CN107973533B (en) * | 2017-12-04 | 2018-09-28 | 佛山市积家装饰材料有限公司 | Waterproof glass mosaic and preparation method thereof and ornament materials |
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