CN108753173A - A kind of sun-proof decolorising agent of shared bicycle - Google Patents
A kind of sun-proof decolorising agent of shared bicycle Download PDFInfo
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- CN108753173A CN108753173A CN201810514857.3A CN201810514857A CN108753173A CN 108753173 A CN108753173 A CN 108753173A CN 201810514857 A CN201810514857 A CN 201810514857A CN 108753173 A CN108753173 A CN 108753173A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D197/00—Coating compositions based on lignin-containing materials
- C09D197/02—Lignocellulosic material, e.g. wood, straw or bagasse
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/18—Fireproof paints including high temperature resistant paints
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/63—Additives non-macromolecular organic
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/65—Additives macromolecular
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- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/70—Additives characterised by shape, e.g. fibres, flakes or microspheres
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- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2237—Oxides; Hydroxides of metals of titanium
- C08K2003/2241—Titanium dioxide
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- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
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- C08L2201/08—Stabilised against heat, light or radiation or oxydation
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- C—CHEMISTRY; METALLURGY
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- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
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- C—CHEMISTRY; METALLURGY
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Abstract
The invention discloses a kind of shared sun-proof decolorising agents of bicycle, are related to sunscreen material correlative technology field；The present invention shares the sun-proof decolorising agent component of bicycle：Atlapulgite, rubber powder, aromatic modified terpene resin, nanometer sepiolite composite powder, microwax, dwarf lilyturf tuber total saponins graft linker, Polar Adsorbent Resin, sepiolite fiber modified bamboo powder, molecular screen primary powder, glass powder, atlapulgite, ceramic, poly alpha methylstyrene resin, microwax, sulphation Aloe Vera Gel, nanometer titanium dioxide；The present invention is directed to the sun-proof decolorising agent of shared bicycle that shared bicycle is developed using existing problem, shared bicycle can be effectively relieved for a long time because of strong light direct beam in the sun-proof decolorising agent, color caused by wind and weather etc. is decolourized, the sun-proof resistance to direct sunlight of decolorising agent of the present invention, liquid impregnates, acid and alkali-resistance, high temperature resistant, and it is safe and non-toxic, environmental pollution will not be caused when applied to material.
Description
Technical field：
The present invention relates to sunscreen material correlative technology fields, and in particular to a kind of shared sun-proof decolorising agent of bicycle.
Background technology：
Since 2016, bicycle has been shared with the attraction of its " solving user's trip last one kilometer ", has become trip new lover.Five
During one, Ma Yun is even more to announce that sharing bicycle exempts from cash pledge.Bicycle, the giants 2017 of ofo two are visitd it is expected that injected volume will it is reported that rubbing
" blowout ", close to 20,000,000, production capacity is estimated up to 30,000,000.All standing is realized in one line city, marches more than 10 tier 2 cities,
Open up 200 three or four line cities.
Bright tire gives the experience of riding for expending muscle power on shared bicycle, this is because they are special rubbers
Inflation-free solid tyre made of glue, whether future is expected to use nylon tire, not only light, also has higher intensity and resistance to
Mill property.And the structure that nylon may be used further include vehicle seat, mud guard, handle, reflector lamp, speed changer, refer to dial, low side brake lever,
Foot-operated, taillight, tire etc..
In shared bicycle, in addition to the foregoing materials using material, the figure layer material of some bright colors is also used, altogether
It enjoys bicycle and little Lan, little Huang occurs, it is small red, it is small green ..., it is colorful, it is colourful.But the use environment of shared bicycle and
Storage place throughout the year outside, can be by wind and weather direct sunlight etc., therefore after causing shared bicycle to be used for a long time, irregular colour
One, lighter etc..
Invention content：
The present invention is directed to the above-mentioned problem of shared bicycle, develops a kind of shared sun-proof decolorising agent of bicycle, this is sun-proof de-
Shared bicycle can be effectively relieved for a long time because color caused by strong light direct beam, wind and weather etc. is decolourized in toner, and the present invention is sun-proof de-
The resistance to direct sunlight of toner, liquid impregnate, acid and alkali-resistance, high temperature resistant, and safe and non-toxic, will not cause environment dirty when applied to material
Dye.
