CN108691194A - A kind of manufacture craft of antibacterial water-proof function fabric - Google Patents
A kind of manufacture craft of antibacterial water-proof function fabric Download PDFInfo
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- CN108691194A CN108691194A CN201810503298.6A CN201810503298A CN108691194A CN 108691194 A CN108691194 A CN 108691194A CN 201810503298 A CN201810503298 A CN 201810503298A CN 108691194 A CN108691194 A CN 108691194A
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- Prior art keywords
- water
- fabric
- proof function
- manufacture craft
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- 239000004744 fabric Substances 0.000 title claims abstract description 49
- 230000000844 anti-bacterial effect Effects 0.000 title claims abstract description 20
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 30
- 230000002940 repellent Effects 0.000 claims abstract description 20
- 239000005871 repellent Substances 0.000 claims abstract description 20
- 238000000034 method Methods 0.000 claims abstract description 18
- 238000012360 testing method Methods 0.000 claims abstract description 16
- -1 washing fastness Substances 0.000 claims abstract description 14
- 229920001661 Chitosan Polymers 0.000 claims abstract description 12
- 230000000845 anti-microbial effect Effects 0.000 claims abstract description 11
- 230000008569 process Effects 0.000 claims abstract description 11
- 229920000742 Cotton Polymers 0.000 claims abstract description 10
- 230000002421 anti-septic effect Effects 0.000 claims abstract description 9
- 239000003431 cross linking reagent Substances 0.000 claims abstract description 8
- 230000003115 biocidal effect Effects 0.000 claims abstract description 7
- 239000003795 chemical substances by application Substances 0.000 claims description 33
- 230000000740 bleeding effect Effects 0.000 claims description 12
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 9
- 125000003709 fluoroalkyl group Chemical group 0.000 claims description 9
- 239000002253 acid Substances 0.000 claims description 6
- 238000006243 chemical reaction Methods 0.000 claims description 6
- 238000002386 leaching Methods 0.000 claims description 6
- SQGYOTSLMSWVJD-UHFFFAOYSA-N silver(1+) nitrate Chemical compound [Ag+].[O-]N(=O)=O SQGYOTSLMSWVJD-UHFFFAOYSA-N 0.000 claims description 6
- 239000000463 material Substances 0.000 claims description 5
- 239000000835 fiber Substances 0.000 claims description 4
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 3
- 239000005977 Ethylene Substances 0.000 claims description 3
- 150000007513 acids Chemical class 0.000 claims description 3
- 239000004202 carbamide Substances 0.000 claims description 3
- 125000002091 cationic group Chemical group 0.000 claims description 3
- 239000000839 emulsion Substances 0.000 claims description 3
- 150000002118 epoxides Chemical class 0.000 claims description 3
- 125000004494 ethyl ester group Chemical group 0.000 claims description 3
- 125000000373 fatty alcohol group Chemical group 0.000 claims description 3
- 230000008595 infiltration Effects 0.000 claims description 3
- 238000001764 infiltration Methods 0.000 claims description 3
- XIXADJRWDQXREU-UHFFFAOYSA-M lithium acetate Chemical compound [Li+].CC([O-])=O XIXADJRWDQXREU-UHFFFAOYSA-M 0.000 claims description 3
- 150000003961 organosilicon compounds Chemical class 0.000 claims description 3
- 239000012188 paraffin wax Substances 0.000 claims description 3
- 238000011056 performance test Methods 0.000 claims description 3
- 229940051841 polyoxyethylene ether Drugs 0.000 claims description 3
- 229920000056 polyoxyethylene ether Polymers 0.000 claims description 3
- 229920001296 polysiloxane Polymers 0.000 claims description 3
- 238000002360 preparation method Methods 0.000 claims description 3
- 229920006395 saturated elastomer Polymers 0.000 claims description 3
- 229910001961 silver nitrate Inorganic materials 0.000 claims description 3
- 229940124530 sulfonamide Drugs 0.000 claims description 3
- 238000010998 test method Methods 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 2
- 239000004599 antimicrobial Substances 0.000 abstract description 2
- 238000005406 washing Methods 0.000 abstract description 2
- 230000005764 inhibitory process Effects 0.000 description 2
- 231100000252 nontoxic Toxicity 0.000 description 2
- 230000003000 nontoxic effect Effects 0.000 description 2
- 230000035699 permeability Effects 0.000 description 2
- 238000004078 waterproofing Methods 0.000 description 2
- 229920002101 Chitin Polymers 0.000 description 1
- 241000588724 Escherichia coli Species 0.000 description 1
