CN108823966A - A kind of nano self-cleaning fabric and preparation method thereof - Google Patents

A kind of nano self-cleaning fabric and preparation method thereof Download PDF

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Publication number
CN108823966A
CN108823966A CN201810345673.9A CN201810345673A CN108823966A CN 108823966 A CN108823966 A CN 108823966A CN 201810345673 A CN201810345673 A CN 201810345673A CN 108823966 A CN108823966 A CN 108823966A
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parts
fiber
accounting
cleaning
preparation
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刘云舒
刘会平
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CHANGNING DIMIAN TEXTILE GARMENTS Co Ltd
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CHANGNING DIMIAN TEXTILE GARMENTS Co Ltd
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    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
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    • D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
    • D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
    • D06M11/46—Oxides or hydroxides of elements of Groups 4 or 14 of the Periodic Table; Titanates; Zirconates; Stannates; Plumbates
    • D—TEXTILES; PAPER
    • D02—YARNS; MECHANICAL FINISHING OF YARNS OR ROPES; WARPING OR BEAMING
    • D02G—CRIMPING OR CURLING FIBRES, FILAMENTS, THREADS, OR YARNS; YARNS OR THREADS
    • D02G3/00—Yarns or threads, e.g. fancy yarns; Processes or apparatus for the production thereof, not otherwise provided for
    • D02G3/02—Yarns or threads characterised by the material or by the materials from which they are made
    • D02G3/04—Blended or other yarns or threads containing components made from different materials
    • D—TEXTILES; PAPER
    • D02—YARNS; MECHANICAL FINISHING OF YARNS OR ROPES; WARPING OR BEAMING
    • D02G—CRIMPING OR CURLING FIBRES, FILAMENTS, THREADS, OR YARNS; YARNS OR THREADS
    • D02G3/00—Yarns or threads, e.g. fancy yarns; Processes or apparatus for the production thereof, not otherwise provided for
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    • D02G3/16—Yarns or threads made from mineral substances
    • D—TEXTILES; PAPER
    • D02—YARNS; MECHANICAL FINISHING OF YARNS OR ROPES; WARPING OR BEAMING
    • D02J—FINISHING OR DRESSING OF FILAMENTS, YARNS, THREADS, CORDS, ROPES OR THE LIKE
    • D02J1/00—Modifying the structure or properties resulting from a particular structure; Modifying, retaining, or restoring the physical form or cross-sectional shape, e.g. by use of dies or squeeze rollers
    • D02J1/22—Stretching or tensioning, shrinking or relaxing, e.g. by use of overfeed and underfeed apparatus, or preventing stretch
    • D02J1/224—Selection or control of the temperature during stretching
    • D—TEXTILES; PAPER
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    • D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
    • D06B15/00—Removing liquids, gases or vapours from textile materials in association with treatment of the materials by liquids, gases or vapours
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    • D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
    • D06B3/00—Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating
    • D06B3/02—Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating of fibres, slivers or rovings
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    • D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/07—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with halogens; with halogen acids or salts thereof; with oxides or oxyacids of halogens or salts thereof
    • D06M11/11—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with halogens; with halogen acids or salts thereof; with oxides or oxyacids of halogens or salts thereof with halogen acids or salts thereof
    • D06M11/13—Ammonium halides or halides of elements of Groups 1 or 11 of the Periodic Table
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    • D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
    • D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
    • D06M11/44—Oxides or hydroxides of elements of Groups 2 or 12 of the Periodic Table; Zincates; Cadmates
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    • D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/51—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with sulfur, selenium, tellurium, polonium or compounds thereof
    • D06M11/55—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with sulfur, selenium, tellurium, polonium or compounds thereof with sulfur trioxide; with sulfuric acid or thiosulfuric acid or their salts
    • D06M11/56—Sulfates or thiosulfates other than of elements of Groups 3 or 13 of the Periodic Table
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    • D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/73—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof
    • D06M11/76—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof with carbon oxides or carbonates
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    • D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/77—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof
    • D06M11/78—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof with silicon; with halides or oxyhalides of silicon; with fluorosilicates
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    • D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/77—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof
    • D06M11/79—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof with silicon dioxide, silicic acids or their salts
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    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
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    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
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    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/53—Polyethers
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    • D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
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    • D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/02—Natural fibres, other than mineral fibres
    • D06M2101/04—Vegetal fibres
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    • D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/16—Synthetic fibres, other than mineral fibres
    • D06M2101/30—Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M2101/32—Polyesters
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    • D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/40—Fibres of carbon
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    • D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/01—Stain or soil resistance
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    • D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B2101/00—Inorganic fibres
    • D10B2101/10—Inorganic fibres based on non-oxides other than metals
    • D10B2101/12—Carbon; Pitch
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    • D10B2201/01—Natural vegetable fibres
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    • D10B2331/00—Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products
    • D10B2331/04—Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products polyesters, e.g. polyethylene terephthalate [PET]

