CN108822652A - A kind of cosmetics coating and preparation method thereof that metal sense is good - Google Patents
A kind of cosmetics coating and preparation method thereof that metal sense is good Download PDFInfo
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- CN108822652A CN108822652A CN201810776631.0A CN201810776631A CN108822652A CN 108822652 A CN108822652 A CN 108822652A CN 201810776631 A CN201810776631 A CN 201810776631A CN 108822652 A CN108822652 A CN 108822652A
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/47—Levelling agents
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2237—Oxides; Hydroxides of metals of titanium
- C08K2003/2241—Titanium dioxide
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/32—Phosphorus-containing compounds
- C08K2003/321—Phosphates
- C08K2003/327—Aluminium phosphate
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Cosmetics (AREA)
Abstract
The invention belongs to technical field of coatings, and in particular to a kind of cosmetics coating and preparation method thereof that metal sense is good, the good cosmetics coating of the metal sense are made of the raw material of following parts by weight：25-55 parts of aqueous acrylic emulsion, 6-11 parts of flame retardant, 4-10 parts of ethyl acetate, 5-12 parts of dilauryl thiodipropionate, 5-10 parts of aluminium triphosphate, 5-12 parts of titanium dioxide, 7-12 parts of trbasic zinc phosphate, 5-11 parts of anti-corrosive aids, 3-12 parts of levelling agent, 5-9 parts of defoaming agent, 3-12 parts of nano-titanium dioxide, 5-10 parts of curing agent, 3-13 parts of wetting agent, 5-11 parts of dispersing agent, 2-12 parts of adhesive agent, 4-10 parts of Herba Asari extract, 10-15 parts of deionized water.The coating is environment protecting water-based paint, environmentally friendly, and environmentally hazardous component is not present；Preparation method technological design is reasonable, high production efficiency；And it can be adjusted according to the needs the metal-like intensity of coating.
Description
Technical field
The present invention relates to technical field of coatings, it is specifically related to a kind of cosmetics coating that metal sense is good and its preparation side
Method.
Background technique
Cosmetics mainly use the materials such as PP, ABS, PC, glass to pack, in order to reach better visual effect, cosmetics
Coating application be also very extensively, and to tend to that the strong surface effect of metal sense can be generated, it is decorative and more to increase
There is aesthetic feeling to make the whole class of product more high-end, although there is numerous coating to can achieve metal-like currently on the market
Effect, however far can not still reach the surface effect strong with metal-like.
Summary of the invention
The purpose of the present invention is to provide a kind of cosmetics coating and preparation method thereof that metal sense is good, to solve above-mentioned back
The problem of proposing in scape technology, the good cosmetics coating of the metal sense uses water prescription, and can make up according to needing to adjust
The metal-like intensity of product outer packing.
To achieve the above object, the present invention provides the following technical solutions：
A kind of cosmetics coating that metal sense is good, is made of the raw material of following parts by weight：
25-55 parts of aqueous acrylic emulsion,
6-11 parts of flame retardant,
4-10 parts of ethyl acetate,
5-12 parts of dilauryl thiodipropionate,
5-10 parts of aluminium triphosphate,
5-12 parts of titanium dioxide,
7-12 parts of trbasic zinc phosphate,
5-11 parts of anti-corrosive aids,
3-12 parts of levelling agent,
5-9 parts of defoaming agent,
3-12 parts of nano-titanium dioxide,
5-10 parts of curing agent,
3-13 parts of wetting agent,
5-11 parts of dispersing agent,
2-12 parts of adhesive agent,
4-10 parts of Herba Asari extract,
10-15 parts of deionized water.
Preferably, the good cosmetics coating of the metal sense is made of the raw material of following parts by weight：
30 parts of aqueous acrylic emulsion,
8 parts of flame retardant,
6 parts of ethyl acetate,
8 parts of dilauryl thiodipropionate,
8 parts of aluminium triphosphate,
8 parts of titanium dioxide,
8 parts of trbasic zinc phosphate,
7 parts of anti-corrosive aids,
6 parts of levelling agent,
8 parts of defoaming agent,
8 parts of nano-titanium dioxide,
7 parts of curing agent,
8 parts of wetting agent,
8 parts of dispersing agent,
6 parts of adhesive agent,
7 parts of Herba Asari extract,
12 parts of deionized water.
Preferably, the levelling agent is modified dimethyl polysiloxane.
Preferably, the modified dimethyl polysiloxane is the polydimethylsiloxanes modified through Cobalt Porphyrin or derivatives thereof
Alkane；
The Cobalt Porphyrin derivative is cobalt protoporphyrin, four rubigan Cobalt Porphyrins or four p-methylphenyl Cobalt Porphyrins.
