CN108745206A - A kind of reaction kettle of chemical industry solid-liquid reaction goes out material separating device - Google Patents
A kind of reaction kettle of chemical industry solid-liquid reaction goes out material separating device Download PDFInfo
- Publication number
- CN108745206A CN108745206A CN201810659243.4A CN201810659243A CN108745206A CN 108745206 A CN108745206 A CN 108745206A CN 201810659243 A CN201810659243 A CN 201810659243A CN 108745206 A CN108745206 A CN 108745206A
- Authority
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- China
- Prior art keywords
- filter cartridge
- rotating filter
- shell
- solid
- reaction kettle
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000007788 liquid Substances 0.000 title claims abstract description 38
- 239000000463 material Substances 0.000 title claims abstract description 20
- 239000000126 substance Substances 0.000 title claims abstract description 20
- 239000007787 solid Substances 0.000 claims abstract description 33
- NJPPVKZQTLUDBO-UHFFFAOYSA-N novaluron Chemical compound C1=C(Cl)C(OC(F)(F)C(OC(F)(F)F)F)=CC=C1NC(=O)NC(=O)C1=C(F)C=CC=C1F NJPPVKZQTLUDBO-UHFFFAOYSA-N 0.000 claims abstract description 12
- 238000007789 sealing Methods 0.000 claims description 21
- 239000002184 metal Substances 0.000 claims description 7
- 229910052751 metal Inorganic materials 0.000 claims description 7
- 239000012530 fluid Substances 0.000 claims description 5
- 238000009434 installation Methods 0.000 claims description 3
- 238000010586 diagram Methods 0.000 description 4
- 239000000376 reactant Substances 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 230000004888 barrier function Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 239000012295 chemical reaction liquid Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 1
- 239000010931 gold Substances 0.000 description 1
- 229910052737 gold Inorganic materials 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 230000013011 mating Effects 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 230000035515 penetration Effects 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000011343 solid material Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J4/00—Feed or outlet devices; Feed or outlet control devices
- B01J4/001—Feed or outlet devices as such, e.g. feeding tubes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D33/00—Filters with filtering elements which move during the filtering operation
- B01D33/06—Filters with filtering elements which move during the filtering operation with rotary cylindrical filtering surfaces, e.g. hollow drums
- B01D33/067—Construction of the filtering drums, e.g. mounting or sealing arrangements
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D33/00—Filters with filtering elements which move during the filtering operation
- B01D33/06—Filters with filtering elements which move during the filtering operation with rotary cylindrical filtering surfaces, e.g. hollow drums
- B01D33/11—Filters with filtering elements which move during the filtering operation with rotary cylindrical filtering surfaces, e.g. hollow drums arranged for outward flow filtration
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D33/00—Filters with filtering elements which move during the filtering operation
- B01D33/44—Regenerating the filter material in the filter
- B01D33/46—Regenerating the filter material in the filter by scrapers, brushes nozzles or the like acting on the cake-side of the filtering element
- B01D33/461—Regenerating the filter material in the filter by scrapers, brushes nozzles or the like acting on the cake-side of the filtering element brushes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D35/00—Filtering devices having features not specifically covered by groups B01D24/00 - B01D33/00, or for applications not specifically covered by groups B01D24/00 - B01D33/00; Auxiliary devices for filtration; Filter housing constructions
- B01D35/30—Filter housing constructions
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The invention discloses a kind of reaction kettles of chemical industry solid-liquid reaction to go out material separating device, including shell, pedestal, motor, cylinder and axis；It is coaxially arranged with rotating filter cartridge in the shell, rotary shaft is located on the central shaft of rotating filter cartridge, lantern ring is arranged in the rotary shaft, there are two lantern ring settings, connecting rod is fixedly connected on the side wall of two lantern rings, the lower end of connecting rod is fixedly connected on the same inclined collecting board；Brush board is equipped with several bristles contacted with rotating filter cartridge.Liquid is detached solid-liquid in inside by the present invention by rotating filter cartridge with solid, liquid is discharged from bottom, solid in rotating filter cartridge is downward along incline structure, solid is mobile in inside, is collected on it after being obstructed by collecting board, and collecting board is always positioned at lower section, ensure that the solid collected moves down on it, so that solid is discharged out of rotating filter cartridge, need not manually be cleared up, it is time saving and energy saving.
