CN108753041A - Aqueous white weaving coating ink-jet ink and preparation method thereof - Google Patents
Aqueous white weaving coating ink-jet ink and preparation method thereof Download PDFInfo
- Publication number
- CN108753041A CN108753041A CN201810428664.6A CN201810428664A CN108753041A CN 108753041 A CN108753041 A CN 108753041A CN 201810428664 A CN201810428664 A CN 201810428664A CN 108753041 A CN108753041 A CN 108753041A
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- China
- Prior art keywords
- ink
- aqueous white
- jet ink
- weaved
- coating ink
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/30—Inkjet printing inks
- C09D11/32—Inkjet printing inks characterised by colouring agents
- C09D11/322—Pigment inks
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/30—Inkjet printing inks
- C09D11/38—Inkjet printing inks characterised by non-macromolecular additives other than solvents, pigments or dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/30—Ink jet printing
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Textile Engineering (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
The invention discloses a kind of aqueous white weaving coating ink-jet inks and preparation method thereof, it is intended to provide one kind and can be adapted for a variety of nozzles, be not easy plug, high whiteness, film-forming flexibility is good, is particularly suitable for aqueous white weaving coating ink-jet ink of the nozzles such as DX5/DX7/5113 and preparation method thereof.The aqueous white weaving coating ink-jet ink is by mass percentage, composed of the following components：Dispersible pigment dispersion 30%-50%, resin 20%-40%, curing agent 0.2%-3%, acid-base modifier 0.1%-0.5%, moisturizer 10%-30%, surfactant 0.2%-2.0%, fungicide 0.1%-0.2%, surplus are water, and the water is deionized water.The present invention is suitable for the digit printing of the dark clothes of materials such as cotton, fiber crops, cotton blend, is applied to the technical field of ink-jet ink.
Description
Technical field
The present invention relates to a kind of ink and preparation method, more particularly to a kind of aqueous white weaving coating ink-jet ink and its
Preparation method.
Background technology
The printing mode suitable for Printings of the dark cloth of materials such as cotton, fiber crops, cotton blends generally has following at present
Two kinds：
1, rubber cement silk-screen：According to client's pattern requirement, first divide version, then make a plate, finally carries out silk-screen and scrape slurry, a pattern needs
More registerings are made, it is higher to operating personnel's skill set requirements, it is suitble to produce in enormous quantities, is not suitable for personalized customization.Rubber cement wire printing plate-making
Trouble, and a registering may only use once, if client needs new flower pattern and pattern that need to make a plate again, cause to waste.
The needs of client's small lot personalization cannot be met.Rubber cement environmental protection at present is not high, higher to operating personnel's skill set requirements, produces
The clothes poor air permeability come, customer experience are bad.
2, digit printing：Computer exports picture instruction, control printer printing, and Bai Caitong goes out, and without plate-making, meets client
Different individual demands.Digit printing is with the obvious advantage in small lot personalization, without plate-making, only computer software is needed to operate,
Meet current digit printing needs well.But the weaving coating drop mass of suitable printer is irregular at present, especially
Its coating chalk ink domestic manufacturer of weaving does good few.Domestic aqueous white coating ink-jet ink system is unstable at present
Fixed, standby poor performance is easy blocking sprayer, and whiteness is not high, and film-forming flexibility is bad, bad to the adaptability of a variety of print heads.Institute
It is selected using external import white coating ink, such as Du Pont's chalk with most of client.Though Du Pont's white textile ink is good,
It is at high price, seriously constrains the stamp of the dark cloth of the materials such as cotton, fiber crops, cotton blend.So there is an urgent need to develop a
The white weaving ink-jet paint ink of close even better than external import in performance, and cost performance higher, to client and consumption
The better usage experience of person.
Invention content
The technical problem to be solved by the present invention is to overcome the deficiencies of the prior art and provide one kind can be adapted for it is a variety of
Nozzle is not easy plug, and high whiteness, film-forming flexibility is good, is particularly suitable for the aqueous white weaving of the nozzles such as DX5/DX7/5113
Coating ink-jet ink and preparation method thereof.