It is realized using following technical scheme using the technical problems to be solved by the invention：
A kind of sun-proof decolorising agent of shared bicycle, the sun-proof decolorising agent include following number component：Atlapulgite 0.5-3
Part, 3-6 parts of rubber powder, terpene resin 2-4 parts aromatic modified, 2-4 parts of nanometer sepiolite composite powder, 1-2 parts of microwax, Radix Ophiopogonis are total
0.5-1 parts of saponin(e graft linker, 0.3-0.5 parts of Polar Adsorbent Resin, bamboo powder 35-40 parts sepiolite fiber modified, molecular sieve
2-3 parts of original powder, 2-3 parts of glass powder, 1-2 parts of atlapulgite, 1-2 parts of ceramic, 0.5-1 parts of poly alpha methylstyrene resin,
0.5-1 parts of microwax, 0.5-1 parts of sulphation Aloe Vera Gel, 0.3-0.5 parts of nanometer titanium dioxide.
The dwarf lilyturf tuber total saponins graft linker is handled by dwarf lilyturf tuber total saponins are modified, and specific preparation method is：To
Turpentine oil and hydrogenated rosin pentaerythritol ester are added in dwarf lilyturf tuber total saponins, in microwave frequency 2450MHz, output work after being sufficiently mixed
Microwave treatment 10min under rate 700W, and be transferred in 0-5 DEG C of environment and stand 30min, add allyl glycidyl ether and vulcanization
Lard continues microwave treatment 10min, is then cooled to 50-55 DEG C of sealing thermal insulation with the cooling rate of 5 DEG C/min after mixing
30min is stood, gained mixture is sent into ball mill, the ground micro mist that fineness is made and is less than 20 μm.
The dwarf lilyturf tuber total saponins, turpentine oil, hydrogenated rosin pentaerythritol ester, allyl glycidyl ether, sulfurized lard
Amount ratio is 30-40:2-4:1-3:0.5-1:0.5-1.5.
The aromatic modified terpene resin is aided with auxiliary agent by terpene resin and is prepared, and specific preparation method is：First by terpene
Olefine resin is warming up to 100-105 DEG C of heat preservation grinding 5-10min with the heating rate of 5 DEG C/min, adds volcanic ash and magnesium silicate
Aluminium continues to be warming up to 130-140 DEG C of heat preservation grinding 10-15min with the heating rate of 5 DEG C/min, then with the cooling of 5 DEG C/min
Speed is cooled to 0-5 DEG C of sealing thermal insulation and stands 15-30min, and asbestos wool, diallyl dimethyl ammoniumchloride and N- hydroxyls is added
Methacrylamide is warming up to 125-130 DEG C of heat preservation grinding 15-30min with the heating rate of 5 DEG C/min again, waits for that nature is cold
But gained mixture is sent into vacuum drier to after room temperature, dry obtained solid through micronizer be made micro mist to get
Aromatic modified terpenes tree.
The terpene resin, volcanic ash, aluminium-magnesium silicate, asbestos wool, diallyl dimethyl ammoniumchloride and N- methylols
The mass ratio of acrylamide is 30-35:1-2:0.8-1.5:0.5-1:0.5-1:0.5-0.8.
Aromatic modified terpene resin can not only significantly increase its specific surface area and enrich after terpene resin and additive modification
Its internal gutter structure, moreover it is possible to enhance and remaining prepares the comixing compatibility between raw material, promotion prepares the uniform mixing of raw material.
Using preceding by pre-processing, processing method is the sulphation Aloe Vera Gel：By Aloe Vera Gel in microwave frequency
Microwave treatment 5-10min under 2450MHz, output power 700W, adds polyethylene glycol oxide and dihydrogen sulfate sodium, after being sufficiently mixed
Continue microwave treatment 5-10min, then with the cooling rate of 5 DEG C/min be cooled to 0-5 DEG C heat preservation stand 30min, and with 5 DEG C/
The heating rate of min is warming up to 110-115 DEG C of heat preservation grinding 10min, and 45-50 DEG C of water is added into gained mixture, fully stirs
It is stood after mixing, that is, completes the pretreatment of sulphation Aloe Vera Gel.
The mass ratio of the sulphation Aloe Vera Gel, polyethylene glycol oxide and dihydrogen sulfate sodium is 0.5-1:0.05-0.1:0.02-
0.03。
Sulphation Aloe Vera Gel can not only enhance the absorption stickiness of Aloe Vera Gel after above-mentioned pretreatment, moreover it is possible to enhance its with
Remaining prepares the comixing compatibility between raw material, and promotion prepares the uniform mixing of raw material.
