CN108703409A - A kind of nicotinic alcohol browning inhibitor solution manufacturing method and application - Google Patents
A kind of nicotinic alcohol browning inhibitor solution manufacturing method and application Download PDFInfo
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- CN108703409A CN108703409A CN201810362546.XA CN201810362546A CN108703409A CN 108703409 A CN108703409 A CN 108703409A CN 201810362546 A CN201810362546 A CN 201810362546A CN 108703409 A CN108703409 A CN 108703409A
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- browning
- nicotinic alcohol
- inhibition agent
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/20—Biochemical treatment
Abstract
The present invention discloses a kind of nicotinic alcohol browning inhibitor solution manufacturing method and application.The piece nicotinic alcohol browning inhibition agent solution of the present invention is by including being made containing following raw material：5~30g/L of sodium sulfite, 10~30g/L of sodium citrate, EDTA10~30g/L, 6~12g/L of ascorbic acid, 1~10g/L of Amadori compounds.Sodium nitrite and ascorbic acid in the roasting piece nicotinic alcohol browning inhibition agent solution are good biological anti-oxidants, the progress of mailland reaction can be effectively relieved, and prevent from leading to polyphenol oxidative dimerization due to oxidation；Sodium citrate, EDTA, Amadori compound can effectively inhibit polyphenol oxidase activity, and enzymatic browning is inhibited to carry out, and effectively inhibit the generation of brown stain during piece nicotinic alcohol.The alcoholization quality of tobacco leaf can be promoted simultaneously so that the aroma quality of alcoholization piece cigarette is more preferable, fragrance is more sufficient.
Description
Technical field
The present invention relates to tobacco mellowing technical fields, more particularly to a kind of nicotinic alcohol browning inhibitor solution manufacturing method
With application.
Background technology
Tobacco mellowing, refer to ripe harvesting tobacco leaf through overbaking and redrying after, by controlling certain humiture,
Allow it that a process of chemical change occurs under artificial condition or natural conditions.The alcoholization processing of tobacco leaf is that cigarette industry produced
An important process in journey has a very important significance to improving cigarette quality and reinforcing cost control.It is various in tobacco leaf
By alcoholization processing many chemical changes and biochemical reaction will occur for chemical composition, to reduce redried leaf tobacco
Some mass defects, keep tabacco fragrance stronger, sucking quality significantly improves.
During the alcoholization of tobacco leaf, the color due to being influenced tobacco leaf by factors such as environment temperature and humidities can slowly be deepened,
Brown stain occurs, or even becomes black, with the increase of Zhong Yan companies raw tobacco material storage in recent years, part tobacco leaf is due to for a long time
Alcoholization cause tobacco leaf brown stain serious, brown stain can to refine piece cigarette color and luster impact, influence the quality of cigarette products, it is heavier
What is wanted is that part alcoholization piece cigarette brown stain seriously cannot be used for cigarette products production, can only manually be destroyed, be looked forward to cigarette industry
Industry causes great loss.
The approach for refining the generation brown stain of piece cigarette is caused mainly to have enzymatic browning and non-enzymatic browning, wherein non-enzymatic browning packet
It includes；Maillard reaction, caramelization, Ascorbic Acid Oxidation decompose, four type of polyphenol oxidative dimerization, in tobacco leaf
Brown stain was aged in flue-cured tobacco naturally mainly caused by enzymatic browning and mailland reaction, polyphenol oxidative dimerization
Cheng Zhong, reasonable controlled Maillard reaction and polyphenol oxidative dimerization carry out in enzymatic reaction relevant enzyme it is active with react
Condition makes tobacco leaf not only improve the formation of the improvement and very popular taste of alcoholization piece cigarette quality during alcoholization, again anti-limited step cigarette
It is lost caused by refining brown stain.
Invention content
In order to overcome the disadvantages and deficiencies of the prior art, the primary purpose of the present invention is that providing piece nicotinic alcohol browning inhibition
Agent solution.The solution can reduce the generation of brown stain during effectively inhibition piece nicotinic alcohol, increase the alcoholization quality of piece cigarette.
The present invention provides a kind of nicotinic alcohol browning inhibition agent solution, the solution includes following component：Sodium sulfite 5
~30g/L, 10~30g/L of sodium citrate, EDTA10~30g/L, 6~12g/L of ascorbic acid, 1~10g/ of Amadori compounds
L。
In the preferred embodiment of the present invention, the solution includes following component：10~25g/L of sodium sulfite, lemon
Sour 15~25g/L of sodium, EDTA13~25g/L, 7~11g/L of ascorbic acid, 2~8g/L of Amadori compounds.