Preferably, the dimethyl silicone polymer preparation method modified through Cobalt Porphyrin or derivatives thereof is as follows：
1) by Cobalt Porphyrin or derivatives thereof and solvent A in mass ratio 1：(25-40) mixing, obtains solution A；
The solvent A is ethyl alcohol, n-hexane, hexamethylene or normal heptane；
2) by dimethyl silicone polymer and solvent A (50-80) in mass ratio：1 mixing, obtains solution B.
3) by solution A and solution B in mass ratio 1：(3.0-5.5) mixing, is stirred 30-90 minutes, and poly- diformazan is added in ultrasound
The crosslinking agent of radical siloxane quality 5-10%, stir 0.3-2 hours to get.
Preferably, the preparation method of the good cosmetics coating of the metal sense, includes the following steps：
1) each component raw material is weighed by weight；
2) aqueous acrylic emulsion, flame retardant, ethyl acetate, thiodipropionic acid dilauryl are sequentially added into dosing apparatus
Then osmanthus ester, aluminium triphosphate, titanium dioxide, trbasic zinc phosphate, warming while stirring are stirred 1 hour to 80 DEG C；
3) keep temperature be 80 DEG C, sequentially add anti-corrosive aids, levelling agent, defoaming agent, nano-titanium dioxide, curing agent,
Wetting agent, dispersing agent, adhesive agent, Herba Asari extract, deionized water are stirred, are uniformly dispersed.
Compared with prior art, the beneficial effects of the invention are as follows：
Environment protecting water-based paint, it is environmentally friendly, environmentally hazardous component is not present；Preparation method technological design is reasonable, raw
It produces high-efficient；And it can be adjusted according to the needs the metal-like intensity of coating.
Specific embodiment
Example 1:
The good cosmetics coating of metal sense, is made of the raw material of following parts by weight：
25 parts of aqueous acrylic emulsion, 6 parts of flame retardant, 4 parts of ethyl acetate, 5 parts of dilauryl thiodipropionate, trimerization
5 parts of aluminum phosphate, 5 parts of titanium dioxide, 7 parts of trbasic zinc phosphate, 5 parts of anti-corrosive aids, 3 parts of levelling agent, 5 parts of defoaming agent, nano-titanium dioxide 3
Part, 5 parts of curing agent, 3 parts of wetting agent, 5 parts of dispersing agent, 2 parts of adhesive agent, 4 parts of Herba Asari extract, 10 parts of deionized water.
Wherein, levelling agent is modified dimethyl polysiloxane.
The modified dimethyl polysiloxane is the dimethyl silicone polymer cobalt improved through porphyrin, and preparation method is as follows：
1) by Cobalt Porphyrin and solvent A in mass ratio 1：(25-40) mixing, obtains solution A；Solvent A is ethyl alcohol, n-hexane, ring
Hexane or normal heptane；
2) by dimethyl silicone polymer and solvent A (50-80) in mass ratio：1 mixing, obtains solution B.
3) by solution A and solution B in mass ratio 1：(3.0-5.5) mixing, is stirred 30-90 minutes, and poly- diformazan is added in ultrasound
The crosslinking agent of radical siloxane quality 5-10%, stir 0.3-2 hours to get.
The preparation method of the good cosmetics coating of the metal sense is as follows：
1) each component raw material is weighed by weight；
2) aqueous acrylic emulsion, flame retardant, ethyl acetate, thiodipropionic acid dilauryl are sequentially added into dosing apparatus
Then osmanthus ester, aluminium triphosphate, titanium dioxide, trbasic zinc phosphate, warming while stirring are stirred 1 hour to 80 DEG C；
3) keep temperature be 80 DEG C, sequentially add anti-corrosive aids, levelling agent, defoaming agent, nano-titanium dioxide, curing agent,
Wetting agent, dispersing agent, adhesive agent, Herba Asari extract, deionized water are stirred, are uniformly dispersed.
Example 2:
The good cosmetics coating of metal sense, is made of the raw material of following parts by weight：
30 parts of aqueous acrylic emulsion, 8 parts of flame retardant, 8 parts of ethyl acetate, 7 parts of dilauryl thiodipropionate, trimerization
8 parts of aluminum phosphate, 8 parts of titanium dioxide, 8 parts of trbasic zinc phosphate, 7 parts of anti-corrosive aids, 6 parts of levelling agent, 7 parts of defoaming agent, nano-titanium dioxide 7
Part, 6 parts of curing agent, 7 parts of wetting agent, 7 parts of dispersing agent, 7 parts of adhesive agent, 7 parts of Herba Asari extract, 12 parts of deionized water.
Wherein, levelling agent is modified dimethyl polysiloxane, which is modified through cobalt protoporphyrin
Dimethyl silicone polymer, preparation method is as follows：
1) by cobalt protoporphyrin and solvent A in mass ratio 1：(25-40) mixing, obtains solution A；Solvent A be ethyl alcohol, n-hexane,
Hexamethylene or normal heptane；
2) by dimethyl silicone polymer and solvent A (50-80) in mass ratio：1 mixing, obtains solution B.