A kind of above-mentioned preparation method of the shared sun-proof decolorising agent of bicycle of the present invention, includes the following steps：
(1) atlapulgite, rubber powder of waste tire, aromatic modified terpene resin, nanometer sepiolite composite powder, nano-titanium are taken
White powder is added in the sulphation Aloe Vera Gel of 2-3 times of mixture weight, 30-50 minutes ultrasonic, is sent into reaction kettle, and temperature is increased
It it is 60-97 DEG C, product is filtered, washed 3-4 times with ethyl alcohol, is placed in 40-50 DEG C of baking oven by insulation reaction 35-40 hours, discharging
Middle drying obtains material I to constant weight；
(2) microwax, dwarf lilyturf tuber total saponins graft linker, Polar Adsorbent Resin, sepiolite fiber modified bamboo powder are mixed,
It is 30-60 minutes ultrasonic, it is sent into reaction kettle, is passed through nitrogen, it is 68-70 DEG C to increase temperature, insulation reaction 3.5-4 hours, discharging,
Product is filtered, is washed 3-4 times with ethyl alcohol, is placed in 70-80 DEG C of baking oven and dries to constant weight, obtain material II；
(3) molecular screen primary powder, glass powder, atlapulgite, ceramic, poly alpha methylstyrene resin, microwax are taken, is added
In the sulphation Aloe Vera Gel for entering its weight 17-20%, it is stirred 20-30 minutes, the second of a concentration of 0.3-0.6mol/L is added dropwise
Acid solution, adjusting pH are 6.5-7.0, are passed through nitrogen, are heated to 25-35 DEG C of holding 30-60min, discharge to obtain material III；
(4) above-mentioned material I, material II, material III are mixed, is preheated 40-60 minutes at 27-35 DEG C, insulated and stirred 30-
It 40 minutes, is filtered to remove big impurity material and obtains sun-proof decolorising agent basis bottom material；
(5) sun-proof decolorising agent basis bottom material is entered to waiting in hydraulic tank, negative pressure is generated using pressure apparatus, it will be in hydraulic tank
Sun-proof decolorising agent basis bottom material be sucked into knockout drum；
(6) control steam heater provides heat to knockout drum and rectifying column, in -0.1~-0.01MPa negative pressure
In the state of be evaporated under reduced pressure, control the temperature in knockout drum and rectifying column between 70 DEG C -150 DEG C, pass through gas-liquid
Separation removes volatilization gas in sun-proof decolorising agent with rectifying, and softens sun-proof decolorising agent by distilling.
The present invention shares single vehicle sun-screening decolorising agent advantages and beneficial effects：
1, the present invention uses existing problem for shared bicycle, and the sun-proof decolorising agent of shared bicycle that the present invention develops should
Shared bicycle can be effectively relieved for a long time because of color decoloration caused by strong light direct beam, wind and weather etc., the present invention in sun-proof decolorising agent
The sun-proof resistance to direct sunlight of decolorising agent, liquid impregnate, acid and alkali-resistance, high temperature resistant, and safe and non-toxic, and ring will not be caused when applied to material
It pollutes in border；
2, shared single vehicle sun-screening decolorising agent prepared by the present invention, can make sun-proof decolorising agent fit in rapidly rubber layer or
Alloy-layer can be also used in mixed way with rubber or alloy, prevented color decoloration or slowed down color decoloration.
Description of the drawings：
Fig. 1：Effect of the sun-proof decolorising agent difference usage amount to the shared sun-proof decoloration of bicycle；
Specific implementation mode：
In order to make the technical means, the creative features, the aims and the efficiencies achieved by the present invention be easy to understand, tie below
Specific embodiment is closed, the present invention is further explained.
Embodiment 1：
A kind of sun-proof decolorising agent of shared bicycle, the sun-proof decolorising agent include following number component：0.5 part of atlapulgite,
3 parts of rubber powder, 2 2.5 parts of part, nanometer sepiolite composite powder of aromatic modified terpene resin, 1.5 parts of microwax, dwarf lilyturf tuber total saponins connect
0.5 part of bridging agent of branch, 0.3 part of Polar Adsorbent Resin, 35 parts of sepiolite fiber modified bamboo powder, 2 parts of molecular screen primary powder, glass powder 2
Part, 1 part of atlapulgite, 1 part of ceramic, 0.6 part of poly alpha methylstyrene resin, 0.7 part of microwax, sulphation Aloe Vera Gel
0.5 part, 0.3 part of nanometer titanium dioxide.
