CN108795582A - A kind of wiper essence and preparation method thereof - Google Patents

A kind of wiper essence and preparation method thereof Download PDF

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Publication number
CN108795582A
CN108795582A CN201710304828.XA CN201710304828A CN108795582A CN 108795582 A CN108795582 A CN 108795582A CN 201710304828 A CN201710304828 A CN 201710304828A CN 108795582 A CN108795582 A CN 108795582A
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CN
China
Prior art keywords
sodium
water
nacl
diformazan
thiazolinone
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710304828.XA
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Chinese (zh)
Inventor
刘海运
蒋忠新
蒋颖
赵海深
赵士嘉
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
HUNAN UNIVERSITY OF COMMERCE
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HUNAN UNIVERSITY OF COMMERCE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by HUNAN UNIVERSITY OF COMMERCE filed Critical HUNAN UNIVERSITY OF COMMERCE
Priority to CN201710304828.XA priority Critical patent/CN108795582A/en
Publication of CN108795582A publication Critical patent/CN108795582A/en
Pending legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02Anionic compounds
    • C11D1/12Sulfonic acids or sulfuric acid esters; Salts thereof
    • C11D1/29Sulfates of polyoxyalkylene ethers
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09KMATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K3/00Materials not provided for elsewhere
    • C09K3/18Materials not provided for elsewhere for application to surfaces to minimize adherence of ice, mist or water thereto; Thawing or antifreeze materials for application to surfaces
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02Inorganic compounds ; Elemental compounds
    • C11D3/04Water-soluble compounds
    • C11D3/046Salts
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/26Organic compounds containing nitrogen
    • C11D3/33Amino carboxylic acids
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/34Organic compounds containing sulfur
    • C11D3/349Organic compounds containing sulfur additionally containing nitrogen atoms, e.g. nitro, nitroso, amino, imino, nitrilo, nitrile groups containing compounds or their derivatives or thio urea
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/38Products with no well-defined composition, e.g. natural products

Abstract

The present invention relates to a kind of wiper essences and preparation method thereof, including following ingredients by weight:Diformazan 0.8~1.5, thiazolinone 0.4~1.5, sodium chloride 0.3~1, EDETATE SODIUM 0.4~1.2, Nacl 0.8~2, polyethers sodium sulphate 0.3~1, water 150-200.The present invention not only goes dirt significant effect, but also can be antifog antifreeze, and concentration property is high, safety coefficient is secure.

