CN108714407A - A kind of industrial chemicals reaction unit - Google Patents

A kind of industrial chemicals reaction unit Download PDF

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Publication number
CN108714407A
CN108714407A CN201810539798.5A CN201810539798A CN108714407A CN 108714407 A CN108714407 A CN 108714407A CN 201810539798 A CN201810539798 A CN 201810539798A CN 108714407 A CN108714407 A CN 108714407A
Authority
CN
China
Prior art keywords
wall
bolted
reaction kettle
industrial chemicals
welded
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201810539798.5A
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Chinese (zh)
Inventor
张彦之
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Zhengzhou Lidiya Medicine Technology Co Ltd
Original Assignee
Zhengzhou Lidiya Medicine Technology Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Zhengzhou Lidiya Medicine Technology Co Ltd filed Critical Zhengzhou Lidiya Medicine Technology Co Ltd
Priority to CN201810539798.5A priority Critical patent/CN108714407A/en
Publication of CN108714407A publication Critical patent/CN108714407A/en
Pending legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/0066Stirrers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00074Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Mixers Of The Rotary Stirring Type (AREA)

Abstract

The invention discloses a kind of industrial chemicals reaction units, including support plate, the support plate top exterior walls are welded with support leg, reaction kettle has been bolted in the support leg top exterior walls, and reaction kettle shell is made of anti-corrosion material, baroceptor has been bolted in reaction kettle side inner wall, and baroceptor is internally provided with microprocessor, reaction kettle side outer wall is provided with opening one, and catheter has been bolted in opening one, pulsometer has been bolted in catheter side outer wall, heater has been bolted on the inner wall of the catheter side.Industrial chemicals is effectively sufficiently stirred by the present invention, improve the utilization rate of industrial chemicals, the time of people is saved, the working efficiency for accelerating people accelerates the time of industrial chemicals reaction, and it is also prevented from raw material and leads to the damage of raw material because reacting slow, the waste to industrial chemicals is avoided, resource has been saved.

