CN108795237A - A kind of inorganic anti-corrosion paint and preparation method thereof - Google Patents
A kind of inorganic anti-corrosion paint and preparation method thereof Download PDFInfo
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- CN108795237A CN108795237A CN201810657334.4A CN201810657334A CN108795237A CN 108795237 A CN108795237 A CN 108795237A CN 201810657334 A CN201810657334 A CN 201810657334A CN 108795237 A CN108795237 A CN 108795237A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D163/00—Coating compositions based on epoxy resins; Coating compositions based on derivatives of epoxy resins
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D197/00—Coating compositions based on lignin-containing materials
- C09D197/02—Lignocellulosic material, e.g. wood, straw or bagasse
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/14—Paints containing biocides, e.g. fungicides, insecticides or pesticides
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/70—Additives characterised by shape, e.g. fibres, flakes or microspheres
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2237—Oxides; Hydroxides of metals of titanium
- C08K2003/2241—Titanium dioxide
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/14—Polymer mixtures characterised by other features containing polymeric additives characterised by shape
- C08L2205/16—Fibres; Fibrils
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Plant Pathology (AREA)
- Paints Or Removers (AREA)
Abstract
The present invention provides a kind of inorganic anti-corrosion paint, is made by liquid phase component and solid phase components, and the weight ratio of solid phase components and liquid phase component is 1:(2~3), wherein:The liquid phase component includes following raw material:5~10 parts of epoxy emulsion, 4~10 parts of Antisepticize and mildew preventive, 3~8 parts of carboxymethyl cellulose, 10~20 parts of ammonium hydroxide;The solid phase components include following raw material:5~10 parts of banana stem fiber, 5~15 parts of calcium sulfate crystal whiskers, 5~20 parts of silica flour, 4~9 parts of titanium dioxide, 4~7 parts of prodan.The liquid phase component of the present invention, the formula and its mixed ratio of solid phase components, so that the film formed after anti-corrosion paint of the present invention is hard, strong adhesive force, there is excellent alkali resistance, contrast ratio, abrasion resistance, elongation at break, water resistance and good impervious effect.
Description
Technical field
The present invention relates to technical field of coatings, more particularly to a kind of inorganic anti-corrosion paint and preparation method thereof.
Background technology
It is surprising to corrode to loss caused by the mankind, and economic loss is huge caused by corrosion every year, huge loss
Stimulate the development of anticorrosive paint.Anticorrosive paint is the coating for referring to the long-lasting protection under harsh corrosive environment, protects the longevity
Life is generally 10 years or more, under the corrosive mediums environment such as acid, alkali, salt and solvent at a certain temperature, can be used 3~5 years.
Anticorrosive paint brushing can form thin film, make building surface and air exclusion on building surface, to play anti-corrosion
Effect.The anti-corrosion film formed after anticorrosive paint is cured should have certain weatherability, water resistance, extensibility, elastoplasticity
And crack resistance, anti-corrosion can be played, prevent blending protective effect.But the resistance to corrosion of existing anticorrosive paint is not also good enough, thus it is anxious
A kind of anticorrosive paint is needed, above-mentioned technical problem is solved.
Invention content
For mirror with this, a kind of inorganic anti-corrosion paint of present invention proposition and preparation method thereof solves above-mentioned technical problem.
The technical proposal of the invention is realized in this way:A kind of inorganic anti-corrosion paint, by liquid phase component and solid phase components system
, the weight ratio of solid phase components and liquid phase component is 1:(2~3), wherein:
The liquid phase component includes following raw material:5~10 parts of epoxy emulsion, 4~10 parts of Antisepticize and mildew preventive, carboxylic first
3~8 parts of base cellulose, 10~20 parts of ammonium hydroxide;
The solid phase components include following raw material:5~10 parts of banana stem fiber, 5~15 parts of calcium sulfate crystal whiskers,
5~20 parts of silica flour, 4~9 parts of titanium dioxide, 4~7 parts of prodan.
Further, the Antisepticize and mildew preventive is by 10:(1~3):The volcanic rock of (2~4) weight ratio, camellia leaf, folium isatidis
It is made.
Further, the liquid phase component includes following raw material:8 parts of epoxy emulsion, 6 parts of Antisepticize and mildew preventive, carboxylic
5 parts of methylcellulose, 15 parts of ammonium hydroxide;The solid phase components include following raw material:8 parts of banana stem fiber, calcium sulfate
10 parts of whisker, 15 parts of silica flour, 7 parts of titanium dioxide, 5 parts of prodan.