Description
Technical field
The present invention relates to a kind of chemical industry equipment, the reaction kettle of specifically a kind of chemical industry solid-liquid reaction goes out material separating device.
Background technology
Reaction kettle is comprehensive reaction vessel, the design according to reaction condition to reaction kettle structure function and configuration attachment.From
Charging-reaction-discharging of beginning can complete pre-set reaction step with higher the degree of automation, to reacting
Temperature, pressure, mechanics control in journey（Stirring, air blast etc.）, the important parameters such as reactant/product concentration carry out stringent tune
Control.Its structure is generally made of autoclave body, transmission device, agitating device, heating device, cooling device, sealing device.It is corresponding mating
Ancillary equipment：Still, condenser, water knockout drum, collecting tank, filter etc..It is that raw material reacts the reaction used for solid-liquid
Kettle needs the solid for generating internal extra solid or reaction to detach, obtains pure reaction after the completion of reaction
Liquid, but it is not mounted directly separator when existing reaction kettle discharge, it needs after collecting internal liquid together again
It is sent in separation equipment and is detached, increase step, but also product is contacted with extraneous air, influence product quality.
Invention content
The purpose of the present invention is to provide a kind of reaction kettles of chemical industry solid-liquid reaction to go out material separating device, above-mentioned to solve
The problem of being proposed in background technology.
To achieve the above object, the present invention provides the following technical solutions：
A kind of reaction kettle of chemical industry solid-liquid reaction goes out material separating device, including shell, pedestal, motor, cylinder and axis；The bottom
Shell and reaction kettle are set on seat, and shell is inclined cylinder, and a rotary shaft, rotary shaft are provided on the central shaft of the shell
Both ends be rotatably connected in inner walls by bearing, and lower end is pierced by shell, and the lower end of rotary shaft is fixedly connected on electricity
On the output shaft of machine；Rotating filter cartridge is coaxially arranged in the shell, rotary shaft is located on the central shaft of rotating filter cartridge, is rotating
It is fixed with multiple supporting rods between axis and rotating filter cartridge, is provided in the corresponding shell in downside of rotating filter cartridge parallel with central shaft
Sealing plate, offer opening on sealing plate, the rotating filter cartridge is passed down through opening, extend into the lower section of sealing plate, rotation
Turn filter cylinder and sealing plate clearance fit, collecting tank, the corresponding shell lower end connection of collecting tank are set as below the sealing plate
There is fluid discharge pipe；Lantern ring is arranged in the rotary shaft, there are two lantern ring settings, fixed on the side wall of two lantern rings
It is connected with connecting rod, the lower end of connecting rod is fixedly connected on the same inclined collecting board, the corresponding sealing plate in lower end of collecting board
On be communicated with the solids discharge pipe with valve；It is fixed with brush board in the corresponding case top in the top of the rotating filter cartridge, is brushed
Plate is equipped with several bristles contacted with rotating filter cartridge；The bottom of the reaction kettle is communicated with discharge tube, and end passes through flange
It is connected with the metal feed tube extending into shell, the end of metal feed tube, which tilts, to be extend into rotating filter cartridge.
Further：The lower end of the shell is rotatably connected on by axis on pedestal, corresponding immediately below the upper end of shell
Vertical cylinder is fixed on pedestal, the output shaft upper end of cylinder is rotatably connected to contact plate by the axis pin of installation, contact plate
Upper surface is contacted with the bottom of shell.
Further：There are the baffle that central shaft is bent in the left and right ends of the rotating filter cartridge.
Further：It is connected by ball bearing rotational between the lantern ring and rotary shaft.
Further：The clump weight for increasing its weight is fixed on the downside of the collecting board.
Further：The length of the collecting board is the 1/3-1/3 of rotating filter cartridge length.
Further：The upper surface of the collecting board offers several downward deflector chutes.
Further：The deflector chute is uniformly distributed, depth 10-20mm.
Compared with prior art, the beneficial effects of the invention are as follows：The present invention by solid-liquid in inside by rotating filter cartridge by liquid
Body is detached with solid, and liquid is discharged from bottom, and the solid in rotating filter cartridge is downward along incline structure, and solid is mobile in inside, is led to
It is collected on it after crossing collecting board barrier, collecting board is always positioned at lower section, ensures that the solid collected moves down on it, makes solid
Body can be discharged out of rotating filter cartridge, need not manually be cleared up, time saving and energy saving；Device can be connected directly between on reaction kettle,
Reactant need not be taken out and be detached again, ensure product quality.