Description

A kind of industrial chemicals reaction unit
Technical field
The present invention relates to chemical equipment technical field more particularly to a kind of industrial chemicals reaction units.
Background technology
Reaction kettle is that one kind being widely used in oil, chemical industry, rubber, pesticide, dyestuff, medicine, food, for completing sulphur The pressure vessel of the technical process such as change, nitrification, hydrogenation, hydrocarbonylation, polymerization, condensation.
In order to promote the reaction speed in reaction kettle and effect, existing reaction kettle to be arranged one at axis generally in tank body A stirring special axis, upper end are connect with the electric machine assembly for being arranged on tank body top, but in reaction kettle operational process, reaction kettle Inside stir evenly it is uneven, reaction it is insufficient, to influence working efficiency, traditional temperature control method is fired by medium It burns acquisition heat to heat up to raw material from bottom, this method not only makes heat be unevenly distributed, but also temperature control is tired Difficulty, easily cause raw material heating temperature unevenness and overheat eventually lead to raw material stoving it is bad in addition damage, traditional stirring means Mostly use it is artificial, it is time-consuming and laborious, and the uniformity stirred is difficult to control, existing reaction kettle there is no the device of secondary agitation, Many raw materials are wasted, therefore, there is an urgent need for a kind of industrial chemicals reaction units of design to solve the above problems.
Invention content
The purpose of the present invention is to solve disadvantages existing in the prior art, and a kind of industrial chemicals reaction dress proposed It sets.
To achieve the goals above, present invention employs following technical solutions:
A kind of industrial chemicals reaction unit, including support plate, the support plate top exterior walls are welded with support leg, the support leg Reaction kettle has been bolted in top exterior walls, and reaction kettle shell is made of anti-corrosion material, and reaction kettle side inner wall is logical It crosses and has been bolted baroceptor, and baroceptor is internally provided with microprocessor, reaction kettle side outer wall is set It is equipped with opening one, and catheter has been bolted in opening one, air pressure has been bolted in catheter side outer wall It pumps, heater has been bolted on the inner wall of the catheter side, reaction kettle side outer wall has been bolted Temperature sensor, the reaction kettle top exterior walls are provided with opening two, and opening two is threaded with feed pipe, the reaction kettle Motor has been bolted in top exterior walls, and Rotational Cylindrical, the Rotational Cylindrical both sides are welded on the outer wall of the motor output shaft Outer wall is welded with the equidistant connecting rod being distributed in a ring, and the connecting rod is welded on one end outer wall far from Rotational Cylindrical and stirs Paddle is mixed, reaction kettle both sides inner wall is welded with striker plate, and striker plate cross section is triangular in shape, and the Rotational Cylindrical is far from electricity One end of machine is welded with turntable, and the turntable surrounding outer wall is welded with the stirring rod being distributed in a ring.
Preferably, reaction kettle side outer wall has been bolted control panel, and control panel and heater it Between be electrically connected.
Preferably, sealing cover, and the specification and feed pipe of sealing cover has been bolted in the reaction kettle top exterior walls Specification be adapted, the surrounding of sealing cover is pasted with sealing strip.
Preferably, liquid level gauge has been bolted in reaction kettle side outer wall, and connects inside liquid level gauge and reaction kettle It is logical.
Preferably, vibrating motor has been bolted in reaction kettle both sides outer wall, and two vibrating motors are mutual Symmetrically.
Preferably, reaction kettle side outer wall is provided with opening three, and water-supply-pipe has been bolted in opening three.
Preferably, water-supply-pipe side outer wall is provided with mounting hole, and valve has been bolted in mounting hole.
Preferably, the agitating paddle outer wall is provided with poke hole, and the diameter of poke hole is identical.
Beneficial effects of the present invention are:
1, by the agitating paddle of setting, effectively industrial chemicals is sufficiently stirred, improves the utilization rate of industrial chemicals, is saved About the time of people, accelerate the working efficiency of people.
2, by the heater of setting, industrial chemicals can effectively be heated, it is anti-to accelerate industrial chemicals The time answered, and be also prevented from raw material and lead to the damage of raw material because reacting slow.
3, by the pulsometer of setting, the industrial chemicals that can will be left in bottom is again stirring for, is avoided to chemical industry The waste of raw material, has saved resource.