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  • Textile Engineering (AREA)
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Abstract

The invention discloses a kind of nano self-cleaning fabrics and preparation method thereof, including following production method：One, material is selected as activated carbon fibre, modified bamboo fiber, modified polyester fiber, terylene silk fiber, wherein the activated carbon fibre accounting is set as 15%, the modified bamboo fiber accounting is set as 8%, the modified polyester fiber accounting is set as 52%, and the accounting of the terylene silk fiber is set as 25%；Two, all blended preceding pretreatments are processed；Three, by treated, material progress is blended, and after the completion of blended, being put into configured mixed solution is impregnated, and soaking time is controlled in 15-25min；Four, the fabric after immersion is sufficiently cleaned with weak base, cleaning is dried later, then imposes compound formulation in fabric surface, and compound formulation is formed a film in fabric surface, finally carries out ultraviolet radiation for sterilizing and disinfecting to it.Automated cleaning may be implemented under ultraviolet irradiation in the present invention, has permanent self-cleaning effect, and fabric also has high-intensitive and elasticity, flexible, breathable.

Description

A kind of nano self-cleaning fabric and preparation method thereof
Technical field
The present invention relates to new material textile technology field, especially a kind of nano self-cleaning fabric and preparation method thereof.
Background technique
Textile is worn, in use process in human body, can accidentally be got wet, is stained with oil, but also can stain many sweat skins Rouge and other various human secretions, these dirts not only influence the use of people, but also are the good rings of microbial reproduction Border.With the acceleration of people's life rhythm, and pursue high-quality life requirement, the tool that each class a operation difference mechanism is developed There is the textile of self-cleaning ability to come into being.The automatically cleaning textile occurred earliest is by all kinds of water-refusing oil-refusing finishing agents Functional after-finishing is carried out to textile, changes the surface property of fiber, makes the surface tension of fiber lower than the surface of water, oil Power, so that water droplet and greasy dirt can not be sprawled in fabric surface and can shake off easily, and water droplet is gone back during landing The original dust of fabric surface can be taken away, to reach the self-cleaning purpose of textile.At present using more finishing agent be containing Fluorine class water-refusing oil-refusing finishing agent.In addition to this, Germany scientist discloses the self-cleaning principle of lotus leaf water repellent in recent years, and applies Patent.The secret of lotus leaf effect essentially consists in its microstructure, and does not lie in its chemical component.It passes through in fabric surface Nanometer particle is added, roughness is improved and forms nanoscale papillary bulge, reach water and oil repellant effect, so that fabric has There is self-cleaning ability.
Although self-cleaning fabric emerges one after another, more processing cost is higher, and is not suitable for current processing factory and carries out Batch sound field, therefore, herein it is proposed that a kind of nano self-cleaning fabric and preparation method thereof.
Summary of the invention
The present invention is to solve above-mentioned phenomenon, using the technical solution of following modification, a kind of nano self-cleaning fabric and its system Preparation Method, including following production method：
One, material is selected as activated carbon fibre, modified bamboo fiber, modified polyester fiber, terylene silk fiber, wherein described Activated carbon fibre accounting is set as 15%, and the modified bamboo fiber accounting is set as 8%, and the modified polyester fiber accounting is set as 52%, the accounting of the terylene silk fiber is set as 25%；
Two, all blended preceding pretreatments are processed；
Three, by treated, material progress is blended, and after the completion of blended, being put into configured mixed solution is impregnated, leaching Time control is steeped in 15-25min；
Four, the fabric after immersion is sufficiently cleaned with weak base, cleaning is dried later, then in fabric surface Compound formulation is imposed, compound formulation is formed a film in fabric surface, ultraviolet radiation for sterilizing and disinfecting finally is carried out to it, that is, completes processing.
As present invention further optimization mode, the blended preceding procedure of processing of step 2 include hereinafter,