- 241000238631 Hexapoda Species 0.000 description 1
- 241000208202 Linaceae Species 0.000 description 1
- 235000004431 Linum usitatissimum Nutrition 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 238000005411 Van der Waals force Methods 0.000 description 1
- 238000007792 addition Methods 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 230000001580 bacterial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- ABDBNWQRPYOPDF-UHFFFAOYSA-N carbonofluoridic acid Chemical compound OC(F)=O ABDBNWQRPYOPDF-UHFFFAOYSA-N 0.000 description 1
- 229920002678 cellulose Polymers 0.000 description 1
- 239000001913 cellulose Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
- 230000003860 sleep quality Effects 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
Classifications
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
- D06M11/38—Oxides or hydroxides of elements of Groups 1 or 11 of the Periodic Table
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/58—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with nitrogen or compounds thereof, e.g. with nitrides
- D06M11/64—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with nitrogen or compounds thereof, e.g. with nitrides with nitrogen oxides; with oxyacids of nitrogen or their salts
- D06M11/65—Salts of oxyacids of nitrogen
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/02—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with hydrocarbons
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/46—Compounds containing quaternary nitrogen atoms
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/03—Polysaccharides or derivatives thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/263—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated carboxylic acids; Salts or esters thereof
- D06M15/277—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated carboxylic acids; Salts or esters thereof containing fluorine
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/53—Polyethers
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/643—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
- D06M2101/06—Vegetal fibres cellulosic
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/10—Repellency against liquids
- D06M2200/12—Hydrophobic properties
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Microbiology (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The invention discloses a kind of manufacture crafts of antibacterial water-proof function fabric, include the following steps:Fabric pre-processes, and reduces its surface tension;Antiseptic is prepared using saturation chitosan solution;Carry out water repellent finish;Carry out antibiotic finish;Antibacterial and water repellency test.After the present invention adds crosslinking agent to mix using chitosan antimicrobial agent and water repellent, final finishing, the good anti-microbial property of providing cotton fabric, washing fastness, water repellency are carried out to cotton fabric using one-bath method, and do not influence its own performance.
Description
Technical field
The present invention relates to a kind of manufacture craft of fabric more particularly to a kind of making works of antibacterial water-proof function fabric
Skill.
Background technology
Necessity when bedding is people's sleep, of close concern to each other with people's lives, therefore, whether the comfort of bedding accords with
Close the sleep quality for requiring to decide user.As the improvement of people's living standards, requirement of the people to bedding comfort
It is higher and higher.Having popularized the bedding fabric used on the market generally has silk, flax, pure cotton, polyester-cotton blend and other mixed cotton etc..These
The fabric of material generally only has the characteristic of material itself, such as soft, alkaline-resisting, sucting wet air permeability etc., but do not have antibacterial,
The additional functions such as waterproof, as people are higher and higher to the concern of multi-functional product, the textile of simple function cannot expire
The use demand of sufficient people.Therefore, there is the antibacterial water proofing property functional fabric that exploitation can be applied on bedding important reality to answer
With value.In addition, antibacterial water proofing property functional fabric all plays an important role in fields such as clothing, interior and outdoor goods.
Invention content
In order to solve the shortcoming present in above-mentioned technology, the present invention provides a kind of antibacterial water-proof function fabrics
Manufacture craft.
