CN108807198A - A method of realizing the encapsulation of microwave hybrid integrated circuit radio frequency bare chip - Google Patents

A method of realizing the encapsulation of microwave hybrid integrated circuit radio frequency bare chip Download PDF

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Publication number
CN108807198A
CN108807198A CN201810517802.8A CN201810517802A CN108807198A CN 108807198 A CN108807198 A CN 108807198A CN 201810517802 A CN201810517802 A CN 201810517802A CN 108807198 A CN108807198 A CN 108807198A
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Prior art keywords
radio frequency
bare chip
integrated circuit
frequency bare
encapsulation
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CN201810517802.8A
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CN108807198B (en
Inventor
董昌慧
李益兵
沈磊
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Nanjing Hengdian advanced Microwave Technology Research Institute Co.,Ltd.
NANJING HENGDIAN ELECTRONICS Co.,Ltd.
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NANJING HENGDIAN ELECTRONIC CO Ltd
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    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01LSEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
    • H01L21/00Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
    • H01L21/02Manufacture or treatment of semiconductor devices or of parts thereof
    • H01L21/04Manufacture or treatment of semiconductor devices or of parts thereof the devices having potential barriers, e.g. a PN junction, depletion layer or carrier concentration layer
    • H01L21/50Assembly of semiconductor devices using processes or apparatus not provided for in a single one of the subgroups H01L21/06 - H01L21/326, e.g. sealing of a cap to a base of a container
    • H01L21/56Encapsulations, e.g. encapsulation layers, coatings
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01LSEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
    • H01L23/00Details of semiconductor or other solid state devices
    • H01L23/28Encapsulations, e.g. encapsulating layers, coatings, e.g. for protection
    • H01L23/29Encapsulations, e.g. encapsulating layers, coatings, e.g. for protection characterised by the material, e.g. carbon
    • H01L23/293Organic, e.g. plastic
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01LSEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
    • H01L23/00Details of semiconductor or other solid state devices
    • H01L23/28Encapsulations, e.g. encapsulating layers, coatings, e.g. for protection
    • H01L23/31Encapsulations, e.g. encapsulating layers, coatings, e.g. for protection characterised by the arrangement or shape
    • H01L23/3157Partial encapsulation or coating
    • H01L23/3171Partial encapsulation or coating the coating being directly applied to the semiconductor body, e.g. passivation layer

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  • Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Computer Hardware Design (AREA)
  • Microelectronics & Electronic Packaging (AREA)
  • Power Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Encapsulation Of And Coatings For Semiconductor Or Solid State Devices (AREA)
  • Structures Or Materials For Encapsulating Or Coating Semiconductor Devices Or Solid State Devices (AREA)

Abstract

The present invention relates to a kind of methods for realizing the encapsulation of microwave hybrid integrated circuit radio frequency bare chip, it is characterized in that, the radio frequency bare chip packaging method includes radio frequency bare chip, vacuum drying oven, plasma cleaning equipment, the colourless moisture protection coatings of EGC-1700, the radio frequency bare chip is applied to realize radio-frequency performance in microwave hybrid integrated circuit, the vacuum drying oven removes steam for the preceding microwave hybrid integrated circuit of radio frequency bare chip encapsulation, cleaning and activation of the plasma cleaning equipment for radio frequency bare chip encapsulation front surface organic matter, the technical solution is simple, fast, cost is relatively low, it is easily achieved.Pass through the encapsulation of radio frequency bare chip, it solves and solves existing to be encapsulated in after the environmental tests such as damp and hot, mould, salt fog that atmosphere is complicated in microwave hybrid integrated circuit, radio frequency bare chip reliability can not ensure that product index is abnormal, and especially microwave circuit frequency is higher influences bigger problem.