Description

A kind of wiper essence and preparation method thereof
Technical field
The present invention relates to windscreen wiper essence detergent, specifically a kind of wiper essence and preparation method thereof.
Background technology
The outer glass of automotive windshield is easy the fouls such as accumulation dust, seriously reduces the saturating of glass due to being exposed to the external world throughout the year Lightness influences the sight of driver, it is easy to cause traffic accident.Wiper essence in the market easily corrodes glass, The ageing of rubber of wiper can usually be accelerated, and the retention time is shorter, generally only several hours, effect is not satisfactory;And And functionality is single, is only capable of playing the role of clean effect, can not realize antifrost antifogging.
Invention content
In view of the above-mentioned problems, the present invention can also prevent while providing a kind of dirt that can be thoroughly removed on vehicle glass Only glass generates refractive power phenomenon, defrosting, antifog wiper essence and preparation method thereof.
Wiper essence provided by the invention, including following ingredients by weight:Diformazan 0.8~1.5, thiazoline Ketone 0.4~1.5, sodium chloride 0.3~1, EDETATE SODIUM 0.4~1.2, Nacl 0.8~2, polyethers sodium sulphate 0.3~1, water 150- 200。
Preferably, the wiper essence is made of the following ingredients remembered by weight:Diformazan 1, thiazolinone 1.2, sodium chloride 0.5, EDETATE SODIUM 0.8, Nacl 1.5, polyethers sodium sulphate 0.8, water 180.
The present invention also provides a kind of preparation methods of wiper essence, which is characterized in that includes the following steps:
(1)Note weighs 0.8~1.5 part of diformazan, 0.4~1.5 part of thiazolinone, 0.3~1 part of sodium chloride, EDTA bis- by weight 0.4~1.2 part of sodium, 0.8~2 part of Nacl, 0.3~1 part of polyethers sodium sulphate, 150-200 parts of water;
(2)By step(1)In water be heated into 100 DEG C;
(3)By step(1)In the diformazan, thiazolinone, sodium chloride, EDETATE SODIUM, Nacl, the polyethers sodium sulphate that weigh pour into step Suddenly(2)Water in mixed;
(4)Stirring;
(5)Precipitation 2~3 days;
(6)Filtering.
Preferably, step(1)In by weight note weigh 1 part of diformazan, 1.2 parts of thiazolinone, 0.5 part of sodium chloride, 0.8 part of EDETATE SODIUM, 1.5 parts of Nacl, 0.8 part of polyethers sodium sulphate, 180 parts of water.
Compared with prior art, the present invention has following advantage:
1, wiper essence clean effect provided by the invention is notable, can be effectively antifog, easy for operation, solves the prior art When running due to windshield has dirt the problem of block vision, traffic accident is reduced;
2, the concentrated type of the invention is high, and required each group component is few in unit automobile glass anti-fog detergent, can but reach with The prior art equally even preferably clean effect;
3, the inventive functionality is various, can not only decontamination, moreover it is possible to anti-fog and antifrost;
4, the wiper essence can also be applied to the glass pane and various glass in house cleaning it is antifog, wide adaptation range.
Specific implementation mode
The present invention is described more detail below, illustrative examples of the invention and explanation are used for explaining the present invention herein, But it is not as a limitation of the invention.
Each raw material of the present invention is actually to be matched with parts by weight.A kind of wiper essence, including by weight The following ingredients of meter:Diformazan 0.8~1.5, thiazolinone 0.4~1.5, sodium chloride 0.3~1, EDETATE SODIUM 0.4~1.2, work Industry salt 0.8~2, polyethers sodium sulphate 0.3~1, water 150-200.
The preparation method of the wiper essence, includes the following steps:
(1)Note weighs 0.8~1.5 part of diformazan, 0.4~1.5 part of thiazolinone, 0.3~1 part of sodium chloride, EDTA bis- by weight 0.4~1.2 part of sodium, 0.8~2 part of Nacl, 0.3~1 part of polyethers sodium sulphate, 150-200 parts of water;
(2)By step(1)In water be heated into 100 DEG C;
(3)By step(1)In the diformazan, thiazolinone, sodium chloride, EDETATE SODIUM, Nacl, the polyethers sodium sulphate that weigh pour into step Suddenly(2)Water in mixed;
(4)Stirring;
(5)Precipitation 2~3 days;
(6)Filtering.
With three embodiments, the present invention is described in detail below:
Embodiment one:
(1)Note weighs 0.8 part of diformazan, 0.4 part of thiazolinone, 0.3 part of sodium chloride, 0.4 part of EDETATE SODIUM, Nacl by weight 0.8 part, 0.3 part of polyethers sodium sulphate, 150 parts of water;
(2)By step(1)In water be heated into 100 DEG C;
(3)By step(1)In the diformazan, thiazolinone, sodium chloride, EDETATE SODIUM, Nacl, the polyethers sodium sulphate that weigh pour into step Suddenly(2)Water in mixed;
(4)Stirring is until invisible slag particle;
(5)Precipitation 2 days;
(6)Sediment is filtered out, wiper essence is obtained.
Embodiment two:
(1)Note weighs 1.5 parts of diformazan, 1.5 parts of thiazolinone, 1 part of sodium chloride, 1.2 parts of EDETATE SODIUM, Nacl 2 by weight Part, 1 part of polyethers sodium sulphate, 200 parts of water;
(2)By step(1)In water be heated into 100 DEG C;
(3)By step(1)In the diformazan, thiazolinone, sodium chloride, EDETATE SODIUM, Nacl, the polyethers sodium sulphate that weigh pour into step Suddenly(2)Water in mixed;
(4)Stirring is until invisible slag particle;
(5)Precipitation 3 days;
(6)Sediment is filtered out, wiper essence is obtained.
Embodiment three:
(1)Note weighs 1 part of diformazan, 1.2 parts of thiazolinone, 0.5 part of sodium chloride, 0.8 part of EDETATE SODIUM, Nacl by weight 1.5 parts, 0.8 part of polyethers sodium sulphate, 180 parts of water;
(2)By step(1)In water be heated into 100 DEG C;
(3)By step(1)In the diformazan, thiazolinone, sodium chloride, EDETATE SODIUM, Nacl, the polyethers sodium sulphate that weigh pour into step Suddenly(2)Water in mixed;
(4)Stirring is until invisible slag particle;
(5)Precipitation 2 days;
(6)Sediment is filtered out, wiper essence is obtained.
It is provided for the embodiments of the invention technical solution above to be described in detail, specific case used herein The principle and embodiment of the embodiment of the present invention are expounded, the explanation of above example is only applicable to help to understand this The principle of inventive embodiments;Meanwhile for those of ordinary skill in the art, embodiment according to the present invention, in specific embodiment party There will be changes in formula and application range, in conclusion the content of the present specification should not be construed as limiting the invention.