Further, the Antisepticize and mildew preventive is by 10:2:The volcanic rock of 3 weight ratios, camellia leaf, folium isatidis are made.
The present invention also provides a kind of preparation methods of inorganic anti-corrosion paint, include the following steps:
It is prepared by S1, Antisepticize and mildew preventive:By camellia leaf, folium isatidis saline sook, rear dry, crushing must mix leaf powder;It will
It is mixed with leaf powder after volcanic rock powder crushing process, Antisepticize and mildew preventive is made;
S2, liquid phase feed pretreatment:It weighs raw material respectively by weight, epoxy emulsion and ammonium hydroxide is mixed, prior to
75~85 DEG C of 20~40min of stirring, add carboxymethyl cellulose, stir 50~70min in 50~60 DEG C, are subsequently cooled to 30
~40 DEG C, Antisepticize and mildew preventive is added, continues 1~2h of stirring, obtains liquid phase mixture;
S3, Solid raw materials pretreatment:Fibers from banana stem is crushed, afterwards with calcium sulfate crystal whiskers, silica flour, titanium white
Powder, prodan are sufficiently mixed, and obtain solid-phase mixture;
S4, it is blended:The liquid phase mixture of S2 steps is sent into dispersion machine, then the solid-phase mixture of S3 steps is slowly added
In the liquid phase mixture for entering S2 steps, 10~20min of dispersion is carried out in 1000~1200r/min, then at 700~800r/min into
Row 25~35min of dispersion, is made inorganic anti-corrosion paint.
Further, in step S1, the immersion concrete operations are:Prior to 45~55 DEG C 10~20min of saline sook, after
In 25~30 DEG C of 40~60min of saline sook.
Further, in step S2, epoxy emulsion and ammonium hydroxide are mixed, prior to 80 DEG C stirring 30min add carboxylic
Methylcellulose stirs 60min in 55 DEG C, is subsequently cooled to 35 DEG C, Antisepticize and mildew preventive is added, and continues to stir 1.5h, obtains liquid phase
Mixture.
Further, in step S3, fibers from banana stem is crushed to 80~100 mesh.
Further, in step S4, dispersion 15min is carried out prior to 1100r/min, is disperseed then at 800r/min
30min。
Compared with prior art, the beneficial effects of the invention are as follows:
The liquid phase component of the present invention, the formula and its mixed ratio of solid phase components so that anti-corrosion paint of the present invention
The film that is formed afterwards is hard, strong adhesive force, has excellent alkali resistance, contrast ratio, abrasion resistance, elongation at break, water resistance
With good impervious effect.
In addition, using the homemade Antisepticize and mildew preventive of the present invention, the performance of coating is further improved.Moreover, the present invention
Preparation method handles liquid phase feed through gradient temperature, in conjunction with the pretreatment of Solid raw materials, is most blended afterwards through multi-level dispersion, into one
Step optimizes the performance of coating.
Specific implementation mode
In order to be best understood from the technology of the present invention content, specific embodiment is provided below, the present invention is described further.
Embodiment 1
A kind of inorganic anti-corrosion paint, is made by liquid phase component and solid phase components, the weight ratio of solid phase components and liquid phase component
It is 1:2, wherein:
The liquid phase component includes following raw material:5 parts of epoxy emulsion, 4 parts of Antisepticize and mildew preventive, carboxymethyl cellulose
3 parts, 10 parts of ammonium hydroxide;The Antisepticize and mildew preventive is by 10:1:The volcanic rock of 2 weight ratios, camellia leaf, folium isatidis are made;
The solid phase components include following raw material:5 parts of banana stem fiber, 5 parts of calcium sulfate crystal whiskers, silica flour 5
Part, 4 parts of titanium dioxide, 4 parts of prodan.
Embodiment 2
A kind of inorganic anti-corrosion paint, is made by liquid phase component and solid phase components, the weight ratio of solid phase components and liquid phase component
It is 1:3, wherein:
The liquid phase component includes following raw material:10 parts of epoxy emulsion, 10 parts of Antisepticize and mildew preventive, carboxymethyl cellulose
Plain 8 parts, 20 parts of ammonium hydroxide;The Antisepticize and mildew preventive is by 10:3:The volcanic rock of 2 weight ratios, camellia leaf, folium isatidis are made;
The solid phase components include following raw material:10 parts of banana stem fiber, 15 parts of calcium sulfate crystal whiskers, silica flour
20 parts, 9 parts of titanium dioxide, 7 parts of prodan.