In order to solve the above technical problems, the technical solution adopted by the present invention is:A kind of antibacterial water-proof function fabric
Manufacture craft includes the following steps:
Step 1: fabric pre-processes:Cotton fabric is put into the sodium hydroxide solution of 10g/L and carries out water-bath;Then plus
Enter a small amount of bleeding agent, 100 degrees Celsius of lower water-baths 30 minutes;
Step 2: the preparation of antiseptic:It will for 0.1-0.5% to being saturated the mass fraction of chitosan solution according to silver nitrate
The two mixes, and a small amount of bleeding agent is added, and it is 4.0 to adjust pH, is protected from light, 50 degrees Celsius of isothermal reaction 1h;
Then the finishing agent to saturation chitosan solution mass fraction for 0.5% and a small amount of bleeding agent is added, adjusts pH
It is 4.0, is protected from light, 50 degrees Celsius of isothermal reaction 1h;
Step 3: carrying out water repellent finish:Two leachings are carried out to fabric using the crosslinking agent of the water repellent finishing agent of 50g/L, 15g/L
Two roll water repellent finish, bath raio 1:30, then dip time 30 minutes, pick-up 80-90% dries 3 points under 100 degrees Celsius
Clock;
Step 4: carrying out antibiotic finish:Fabric is subjected to two leachings two in the antiseptic prepared and rolls antibiotic finish, bath raio
1:30, then dip time 30 minutes, pick-up 80-90% is dried 3 minutes under 100 degrees Celsius, then under 135 degrees Celsius
Drying 3 minutes;
Step 5: performance test:Carry out anti-microbial property and water repellency test.
Bleeding agent is fatty alcohol polyoxyethylene ether, for reducing the surface tension of fabric, to promote various types of materials to fibre
Process process is accelerated in the infiltration of dimension.
Finishing agent is quaternary cationics.
Water repellent finishing agent is paraffin class finishing agent or modified fat acid or polysiloxane emulsion or finishing agent containing fluoroalkyl.Contain
Fluoroalkyl finishing agent is fluoroalkyl Type of Collective object or acrylic acid fluorocarbon sulfonamides base ethyl ester or Quilone water repellents.
Crosslinking agent is amide-formaldehyde class compound or urea aldehyde compound or Polycarboxylic acids or epoxide
Or ethylene imide compound or organosilicon compound.
Anti-microbial property test is using AATCC-90 haloing test method(s)s in step 5.
Water repellency test uses AATCC22-1977 fabric surface moisture resistance methods of testing in step 5.
After the present invention adds crosslinking agent to mix using chitosan antimicrobial agent and water repellent, cotton fabric is carried out using one-bath method
Final finishing, the good anti-microbial property of providing cotton fabric, washing fastness, water repellency, and its own performance is not influenced.
Specific implementation mode
The present invention will be further described in detail with reference to the specific embodiments.
A kind of manufacture craft of antibacterial water-proof function fabric, includes the following steps:
Step 1: fabric pre-processes:Cotton fabric is put into the sodium hydroxide solution of 10g/L and carries out water-bath;Then plus
Enter a small amount of bleeding agent, 100 degrees Celsius of lower water-baths 30 minutes;Bleeding agent is fatty alcohol polyoxyethylene ether, for reducing the table of fabric
Face tension accelerates process process to promote infiltration of the various types of materials to fiber;Its additive amount can be carried out according to the total amount of process
It determines.
Step 2: the preparation of antiseptic:It is 0.3% by the two to the mass fraction for being saturated chitosan solution according to silver nitrate
A small amount of bleeding agent is added in mixing, and it is 4.0 to adjust pH, is protected from light, 50 degrees Celsius of isothermal reaction 1h;
Then the finishing agent to saturation chitosan solution mass fraction for 0.5% and a small amount of bleeding agent is added, adjusts pH
It is 4.0, is protected from light, 50 degrees Celsius of isothermal reaction 1h;Finishing agent is quaternary cationics.