Claims (4)

1. a kind of wiper essence, it is characterised in that:Including following ingredients by weight:Diformazan 0.8~1.5, thiazole Quinoline ketone 0.4~1.5, sodium chloride 0.3~1, EDETATE SODIUM 0.4~1.2, Nacl 0.8~2, polyethers sodium sulphate 0.3~1, water 150-200。
2. wiper essence according to claim 1, it is characterised in that:It is made of the following ingredients remembered by weight:Two First 1, thiazolinone 1.2, sodium chloride 0.5, EDETATE SODIUM 0.8, Nacl 1.5, polyethers sodium sulphate 0.8, water 180.
3. a kind of preparation method of wiper essence, which is characterized in that include the following steps:
(1)Note weighs 0.8~1.5 part of diformazan, 0.4~1.5 part of thiazolinone, 0.3~1 part of sodium chloride, EDTA bis- by weight 0.4~1.2 part of sodium, 0.8~2 part of Nacl, 0.3~1 part of polyethers sodium sulphate, 150-200 parts of water;
(2)By step(1)In water be heated into 100 DEG C;
(3)By step(1)In the diformazan, thiazolinone, sodium chloride, EDETATE SODIUM, Nacl, the polyethers sodium sulphate that weigh pour into step Suddenly(2)Water in mixed;
(4)Stirring;
(5)Precipitation 2~3 days;
(6)Filtering.
4. the preparation method of highly concentrated miniature automobile glass anti-fog detergent according to claim 3, it is characterised in that:Step (1)In by weight note weigh 1 part of diformazan, 1.2 parts of thiazolinone, 0.5 part of sodium chloride, 0.8 part of EDETATE SODIUM, Nacl 1.5 Part, 0.8 part of polyethers sodium sulphate, 180 parts of water.
CN201710304828.XA 2017-05-03 2017-05-03 A kind of wiper essence and preparation method thereof Pending CN108795582A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710304828.XA CN108795582A (en) 2017-05-03 2017-05-03 A kind of wiper essence and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201710304828.XA CN108795582A (en) 2017-05-03 2017-05-03 A kind of wiper essence and preparation method thereof

Publications (1)

Publication Number Publication Date
CN108795582A true CN108795582A (en) 2018-11-13

Family

ID=64054459

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201710304828.XA Pending CN108795582A (en) 2017-05-03 2017-05-03 A kind of wiper essence and preparation method thereof

Country Status (1)

Country Link
CN (1) CN108795582A (en)

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Application publication date: 20181113