The technical solution adopted in the present invention is：The aqueous white weaves coating ink-jet ink by mass percentage, by
Following components forms：Dispersible pigment dispersion 30%-50%, resin 20%-40%, curing agent 0.2%-3%, acid-base modifier 0.1%-0.5%,
Moisturizer 10%-30%, surfactant 0.2%-2.0%, fungicide 0.1%-0.2%, surplus are water, and the water is deionized water.
Further, the average grain diameter D50 of the dispersible pigment dispersion is not more than 300nm.
Further, the resin solid content is 30-40%, and elongation percentage is 500% or more.
Further, the acid-base modifier is at least one of triethanolamine, ammonium hydroxide, sodium hydroxide, AMP-95.
Further, the surfactant is aqueous nonionic surfactant.
Further, the moisturizer is glycerine, PEG2000, triethylene glycol, 1,5-PD, Isosorbide-5-Nitrae-propylene glycol, ten polyglycereol
At least one such as alcohol.
Further, the fungicide is 1,2-benzisothiazolin-3-one, at least one in BIT-20, Proxel GXL
Kind.
The preparation method of the aqueous white weaving coating ink-jet ink, includes the following steps：
A, it is uniformly mixed moisturizer, acid-base modifier, surfactant, fungicide, deionized water to obtain mixed liquor；
B, resin, curing agent up are sequentially added in step gained mixed liquor, be uniformly mixed, ensure stirring more than half an hour；
C, dispersible pigment dispersion is added into step b, is uniformly mixed, and be aged four hours；
D, PP membrane filtration twice of the gained mixed liquor with aperture precision no more than 0.45 micron in step c, takes filtrate.
The beneficial effects of the invention are as follows：By mass percentage due to aqueous white weaving coating ink-jet ink, by with
The following group is grouped as：Dispersible pigment dispersion 30%-50%, resin 20%-40%, curing agent 0.2%-3%, acid-base modifier 0.1%-0.5% are protected
Humectant 10%-30%, surfactant 0.2%-2.0%, fungicide 0.1%-0.2%, surplus are water, to distinctive be matched by this
Square technology solves the domestic standby poor performance of chalk coating ink, and easy plug, whiteness is inadequate, and the technology of film-forming flexibility difference is asked
Topic.Aqueous white weaving coating ink prepared by the present invention is highly suitable for the digital decorating machine of the nozzles such as DX5, DX7,5113,
In the not dry head of the standby test of printer, not plug, continuous print performance is good, and whiteness is high, and flexibility is good.
Specific implementation mode
With reference to specific embodiment, the present invention is further illustrated, and however, it is not limited to this.
Embodiment one
It is weighed by quality：25 parts of White Pigment Dispersion liquid（The AW PRO+ of diamond company）, 25 parts of HI-CUT for expanding intelligent trade
EP1913 resins, 1 part of curing agent Yang Song trades BL2116,0.1 part of acid-base modifier triethanolamine, 10 parts of moisturizer glycerine, 8
Part moisturizer 1,5-PD, 1 part of surfactant surfynol, 465,0.5 part of surfactant surfynol 604,29.4
Part deionized water.
Embodiment two
It is weighed by quality：20 parts of white color dispersible pigment dispersions（The AW PRO+ of diamond company）, 50 parts of Yang Song trade PU2407 trees
Fat, 0.5 part of acid-base modifier AMP-95,5 parts of moisturizer glycerine, 20 parts of moisturizer Isosorbide-5-Nitrae-propylene glycol, 1.5 parts of surfactants
465,0.3 part of surfynol, 607,2.7 parts of surfactant surfynol deionized waters.
Embodiment three
1）It is weighed by quality：20 parts of white color dispersible pigment dispersions（The AW PRO+ of diamond company）, 50 parts are expanded intelligent trade HI-CUT
EP1913 resins, 0.5 part of acid-base modifier AMP-95,5 parts of moisturizer glycerine, 15 parts of moisturizer Isosorbide-5-Nitrae-propylene glycol, 1.2 parts of tables
Face activating agent expands intelligent trade KS1006,0.3 part of surfactant surfynol, 607,8 parts of deionized waters.
Further performance test is made to coating ink made from the method for the present invention below.