The dwarf lilyturf tuber total saponins graft linker is handled by dwarf lilyturf tuber total saponins are modified, and specific preparation method is：To
Turpentine oil and hydrogenated rosin pentaerythritol ester are added in dwarf lilyturf tuber total saponins, in microwave frequency 2450MHz, output work after being sufficiently mixed
Microwave treatment 10min under rate 700W, and be transferred in 0-5 DEG C of environment and stand 30min, add allyl glycidyl ether and vulcanization
Lard continues microwave treatment 10min, it is quiet to be then cooled to 50 DEG C of sealing thermal insulations with the cooling rate of 5 DEG C/min after mixing
30min is set, gained mixture is sent into ball mill, the ground micro mist that fineness is made and is less than 20 μm.
The dwarf lilyturf tuber total saponins, turpentine oil, hydrogenated rosin pentaerythritol ester, allyl glycidyl ether, sulfurized lard
Amount ratio is 30:2:1:0.5:0.5.
The aromatic modified terpene resin is aided with auxiliary agent by terpene resin and is prepared, and specific preparation method is：First by terpene
Olefine resin is warming up to 100 DEG C of heat preservation grinding 5min with the heating rate of 5 DEG C/min, adds volcanic ash and aluminium-magnesium silicate, continues
135 DEG C of heat preservation grinding 15min are warming up to the heating rate of 5 DEG C/min, 0-5 is then cooled to the cooling rate of 5 DEG C/min
DEG C sealing thermal insulation stands 20min, and asbestos wool, diallyl dimethyl ammoniumchloride and N hydroxymethyl acrylamide is added, then
The secondary heating rate with 5 DEG C/min be warming up to 125 DEG C heat preservation grinding 16min, after naturally cool to after room temperature by gained mixture
It is sent into vacuum drier, micro mist is made to get aromatic modified terpenes tree through micronizer in dry obtained solid.
The terpene resin, volcanic ash, aluminium-magnesium silicate, asbestos wool, diallyl dimethyl ammoniumchloride and N- methylols
The mass ratio of acrylamide is 35:1.5:0.8:0.5:0.6:0.5.
Using preceding by pre-processing, processing method is the sulphation Aloe Vera Gel：By Aloe Vera Gel in microwave frequency
Microwave treatment 8min under 2450MHz, output power 700W, adds polyethylene glycol oxide and dihydrogen sulfate sodium, is sufficiently mixed subsequent
Then continuous microwave treatment 10min is cooled to 0-5 DEG C of heat preservation with the cooling rate of 5 DEG C/min and stands 30min, and with 5 DEG C/min's
Heating rate is warming up to 115 DEG C of heat preservation grinding 10min, and 45 DEG C of water are added into gained mixture, are stood after being sufficiently stirred, i.e., complete
At the pretreatment of sulphation Aloe Vera Gel.
The mass ratio of the sulphation Aloe Vera Gel, polyethylene glycol oxide and dihydrogen sulfate sodium is 1:0.1:0.02.
A kind of above-mentioned preparation method of the shared sun-proof decolorising agent of bicycle of the present invention, includes the following steps：
(1) atlapulgite, rubber powder of waste tire, aromatic modified terpene resin, nanometer sepiolite composite powder, nano-titanium are taken
White powder is added in the sulphation Aloe Vera Gel of 2-3 times of mixture weight, and ultrasound 30 minutes is sent into reaction kettle, is increased temperature and is
60 DEG C, product is filtered, is washed 3 times with ethyl alcohol by insulation reaction 35 hours, discharging, is placed in 40 DEG C of baking oven and is dried to constant weight,
Obtain material I；
(2) microwax, dwarf lilyturf tuber total saponins graft linker, Polar Adsorbent Resin, sepiolite fiber modified bamboo powder are mixed,
Ultrasound 30 minutes is sent into reaction kettle, and nitrogen is passed through, and it is 68 DEG C to increase temperature, insulation reaction 3.5 hours, and product is taken out in discharging
Filter, is washed 3 times with ethyl alcohol, is placed in 70 DEG C of baking oven and is dried to constant weight, obtains material II；
(3) molecular screen primary powder, glass powder, atlapulgite, ceramic, poly alpha methylstyrene resin, microwax are taken, is added
It in the sulphation Aloe Vera Gel for entering its weight 17%, is stirred 20 minutes, the acetic acid solution of a concentration of 0.3mol/L is added dropwise, adjust
PH is 6.5, is passed through nitrogen, is heated to 25 DEG C of holding 35min, discharge to obtain material III；
(4) above-mentioned material I, material II, material III are mixed, is preheated 40 minutes at 30 DEG C, insulated and stirred 35 minutes, mistake
It filters out big impurity material and obtains sun-proof decolorising agent basis bottom material；
(5) sun-proof decolorising agent basis bottom material is entered to waiting in hydraulic tank, negative pressure is generated using pressure apparatus, it will be in hydraulic tank
Sun-proof decolorising agent basis bottom material be sucked into knockout drum；
(6) control steam heater provides heat to knockout drum and rectifying column, in -0.1~-0.01MPa negative pressure
In the state of be evaporated under reduced pressure, the temperature in control knockout drum and rectifying column passes through gas-liquid separation and rectifying at 90 DEG C
Volatilization gas in sun-proof decolorising agent is removed, and softens sun-proof decolorising agent by distilling.