Description of the drawings
Fig. 1 is the structural schematic diagram that a kind of reaction kettle of chemical industry solid-liquid reaction goes out material separating device.
Fig. 2 is the structural schematic diagram that a kind of reaction kettle of chemical industry solid-liquid reaction goes out collecting board in material separating device.
Fig. 3 is the attachment structure schematic diagram that a kind of reaction kettle of chemical industry solid-liquid reaction goes out contact plate in material separating device.
Fig. 4 is schematic diagram when a kind of reaction kettle of chemical industry solid-liquid reaction goes out material separating device use.
In figure：1- shells, 2- pedestals, 3- reaction kettles, 4- motors, 5- cylinders, 6- axis, 7- discharge tubes, 8- metal feeds
Pipe, 9- rotary shafts, 10- bearings, 11- rotating filter cartridges, 12- sealing plates, 13- supporting rods, 14- lantern rings, 15- connecting rods, 16- are collected
Plate, 17- clump weights, 18- fluid discharge pipes, 19- solids discharge pipes, 20- collecting tanks, 21- brush boards, 22- bristles, 23- deflector chutes,
24- contact plates, 25- axis pins.
Specific implementation mode
Please refer to figure, in the embodiment of the present invention, a kind of reaction kettle of chemical industry solid-liquid reaction goes out material separating device, including shell
Body 1, pedestal 2, motor 4, cylinder 5 and axis 6；Shell 1 and reaction kettle 3 are set on the pedestal 2, and shell 1 is inclined cylinder, shell
The lower end of body 1 is rotatably connected on by axis 6 on pedestal 2, and vertical gas is fixed on corresponding pedestal 2 immediately below the upper end of shell 1
The output shaft upper end of cylinder 5, cylinder 5 is rotatably connected to contact plate 24, the upper surface of contact plate 24 and shell by the axis pin 25 of installation
The bottom of body 1 contacts, and is fitted on shell 1, and opposite can slide, and the upper end of shell 1 is pushed by cylinder 5, makes shell 1
Angle of inclination adjust as needed.
A rotary shaft 9 is provided on the central shaft of the shell 1, the both ends of rotary shaft 9 are rotatably connected on by bearing 10
On 1 inner wall of shell, and lower end is pierced by shell 1, and the lower end of rotary shaft 9 is fixedly connected on the output shaft of motor 4, passes through motor
4 driving rotary shafts 9 rotate.
Rotating filter cartridge 11 is coaxially arranged in the shell 1, rotating filter cartridge 11 is process by strainer, rotating filter cartridge 11
There are the baffle that central shaft is bent in left and right ends, and make liquid that can be located in rotating filter cartridge 11, rotary shaft 9 is located at rotating filter cartridge
On 11 central shaft, it is fixed with multiple supporting rods 13 between rotary shaft 9 and rotating filter cartridge 11, rotating filter cartridge 11 is made to follow rotation
Axis 9 rotates, and is provided with the sealing plate 12 parallel with central shaft in the corresponding shell in the downside of rotating filter cartridge 11 1, on sealing plate 12
Opening is offered, the rotating filter cartridge 11 is passed down through opening, extend into the lower section of sealing plate 12, rotating filter cartridge 11 and sealing
12 clearance fit of plate, so that rotating filter cartridge 11 is extend into sealing plate 12 does not influence rotating filter cartridge 11 rotation of itself, the sealing
The lower section of plate 12 is set as collecting tank 20, for collecting filtered liquid on rotating filter cartridge 11,20 corresponding shell 1 of collecting tank
Lower end is communicated with fluid discharge pipe 18, and the liquid after separation is collected.