In another preferred embodiment of the present invention, the solution includes following component：15~20g/L of sodium sulfite, lemon
18~22g/L of lemon acid sodium, EDTA17~22/L, 8~10g/L of ascorbic acid, 4~6g/L of Amadori compounds.
In another preferred embodiment of the present invention, the solution includes following component：Sodium sulfite 16g/L, citric acid
Sodium 19g/L, EDTA20g/L, ascorbic acid 9g/L, Amadori compound 5g/L.
In another preferred embodiment of the present invention, dilute hydrochloric acid solution 0.01mol/L is also contained in the solution.
In another preferred embodiment of the present invention, the pH of the solution is about 6.
Another object of the present invention is to provide the preparation methods of the piece nicotinic alcohol browning inhibition agent solution.
The preparation method of the piece nicotinic alcohol browning inhibition agent solution, includes the following steps：
A, 5~30g/L of sodium sulfite is weighed with quality and 10~30g/L of sodium citrate is soluble in water, stirred to all molten
Solution, is configured to a liquid；
B, it is soluble in water that 10~30g/L of EDTA are weighed, stirs to whole dissolvings, is configured to b liquid；
C, it is soluble in water to weigh 1~10g/L of Amadori compounds, stirs to whole dissolvings, is configured to c liquid；
D, a liquid, b liquid and c liquid are mixed, stirs evenly, is configured to d liquid；
E, weigh 6~12g/L of ascorbic acid, pour into d liquid, stir evenly, with acid solution adjust pH to 6 or so, constant volume,
Up to the piece nicotinic alcohol browning inhibition agent solution.
In the preferred embodiment of the present invention, the amount that sodium sulfite is weighed in the step A is 10~25g/L, preferably
15~20g/L；The amount of sodium citrate is 15~25g/L, preferably 18~22g/L.
The present invention another preferred embodiment in, weighed in the step B EDTA amount be 13~25g/L, preferably 17
~22/L.
In another preferred embodiment of the present invention, the amount that Amadori compounds are weighed in the step C is 2~8g/L,
It is preferred that 4~6g/L.
In another preferred embodiment of the present invention, the amount that ascorbic acid is weighed in the step E is 7~11g/L, preferably
8~10g/L.
In another preferred embodiment of the present invention, the condition stirred evenly described in the step D or E be with 80~
120r/min is stirred evenly.
In another preferred embodiment of the present invention, the acid solution described in step E is selected from：Hydrochloric acid or sulfuric acid.
In another preferred embodiment of the present invention, the acid solutions described in step E are 0.01mol/L.
In another preferred embodiment of the present invention, the preparation method of the piece nicotinic alcohol browning inhibition agent solution, packet
Include following steps：
A, sodium sulfite 16g/L is weighed with quality and sodium citrate 19g/L is soluble in water, stirring to whole dissolvings is prepared
At a liquid；
B, it is soluble in water that EDTA 20g/L are weighed, stirs to whole dissolvings, is configured to b liquid；
C, it is soluble in water to weigh Amadori compounds 5g/L, stirs to whole dissolvings, is configured to c liquid；
D, a liquid, b liquid and c liquid are mixed, stirs evenly, is configured to d liquid；
E, ascorbic acid 9g/L is weighed, pours into d liquid, stirs evenly, it is left to adjust pH to 6 with 0.01mol/L hydrochloric acid solutions
The right side is settled to 1000ml to get the piece nicotinic alcohol browning inhibition agent solution.
Second object of the present invention is to provide described nicotinic alcohol browning inhibition agent solution in flue-cured tobacco preparation process
Application.
In the preferred embodiment of the present invention, described nicotinic alcohol browning inhibition agent solution is in flue-cured tobacco preparation process
Using refer to reduce cured tobacco leaf fade in application.
In another preferred embodiment of the present invention, the piece cigarette is different producing area, whole grade pieces of different cultivars
Cigarette.
In another preferred embodiment of the present invention, the flue-cured tobacco cultivars of the preparation are cloud and mist 87.
Third object of the present invention is to provide the application process of the piece nicotinic alcohol browning inhibition agent solution.