Description of the drawings
Fig. 1 is a kind of structural schematic diagram of industrial chemicals reaction unit proposed by the present invention;
Fig. 2 is a kind of agitating paddle structural schematic diagram of industrial chemicals reaction unit proposed by the present invention;
Fig. 3 is a kind of turntable structure schematic diagram of industrial chemicals reaction unit proposed by the present invention.
In figure:1 support plate, 2 support legs, 3 reaction kettles, 4 baroceptors, 5 heaters, 6 pulsometers, 7 temperature sensors, 8 control panels, 9 feed pipes, 10 sealing covers, 11 motors, 12 Rotational Cylindricals, 13 liquid level gauges, 14 agitating paddles, 15 connecting rods, 16 vibrations Motor, 17 striker plates, 18 stirring rods, 19 water-supply-pipes, 20 valves, 21 turntables, 22 poke holes, 23 catheters.
Specific implementation mode
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete Site preparation describes, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.
Referring to Fig.1-3, a kind of industrial chemicals reaction unit, including support plate 1,1 top exterior walls of support plate are welded with support Leg 2, reaction kettle 3 has been bolted in 2 top exterior walls of support leg, and 3 shell of reaction kettle is made of anti-corrosion material, reaction kettle 3 Baroceptor 4 has been bolted in side inner wall, and baroceptor 4 is internally provided with microprocessor, air pressure sensing Device 4 can effectively detect the air pressure in reaction kettle 3, and 3 side outer wall of reaction kettle is provided with opening one, and opening one passes through bolt It is connected with catheter 23,23 side outer wall of catheter has been bolted pulsometer 6, has passed through spiral shell on 23 side inner wall of catheter It tethers and is connected to heater 5, heater 5 can heat the liquid in catheter 23, and 3 side outer wall of reaction kettle passes through bolt It is connected with temperature sensor 7,3 top exterior walls of reaction kettle are provided with opening two, and opening two is threaded with feed pipe 9, react Motor 11 has been bolted in 3 top exterior walls of kettle, and Rotational Cylindrical 12,12 liang of Rotational Cylindrical are welded on the outer wall of 11 output shaft of motor Side outer wall is welded with the equidistant connecting rod 15 being distributed in a ring, and connecting rod 15 is welded on one end outer wall far from Rotational Cylindrical 12 There is agitating paddle 14,3 both sides inner wall of reaction kettle is welded with striker plate 17, and 17 cross section of striker plate is triangular in shape, striker plate 17 The stirring of industrial chemicals can effectively be helped, the one end of Rotational Cylindrical 12 far from motor 3 is welded with turntable 21, outside 21 surrounding of turntable Wall is welded with the stirring rod 18 being distributed in a ring.
In the present invention, control panel 8, and control panel 8 and heater 5 has been bolted in 3 side outer wall of reaction kettle Between be electrically connected, sealing cover 10, and the specification of sealing cover 10 and charging has been bolted in 3 top exterior walls of reaction kettle The specification of pipe 9 is adapted, and the surrounding of sealing cover 10 is pasted with sealing strip, and reaction kettle is effectively sealed by sealing cover 10, Liquid level gauge 13 has been bolted in 3 side outer wall of reaction kettle, and liquid level gauge 13 is connected to 3 inside of reaction kettle, 3 both sides of reaction kettle Vibrating motor 16 has been bolted in outer wall, and two vibrating motors 16 are symmetrical, and 3 side outer wall of reaction kettle is provided with Opening three, and water-supply-pipe 19 has been bolted in opening three, 19 side outer wall of water-supply-pipe is provided with mounting hole, and mounting hole passes through It is bolted valve 20,14 outer wall of agitating paddle is provided with poke hole 22, and the diameter of poke hole 22 is identical, and poke hole 22 can have Industrial chemicals is stirred by effect.
Operation principle:In use, industrial chemicals is added out of feed pipe 9 in reaction kettle 3 user, start motor 11, The output shaft of motor 11 drives Rotational Cylindrical 12 to be rotated, and the drive agitating paddle 14 of Rotational Cylindrical 12 and stirring rod 18 are stirred and turn It is dynamic, it opens valve 20 and water is allowed to flow into reaction kettle 3 out of water-supply-pipe 19, the liquid in 3 bottom of reaction kettle is flowed by pulsometer 6 In catheter 23, heater 5 heats the liquid in catheter 23 by control panel 8, and baroceptor 4 can will be anti- Answer the air pressure in kettle 3 to be shown on control panel 8, Vibration on Start-up motor 16 by the chemical granule for being adsorbed on reaction kettle inner wall shake into In reaction kettle 3.
The foregoing is only a preferred embodiment of the present invention, but scope of protection of the present invention is not limited thereto, Any one skilled in the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention and its Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.