Description

A method of realizing the encapsulation of microwave hybrid integrated circuit radio frequency bare chip
Technical field
The present invention relates to a kind of packaging methods, and in particular to a kind of realization microwave hybrid integrated circuit radio frequency bare chip encapsulation Method, belong to radio frequency bare chip encapsulation technology field.
Background technology
It is exactly briefly Foundry that encapsulation, which is the process that integrated circuit assembly is radio frequency bare chip final products, The integrated circuit die produced is placed on the substrate that one piece is played the role of carrying, and pin is extracted, then fixed packaging As an entirety;
As the core component of radar, in microwave hybrid integrated circuit, to ensure the originals such as circuit loss is small, parasitic parameter is low Cause, hybrid integrated multi-chip module (MCM) are usually by multiple radio frequency bare chip High Density Packagings on multilayer interconnection substrate, so Post package is in same shell, to form highdensity microelectronic product, but due to hybrid integrated multi-chip module application environment Complexity and itself cavity in synthesis atmosphere, the application reliability of radio frequency bare chip is often relatively low.Encapsulation is as a kind of normal The protected mode seen, the application in radio frequency bare chip is very necessary, needs the case where not influencing radio frequency bare chip electrical property Under, propose a kind of packaging method of new radio frequency bare chip.At present in microwave hybrid integrated circuit circuit radio frequency naked core in industry Piece encapsulation usually has following several method:
1. pair microwave hybrid integrated circuit carries out Laser seal welding or parallel soldering and sealing, radio frequency bare chip is encapsulated in Microwave Hybrid In the shell of integrated circuit, make itself and air exclusion, but the product after laser, parallel soldering and sealing occurs doing over again when reprocessing, cover board is torn open It except difficulty and can not recycle, maintenanceability is general, and parallel soldering and sealing is suitable only for special material such as Kovar alloy.
2. carrying out " Parylene " vacuum deposition inside pair microwave hybrid integrated circuit, Parylene is a kind of paraxylene Polymer.Parylene coatings are prepared with unique vacuum vapor deposition technique, " raw in substrate surface by active small molecular It is long " go out completely conformal polymer thin membrane coat, about 0.1 μm~100 μm of film coating deposition thickness.The complex technical process, Need special equipment, cost higher.
3. pair microwave hybrid integrated circuit radio frequency bare chip is using epoxy glue, silicon rubber, silica gel etc..But epoxy glue is easily inhaled Water, silica gel, silicon rubber has higher CTE, while coefficient of elasticity is higher, in environmental temperature experiment, the expansion of colloid itself The spun gold of bonding can be pulled with stress caused by contraction, causes to fail.Also, the dielectric constant due to above-mentioned glue and loss Tangent angle and air dielectric difference are larger, are affected to what radio frequency bare chip was brought, cannot be satisfied the requirement on electric performance of product.
Invention content
The purpose of the present invention is provide a kind of simple, quick, cost to provide microwave hybrid integrated circuit radio frequency bare chip It is relatively low, be easy to the packaging method reprocessed.This method can be applied on the microwave hybrid integrated circuit within Ku wave bands (18GHz), Encapsulation is smaller to the Index Influence of product, stablizes in each environmental test stage index, the coating on radio frequency bare chip surface will not Spun gold is caused to pull.Radio frequency bare chip its thermal diffusivity after encapsulation will not be by large effect.
To achieve the goals above, a kind of method for realizing the encapsulation of microwave hybrid integrated circuit radio frequency bare chip of the present invention is It is achieved:The method for realizing the encapsulation of microwave hybrid integrated circuit radio frequency bare chip, its step are as follows:
1) microwave hybrid integrated circuit containing radio frequency bare chip for needing to encapsulate is got out in ultra-clean chamber;
2) microwave hybrid integrated circuit is positioned in vacuum drying oven and carries out high-temperature baking removal steam;
3) use plasma cleaning equipment to the cleaning of radio frequency bare chip and surface in the microwave hybrid integrated circuit after baking Activation;
4) the colourless moisture protection coatings of EGC-1700 are used to carry out drop coating encapsulation to radio frequency bare chip surface;
5) it after the solidification of radio frequency bare chip face coat, observes under an electron microscope, to the unencapsulated naked radio frequency of the frequency arrived It is repaired on bare chip surface.
As an improvement of the present invention, in the step 2), before the encapsulation of radio frequency bare chip, vacuum bakeout should be carried out, is gone Steam, baking time are directly proportional to the weight of microwave hybrid integrated circuit.