The application process of the piece nicotinic alcohol browning inhibition agent solution, includes the following steps：
(1) tobacco purchasing is completed, and the tobacco leaf hot wind leaves moisting process in beating and double roasting stage, tobacco leaf material is fed by arrival end,
It is acted on by harrow nail in the rotation of leaves moisting machine cylinder and cylinder, tobacco leaf is rolled from entrance to outlet；
(2) steam and water spout are placed respectively in the entrance of tobacco leaf moisting machine and outlet, with nicotinic alcohol browning inhibition agent solution generation
For the water setting circulating air system of tobacco leaf moisting machine, the water vapour pressure in tobacco leaf moisting machine in air shows water vapor pressure more than tobacco leaf
Power, temperature show temperature higher than tobacco leaf, are conducive to the attachment of nicotinic alcohol browning inhibition agent solution and show with tobacco leaf while reaching tobacco leaf
Warming and humidifying effect；
(3) it checks nicotinic alcohol browning inhibition agent solution surplus, is replenished in time；
(4) after piece cigarette completes hot wind leaves moisting program, leaf stalk separation is carried out, storage and the natural alcoholization of smoked sheet are then carried out.
In the preferred embodiment of the present invention, the piece nicotinic alcohol browning inhibition agent solution is the piece cigarette that will be prepared
Refine browning inhibition agent solution and dilutes the solution after 20~30 times；
The principle of the present invention is：
Sodium sulfite conduct is widely used and effective nonenzymatic browning reaction inhibitor.The carbonyl of Maillard reaction products can be with
It is combined with inferior sulfate radical and forms additive compound, addition product can be condensed with amino-compound, but condensation product cannot be again into one
Step generates alkali and a glucosyl group amine, prevents the further generation of Maillard reaction, thus has apparent inhibition.It is anti-bad
Hematic acid, as reducing agent, can generate reduction, certain intermediate reactions be prevented or slow down, to avoid or reduce with sodium sulfite
The generation of browning substances.Sodium citrate and EDTA are two different metal-chelators, and wherein sodium citrate is a kind of good
All-round chelating agent, has good sequestering power to various metals ion, can chelate most of divalent and trivalent metal ion, right
Cu2+、Fe2+、Fe3+With good sequestering power；EDTA has calcium and magnesium ion as common metal-chelator stronger
Chelation, two kinds of metal-chelators can effectively chelate the activator of the phenolase such as copper, iron, the magnesium in alcoholization piece cigarette, avoid gold
The generation of brown stain can be inhibited or mitigate by belonging to the catalytic action of ion.This kind of amino reductone substance of Amadori compounds has
Chelating, reduction and the characteristic for eliminating oxygen can have good anti-oxidation characteristics, and right with chelating Fe, Zn, Cu plasma
The activity of polyphenol oxidase is inhibited, to inhibit enzymatic browning, and can effectively facilitate during alcoholization aldehydes,
Furans, pyrroles, pyranone.Etc. the formation of important aroma substance.
Enzymatic browning and Maillard reaction, polyphenol oxidative dimerization into exercising alcoholization piece infuscate substance accumulation
Main path, and cause to refine the main reason for brown stain occurs for piece cigarette.Sodium sulfite, sodium citrate, EDTA, ascorbic acid,
Amadori compound these types substances configure nicotinic alcohol browning inhibition agent solution in blocks and can be effectively relieved according to a certain percentage
The progress of mailland reaction and polyphenol oxidative dimerization, it is inhibited to polyphenol oxidase activity, it can effectively reduce
The generation of oxidation during piece nicotinic alcohol makes the accumulation reduction of atrament during piece nicotinic alcohol, alcoholization is effectively relieved
Piece cigarette brown stain situation, and have a certain upgrade to the alcoholization quality of tobacco leaf.
The present invention compared with the existing technology, has the following advantages and effect：
Sodium nitrite and ascorbic acid in the piece nicotinic alcohol browning inhibition agent solution of the present invention are good biological antioxygens
Agent, can be effectively relieved the progress of mailland reaction, and prevent from leading to polyphenol oxidative dimerization due to oxidation；
Sodium citrate, EDTA, Amadori compound can effectively inhibit polyphenol oxidase activity, and enzymatic browning is inhibited to carry out, and effectively press down
The generation of brown stain during film-making nicotinic alcohol, while the alcoholization quality of tobacco leaf can be promoted so that the aroma quality of alcoholization piece cigarette is more
Well, fragrance is more sufficient.
Specific implementation mode
With reference to embodiment, the present invention is described in further detail, and embodiments of the present invention are not limited thereto.