Embodiment 3
A kind of inorganic anti-corrosion paint, is made by liquid phase component and solid phase components, the weight ratio of solid phase components and liquid phase component
It is 1:2.5, wherein:
The liquid phase component includes following raw material:8 parts of epoxy emulsion, 6 parts of Antisepticize and mildew preventive, carboxymethyl cellulose
5 parts, 15 parts of ammonium hydroxide;The Antisepticize and mildew preventive is by 10:2:The volcanic rock of 3 weight ratios, camellia leaf, folium isatidis are made;
The solid phase components include following raw material:8 parts of banana stem fiber, 10 parts of calcium sulfate crystal whiskers, silica flour
15 parts, 7 parts of titanium dioxide, 5 parts of prodan.
The preparation method of 1~3 inorganic anti-corrosion paint of above-described embodiment, includes the following steps:
It is prepared by S1, Antisepticize and mildew preventive:By camellia leaf, folium isatidis saline sook, prior to 50 DEG C saline sook 15min, after
In 28 DEG C of saline sook 50min;Dry afterwards, crushing, must mix leaf powder;It will be mixed with leaf powder after volcanic rock powder crushing process,
Antisepticize and mildew preventive is made;
S2, liquid phase feed pretreatment:It weighs raw material respectively by weight, epoxy emulsion and ammonium hydroxide is mixed, prior to
80 DEG C of stirring 30min, add carboxymethyl cellulose, stir 60min in 55 DEG C, are subsequently cooled to 35 DEG C, anticorrosive mildewproof is added
Agent continues to stir 1.5h, obtains liquid phase mixture;
S3, Solid raw materials pretreatment:Fibers from banana stem is crushed, is crushed to after 100 mesh and calcium sulfate crystal whiskers, stone
Ying Fen, titanium dioxide, prodan are sufficiently mixed, and obtain solid-phase mixture;
S4, it is blended:The liquid phase mixture of S2 steps is sent into dispersion machine, then the solid-phase mixture of S3 steps is slowly added
In the liquid phase mixture for entering S2 steps, dispersion 15min is carried out prior to 1100r/min, dispersion 30min is carried out then at 800r/min,
Inorganic anti-corrosion paint is made.
Embodiment 4
The present embodiment is identical as the formula of embodiment 3, difference lies in, the preparation method of the inorganic anti-corrosion paint, packet
Include following steps:
It is prepared by S1, Antisepticize and mildew preventive:By camellia leaf, folium isatidis saline sook, prior to 45 DEG C saline sook 20min, after
In 25 DEG C of saline sook 60min;Dry afterwards, crushing, must mix leaf powder;It will be mixed with leaf powder after volcanic rock powder crushing process,
Antisepticize and mildew preventive is made;
S2, liquid phase feed pretreatment:It weighs raw material respectively by weight, epoxy emulsion and ammonium hydroxide is mixed, prior to
75 DEG C of stirring 40min, add carboxymethyl cellulose, stir 70min in 50 DEG C, are subsequently cooled to 30 DEG C, anticorrosive mildewproof is added
Agent continues to stir 2h, obtains liquid phase mixture;
S3, Solid raw materials pretreatment:Fibers from banana stem is crushed, is crushed to after 80 mesh and calcium sulfate crystal whiskers, stone
Ying Fen, titanium dioxide, prodan are sufficiently mixed, and obtain solid-phase mixture;
S4, it is blended:The liquid phase mixture of S2 steps is sent into dispersion machine, then the solid-phase mixture of S3 steps is slowly added
In the liquid phase mixture for entering S2 steps, dispersion 20min is carried out in 1000r/min, dispersion 25min is carried out then at 700r/min, is made
Obtain inorganic anti-corrosion paint.
Embodiment 5
The present embodiment is identical as the formula of embodiment 3, difference lies in, the preparation method of the inorganic anti-corrosion paint, packet
Include following steps:
It is prepared by S1, Antisepticize and mildew preventive:By camellia leaf, folium isatidis saline sook, prior to 55 DEG C saline sook 10min, after
In 30 DEG C of saline sook 40min;Dry afterwards, crushing, must mix leaf powder;It will be mixed with leaf powder after volcanic rock powder crushing process,
Antisepticize and mildew preventive is made;
S2, liquid phase feed pretreatment:It weighs raw material respectively by weight, epoxy emulsion and ammonium hydroxide is mixed, prior to
85 DEG C of stirring 20min, add carboxymethyl cellulose, stir 50min in 60 DEG C, are subsequently cooled to 40 DEG C, anticorrosive mildewproof is added
Agent continues to stir 1h, obtains liquid phase mixture;
S3, Solid raw materials pretreatment:Fibers from banana stem is crushed, is crushed to after 100 mesh and calcium sulfate crystal whiskers, stone
Ying Fen, titanium dioxide, prodan are sufficiently mixed, and obtain solid-phase mixture;
S4, it is blended:The liquid phase mixture of S2 steps is sent into dispersion machine, then the solid-phase mixture of S3 steps is slowly added
In the liquid phase mixture for entering S2 steps, dispersion 10min is carried out in 1200r/min, dispersion 25min is carried out then at 800r/min, is made
Obtain inorganic anti-corrosion paint.