As an improvement of the present invention, in the step 3), before the encapsulation of radio frequency bare chip, plasma cleaning should be carried out, Wherein nitrogen is used as backfill, first uses oxygen plasma to carry out organic matter to radio frequency bare chip surface and aoxidizes, secondly uses argon Plasma removes radio frequency bare chip surface organic matter and pad activates, and plasma cleaning contributes to EGC-1700 colourless moisture-proof Protective coating is sprawled.
As an improvement of the present invention, in the step 3), radio frequency bare chip has been cleaned using plasma cleaning equipment Cheng Hou, the packaging time away from the colourless moisture protection coatings of EGC-1700 are no more than 2 hours.
As an improvement of the present invention, in the step 4), colourless moisture-proof guarantors of EGC-1700 that radio frequency bare chip uses It when protecting coating encapsulation, is operated using automatic dispensing machine, selection personality card lancet head internal diameter is 0.09mm, and syringe needle outer diameter is 0.26mm。
As an improvement of the present invention, in the step 4), colourless moisture-proof guarantors of EGC-1700 that radio frequency bare chip uses Shield coating is carried out using drop coating by the way of, and when drop coating, bayonet syringe needle is 1.5~2mm away from radio frequency bare chip surface distance.
As an improvement of the present invention, the colourless moisture protection coatings of EGC-1700 that radio frequency bare chip uses, using certainly Dynamic dispenser is operated, and according to the size of chip, setting note drop time, timing quantifies protective coating.
As an improvement of the present invention, the colourless moisture protection coatings of EGC-1700 that radio frequency bare chip uses use drop coating Mode carry out, coating layer thickness be no more than 1 μm,
As an improvement of the present invention, the colourless moisture protection coatings of EGC-1700 that radio frequency bare chip uses can be used 3MTMNovecTM7100DL diluents are wiped.
The colourless moisture protection coatings of EGC-1700 that radio frequency bare chip uses, are operated using automatic dispensing machine, according to Outlet pressure is arranged in the size of chip, and the note drop time, timing quantifies protective coating.Subordinate list 1 is different radio frequency naked core sheet gauge The drop coating technological parameter of the colourless moisture protection coating of lattice.
Table 1
Compared with the existing technology, the invention has the advantages that:
1) the characteristics of technical solution is simple, effective, and the program is according to microwave hybrid integrated circuit and radio frequency bare chip is special Door devises a kind of packaging method, and when using this packaging method, the reliability of radio frequency bare chip can be carried preferably It is high;
2) program is realized that encapsulation process is quick by way of drop coating on radio frequency bare chip surface, in the short time The effective protection of RF radio frequency bare chip may be implemented, maintenanceability is good, and maintenance cost is relatively low;
3) package thickness of the present invention on microwave hybrid integrated circuit radio frequency bare chip surface is no more than 1 μm, can be effective Ground meets the cooling requirements of radio frequency bare chip;
4) present invention can apply on the microwave hybrid integrated circuit within Ku wave bands (18GHz), encapsulate to product Index Influence is smaller;
5) present invention stablizes in each environmental test stage index, and product index is without exception;
6) the technical solution cost is relatively low, compared to existing high-frequency circuit Parylene guard methods, convenient for further Popularization and application.
Caused by the synthesis atmosphere in complexity and itself cavity to solve hybrid integrated multi-chip module application environment The relatively low problem of radio frequency bare chip application reliability, while it is simple, effectively to meet operation scheme, maintenanceability is good, good heat dissipation, Equal requirement at low cost.A kind of present invention colourless moisture protection coatings of EGC-1700, pass through high-temperature baking, plasma cleaning, guarantor The mode for protecting the spot printing of coating realizes the encapsulation on radio frequency bare chip surface.Making it neither influences the reliability of product, while to Ku The Index Influence of the following product of wave band is also smaller.
The colourless moisture protection coatings of EGC-1700 are Minnesota Mining and Manufacturing Company's production, are in a kind of hydrofluoroether solvent containing quality point The fluorinated acrylic polymer of number 2%.At present in industry when microwave hybrid integrated circuit circuit radio frequency bare chip is encapsulated to micro- Wave hydrid integrated circuit carries out Laser seal welding or parallel soldering and sealing, but product does over again and reprocesses difficulty;To in microwave hybrid integrated circuit Portion carries out " Parylene " vacuum deposition, and complex technical process needs special equipment, cost higher;It is integrated to Microwave Hybrid Using epoxy glue, silicon rubber, silica gel packaging, the radio-frequency performance and reliability of product can not ensure circuit radio frequency bare chip.And The colourless moisture protections of EGC-1700 apply, and can be answered on the microwave hybrid integrated circuit within Ku wave bands (18GHz) by experiment With technical solution is simple, effective, and good heat dissipation effect, maintenanceability is good, stablizes in each environmental test stage index, product refers to It marks without exception.