Embodiment 1
A kind of nicotinic alcohol browning inhibition agent solution, each component in the solution are made according to the following ratio, and carrier is water：
Sodium sulfite 10g/L, sodium citrate 15g/L, EDTA15g/L, ascorbic acid 7g/L, Amadori compound 2g/L；
The preparation method of the piece nicotinic alcohol browning inhibition agent solution, includes the following steps：
A, the 10g sodium sulfites weighed and 15g sodium citrates is soluble in water, it stirs to whole dissolvings, is configured to a liquid；
B, the 15gEDTA weighed is soluble in water, it stirs to whole dissolvings, is configured to b liquid；
C, the 2gAmadori compounds weighed are dissolved in water alcohol, stir to whole dissolvings, is configured to c liquid；
D, a liquid, b liquid and c liquid will be mixed, and will stir evenly, is configured to d liquid；
E, the 7g ascorbic acid that will be weighed is poured into d liquid, is stirred evenly, and 0.01mol/L dilute hydrochloric acid solutions adjust PH to 6
Left and right, is settled to 1000ml to get the piece nicotinic alcohol browning inhibition agent solution.
The application process of the piece nicotinic alcohol browning inhibition agent solution, includes the following steps：
Tobacco purchasing is completed, in the tobacco leaf hot wind leaves moisting process in beating and double roasting stage；
Steam and water spout are placed respectively with outlet in the entrance of tobacco leaf moisting machine, with 20 times of piece nicotinic alcohol browning inhibition of dilution
Agent solution replaces the water of tobacco leaf moisting machine that circulating air system is arranged, and the water vapour pressure in tobacco leaf moisting machine in air shows water more than tobacco leaf
Steam pressure, temperature show temperature higher than tobacco leaf, are conducive to the attachment of nicotinic alcohol browning inhibition agent solution and show while reaching with tobacco leaf
To tobacco leaf warming and humidifying effect；
It checks nicotinic alcohol browning inhibition agent solution surplus, is replenished in time, after piece cigarette completes hot wind leaves moisting program, carry out leaf stalk
Then separation carries out storage and the natural alcoholization of smoked sheet.
Embodiment 2
The piece nicotinic alcohol browning inhibition agent solution, preferably by including being made containing following raw material, carrier is water：Sulfurous acid
Sodium 20g/L, sodium citrate 22g/L, EDTA25g/L, ascorbic acid 10g/L, Amadori compound 6g/L.
The preparation method of the piece nicotinic alcohol browning inhibition agent solution, includes the following steps：
A, the 20g sodium sulfites weighed and 22g sodium citrates is soluble in water, it stirs to whole dissolvings, is configured to a liquid；
B, the 25gEDTA weighed is soluble in water, it stirs to whole dissolvings, is configured to b liquid；
C, the 6gAmadori compounds weighed is soluble in water, it stirs to whole dissolvings, is configured to c liquid；
D, a liquid, b liquid and c liquid are mixed, stirs evenly, is configured to d liquid；
E, it by weigh 10, ascorbic acid, pours into d liquid, stirs evenly, 0.01mol/L dilute hydrochloric acid solutions adjust PH
To 6 or so, 1000ml is settled to get the piece nicotinic alcohol browning inhibition agent solution.
The application process of the piece nicotinic alcohol browning inhibition agent solution, includes the following steps：
Tobacco purchasing is completed, in the tobacco leaf hot wind leaves moisting process in beating and double roasting stage；
Steam and water spout are placed respectively with outlet in the entrance of tobacco leaf moisting machine, with 30 times of piece nicotinic alcohol browning inhibition of dilution
Agent solution replaces the water of tobacco leaf moisting machine that circulating air system is arranged, and the water vapour pressure in tobacco leaf moisting machine in air shows water more than tobacco leaf
Steam pressure, temperature show temperature higher than tobacco leaf, are conducive to the attachment of nicotinic alcohol browning inhibition agent solution and show while reaching with tobacco leaf
To tobacco leaf warming and humidifying effect；
It checks nicotinic alcohol browning inhibition agent solution surplus, is replenished in time, after piece cigarette completes hot wind leaves moisting program, carry out leaf stalk
Then separation carries out storage and the natural alcoholization of smoked sheet.