One, fluency and the test of standby property
Aqueous white weaving coating ink prepared by above-described embodiment one to three is taken, is given birth in Zhuhai Cheng Jie numeral science and technology Co., Ltd
20 editions are printed on the TS5113 flat-panel printers of 5113 nozzle of use of production, hole of breaking is less than 3 holes；It is produced in Dongguan Xiang Yu companies
The flat-panel printer using DX5 nozzles on print 20 editions, break hole be less than 3 holes.Illustrate that ink of the present invention is printed in mainstream to spray
Fluency is excellent on the printer of head.Temperature is 18-30 DEG C, under conditions of humidity is 40-80%, persistently shuts down 8 days, opens again
Machine is tested, and mesh is intact.
Two, whiteness test and dry and wet wipe test
Same printer upper Du Pont's chalk and chalk of the present invention respectively, other conditions are all identical, print respectively white blocks with
Bai Caitong goes out pattern, test result indifference.
The dry and wet rubbing fastness test of printing fabric, color fastness test result point are carried out with national standard GB/T 3920-2008 methods
It is 5 grades, wherein 1 grade is minimum, 5 grades of highests；In coating textile printing, dry and wet rubbing fastness is more than or equal to 3 grades preferably.Take above-mentioned reality
The coating ink for applying the preparation of example one to three, white blocks and white coloured picture case are printed using the printer of 5113 nozzles on dark cloth,
The dry and wet rubbing fastness test of printing fabric is carried out with national standard GB/T 3920-2008 methods, test result is shown, coating of the present invention
The dry and wet of ink wipes color fastness and is more than 3 grades, has good dry and wet crock fastness.
Above-mentioned test result explanation, coating ink prepared by the present invention adapt to the nozzle printings machine such as DX5,5113, apply completely
The stamp that material ink prints on the fabric is all very excellent in terms of whiteness, water resistance, dry and wet crock fastness.
The present invention is suitable for the digit printing of the dark clothes of materials such as cotton, fiber crops, cotton blend, is applied to the skill of ink-jet ink
Art field.
Although the embodiment of the present invention is described with practical solution, the limit to meaning of the present invention is not constituted
It makes, for those skilled in the art, is all to the modification of its embodiment and with the combination of other schemes according to this specification
Obviously.
Claims (9)
- The coating ink-jet ink 1. a kind of aqueous white is weaved, it is characterised in that：The aqueous white weaving coating ink-jet ink is pressed Mass percent, it is composed of the following components：Dispersible pigment dispersion 30%-50%, resin 20%-40%, curing agent 0.2%-3%, soda acid tune Agent 0.1%-0.5% is saved, moisturizer 10%-30%, surfactant 0.2%-2.0%, fungicide 0.1%-0.2%, surplus is water.
- The coating ink-jet ink 2. aqueous white according to claim 1 is weaved, it is characterised in that：The dispersible pigment dispersion Average grain diameter D50 is not more than 300nm.
- The coating ink-jet ink 3. aqueous white according to claim 1 is weaved, it is characterised in that：The resin solid content is 30-40%, elongation percentage are 500% or more.
- The coating ink-jet ink 4. aqueous white according to claim 1 is weaved, it is characterised in that：The acid-base modifier is At least one of triethanolamine, ammonium hydroxide, sodium hydroxide, AMP-95.
- The coating ink-jet ink 5. aqueous white according to claim 1 is weaved, it is characterised in that：The surfactant is Aqueous nonionic surfactant.
- The coating ink-jet ink 6. aqueous white according to claim 1 is weaved, it is characterised in that：The water is deionization Water.
- The coating ink-jet ink 7. aqueous white according to claim 1 is weaved, it is characterised in that：The moisturizer is sweet Oil, PEG2000, triethylene glycol, 1,5-PD, at least one such as Isosorbide-5-Nitrae-propylene glycol, ten polyglycereol alcohol.
- The coating ink-jet ink 8. aqueous white according to claim 1 is weaved, it is characterised in that：The fungicide is 1,2- Benzisothiazole-3-ketone, BIT-20, at least one of Proxel GXL.