Embodiment 2：
A kind of sun-proof decolorising agent of shared bicycle, the sun-proof decolorising agent include following number component：3 parts of atlapulgite, rubber
4.5 parts of rubber powder, 2.5 3 parts of part, nanometer sepiolite composite powder of aromatic modified terpene resin, 1 part of microwax, dwarf lilyturf tuber total saponins grafting
0.5 part of bridging agent, 0.5 part of Polar Adsorbent Resin, 35 parts of sepiolite fiber modified bamboo powder, 2 parts of molecular screen primary powder, 3 parts of glass powder,
2 parts of atlapulgite, 1 part of ceramic, 0.5 part of poly alpha methylstyrene resin, 0.5 part of microwax, sulphation Aloe Vera Gel 0.6
Part, 0.3 part of nanometer titanium dioxide.
The dwarf lilyturf tuber total saponins graft linker is handled by dwarf lilyturf tuber total saponins are modified, and specific preparation method is：To
Turpentine oil and hydrogenated rosin pentaerythritol ester are added in dwarf lilyturf tuber total saponins, in microwave frequency 2450MHz, output work after being sufficiently mixed
Microwave treatment 10min under rate 700W, and be transferred in 0-5 DEG C of environment and stand 30min, add allyl glycidyl ether and vulcanization
Lard continues microwave treatment 10min, it is quiet to be then cooled to 55 DEG C of sealing thermal insulations with the cooling rate of 5 DEG C/min after mixing
30min is set, gained mixture is sent into ball mill, the ground micro mist that fineness is made and is less than 20 μm.
The dwarf lilyturf tuber total saponins, turpentine oil, hydrogenated rosin pentaerythritol ester, allyl glycidyl ether, sulfurized lard
Amount ratio is 35:2.5:1:0.5:0.5.
The aromatic modified terpene resin is aided with auxiliary agent by terpene resin and is prepared, and specific preparation method is：First by terpene
Olefine resin is warming up to 105 DEG C of heat preservation grinding 10min with the heating rate of 5 DEG C/min, adds volcanic ash and aluminium-magnesium silicate, continues
135 DEG C of heat preservation grinding 15min are warming up to the heating rate of 5 DEG C/min, 0-5 is then cooled to the cooling rate of 5 DEG C/min
DEG C sealing thermal insulation stands 20min, and asbestos wool, diallyl dimethyl ammoniumchloride and N hydroxymethyl acrylamide is added, then
The secondary heating rate with 5 DEG C/min be warming up to 125 DEG C heat preservation grinding 20min, after naturally cool to after room temperature by gained mixture
It is sent into vacuum drier, micro mist is made to get aromatic modified terpenes tree through micronizer in dry obtained solid.
The terpene resin, volcanic ash, aluminium-magnesium silicate, asbestos wool, diallyl dimethyl ammoniumchloride and N- methylols
The mass ratio of acrylamide is 30:1:0.8:1:0.5:0.5.
Using preceding by pre-processing, processing method is the sulphation Aloe Vera Gel：By Aloe Vera Gel in microwave frequency
Microwave treatment 5min under 2450MHz, output power 700W, adds polyethylene glycol oxide and dihydrogen sulfate sodium, is sufficiently mixed subsequent
Then continuous microwave treatment 5-10min is cooled to 0-5 DEG C of heat preservation with the cooling rate of 5 DEG C/min and stands 30min, and with 5 DEG C/min
Heating rate be warming up to 110 DEG C heat preservation grinding 10min, into gained mixture be added 50 DEG C of water, stood after being sufficiently stirred, i.e.,
Complete the pretreatment of sulphation Aloe Vera Gel.