3) by solution A and solution B in mass ratio 1：(3.0-5.5) mixing, is stirred 30-90 minutes, and poly- diformazan is added in ultrasound
The crosslinking agent of radical siloxane quality 5-10%, stir 0.3-2 hours to get.
The preparation method of the good cosmetics coating of the metal sense is as follows：
1) each component raw material, is weighed by weight；
2) aqueous acrylic emulsion, flame retardant, ethyl acetate, thio-2 acid two, are sequentially added into dosing apparatus
Then lauryl, aluminium triphosphate, titanium dioxide, trbasic zinc phosphate, warming while stirring are stirred 1 hour to 80 DEG C；
3), keep temperature be 80 DEG C, sequentially add anti-corrosive aids, levelling agent, defoaming agent, nano-titanium dioxide, curing agent,
Wetting agent, dispersing agent, adhesive agent, Herba Asari extract, deionized water are stirred, are uniformly dispersed.
Example 3:
The good cosmetics coating of metal sense, is made of the raw material of following parts by weight：
50 parts of aqueous acrylic emulsion, 7 parts of flame retardant, 8 parts of ethyl acetate, 8 parts of dilauryl thiodipropionate, trimerization
8 parts of aluminum phosphate, 9 parts of titanium dioxide, 11 parts of trbasic zinc phosphate, 10 parts of anti-corrosive aids, 11 parts of levelling agent, 8 parts of defoaming agent, nano-titanium dioxide
9 parts, 9 parts of curing agent, 12 parts of wetting agent, 10 parts of dispersing agent, 9 parts of adhesive agent, 8 parts of Herba Asari extract, 13 parts of deionized water.
Wherein, levelling agent is modified dimethyl polysiloxane.The modified dimethyl polysiloxane is through four rubigan porphins
Quinoline cobalt or the cobalt improved dimethyl silicone polymer of four p-methylphenyl porphyrins, preparation method are as follows：
1) by four rubigan Cobalt Porphyrins or four p-methylphenyl Cobalt Porphyrins and solvent A in mass ratio 1：(25-40) mixing, obtains
Solution A；Solvent A is ethyl alcohol, n-hexane, hexamethylene or normal heptane；
2) by dimethyl silicone polymer and solvent A (50-80) in mass ratio：1 mixing, obtains solution B.
3) by solution A and solution B in mass ratio 1：(3.0-5.5) mixing, is stirred 30-90 minutes, and poly- diformazan is added in ultrasound
The crosslinking agent of radical siloxane quality 5-10%, stir 0.3-2 hours to get.
The preparation method of the good cosmetics coating of the metal sense is as follows：
1) each component raw material, is weighed by weight；
2) aqueous acrylic emulsion, flame retardant, ethyl acetate, thio-2 acid two, are sequentially added into dosing apparatus
Then lauryl, aluminium triphosphate, titanium dioxide, trbasic zinc phosphate, warming while stirring are stirred 1 hour to 80 DEG C；
3), keep temperature be 80 DEG C, sequentially add anti-corrosive aids, levelling agent, defoaming agent, nano-titanium dioxide, curing agent,
Wetting agent, dispersing agent, adhesive agent, Herba Asari extract, deionized water are stirred, are uniformly dispersed.
The good cosmetics coating of metal sense made from embodiment 1, embodiment 2, embodiment 3 is observed, it is found that
The worth paint metal sense of embodiment 1, embodiment 2, embodiment 3 has successively obtained significant enhancing；Metal sense effect can pass through
The content of the middle levelling agent of coating is adjusted, and further, the content of levelling agent modified dimethyl polysiloxane is different, metal
Feel effect difference, technology is dry to be enhanced with the increase of the content of modified dimethyl polysiloxane.
The bound of each raw material cited by the present invention and each raw material of the present invention, section value and technological parameter
Bound, the section value of (such as temperature, time) can realize the present invention, embodiment numerous to list herein.
The above is a preferred embodiment of the present invention, cannot limit the right model of the present invention with this certainly
It encloses, it is noted that for those skilled in the art, without departing from the principle of the present invention, may be used also
To make several improvement and variation, these, which improve and change, is also considered as protection scope of the present invention.
Claims (6)
1. a kind of cosmetics coating that metal sense is good, which is characterized in that be made of the raw material of following parts by weight：
25-55 parts of aqueous acrylic emulsion,
6-11 parts of flame retardant,
4-10 parts of ethyl acetate,
5-12 parts of dilauryl thiodipropionate,
5-10 parts of aluminium triphosphate,
5-12 parts of titanium dioxide,
7-12 parts of trbasic zinc phosphate,
5-11 parts of anti-corrosive aids,
3-12 parts of levelling agent,
5-9 parts of defoaming agent,
3-12 parts of nano-titanium dioxide,
5-10 parts of curing agent,
3-13 parts of wetting agent,
5-11 parts of dispersing agent,
2-12 parts of adhesive agent,
4-10 parts of Herba Asari extract,
10-15 parts of deionized water.