Embodiment 3
The piece nicotinic alcohol browning inhibition agent solution, most preferably by including being made containing following raw material, carrier is water：Sulfurous
Sour sodium 16g/L, sodium citrate 19g/L, EDTA20g/L, ascorbic acid 9g/L, Amadori compound 5g/L,
The preparation method of the piece nicotinic alcohol browning inhibition agent solution, includes the following steps：
A, 16g sodium sulfites are weighed and 19g sodium citrates are soluble in water, stirs to whole dissolvings, is configured to a liquid；
B, it is soluble in water to weigh 20gEDTA, stirs to whole dissolvings, is configured to b liquid；
C, it is soluble in water that 5gAmadori compounds are weighed, stirs to whole dissolvings, is configured to c liquid；
D, a liquid, b liquid and c liquid are mixed, stirs evenly, is configured to d liquid；
E, the 9g ascorbic acid that will be weighed is poured into d liquid, is stirred evenly, and 0.01mol/L dilution heat of sulfuric acid adjusts PH to 6
Left and right, is settled to 1000ml to get the piece nicotinic alcohol browning inhibition agent solution.
The application process of the piece nicotinic alcohol browning inhibition agent solution, includes the following steps：
Tobacco purchasing is completed, in the tobacco leaf hot wind leaves moisting process in beating and double roasting stage；
Steam and water spout are placed respectively with outlet in the entrance of tobacco leaf moisting machine, with 25 times of piece nicotinic alcohol browning inhibition of dilution
Agent solution replaces the water of tobacco leaf moisting machine that circulating air system is arranged, and the water vapour pressure in tobacco leaf moisting machine in air shows water more than tobacco leaf
Steam pressure, temperature show temperature higher than tobacco leaf, are conducive to the attachment of nicotinic alcohol browning inhibition agent solution and show while reaching with tobacco leaf
To tobacco leaf warming and humidifying effect；
It checks nicotinic alcohol browning inhibition agent solution surplus, is replenished in time, after piece cigarette completes hot wind leaves moisting program, carry out leaf stalk
Then separation carries out storage and the natural alcoholization of smoked sheet.
Embodiment 4
Tobacco purchasing finishes, multiple with the method processing in embodiment 1 in the tobacco leaf hot wind leaves moisting process in beating and double roasting stage
Flue-cured tobacco after piece cigarette completes hot wind leaves moisting program, carries out leaf stalk separation, B2F, C3F, X2F is taken to carry out storage and the nature of piece cigarette
Refine this as 1 (browning inhibitor) of processing.Tobacco purchasing finishes, and after completing tobacco threshing and redrying, B2F, C3F is taken to carry out piece cigarette
Storage and natural alcoholization this for processing 2 (controls).Sampling is primary when 18 months, 24 months, 30 months of each processing storage,
The brown stain situation of tobacco leaf, the evaluation and analysis index of B2F tobacco leaves are measured respectively.Experiment was carried out in 2014 in Meizhou tobacco leaf rebaking factory, institute
Tobacco sample is taken to be stored in constant temperature and humidity incubator, 27 degrees Celsius of temperature, humidity 70%, browning index=100 × ∑ is (at different levels
Browned area × typical value at different levels)/(investigation total tablet cigarette area × superlative degree typical value).
Table 1 respectively handles the brown stain situation of tobacco leaf
As shown in Table 1, when refining 18 months, after beating and double roasting tobacco leaf carries out leaves moisting using flue-cured tobacco browning inhibitor,
The browning index of B2F, C3F, X2F are below control treatment, have dropped 11.89,16.71,13.43 respectively；In alcoholization 24 months
When, after beating and double roasting tobacco leaf carries out leaves moisting using flue-cured tobacco browning inhibitor, the browning index of B2F, C3F, X2F are below at control
Reason, has dropped 25.06,24.52,22.16 respectively；When refining 30 months, beating and double roasting tobacco leaf uses flue-cured tobacco browning inhibitor
After carrying out leaves moisting, the browning index of B2F, C3F, X2F are below control treatment, have dropped 30.29,31.99,28.15 respectively.
Beating and double roasting tobacco leaf carries out leaves moisting using flue-cured tobacco browning inhibitor, in the upper, middle and lower position tobacco leaf browning index of 3 periods
It is below normal processing, illustrates that the piece nicotinic alcohol browning inhibition agent solution for spraying the preparation of embodiment 1 can effectively inhibit roasting rear cigarette
Cured tobacco leaf storage alcoholization brown stain situation is alleviated in the generation of brown pigment and related brown material during leaf storage alcoholization.