The mass ratio of the sulphation Aloe Vera Gel, polyethylene glycol oxide and dihydrogen sulfate sodium is 0.5:0.05:0.02.
To carrying out experiment investigation respectively in embodiment provided by the invention, prepared by embodiment 1 and embodiment 2 sun-proof de-
Toner is used in shared bicycle, is control, result such as table 1, shown not use sun-proof decolorising agent；
The sun-proof decolorising agent strong illumination rear defence decolorizing effect (6 months) of the different usage amounts of table 1
| Sun-proof decolorising agent (g/L) | Embodiment 1 | Embodiment 2 | Control group |
| 2 | 9.8 | 10.3 | 43.1 |
| 4 | 20.3 | 21.5 | / |
| 6 | 39.5 | 43.6 | / |
| 8 | 53.2 | 58.7 | / |
| 10 | 66.5 | 67.2 | / |
| 12 | 78.3 | 87.8 | / |
| 14 | 97.9 | 98.4 | / |
In above-mentioned sun-proof Decolorant Test：Sun-proof decolorising agent is used in shared bicycle coating material, under the conditions of strong light direct beam：
3-6 months under 5000-10000 ± LX direct projections, color change is observed.
It is obtained by the above experimental result：Sun-proof decolorising agent has an effective sun-proof decolorizing effect to coating color, and with making
Dosage is continuously increased, the decoloration of sun-proof color can nearly 100%, and sun-proof decolorising agent is small to water pollution, and residual quantity is small.
The above shows and describes the basic principles and main features of the present invention and the advantages of the present invention.The technology of the industry
Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the above embodiments and description only describe this
The principle of invention, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, these changes
Change and improvement all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appended claims and its
Equivalent thereof.
Claims (7)
1. a kind of sun-proof decolorising agent of shared bicycle, it is characterised in that：Including following number component：0.5-3 parts of atlapulgite, rubber
3-6 parts of powder, terpene resin 2-4 parts aromatic modified, 2-4 parts of nanometer sepiolite composite powder, 1-2 parts of microwax, dwarf lilyturf tuber total saponins connect
0.5-1 parts of bridging agent of branch, 0.3-0.5 parts of Polar Adsorbent Resin, bamboo powder 35-40 parts sepiolite fiber modified, molecular screen primary powder 2-3
Part, 2-3 parts of glass powder, 1-2 parts of atlapulgite, 1-2 parts of ceramic, 0.5-1 parts of poly alpha methylstyrene resin, microwax
0.5-1 parts, 0.5-1 parts of sulphation Aloe Vera Gel, 0.3-0.5 parts of nanometer titanium dioxide.
2. the sun-proof decolorising agent of shared bicycle according to claim 1, it is characterised in that：The dwarf lilyturf tuber total saponins grafting connection
Agent is handled by dwarf lilyturf tuber total saponins are modified, and specific preparation method is：Turpentine oil and hydrogenation pine are added into dwarf lilyturf tuber total saponins
Fragrant pentaerythritol ester, after being sufficiently mixed under microwave frequency 2450MHz, output power 700W microwave treatment 10min, and be transferred to 0-
30min is stood in 5 DEG C of environment, allyl glycidyl ether and sulfurized lard is added, continues microwave treatment after mixing
Then 10min is cooled to 50-55 DEG C of sealing thermal insulation with the cooling rate of 5 DEG C/min and stands 30min, gained mixture is sent into ball
In grinding machine, the ground micro mist that fineness is made and is less than 20 μm.
3. the sun-proof decolorising agent of shared bicycle according to claim 2, it is characterised in that：The dwarf lilyturf tuber total saponins, turpentine oil,
Hydrogenated rosin pentaerythritol ester, allyl glycidyl ether, sulfurized lard amount ratio be 30-40:2-4:1-3:0.5-1:
0.5-1.5。
4. the sun-proof decolorising agent of shared bicycle according to claim 1, it is characterised in that：The aromatic modified terpene resin by
Terpene resin is aided with auxiliary agent and is prepared, and specific preparation method is：First terpene resin is warming up to the heating rate of 5 DEG C/min
100-105 DEG C of heat preservation grinding 5-10min, adds volcanic ash and aluminium-magnesium silicate, continuation is warming up to the heating rate of 5 DEG C/min
130-140 DEG C of heat preservation grinding 10-15min, is then cooled to 0-5 DEG C of sealing thermal insulation with the cooling rate of 5 DEG C/min and stands 15-
30min, and asbestos wool, diallyl dimethyl ammoniumchloride and N hydroxymethyl acrylamide is added, again with the liter of 5 DEG C/min
Warm speed is warming up to 125-130 DEG C of heat preservation grinding 15-30min, and gained mixture is sent into vacuum after naturally cool to after room temperature
In drying machine, micro mist is made to get aromatic modified terpenes tree through micronizer in dry obtained solid.