- 9. a kind of preparation method of aqueous white weaving coating ink-jet ink as described in claim 1, it is characterised in that：The system Preparation Method includes the following steps：A, it is uniformly mixed moisturizer, acid-base modifier, surfactant, fungicide, deionized water to obtain mixed liquor；B, it toward resin, curing agent is sequentially added in mixed liquor obtained by step a, is uniformly mixed, ensures stirring more than half an hour；C, dispersible pigment dispersion is added into step b, is uniformly mixed, and be aged four hours；D, PP membrane filtration twice of the gained mixed liquor with aperture precision no more than 0.45 micron in step c, takes filtrate.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810428664.6A CN108753041A (en) | 2018-05-07 | 2018-05-07 | Aqueous white weaving coating ink-jet ink and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810428664.6A CN108753041A (en) | 2018-05-07 | 2018-05-07 | Aqueous white weaving coating ink-jet ink and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108753041A true CN108753041A (en) | 2018-11-06 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810428664.6A Pending CN108753041A (en) | 2018-05-07 | 2018-05-07 | Aqueous white weaving coating ink-jet ink and preparation method thereof |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109337445A (en) * | 2018-11-23 | 2019-02-15 | 山东如意科技集团有限公司 | A kind of digit printing coating ink |
| CN111270532A (en) * | 2020-03-26 | 2020-06-12 | 深圳市墨库图文技术有限公司 | Fluorescent paint ink applied to spinning and preparation method thereof |
| CN112552742A (en) * | 2020-12-09 | 2021-03-26 | 上海大学 | White coating ink for textile inkjet printing and preparation method thereof |
| CN113214705A (en) * | 2020-12-12 | 2021-08-06 | 珠海君奥新材料科技有限公司 | Pyrograph water-based white ink suitable for Epson nozzle and preparation method thereof |
| CN113215839A (en) * | 2020-12-12 | 2021-08-06 | 珠海君奥新材料科技有限公司 | Water-based paint direct-injection white ink suitable for industrial head |
| CN116497613A (en) * | 2023-04-21 | 2023-07-28 | 珠海佳印数码科技有限公司 | High-whiteness non-precipitation white ink for textile coating and application thereof |
Citations (3)
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| CN102702851A (en) * | 2012-06-08 | 2012-10-03 | 东莞劲胜精密组件股份有限公司 | White aqueous jet ink |
| US20130066006A1 (en) * | 2011-09-13 | 2013-03-14 | Seiko Epson Corporation | White ink jet ink for textile printing |
| CN105670387A (en) * | 2016-03-16 | 2016-06-15 | 深圳市墨库图文技术有限公司 | Industrial spray head digital printing coating ink and preparation method thereof |
-
2018
- 2018-05-07 CN CN201810428664.6A patent/CN108753041A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20130066006A1 (en) * | 2011-09-13 | 2013-03-14 | Seiko Epson Corporation | White ink jet ink for textile printing |
| CN102702851A (en) * | 2012-06-08 | 2012-10-03 | 东莞劲胜精密组件股份有限公司 | White aqueous jet ink |
| CN105670387A (en) * | 2016-03-16 | 2016-06-15 | 深圳市墨库图文技术有限公司 | Industrial spray head digital printing coating ink and preparation method thereof |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109337445A (en) * | 2018-11-23 | 2019-02-15 | 山东如意科技集团有限公司 | A kind of digit printing coating ink |
| CN111270532A (en) * | 2020-03-26 | 2020-06-12 | 深圳市墨库图文技术有限公司 | Fluorescent paint ink applied to spinning and preparation method thereof |
| CN112552742A (en) * | 2020-12-09 | 2021-03-26 | 上海大学 | White coating ink for textile inkjet printing and preparation method thereof |
| CN113214705A (en) * | 2020-12-12 | 2021-08-06 | 珠海君奥新材料科技有限公司 | Pyrograph water-based white ink suitable for Epson nozzle and preparation method thereof |
| CN113215839A (en) * | 2020-12-12 | 2021-08-06 | 珠海君奥新材料科技有限公司 | Water-based paint direct-injection white ink suitable for industrial head |
| CN116497613A (en) * | 2023-04-21 | 2023-07-28 | 珠海佳印数码科技有限公司 | High-whiteness non-precipitation white ink for textile coating and application thereof |
| CN116497613B (en) * | 2023-04-21 | 2023-09-22 | 珠海佳印数码科技有限公司 | High-whiteness non-precipitation white ink for textile coating and application thereof |
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| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20181106 |
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| RJ01 | Rejection of invention patent application after publication |