The judging parameter of 2 C3F tobacco leaves of table compares
Aroma quality：Good (10), preferable (8), general (6) are poor (4), poor (2).Perfume quantity：Foot (10), relatively sufficient (8), has
(6), micro- to have (4), it is flat (2).It is jealous：Pure comfortable (12), still comfortable (9), micro- uncomfortable (7), slightly bitter peppery (4) are bitter peppery
(1).Miscellaneous gas：It is micro- to have (8) without (10), have (6), heavier (4), weight (1).Irritation：It is micro- to have (8) without (10), have (6), it is heavier
(4), weight (1).Strength：Moderate (8), larger (6+) smaller (6-), big (4+) small (4-)
As shown in Table 2, the piece cigarette perfume makings of C3F pieces cigarette control treatment when refining 18 months, 24 months, 30 months is more preferable
It increases with perfume quantity, wherein at 30 months, aroma quality scores 0.5 point high compared with the control with perfume quantity；Beat leaf
Redried leaf tobacco refines the jealous more comfortable of piece cigarette after carrying out leaves moisting using flue-cured tobacco browning inhibitor, and miscellaneous gas is reduced with irritation；
In terms of strength, except when refining 30 months, strength is bigger than normal outer, in alcoholization 18 months, 24 months, strength became more moderate.
Illustrate, perfume quantity and perfume are effectively increased after carrying out leaves moisting using the flue-cured tobacco browning inhibitor in embodiment 1 in beating and double roasting
Makings, jealous more comfortable with camera lens, miscellaneous gas and irritation are less, improve the alcoholization Quality advance of tobacco leaf.
Embodiment 5
Tobacco purchasing finishes, multiple with the method processing in embodiment 2 in the tobacco leaf hot wind leaves moisting process in beating and double roasting stage
Flue-cured tobacco after piece cigarette completes hot wind leaves moisting program, carries out leaf stalk separation, B2F, C3F, X2F is taken to carry out storage and the nature of piece cigarette
Refine this as 1 (browning inhibitor) of processing.Tobacco purchasing finishes, and after completing tobacco threshing and redrying, B2F, C3F is taken to carry out piece cigarette
Storage and natural alcoholization this for processing 2 (controls).Sampling is primary when 18 months, 30 months, 42 months of each processing storage,
The brown stain situation of tobacco leaf, the evaluation and analysis index of tobacco leaf are measured respectively.Experiment was carried out in 2014 in Meizhou tobacco leaf rebaking factory, taken cigarette
Leaf sample is stored in constant temperature and humidity incubator, 27 degrees Celsius of temperature, humidity 70%, (the brown stains at different levels of browning index=100 × ∑
Area × typical value at different levels)/(investigation total tablet cigarette area × superlative degree typical value).
Table 3 respectively handles the brown stain situation of tobacco leaf
The judging parameter of 4 C3F tobacco leaves of table compares
As shown in Table 3, when refining 18 months, after beating and double roasting tobacco leaf carries out leaves moisting using flue-cured tobacco browning inhibitor,
The browning index of B2F, C3F, X2F are below control treatment, have dropped 9.16,15.26,12.04 respectively；In alcoholization 24 months
When, after beating and double roasting tobacco leaf carries out leaves moisting using flue-cured tobacco browning inhibitor, the browning index of B2F, C3F, X2F are below at control
Reason, has dropped 20.83,23.24,21.21 respectively；When refining 30 months, beating and double roasting tobacco leaf uses flue-cured tobacco browning inhibitor
After carrying out leaves moisting, the browning index of B2F, C3F, X2F are below control treatment, have dropped 27.60,29.95,26.16 respectively.
Beating and double roasting tobacco leaf carries out leaves moisting using flue-cured tobacco browning inhibitor, in the upper, middle and lower position tobacco leaf browning index of 3 periods
It is below normal processing, illustrates that the piece nicotinic alcohol browning inhibition agent solution for spraying the preparation of embodiment 2 can effectively inhibit roasting rear cigarette
Cured tobacco leaf storage alcoholization brown stain situation is alleviated in the generation of brown pigment and related brown material during leaf storage alcoholization.