Embodiment 6
The present embodiment is identical as the formula of embodiment 3, and difference lies in the preparation method of the inorganic anti-corrosion paint is:
Commercial anticorrosive mould inhibitor is taken, and liquid phase feed and Solid raw materials difference mixture is uniform, obtains liquid phase mixture and solid-phase mixture,
Prepared solid-phase mixture is slowly poured into liquid phase mixture again, is sufficiently stirred, inorganic anti-corrosion paint is obtained.
Comparative example 1
Difference lies in be made, solid phase components and liquid phase group this comparative example by liquid phase component and solid phase components with embodiment 3
The weight ratio divided is 1:1.
Comparative example 2
Difference lies in the liquid phase component includes following raw material to this comparative example with embodiment 3:Epoxy emulsion 3
Part, 12 parts of Antisepticize and mildew preventive, 9 parts of carboxymethyl cellulose, 22 parts of ammonium hydroxide.
Comparative example 3
Difference lies in the solid phase components include following raw material to this comparative example with embodiment 3:Banana stem is fine
12 parts of dimension, 2 parts of calcium sulfate crystal whiskers, 3 parts of silica flour, 11 parts of titanium dioxide, 9 parts of prodan.
One, inorganic anti-corrosion paint made from embodiment 1-5 and comparative example 1~3 is tested for the property, test result is such as
Under:
The above results show that inorganic anti-corrosion paint of the invention has excellent alkali resistance, contrast ratio, abrasion resistance, breaks
Split elongation, water resistance and good impervious effect.Wherein, the performance of embodiment 3 is best, shows in each embodiment to be best
Proportioning, optimised process;Comparative example 1~3 and embodiment 3 compare, show the liquid phase component of the present invention, the formula of solid phase components and
Its mixed ratio plays extremely critical influence to the anticorrosive paint performance of the present invention;Wherein embodiment 6 is compared with embodiment 3,
Show present invention self-control Antisepticize and mildew preventive, and is most passed through afterwards in conjunction with the pretreatment of Solid raw materials through gradient temperature processing liquid phase feed
Multi-level dispersion is blended, and has advanced optimized the performance of coating.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all essences in the present invention
With within principle, any modification, equivalent replacement, improvement and so on should all be included in the protection scope of the present invention god.
Claims (9)
1. a kind of inorganic anti-corrosion paint, it is characterised in that:It is made by liquid phase component and solid phase components, solid phase components and liquid phase component
Weight ratio be 1:(2~3), wherein:
The liquid phase component includes following raw material:5~10 parts of epoxy emulsion, 4~10 parts of Antisepticize and mildew preventive, carboxymethyl are fine
Dimension plain 3~8 parts, 10~20 parts of ammonium hydroxide;
The solid phase components include following raw material:5~10 parts of banana stem fiber, 5~15 parts of calcium sulfate crystal whiskers, quartz
5~20 parts of powder, 4~9 parts of titanium dioxide, 4~7 parts of prodan.
2. a kind of inorganic anti-corrosion paint as described in claim 1, it is characterised in that:The Antisepticize and mildew preventive is by 10:(1~3):
The volcanic rock of (2~4) weight ratio, camellia leaf, folium isatidis are made.
3. a kind of inorganic anti-corrosion paint as claimed in claim 1 or 2, it is characterised in that:The liquid phase component includes following heavy
Measure part raw material:8 parts of epoxy emulsion, 6 parts of Antisepticize and mildew preventive, 5 parts of carboxymethyl cellulose, 15 parts of ammonium hydroxide;The solid phase components include
Following raw material:8 parts of banana stem fiber, 10 parts of calcium sulfate crystal whiskers, 15 parts of silica flour, 7 parts of titanium dioxide, prodan 5
Part.
4. a kind of inorganic anti-corrosion paint as claimed in claim 2, it is characterised in that:The Antisepticize and mildew preventive is by 10:2:3 weight
The volcanic rock of ratio, camellia leaf, folium isatidis are made.