S1 is carried out high-temperature shaping to the material of step one kind, the process of high power post-tensioning is extenuated using multistage high temperature, Under conditions of temperature is 150 DEG C -220 DEG C, silk fiber is processed, it is ensured that activated carbon fibre, modified bamboo fiber are modified and gather Total draw ratio of ester fiber is 6.2-7.0, is then carried out under conditions of temperature is 150 DEG C to the material stretched high Warm relaxation heat setting, the sizing of terylene silk fiber elder generation's high temperature and pressure, temperature control 150 DEG C, and pressure control is greater than 3kg；
S2 is adjusted activated carbon fibre, modified bamboo fiber, modified polyester fiber, terylene silk fiber attribute, is made using tensioner Balancing tension reuses two-for-one twister twisting sizing, tension, expansion and contraction and the silk of terylene is made to reach synchronous；
S3 dyes activated carbon fibre, modified bamboo fiber, modified polyester fiber, terylene silk fiber, and dyeing temperature is 45 DEG C, after dried, drying first carry out cold wind drying, dried using air-cooler, drying time control bit 20- Then 45min carries out hot-air seasoning again, drying time control is 0.8-1.2h, and overall process dries slowly after drying fastly early period, finally certainly It is so cooling.
As present invention further optimization mode, the mixed solution percentage concentration selects nano-silica in 60-85% Change titanium, zinc oxide, silica, sodium bicarbonate aqueous solution to pass through according to 1.4:2:0.75:0.8 ratio be sufficiently mixed and At.
As present invention further optimization mode, the compound formulation is set as nano antibacterial agent, the nano antibacterial agent Including following material score, 5-12 parts of nanoscale silicon powder, 3-12 parts of fatty alcohol, de- 4-8 parts of second phthalein chitin, silver chlorate 7-20 Part, 2-3.5 parts of anti-bacterial fibre, 3.5-8 parts of titanyl sulfate, 4.5-10 parts of sodium carbonate, 5.5-13 parts of polyethylene glycol.
As present invention further optimization mode, the compound formulation further includes following material score, nanoscale silicon powder 12 parts, 12 parts of fatty alcohol, de- 8 parts of second phthalein chitin, 20 parts of silver chlorate, 3.5 parts of anti-bacterial fibre, 8 parts of titanyl sulfate, sodium carbonate 10 Part, 13 parts of polyethylene glycol.
As present invention further optimization mode, the production of the compound formulation include it is as follows,
Nanoscale silicon powder, titanyl sulfate, sodium carbonate are added in ball grinder, at 180-240 revs/min by A according to number of components Ball milling under clock revolving speed after being sufficiently mixed reaction, is protected down using argon inert gas, 0.8-1.2h is calcined at 240-480 DEG C, It is dry to grind by the powder washing filtering after annealing；
Fatty alcohol, de- second phthalein chitin, anti-bacterial fibre, titanyl sulfate, polyethylene glycol is added in B in a kettle, and stirring is extremely 1-1.5h is reacted in dissolution, and the composite material of step A is added, is cooled to room temperature, forms highly viscous compound formulation stoste.
Nano self-cleaning fabric of the invention is by carrying out processing fabric, and the mixed solution designed using multiple fiber It can penetrate into respective material, while form one layer of special nano protective film in the external of fabric using mixed solution, Dust, smell, bacterium, color stain and the function of decomposing the substances such as harmful organic substances such as formaldehyde can be excluded under ultraviolet light, and It is strong with interfibrous binding force, not easily to fall off, has permanent self-cleaning effect, fabric also has high-intensitive and elasticity, soft It is soft ventilative.
Specific embodiment
Below in conjunction in the embodiment of the present invention, technical solution in the embodiment of the present invention is clearly and completely retouched It states, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Based on the present invention In embodiment, every other implementation obtained by those of ordinary skill in the art without making creative efforts Example, shall fall within the protection scope of the present invention.
The present invention provides a kind of technical solution：A kind of nano self-cleaning fabric and preparation method thereof, including following production side Method：
One, material is selected as activated carbon fibre, modified bamboo fiber, modified polyester fiber, terylene silk fiber, wherein described Activated carbon fibre accounting is set as 15%, and the modified bamboo fiber accounting is set as 8%, and the modified polyester fiber accounting is set as 52%, the accounting of the terylene silk fiber is set as 25%；
Two, all blended preceding pretreatments are processed；