As shown in Table 4, C3F tobacco leaves are when storage is refined 18 months, 24 months, 30 months, at browning inhibition agent solution
The tobacco aroma quality of reason is more preferable, and perfume quantity is more sufficient；Compared with the tobacco leaf through browning inhibitor solution treatment, the C3F of control treatment
Tobacco leaf it is jealous poor, miscellaneous gas is larger with irritation, and strength is smaller.Control treatment was in storage alcoholization 18 months, 24 months, 30
Total score of the smokeing panel test when moon is below through piece nicotinic alcohol browning inhibitor solution treatment.Illustrate, embodiment 2 is used in beating and double roasting
In flue-cured tobacco browning inhibitor carry out leaves moisting after effectively increase perfume quantity and aroma quality, jealous more comfortable with strength, miscellaneous gas with
Irritation is less, improves the alcoholization Quality advance of tobacco leaf.
Embodiment 6
Tobacco purchasing finishes, multiple with the method processing in embodiment 3 in the tobacco leaf hot wind leaves moisting process in beating and double roasting stage
Flue-cured tobacco after piece cigarette completes hot wind leaves moisting program, carries out leaf stalk separation, B2F, C3F, X2F is taken to carry out storage and the nature of piece cigarette
Refine this as 1 (browning inhibitor) of processing.Tobacco purchasing finishes, and after completing tobacco threshing and redrying, B2F, C3F is taken to carry out piece cigarette
Storage and natural alcoholization this for processing 2 (controls).Sampling is primary when 18 months, 30 months, 42 months of each processing storage,
The brown stain situation of tobacco leaf, the evaluation and analysis index of tobacco leaf are measured respectively.Experiment was carried out in 2014 in Meizhou tobacco leaf rebaking factory, taken cigarette
Leaf sample is stored in constant temperature and humidity incubator, 27 degrees Celsius of temperature, humidity 70%, (the brown stains at different levels of browning index=100 × ∑
Area × typical value at different levels)/(investigation total tablet cigarette area × superlative degree typical value).
Table 5 respectively handles the brown stain situation of tobacco leaf
The judging parameter of 6 C3F tobacco leaves of table compares
As shown in Table 5, when refining 18 months, after beating and double roasting tobacco leaf carries out leaves moisting using flue-cured tobacco browning inhibitor,
The browning index of B2F, C3F, X2F are below control treatment, have dropped 13.13,17.48,14.07 respectively；In alcoholization 24 months
When, after beating and double roasting tobacco leaf carries out leaves moisting using flue-cured tobacco browning inhibitor, the browning index of B2F, C3F, X2F are below at control
Reason, has dropped 27.04,26.65,23.80 respectively；When refining 30 months, beating and double roasting tobacco leaf uses flue-cured tobacco browning inhibitor
After carrying out leaves moisting, the browning index of B2F, C3F, X2F are below control treatment, have dropped 32.61,34.70,29.02 respectively.
Beating and double roasting tobacco leaf carries out leaves moisting using flue-cured tobacco browning inhibitor, in the upper, middle and lower position tobacco leaf browning index of 3 periods
It is below normal processing, illustrates that the piece nicotinic alcohol browning inhibition agent solution for spraying the preparation of embodiment 2 can effectively inhibit roasting rear cigarette
Cured tobacco leaf storage alcoholization brown stain situation is alleviated in the generation of brown pigment and related brown material during leaf storage alcoholization.
As shown in Table 6, C3F tobacco leaves are when storage is refined 18 months, 24 months, 30 months, at browning inhibition agent solution
The tobacco aroma quality of reason is more preferable, and perfume quantity is more sufficient；Compared with the tobacco leaf through browning inhibitor solution treatment, the C3F of control treatment
Tobacco leaf it is jealous poor, miscellaneous gas is larger with irritation, and strength is smaller.Control treatment was in storage alcoholization 18 months, 24 months, 30
Total score of the smokeing panel test when moon is below through piece nicotinic alcohol browning inhibitor solution treatment.Illustrate, embodiment 3 is used in beating and double roasting
In flue-cured tobacco browning inhibitor carry out leaves moisting after effectively increase perfume quantity and aroma quality, jealous more comfortable with strength, miscellaneous gas with
Irritation is less, improves the alcoholization Quality advance of tobacco leaf.
Claims (11)
1. a kind of nicotinic alcohol browning inhibition agent solution, which is characterized in that based on mass percentage, the solution includes following
Ingredient：5~30g/L of sodium sulfite, 10~30g/L of sodium citrate, EDTA10~30g/L, 6~12g/L of ascorbic acid,
1~10g/L of Amadori compounds.
2. according to claim 1 nicotinic alcohol browning inhibition agent solution, which is characterized in that based on mass percentage,
The solution includes following component：10~25g/L of sodium sulfite, 15~25g/L of sodium citrate, EDTA13~25g/L, Vitamin C
7~11g/L of acid, 2~8g/L of Amadori compounds.