Description of the drawings
Fig. 1 is the schematic diagram after the encapsulation of microwave hybrid integrated circuit radio frequency bare chip.
Fig. 2 is a kind of flow chart of method that realizing the encapsulation of microwave hybrid integrated circuit radio frequency bare chip.
Fig. 3 is damp heat test curve.
Specific implementation mode
In order to deepen the understanding of the present invention, the present embodiment is described in detail with reference to example.
Applicant designs and produces certain model amplifier product, and working frequency frequency is 6GHz~18GHz, and when design uses The microwave assembly technology technology that radio frequency bare chip is shelved.It is required that product meets damp heat test GJB 150.9A-2009 and mould test The test requirements document of GJB150.10A-2009, salt spray test GJB 150.11A-2009, while product later period maintenance is convenient, repair It is at low cost.
Process program
1. selecting the colourless moisture protection coatings of EGC-1700 of Minnesota Mining and Manufacturing Company's production, contained in a kind of hydrofluoroether solvent The fluorinated acrylic polymer of mass fraction 2%;
2. getting out the microwave hybrid integrated circuit containing radio frequency bare chip for needing to encapsulate in ultra-clean chamber;
3. by microwave hybrid integrated circuit be positioned in vacuum drying oven carry out high-temperature baking remove steam, baking time with it is micro- The weight of wave hydrid integrated circuit is directly proportional;
4. using plasma cleaning equipment to the cleaning of radio frequency bare chip and surface in the microwave hybrid integrated circuit after baking Activation, is backfilled using nitrogen, and oxidation reaction occurs for oxygen and the organic matter on RF radio frequency bare chip surface, and argon gas is to RF radio frequency The organic matter on bare chip surface bombard while being activated to pad;
5. carrying out drop coating encapsulation to radio frequency bare chip surface using the colourless moisture protection coatings of EGC-1700, packaging time exists It after the completion of plasma cleaning in 2 hours, is packaged using automatic dispensing machine, using personality card lancet head, package thickness does not surpass Cross 1 μm;
6. after the solidification of radio frequency bare chip face coat, observe under an electron microscope, to the unencapsulated naked radio frequency of the frequency arrived It is repaired on bare chip surface.
Entire solution process flow chart is as shown in Figure 2.
Test example
Microwave hybrid integrated circuit to carrying out radio frequency bare chip surface encapsulation by above-mentioned process program is tested.Microwave The front and back electrical property canonical parameter of radio frequency bare chip encapsulation is referring to table 2 in hydrid integrated circuit.
Test parameter Before encapsulation After encapsulation Unit
Test frequency Center frequency point@12GHz Center frequency point@12GHz GHz
Gain 17 16.9 dB
Noise coefficient 2 2.05 dB
1. damp heat test is executed by Fig. 2,10 cycles of test period, 240 hours;
The index before and after damp heat test is compared, variation is smaller, meets product index protocol requirement.Test index such as 3 institute of table Show.
Test parameter Before experiment After experiment Unit
Test frequency Center frequency point@12GHz Center frequency point@12GHz GHz
Gain 16.9 16.8 dB
Noise coefficient 2.05 2.1 dB
2. mould test experimental condition:A) test period:28d;B) experiment selects strain to be shown in Table 4;C) qualified grade:1 grade.
Serial number Strain name Bacterium numbering
1 Aspergillus flavus AS3.3950
2 Aspergillus versicolor AS3.3885
3 Penicillium funiculosum AS3.3875
4 Chaetomium globosum AS3.4254
5 Aspergillus niger AS3.3928
After experiment, microwave hybrid integrated circuit radio frequency bare chip surface is checked, there is less mould on radio frequency bare chip surface It is distributed, the radio frequency bare chip face coat below mould is high-visible, meets 1 grade of requirement in GJB 150.10A-2009 standards.
3. salt spray test condition:A) temperature is 35 DEG C before chamber spraying, and the time is at least 2h;B) salting liquid:Salt is molten The concentration of liquid should be 5%+1%, and pH value is between 6.5~7.2;C) salt fog deposition:In 80cm2Horizontal collecting region in, protect The sedimentation rate for demonstrate,proving salting liquid is (1~3) mL/h.
It after experiment, tests to microwave hybrid integrated circuit and radio frequency bare chip, does not find that corrosion and failure, satisfaction are wanted It asks.
It is tested and is illustrated by above three, after this process program, product meets damp heat test GJB 150.9A- The test requirements document of 2009 and mould test GJB 150.10A-2009, salt spray test GJB 150.11A-2009.
From the point of view of said program, the colourless moisture protections of EGC-1700 apply, can be within Ku wave bands (18GHz) by experiment Microwave hybrid integrated circuit on apply, technical solution is simple, effectively, and good heat dissipation effect, maintenanceability is good, is tried in each environment Stage index stabilization is tested, product index is without exception.
It should be noted that above-described embodiment, encapsulation range not for the purpose of limiting the invention, in above-mentioned technical proposal On the basis of made equivalents or replacement each fall within the range packaged by the claims in the present invention.