Three, by treated, material progress is blended, and after the completion of blended, being put into configured mixed solution is impregnated, leaching Time control is steeped in 15-25min；
Four, the fabric after immersion is sufficiently cleaned with weak base, cleaning is dried later, then in fabric surface Compound formulation is imposed, compound formulation is formed a film in fabric surface, ultraviolet radiation for sterilizing and disinfecting finally is carried out to it, that is, completes processing.
The blended preceding procedure of processing of step 2 include hereinafter,
S1 is carried out high-temperature shaping to the material of step one kind, the process of high power post-tensioning is extenuated using multistage high temperature, Under conditions of temperature is 150 DEG C -220 DEG C, silk fiber is processed, it is ensured that activated carbon fibre, modified bamboo fiber are modified and gather Total draw ratio of ester fiber is 6.2-7.0, is then carried out under conditions of temperature is 150 DEG C to the material stretched high Warm relaxation heat setting, the sizing of terylene silk fiber elder generation's high temperature and pressure, temperature control 150 DEG C, and pressure control is greater than 3kg；
S2 is adjusted activated carbon fibre, modified bamboo fiber, modified polyester fiber, terylene silk fiber attribute, is made using tensioner Balancing tension reuses two-for-one twister twisting sizing, tension, expansion and contraction and the silk of terylene is made to reach synchronous；
S3 dyes activated carbon fibre, modified bamboo fiber, modified polyester fiber, terylene silk fiber, and dyeing temperature is 45 DEG C, after dried, drying first carry out cold wind drying, dried using air-cooler, drying time control bit 20- Then 45min carries out hot-air seasoning again, drying time control is 0.8-1.2h, and overall process dries slowly after drying fastly early period, finally certainly It is so cooling.
The mixed solution percentage concentration selects nano-titanium dioxide, zinc oxide, silica, bicarbonate in 60-85% Sodium water solution passes through according to 1.4:2:0.75:0.8 ratio is prepared by fully mixing.
The compound formulation is set as nano antibacterial agent, and the nano antibacterial agent includes following material score, nanoscale silicon powder 5-12 parts, 3-12 parts of fatty alcohol, de- 4-8 parts of second phthalein chitin, 7-20 parts of silver chlorate, 2-3.5 parts of anti-bacterial fibre, titanyl sulfate 3.5-8 parts, 4.5-10 parts of sodium carbonate, 5.5-13 parts of polyethylene glycol.
The compound formulation further includes following material score, 12 parts of nanoscale silicon powder, 12 parts of fatty alcohol, de- second phthalein chitin 8 parts, 20 parts of silver chlorate, 3.5 parts of anti-bacterial fibre, 8 parts of titanyl sulfate, 10 parts of sodium carbonate, 13 parts of polyethylene glycol.
The production of the compound formulation include it is as follows,
Nanoscale silicon powder, titanyl sulfate, sodium carbonate are added in ball grinder, at 180-240 revs/min by A according to number of components Ball milling under clock revolving speed after being sufficiently mixed reaction, is protected down using argon inert gas, 0.8-1.2h is calcined at 240-480 DEG C, It is dry to grind by the powder washing filtering after annealing；
Fatty alcohol, de- second phthalein chitin, anti-bacterial fibre, titanyl sulfate, polyethylene glycol is added in B in a kettle, and stirring is extremely 1-1.5h is reacted in dissolution, and the composite material of step A is added, is cooled to room temperature, forms highly viscous compound formulation stoste.
To sum up, nano self-cleaning fabric of the invention by carrying out processing fabric using multiple fiber, and designs mixed Closing solution can penetrate into respective material, while form one layer of special nanometer protection in the external of fabric using mixed solution Film can exclude dust, smell, bacterium, color stain and the function for decomposing the substances such as harmful organic substances such as formaldehyde under ultraviolet light Can, and it is strong with interfibrous binding force, and it is not easily to fall off, there is permanent self-cleaning effect, fabric also has high-intensitive and bullet Property, flexible, breathable.
Finally it should be noted that：The foregoing is only a preferred embodiment of the present invention, is not intended to restrict the invention, Although the present invention is described in detail referring to the foregoing embodiments, for those skilled in the art, still may be used To modify the technical solutions described in the foregoing embodiments or equivalent replacement of some of the technical features. All within the spirits and principles of the present invention, any modification, equivalent replacement, improvement and so on should be included in of the invention Within protection scope.