3. according to claim 1 nicotinic alcohol browning inhibition agent solution, which is characterized in that based on mass percentage,
The solution includes following component：15~20g/L of sodium sulfite, 18~22g/L of sodium citrate, EDTA17~22/L, Vitamin C
8~10g/L of acid, 4~6g/L of Amadori compounds.
4. according to claim 1 nicotinic alcohol browning inhibition agent solution, which is characterized in that based on mass percentage,
The solution includes following component：Sodium sulfite 16g/L, sodium citrate 19g/L, EDTA18g/L, ascorbic acid 9g/L,
Amadori compounds 5g/L.
5. according to claim 1-4 any one of them piece nicotinic alcohol browning inhibition agent solutions, which is characterized in that the solution is used
In preparation flue-cured tobacco cultivars be cloud and mist 87.
6. the preparation method of claim 1-5 any one of them piece nicotinic alcohol browning inhibition agent solutions, it is characterised in that including
Following steps：
A, it is soluble in water with sodium citrate to weigh sodium sulfite, stirs to whole dissolvings, is configured to a liquid；
B, it is soluble in water to weigh EDTA, stirs to whole dissolvings, is configured to b liquid；
C, it is soluble in water that Amadori compounds are weighed, stirs to whole dissolvings, is configured to c liquid；
D, a liquid, b liquid and c liquid are mixed, stirs evenly, is configured to d liquid；
E, the ascorbic acid that will be weighed is poured into d liquid, is stirred evenly, and acid solution adjusts pH to 6 or so, and constant volume is to get described
Piece nicotinic alcohol browning inhibition agent solution.
7. the preparation method of according to claim 6 nicotinic alcohol browning inhibition agent solution, which is characterized in that in step D
The condition stirred evenly is to be stirred evenly with 80~120r/min.
8. the preparation method of according to claim 6 nicotinic alcohol browning inhibition agent solution, which is characterized in that in step E
The acid solution is selected from：Hydrochloric acid or sulfuric acid.
9. claim 1-5 any one of them piece nicotinic alcohol browning inhibition agent solutions answering in reducing cured tobacco leaf and fading
With.
10. the application process of claim 1-5 any one of them piece nicotinic alcohol browning inhibition agent solutions, it is characterised in that including
Following steps：
(1) tobacco purchasing is completed, and the tobacco leaf hot wind leaves moisting process in beating and double roasting stage, tobacco leaf material is fed by arrival end, is relied on
Harrow nail acts in the rotation of leaves moisting machine cylinder and cylinder, and tobacco leaf is rolled from entrance to outlet；
(2) steam and water spout are placed respectively in the entrance of tobacco leaf moisting machine and outlet, replace moistening with nicotinic alcohol browning inhibition agent solution
The water of leaf machine is arranged circulating air system, and the water vapour pressure in tobacco leaf moisting machine in air shows water vapour pressure more than tobacco leaf, warm
Degree higher than tobacco leaf shows temperature, is conducive to nicotinic alcohol browning inhibition agent solution and adheres to show while reaching tobacco leaf to heat with tobacco leaf
Moisturization effect；
(3) it checks nicotinic alcohol browning inhibition agent solution surplus, is replenished in time；
(4) after piece cigarette completes hot wind leaves moisting program, leaf stalk separation is carried out, storage and the natural alcoholization of smoked sheet are then carried out.
11. the application process of according to claim 9 nicotinic alcohol browning inhibition agent solution, which is characterized in that step (2)
(3) the piece nicotinic alcohol browning inhibition agent solution described in is by any piece nicotinic alcohol browning inhibitors of claim 1-4
Solution dilutes the solution after 20~30 times.
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| CN201810362546.XA CN108703409A (en) | 2018-04-20 | 2018-04-20 | A kind of nicotinic alcohol browning inhibitor solution manufacturing method and application |
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| CN112586800A (en) * | 2020-12-03 | 2021-04-02 | 河南农业大学 | Cured tobacco modulation fixative and preparation method and application thereof |
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Cited By (3)
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| CN112586800A (en) * | 2020-12-03 | 2021-04-02 | 河南农业大学 | Cured tobacco modulation fixative and preparation method and application thereof |
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| CN114532566A (en) * | 2022-03-02 | 2022-05-27 | 湖北省烟草科学研究院 | Tobacco anti-browning agent and application thereof |
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Application publication date: 20181026 |