It is arranged with lantern ring 14 in the rotary shaft 9, so that rotary shaft 9 is relatively rotated with lantern ring 14, it is preferred that lantern ring 14
It is connect by ball bearing rotational between rotary shaft 9, there are two the settings of lantern ring 14, fixed on the side wall of two lantern rings 14 to connect
It is connected to connecting rod 15, the lower end of connecting rod 15 is fixedly connected on the same inclined collecting board 16, and collecting board 16 and rotary shaft 9 are flat
Row, the downside of collecting board 16 are fixed with the clump weight 17 for increasing its weight, remain collecting board 16 the lower section of rotary shaft 9 not
Dynamic, the length of collecting board 16 is the 1/3-1/3 of 11 length of rotating filter cartridge, can obstruct the solid fallen from above, solid is made to fall
On collecting board 16, several downward deflector chutes 23 are offered in the upper surface of collecting board 16, make solid and a part of liquid
Body moves down on collecting board 16, and deflector chute 23 is uniformly distributed, and the lower end of depth 10-20mm, collecting board 16 are corresponding
The solids discharge pipe 19 with valve is communicated on sealing plate 12, the solid material for storing a period of time can be by solids discharge pipe
19 discharges；It is fixed with brush board 21 on corresponding 1 top of shell in the top of the rotating filter cartridge 11, the width of brush board 21 is more than rotation
Turn the width of filter cylinder 11, brush board 21 is equipped with several bristles 22 contacted with rotating filter cartridge 11, by the solid on rotating filter cartridge 11
Brush is lower to be detached from, convenient for falling on collecting board 16.
The bottom of the reaction kettle 3 is communicated with discharge tube 7, and end has the gold extending into shell 1 by flanged joint
Belong to feed pipe 8, the end of metal feed tube 8, which tilts, to be extend into rotating filter cartridge 11, and the material that reaction kettle 3 is discharged is sent to rotation
Turn in filter cylinder 11.
In use, liquid is sent to by discharge tube 7 in shell 1 after reaction in reaction kettle 3, sprayed from metal feed tube 8
It is mapped in rotating filter cartridge 11, motor 4 drives rotating filter cartridge 11 to rotate, and falls the solid-liquid in rotating filter cartridge 11, is made by its rotation
Its penetration by liquid rotating filter cartridge 11 drops into the collecting tank 20 of lower section, and liquid is discharged by fluid discharge pipe 18, is filtered in rotation
Solid in cylinder 11 follows be moved to top after, fallen after by its own gravity, since rotating filter cartridge 11 is to tilt, make internal consolidate
Body constantly moves down, and the solid fallen when above collecting board 16 is fallen on collecting board 16, is sent downwards along collecting board 16
Enter 19 position of the solids discharge pipe collection to its lower end, be discharged finally by solids discharge pipe 19, the bristle 22 of top will rotate
It is adhered under solid particle brush on filter cylinder 11, avoids solids adhering on rotating filter cartridge 11, be convenient for blanking.The present invention will be including solid-liquid
Portion is detached liquid with solid by rotating filter cartridge, and liquid is discharged from bottom, and the solid in rotating filter cartridge is downward along incline structure,
Solid is mobile in inside, is collected on it after being obstructed by collecting board, and collecting board is always positioned at lower section, ensures that the solid collected exists
It moves down thereon, solid is enable to be discharged out of rotating filter cartridge, need not manually be cleared up, it is time saving and energy saving；Device can be straight
It is connected on reaction kettle in succession, reactant need not be taken out and be detached again, ensure product quality.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped
Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should
It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
The other embodiment being appreciated that.
Claims (8)
1. a kind of reaction kettle of chemical industry solid-liquid reaction goes out material separating device, including shell（1）, pedestal（2）, motor（4）, cylinder
（5）And axis（6）；The pedestal（2）Upper setting shell（1）And reaction kettle（3）, which is characterized in that shell（1）For inclined circle
Cylinder, the shell（1）Central shaft on be provided with a rotary shaft（9）, rotary shaft（9）Both ends pass through bearing（10）Rotation connection
In shell（1）On inner wall, and lower end is pierced by shell（1）, rotary shaft（9）Lower end be fixedly connected on motor（4）Output shaft
On；The shell（1）Inside it is coaxially arranged with rotating filter cartridge（11）, rotary shaft（9）Positioned at rotating filter cartridge（11）Central shaft on,
Rotary shaft（9）With rotating filter cartridge（11）Between be fixed with multiple supporting rods（13）, rotating filter cartridge（11）The corresponding shell in downside
（1）Inside it is provided with the sealing plate parallel with central shaft（12）, sealing plate（12）On offer opening, the rotating filter cartridge（11）
It is passed down through opening, extend into sealing plate（12）Lower section, rotating filter cartridge（11）With sealing plate（12）Clearance fit, the sealing
Plate（12）Lower section be set as collecting tank（20）, collecting tank（20）Corresponding shell（1）Lower end is communicated with fluid discharge pipe（18）；
In the rotary shaft（9）On be arranged with lantern ring（14）, lantern ring（14）There are two settings, two lantern rings（14）Side wall on it is solid
Surely it is connected with connecting rod（15）, connecting rod（15）Lower end be fixedly connected on the same inclined collecting board（16）On, collecting board（16）
The corresponding sealing plate in lower end（12）On be communicated with the solids discharge pipe with valve（19）；In the rotating filter cartridge（11）Top
Corresponding shell（1）Brush board is fixed on top（21）, brush board（21）It is equipped with several and rotating filter cartridge（11）The bristle of contact
（22）；The reaction kettle（3）Bottom be communicated with discharge tube（7）, end extend into shell by flanged joint（1）Interior
Metal feed tube（8）, metal feed tube（8）End tilt extend into rotating filter cartridge（11）In.