Claims (9)

1. a kind of method for realizing the encapsulation of microwave hybrid integrated circuit radio frequency bare chip, its step are as follows:
1) microwave hybrid integrated circuit containing radio frequency bare chip for needing to encapsulate is got out in ultra-clean chamber;
2) microwave hybrid integrated circuit is positioned in vacuum drying oven and carries out high-temperature baking removal steam;
3) use plasma cleaning equipment to the cleaning of radio frequency bare chip and surface active in the microwave hybrid integrated circuit after baking;
4) the colourless moisture protection coatings of EGC-1700 are used to carry out drop coating encapsulation to radio frequency bare chip surface;
5) it after the solidification of radio frequency bare chip face coat, observes under an electron microscope, to the naked radio frequency naked core of the unencapsulated frequency arrived It is repaired on piece surface.
2. a kind of method for realizing the encapsulation of microwave hybrid integrated circuit radio frequency bare chip according to claim 1, feature It is, in the step 2), before the encapsulation of radio frequency bare chip, vacuum bakeout should be carried out, remove steam, baking time and Microwave Hybrid collection It is directly proportional at the weight of circuit.
3. a kind of method for realizing the encapsulation of microwave hybrid integrated circuit radio frequency bare chip according to claim 1, feature It is, in the step 3), before the encapsulation of radio frequency bare chip, plasma cleaning should be carried out, wherein nitrogen is used as backfill, first uses oxygen Plasma carries out organic matter to radio frequency bare chip surface and aoxidizes, and is secondly had to radio frequency bare chip surface using argon plasma Machine object removes and pad activation, plasma cleaning contribute to sprawling for the colourless moisture protection coatings of EGC-1700.
4. a kind of method for realizing the encapsulation of microwave hybrid integrated circuit radio frequency bare chip according to claim 1, feature It is, in the step 3), after the completion of radio frequency bare chip is using plasma cleaning equipment cleaning, away from the colourless moisture-proof guarantors of EGC-1700 The packaging time for protecting coating is no more than 2 hours.
5. a kind of method for realizing the encapsulation of microwave hybrid integrated circuit radio frequency bare chip according to claim 1, feature It is, in the step 4), when the colourless moisture protection coatings of EGC-1700 that radio frequency bare chip uses encapsulate, using automatically dropping glue Machine is operated, and selection personality card lancet head internal diameter is 0.09mm, and syringe needle outer diameter is 0.26mm.
6. a kind of method for realizing the encapsulation of microwave hybrid integrated circuit radio frequency bare chip according to claim 1, feature It is, in the step 4), the colourless moisture protection coatings of EGC-1700 that radio frequency bare chip uses are carried out by the way of drop coating, When drop coating, bayonet syringe needle is 1.5~2mm away from radio frequency bare chip surface distance.
7. a kind of method for realizing the encapsulation of microwave hybrid integrated circuit radio frequency bare chip according to claim 1, feature It is, the colourless moisture protection coatings of the EGC-1700 that radio frequency bare chip uses are operated using automatic dispensing machine, according to chip Size, be arranged outlet pressure, note drop the time, timing, quantify protective coating.Subordinate list 1 is different radio frequency bare chip specification The drop coating technological parameter of colourless moisture protection coating.
8. a kind of method for realizing the encapsulation of microwave hybrid integrated circuit radio frequency bare chip according to claim 1, feature It is, the colourless moisture protection coatings of the EGC-1700 that radio frequency bare chip uses in the step 4) are carried out by the way of drop coating, Coating layer thickness is no more than 1 μm.
9. a kind of method for realizing the encapsulation of microwave hybrid integrated circuit radio frequency bare chip according to claim 1, feature It is, the colourless moisture protection coatings of the EGC-1700 that radio frequency bare chip uses in the step 4) use 3MTMNovecTM7100DL Diluent is wiped.
CN201810517802.8A 2018-05-25 2018-05-25 Method for realizing microwave hybrid integrated circuit radio frequency bare chip packaging Active CN108807198B (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110610850A (en) * 2019-09-16 2019-12-24 西安空间无线电技术研究所 Cleaning method for glass substrate after laser hole making
CN111952152A (en) * 2020-08-04 2020-11-17 安徽华东光电技术研究所有限公司 Bare chip packaging method
CN113109610A (en) * 2021-04-06 2021-07-13 北京中微普业科技有限公司 RF bare chip flat probe test tool