Claims (8)

1. a kind of industrial chemicals reaction unit, including support plate(1), which is characterized in that the support plate(1)Top exterior walls are welded There is support leg(2), the support leg(2)Reaction kettle has been bolted in top exterior walls(3), and reaction kettle(3)Shell is by preventing Rotten material is made, the reaction kettle(3)Baroceptor has been bolted in side inner wall(4), and baroceptor(4)It is interior Portion is provided with microprocessor, the reaction kettle(3)Side outer wall is provided with opening one, and opening one has been bolted and has led Liquid pipe(23), the catheter(23)Pulsometer has been bolted in side outer wall(6), the catheter(23)Side inner wall On heater has been bolted(5), the reaction kettle(3)Temperature sensor has been bolted in side outer wall(7), institute State reaction kettle(3)Top exterior walls are provided with opening two, and opening two is threaded with feed pipe(9), the reaction kettle(3)Top Motor has been bolted in outer wall(11), the motor(11)It is welded with Rotational Cylindrical on the outer wall of output shaft(12), described turn Dynamic column(12)Both sides outer wall is welded with the equidistant connecting rod being distributed in a ring(15), the connecting rod(15)Far from Rotational Cylindrical (12)One end outer wall on be welded with agitating paddle(14), the reaction kettle(3)Both sides inner wall is welded with striker plate(17), and keep off Flitch(17)Cross section is triangular in shape, the Rotational Cylindrical(12)Far from motor(11)One end be welded with turntable(21), described turn Disk(21)Surrounding outer wall is welded with the stirring rod being distributed in a ring(18).
2. a kind of industrial chemicals reaction unit according to claim 1, which is characterized in that the reaction kettle(3)Outside side Control panel has been bolted in wall(8), and control panel(8)With heater(5)Between be electrically connected.
3. a kind of industrial chemicals reaction unit according to claim 1, which is characterized in that the reaction kettle(3)Outside top Sealing cover has been bolted in wall(10), and sealing cover(10)Specification and feed pipe(9)Specification be adapted, sealing cover (10)Surrounding be pasted with sealing strip.
4. a kind of industrial chemicals reaction unit according to claim 1, which is characterized in that the reaction kettle(3)Outside side Liquid level gauge has been bolted in wall(13), and liquid level gauge(13)With reaction kettle(3)Inside connection.
5. a kind of industrial chemicals reaction unit according to claim 1, which is characterized in that the reaction kettle(3)Outside both sides Vibrating motor has been bolted in wall(16), and two vibrating motors(16)Symmetrically.
6. a kind of industrial chemicals reaction unit according to claim 1, which is characterized in that the reaction kettle(3)Outside side Wall is provided with opening three, and water-supply-pipe has been bolted in opening three(19).
7. a kind of industrial chemicals reaction unit according to claim 6, which is characterized in that the water-supply-pipe(19)Outside side Wall is provided with mounting hole, and valve has been bolted in mounting hole(20).
8. a kind of industrial chemicals reaction unit according to claim 1, which is characterized in that the agitating paddle(14)Outer wall is opened There is poke hole(22), and poke hole(22)Diameter it is identical.
CN201810539798.5A 2018-05-30 2018-05-30 A kind of industrial chemicals reaction unit Pending CN108714407A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201810539798.5A CN108714407A (en) 2018-05-30 2018-05-30 A kind of industrial chemicals reaction unit

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Application Number Priority Date Filing Date Title
CN201810539798.5A CN108714407A (en) 2018-05-30 2018-05-30 A kind of industrial chemicals reaction unit

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Publication Number Publication Date
CN108714407A true CN108714407A (en) 2018-10-30

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CN201810539798.5A Pending CN108714407A (en) 2018-05-30 2018-05-30 A kind of industrial chemicals reaction unit

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114832757A (en) * 2022-04-22 2022-08-02 正大制药(青岛)有限公司 Preparation method for producing flucalcitol

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20030223917A1 (en) * 2002-05-31 2003-12-04 Seoung-Cheol Yang Batch-type polyester polymerization apparatus
CN205340769U (en) * 2015-12-18 2016-06-29 上海上萃精细化工有限公司 Outer heating device of reation kettle
CN106925195A (en) * 2015-12-31 2017-07-07 中国石油天然气股份有限公司 A kind of hydro-thermal method prepares the device of powder body material
CN107029605A (en) * 2017-03-22 2017-08-11 无锡职业技术学院 A kind of oscillatory type quick mixer

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20030223917A1 (en) * 2002-05-31 2003-12-04 Seoung-Cheol Yang Batch-type polyester polymerization apparatus
CN205340769U (en) * 2015-12-18 2016-06-29 上海上萃精细化工有限公司 Outer heating device of reation kettle
CN106925195A (en) * 2015-12-31 2017-07-07 中国石油天然气股份有限公司 A kind of hydro-thermal method prepares the device of powder body material
CN107029605A (en) * 2017-03-22 2017-08-11 无锡职业技术学院 A kind of oscillatory type quick mixer

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
王松汉: "《石油化工设计手册 第3卷》", 31 January 2002 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114832757A (en) * 2022-04-22 2022-08-02 正大制药(青岛)有限公司 Preparation method for producing flucalcitol

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Application publication date: 20181030

RJ01 Rejection of invention patent application after publication