5. the sun-proof decolorising agent of shared bicycle according to claim 4, it is characterised in that：The terpene resin, volcanic ash, silicon
Sour magnalium, asbestos wool, diallyl dimethyl ammoniumchloride and N hydroxymethyl acrylamide mass ratio be 30-35:1-2:
0.8-1.5:0.5-1:0.5-1:0.5-0.8。
6. the sun-proof decolorising agent of shared bicycle according to claim 1, it is characterised in that：Before the sulphation Aloe Vera Gel use
By pretreatment, processing method is：By Aloe Vera Gel under microwave frequency 2450MHz, output power 700W microwave treatment 5-
10min adds polyethylene glycol oxide and dihydrogen sulfate sodium, after being sufficiently mixed continue microwave treatment 5-10min, then with 5 DEG C/
The cooling rate of min is cooled to 0-5 DEG C of heat preservation and stands 30min, and is warming up to 110-115 DEG C of guarantor with the heating rate of 5 DEG C/min
Temperature grinding 10min, 45-50 DEG C of water is added into gained mixture, is stood after being sufficiently stirred, that is, completes the pre- of sulphation Aloe Vera Gel
Processing.
7. the sun-proof decolorising agent of shared bicycle according to claim 6, it is characterised in that：The sulphation Aloe Vera Gel, polyoxy
The mass ratio for changing ethylene and dihydrogen sulfate sodium is 0.5-1:0.05-0.1:0.02-0.03.
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| CN201810514857.3A CN108753173A (en) | 2018-05-25 | 2018-05-25 | A kind of sun-proof decolorising agent of shared bicycle |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201810514857.3A CN108753173A (en) | 2018-05-25 | 2018-05-25 | A kind of sun-proof decolorising agent of shared bicycle |
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ID=64005736
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106587196A (en) * | 2016-12-16 | 2017-04-26 | 安徽苏启化工有限公司 | Primary decolorizer for treating high-chromaticity chemical industry wastewater |
| CN106752192A (en) * | 2016-12-30 | 2017-05-31 | 安徽真信涂料有限公司 | A kind of outdoor metal guardrail proprietary powder coatingses |
| CN106745695A (en) * | 2017-01-23 | 2017-05-31 | 和县伊迈炭业有限责任公司 | A kind of tower biological filter builds and uses paper honeycomb filtrate |
| CN106752273A (en) * | 2016-12-30 | 2017-05-31 | 安徽真信涂料有限公司 | A kind of aluminium section bar protective coating dedicated weather-proof agent and preparation method thereof |
| CN106752272A (en) * | 2016-12-30 | 2017-05-31 | 安徽真信涂料有限公司 | A kind of aluminium section bar protective coating preparation adhesion promoter |
-
2018
- 2018-05-25 CN CN201810514857.3A patent/CN108753173A/en not_active Withdrawn
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106587196A (en) * | 2016-12-16 | 2017-04-26 | 安徽苏启化工有限公司 | Primary decolorizer for treating high-chromaticity chemical industry wastewater |
| CN106752192A (en) * | 2016-12-30 | 2017-05-31 | 安徽真信涂料有限公司 | A kind of outdoor metal guardrail proprietary powder coatingses |
| CN106752273A (en) * | 2016-12-30 | 2017-05-31 | 安徽真信涂料有限公司 | A kind of aluminium section bar protective coating dedicated weather-proof agent and preparation method thereof |
| CN106752272A (en) * | 2016-12-30 | 2017-05-31 | 安徽真信涂料有限公司 | A kind of aluminium section bar protective coating preparation adhesion promoter |
| CN106745695A (en) * | 2017-01-23 | 2017-05-31 | 和县伊迈炭业有限责任公司 | A kind of tower biological filter builds and uses paper honeycomb filtrate |
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