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20100102436A1 (en) * 2008-10-20 2010-04-29 United Test And Assembly Center Ltd. Shrink package on board
CN104124216A (en) * 2014-07-03 2014-10-29 天水华天科技股份有限公司 Substrate chip carrier CSP package and production method thereof
CN204067330U (en) * 2014-07-03 2014-12-31 天水华天科技股份有限公司 A kind of substrate chip support C SP packaging part

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20100102436A1 (en) * 2008-10-20 2010-04-29 United Test And Assembly Center Ltd. Shrink package on board
CN104124216A (en) * 2014-07-03 2014-10-29 天水华天科技股份有限公司 Substrate chip carrier CSP package and production method thereof
CN204067330U (en) * 2014-07-03 2014-12-31 天水华天科技股份有限公司 A kind of substrate chip support C SP packaging part

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110610850A (en) * 2019-09-16 2019-12-24 西安空间无线电技术研究所 Cleaning method for glass substrate after laser hole making
CN110610850B (en) * 2019-09-16 2022-01-04 西安空间无线电技术研究所 Cleaning method for glass substrate after laser hole making
CN111952152A (en) * 2020-08-04 2020-11-17 安徽华东光电技术研究所有限公司 Bare chip packaging method
CN111952152B (en) * 2020-08-04 2023-06-06 安徽华东光电技术研究所有限公司 Bare chip packaging method
CN113109610A (en) * 2021-04-06 2021-07-13 北京中微普业科技有限公司 RF bare chip flat probe test tool

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Effective date of registration: 20211008

Address after: No. 9, Jinma Road, Maqun Science Park, Qixia District, Nanjing, Jiangsu 210046

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