2. a kind of reaction kettle of chemical industry solid-liquid reaction according to claim 1 goes out material separating device, it is characterised in that：Institute
State shell（1）Lower end pass through axis（6）It is rotatably connected on pedestal（2）On, shell（1）Upper end immediately below corresponding pedestal（2）
The vertical cylinder of upper fixation（5）, cylinder（5）The output shaft upper end axis pin that passes through installation（25）It is rotatably connected to contact plate
（24）, contact plate（24）Upper surface and shell（1）Bottom contact.
3. going out material separating device according to a kind of reaction kettle of chemical industry solid-liquid reaction described in claim 1, it is characterised in that：It is described
Rotating filter cartridge（11）Left and right ends have central shaft bend baffle.
4. going out material separating device according to a kind of reaction kettle of chemical industry solid-liquid reaction described in claim 1, it is characterised in that：It is described
Lantern ring（14）With rotary shaft（9）Between connected by ball bearing rotational.
5. going out material separating device according to a kind of reaction kettle of chemical industry solid-liquid reaction described in claim 1, it is characterised in that：It is described
Collecting board（16）Downside be fixed with increase its weight clump weight（17）.
6. going out material separating device according to a kind of reaction kettle of chemical industry solid-liquid reaction described in claim 1, it is characterised in that：It is described
Collecting board（16）Length be rotating filter cartridge（11）The 1/3-1/3 of length.
7. going out material separating device according to a kind of reaction kettle of chemical industry solid-liquid reaction described in claim 1, it is characterised in that：It is described
Collecting board（16）Upper surface offer several downward deflector chutes（23）.
8. the reaction kettle according to a kind of chemical industry solid-liquid reaction described in claim 7 goes out material separating device, it is characterised in that：It is described
Deflector chute（23）It is uniformly distributed, depth 10-20mm.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810659243.4A CN108745206A (en) | 2018-06-25 | 2018-06-25 | A kind of reaction kettle of chemical industry solid-liquid reaction goes out material separating device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810659243.4A CN108745206A (en) | 2018-06-25 | 2018-06-25 | A kind of reaction kettle of chemical industry solid-liquid reaction goes out material separating device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108745206A true CN108745206A (en) | 2018-11-06 |
Family
ID=63977131
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810659243.4A Pending CN108745206A (en) | 2018-06-25 | 2018-06-25 | A kind of reaction kettle of chemical industry solid-liquid reaction goes out material separating device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108745206A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110652774A (en) * | 2019-11-14 | 2020-01-07 | 佛山市绿尔压滤机设备有限公司 | Solid-liquid separation device |
| CN110917699A (en) * | 2020-01-07 | 2020-03-27 | 黄河水利职业技术学院 | Sewage treatment device and treatment method thereof |
| CN112237757A (en) * | 2019-07-17 | 2021-01-19 | 青岛迪美热电设备有限公司 | Emulsion filter |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112237757A (en) * | 2019-07-17 | 2021-01-19 | 青岛迪美热电设备有限公司 | Emulsion filter |
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| CN110917699A (en) * | 2020-01-07 | 2020-03-27 | 黄河水利职业技术学院 | Sewage treatment device and treatment method thereof |
| CN110917699B (en) * | 2020-01-07 | 2020-09-04 | 黄河水利职业技术学院 | Sewage treatment device and treatment method thereof |
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Application publication date: 20181106 |