Claims (6)

1. a kind of nano self-cleaning fabric and preparation method thereof, which is characterized in that including following production method：
One, material is selected as activated carbon fibre, modified bamboo fiber, modified polyester fiber, terylene silk fiber, wherein the activity Carbon fibe accounting is set as 15%, and the modified bamboo fiber accounting is set as 8%, and the modified polyester fiber accounting is set as 52%, institute The accounting for stating terylene silk fiber is set as 25%；
Two, all blended preceding pretreatments are processed；
Three, treated material is carried out blended, after the completion of blended, being put into configured mixed solution is impregnated, when immersion Between control in 15-25min；
Four, the fabric after immersion is sufficiently cleaned with weak base, cleaning is dried later, is then imposed in fabric surface Compound formulation is formed a film in fabric surface, finally carries out ultraviolet radiation for sterilizing and disinfecting to it, that is, complete processing by compound formulation.
2. a kind of nano self-cleaning fabric according to claim 1 and preparation method thereof, which is characterized in that step 2 is mixed Spin before procedure of processing include hereinafter,
S1 is carried out high-temperature shaping to the material of step one kind, the process of high power post-tensioning is extenuated using multistage high temperature, in temperature Under conditions of degree is 150 DEG C -220 DEG C, silk fiber is processed, it is ensured that activated carbon fibre, modified bamboo fiber, modified poly ester are fine Total draw ratio of dimension is 6.2-7.0, then carries out high temperature pine to the material stretched under conditions of temperature is 150 DEG C Relaxation thermal finalization, the sizing of terylene silk fiber elder generation's high temperature and pressure, temperature control 150 DEG C, and pressure control is greater than 3kg；
S2 adjusts activated carbon fibre, modified bamboo fiber, modified polyester fiber, terylene silk fiber attribute, makes tension using tensioner Equilibrium reuses two-for-one twister twisting sizing, tension, expansion and contraction and the silk of terylene is made to reach synchronous；
S3 dyes activated carbon fibre, modified bamboo fiber, modified polyester fiber, terylene silk fiber, dyeing temperature 45 DEG C, after dried, drying first carry out cold wind drying, dried using air-cooler, drying time control bit 20-45min, Then hot-air seasoning is carried out again, and drying time control is 0.8-1.2h, and overall process dries slowly after drying fastly early period, last naturally cold But.
3. a kind of nano self-cleaning fabric according to claim 1 and preparation method thereof, which is characterized in that the mixing is molten Liquid percentage concentration in 60-85%, select nano-titanium dioxide, zinc oxide, silica, sodium bicarbonate aqueous solution by according to 1.4:2:0.75:0.8 ratio is prepared by fully mixing.
4. a kind of nano self-cleaning fabric according to claim 1 and preparation method thereof, which is characterized in that the compound system Agent is set as nano antibacterial agent, and the nano antibacterial agent includes following material score, 5-12 parts of nanoscale silicon powder, fatty alcohol 3-12 Part, de- 4-8 parts of second phthalein chitin, 7-20 parts of silver chlorate, 2-3.5 parts of anti-bacterial fibre, 3.5-8 parts of titanyl sulfate, sodium carbonate 4.5- 10 parts, 5.5-13 parts of polyethylene glycol.
5. a kind of nano self-cleaning fabric according to claim 4 and preparation method thereof, which is characterized in that the compound system Agent further includes following material score, and 12 parts of nanoscale silicon powder, de- 8 parts of second phthalein chitin, 20 parts of silver chlorate, resists 12 parts of fatty alcohol 3.5 parts of bacterium fiber, 8 parts of titanyl sulfate, 10 parts of sodium carbonate, 13 parts of polyethylene glycol.
6. a kind of nano self-cleaning fabric according to claim 4 and preparation method thereof, which is characterized in that the compound system The production of agent include it is as follows,
Nanoscale silicon powder, titanyl sulfate, sodium carbonate are added in ball grinder by A according to number of components, are turned at 180-240 revs/min The lower ball milling of speed, after being sufficiently mixed reaction, is protected down using argon inert gas, 0.8-1.2h is calcined at 240-480 DEG C, will moved back Powder washing filtering after fire, it is dry to grind；
Fatty alcohol, de- second phthalein chitin, anti-bacterial fibre, titanyl sulfate, polyethylene glycol are added in a kettle, stirs to molten by B Solution reacts 1-1.5h, and the composite material of step A is added, is cooled to room temperature, forms highly viscous compound formulation stoste.
CN201810345673.9A 2018-04-17 2018-04-17 A kind of nano self-cleaning fabric and preparation method thereof Pending CN108823966A (en)

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Application publication date: 20181116