2. a kind of cosmetics coating that metal sense is good as described in claim 1, which is characterized in that by the raw material of following parts by weight
It is made：
30 parts of aqueous acrylic emulsion,
8 parts of flame retardant,
6 parts of ethyl acetate,
8 parts of dilauryl thiodipropionate,
8 parts of aluminium triphosphate,
8 parts of titanium dioxide,
8 parts of trbasic zinc phosphate,
7 parts of anti-corrosive aids,
6 parts of levelling agent,
8 parts of defoaming agent,
8 parts of nano-titanium dioxide,
7 parts of curing agent,
8 parts of wetting agent,
8 parts of dispersing agent,
6 parts of adhesive agent,
7 parts of Herba Asari extract,
12 parts of deionized water.
3. the good cosmetics coating of metal sense as claimed in claim 1 or 2, which is characterized in that the levelling agent is modified poly-
Dimethyl siloxane.
4. the good cosmetics coating of metal sense as claimed in claim 3, which is characterized in that the modified dimethyl polysiloxane
For the dimethyl silicone polymer modified through Cobalt Porphyrin or derivatives thereof；
The Cobalt Porphyrin derivative is cobalt protoporphyrin, four rubigan Cobalt Porphyrins or four p-methylphenyl Cobalt Porphyrins.
5. the good cosmetics coating of metal sense as claimed in claim 4, which is characterized in that it is characterized in that, described through porphyrin
The modified dimethyl silicone polymer preparation method of cobalt or derivatives thereof is as follows：
1) by Cobalt Porphyrin or derivatives thereof and solvent A in mass ratio 1：(25-40) mixing, obtains solution A；
The solvent A is ethyl alcohol, n-hexane, hexamethylene or normal heptane；
2) by dimethyl silicone polymer and solvent A (50-80) in mass ratio：1 mixing, obtains solution B.
3) by solution A and solution B in mass ratio 1：(3.0-5.5) mixing, is stirred 30-90 minutes, and poly dimethyl silicon is added in ultrasound
The crosslinking agent of oxygen alkane quality 5-10%, stir 0.3-2 hours to get.
6. a kind of method for preparing the good cosmetics coating of metal sense of any of claims 1 or 2, which is characterized in that including such as
Lower step：
1) each component raw material is weighed by weight；
2) aqueous acrylic emulsion, flame retardant, ethyl acetate, thiodipropionic acid dilauryl osmanthus are sequentially added into dosing apparatus
Then ester, aluminium triphosphate, titanium dioxide, trbasic zinc phosphate, warming while stirring are stirred 1 hour to 80 DEG C；
3) keeping temperature is 80 DEG C, sequentially adds anti-corrosive aids, levelling agent, defoaming agent, nano-titanium dioxide, curing agent, wetting
Agent, dispersing agent, adhesive agent, Herba Asari extract, deionized water are stirred, are uniformly dispersed.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810776631.0A CN108822652A (en) | 2018-07-13 | 2018-07-13 | A kind of cosmetics coating and preparation method thereof that metal sense is good |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810776631.0A CN108822652A (en) | 2018-07-13 | 2018-07-13 | A kind of cosmetics coating and preparation method thereof that metal sense is good |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108822652A true CN108822652A (en) | 2018-11-16 |
Family
ID=64140589
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810776631.0A Pending CN108822652A (en) | 2018-07-13 | 2018-07-13 | A kind of cosmetics coating and preparation method thereof that metal sense is good |
Country Status (1)
| Country | Link |
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| CN (1) | CN108822652A (en) |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105153838A (en) * | 2015-07-11 | 2015-12-16 | 安徽欧尚建材有限公司 | Aqueous environmentally-friendly coating |
| CN106833199A (en) * | 2017-02-03 | 2017-06-13 | 安徽华晟涂料有限公司 | A kind of environment protecting water-based paint and preparation method thereof |
-
2018
- 2018-07-13 CN CN201810776631.0A patent/CN108822652A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105153838A (en) * | 2015-07-11 | 2015-12-16 | 安徽欧尚建材有限公司 | Aqueous environmentally-friendly coating |
| CN106833199A (en) * | 2017-02-03 | 2017-06-13 | 安徽华晟涂料有限公司 | A kind of environment protecting water-based paint and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 孙荣伟: "贵族真铜金属漆及其制备方法和施工工艺", 《化工管理》 * |
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Application publication date: 20181116 |
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