5. a kind of preparation method of inorganic anti-corrosion paint as claimed in claim 2, it is characterised in that:Include the following steps:
It is prepared by S1, Antisepticize and mildew preventive:By camellia leaf, folium isatidis saline sook, rear dry, crushing must mix leaf powder;By volcano
It is mixed with leaf powder after rock powder crushing process, Antisepticize and mildew preventive is made;
S2, liquid phase feed pretreatment:It weighs raw material respectively by weight, epoxy emulsion and ammonium hydroxide is mixed, prior to 75~
85 DEG C of 20~40min of stirring, add carboxymethyl cellulose, stir 50~70min in 50~60 DEG C, are subsequently cooled to 30~40
DEG C, Antisepticize and mildew preventive is added, continues 1~2h of stirring, obtains liquid phase mixture;
S3, Solid raw materials pretreatment:Fibers from banana stem is crushed, afterwards with calcium sulfate crystal whiskers, silica flour, titanium dioxide, fluorine
Sodium metasilicate is sufficiently mixed, and obtains solid-phase mixture;
S4, it is blended:The liquid phase mixture of S2 steps is sent into dispersion machine, then the solid-phase mixture of S3 steps is slowly added into S2
In the liquid phase mixture of step, 10~20min of dispersion is carried out in 1000~1200r/min, is divided then at 700~800r/min
25~35min is dissipated, inorganic anti-corrosion paint is made.
6. a kind of preparation method of inorganic anti-corrosion paint as claimed in claim 5, it is characterised in that:In step S1, the leaching
Steeping concrete operations is:Prior to 45~55 DEG C 10~20min of saline sook, after in 25~30 DEG C of 40~60min of saline sook.
7. such as a kind of preparation method of inorganic anti-corrosion paint described in claim 5 or 6, it is characterised in that:In step S2, by ring
Oxygen lotion and ammonium hydroxide are mixed, and prior to 80 DEG C stirring 30min add carboxymethyl cellulose, stir 60min in 55 DEG C, so
Antisepticize and mildew preventive is added to 35 DEG C in postcooling, continues to stir 1.5h, obtains liquid phase mixture.
8. such as a kind of preparation method of inorganic anti-corrosion paint described in claim 5 or 6, it is characterised in that:It, will be fragrant in step S3
Any of several broadleaf plants stem fiber is crushed to 80~100 mesh.
9. such as a kind of preparation method of inorganic anti-corrosion paint described in claim 5 or 6, it is characterised in that:In step S4, prior to
1100r/min carries out dispersion 15min, and dispersion 30min is carried out then at 800r/min.
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JPS60248779A (en) * | 1984-05-24 | 1985-12-09 | Dainippon Toryo Co Ltd | Water-based corrosion-proofing coating composition |
CN103253910A (en) * | 2013-04-24 | 2013-08-21 | 中国石油大学(北京) | Novel cement-based composite anti-corrosive paint |
CN104693956A (en) * | 2013-12-05 | 2015-06-10 | 青岛惠城石化科技有限公司 | Cement-based polymer anticorrosion coating and preparing method thereof |
CN105017822A (en) * | 2015-08-19 | 2015-11-04 | 合肥科德电力表面技术有限公司 | Water-soluble, high-temperature-resistant and anti-corrosive inorganic silicate paint and preparation method thereof |
CN106047087A (en) * | 2016-08-22 | 2016-10-26 | 湖南太子化工涂料有限公司 | Room temperature self-drying two-component epoxy heavy anti-corrosion prime coat and preparation method thereof |
-
2018
- 2018-06-25 CN CN201810657334.4A patent/CN108795237B/en active Active
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS60248779A (en) * | 1984-05-24 | 1985-12-09 | Dainippon Toryo Co Ltd | Water-based corrosion-proofing coating composition |
CN103253910A (en) * | 2013-04-24 | 2013-08-21 | 中国石油大学(北京) | Novel cement-based composite anti-corrosive paint |
CN104693956A (en) * | 2013-12-05 | 2015-06-10 | 青岛惠城石化科技有限公司 | Cement-based polymer anticorrosion coating and preparing method thereof |
CN105017822A (en) * | 2015-08-19 | 2015-11-04 | 合肥科德电力表面技术有限公司 | Water-soluble, high-temperature-resistant and anti-corrosive inorganic silicate paint and preparation method thereof |
CN106047087A (en) * | 2016-08-22 | 2016-10-26 | 湖南太子化工涂料有限公司 | Room temperature self-drying two-component epoxy heavy anti-corrosion prime coat and preparation method thereof |
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