Chitosan is the deacetylated product of chitin, is mainly derived from the crust of animal, insect, has good antibacterial
Property, safety non-toxic also has good sucting wet air permeability, reactivity, bioactivity, adsorptivity, fibre forming property etc. unique
Physicochemical property.In addition, contain a large amount of hydroxyl in chitosan, it can be good by hydrogen bond or Van der Waals force and the cellulose in fabric
Be combined together, it is not easy to fall off.
Therefore, antiseptic is prepared based on chitosan, can not only assign fabric good anti-microbial property, Er Qiean
Entirely, nontoxic, meet environmentally protective industry standard instantly.
Step 3: carrying out water repellent finish:Two leachings are carried out to fabric using the crosslinking agent of the water repellent finishing agent of 50g/L, 15g/L
Two roll water repellent finish, bath raio 1:30, then dip time 30 minutes, pick-up 80% is dried 3 minutes under 100 degrees Celsius.
Wherein water repellent finishing agent is paraffin class finishing agent or modified fat acid or polysiloxane emulsion or is arranged containing fluoroalkyl
Agent.And finishing agent containing fluoroalkyl includes fluoroalkyl Type of Collective object, acrylic acid fluorocarbon sulfonamides base ethyl ester, Quilone
Water repellent (i.e. perfluorocarboxylic acid complex compound).
Crosslinking agent is amide-formaldehyde class compound or urea aldehyde compound or Polycarboxylic acids or epoxide
Or ethylene imide compound or organosilicon compound.
Step 4: carrying out antibiotic finish:Fabric is subjected to two leachings two in the antiseptic prepared and rolls antibiotic finish, bath raio
1:30, then dip time 30 minutes, pick-up 80% is dried 3 minutes under 100 degrees Celsius, then is dried under 135 degrees Celsius
3 minutes;
Step 5: performance test:Carry out anti-microbial property and water repellency test.Anti-microbial property test is using AATCC-
90 haloing test method(s)s;Water repellency test uses AATCC22-1977 fabric surface moisture resistance methods of testing.
The bacterial strain that anti-microbial property test is selected is ATCC-8099 Escherichia coli, and test result is:This product can be formed
Effective inhibition zone width of 0.5cm, and inhibition zone is not formed without the fabric that the antiseptic arranges, it can therefore be seen that logical
The fabric for crossing this method formation has good anti-microbial property.
According to AATCC22-1977 fabric surface moisture resistance methods of testing, ability meter is got wet to fabric by 35 types of TNG
Water repellency tested, as a result show this product water repellent rank be 4 grades, be significantly higher than the water repellent of existing product on the market
2-3 grades of index.
The above embodiment is not limitation of the present invention, and the present invention is also not limited to the example above, this technology neck
The variations, modifications, additions or substitutions that the technical staff in domain is made within the scope of technical scheme of the present invention, also belong to this hair
Bright protection domain.
Claims (8)
1. a kind of manufacture craft of antibacterial water-proof function fabric, it is characterised in that:Include the following steps:
Step 1: fabric pre-processes:Cotton fabric is put into the sodium hydroxide solution of 10g/L and carries out water-bath;Then it is added few
Measure bleeding agent, 100 degrees Celsius of lower water-baths 30 minutes;
Step 2: the preparation of antiseptic:It is 0.1-0.5% by the two to the mass fraction for being saturated chitosan solution according to silver nitrate
A small amount of bleeding agent is added in mixing, and it is 4.0 to adjust pH, is protected from light, 50 degrees Celsius of isothermal reaction 1h;
Then the finishing agent to saturation chitosan solution mass fraction for 0.5% and a small amount of bleeding agent is added, adjusting pH is
4.0, it is protected from light, 50 degrees Celsius of isothermal reaction 1h;
Step 3: carrying out water repellent finish:Two leachings two are carried out using the crosslinking agent of the water repellent finishing agent of 50g/L, 15g/L to fabric to roll
Water repellent finish, bath raio 1:30, then dip time 30 minutes, pick-up 80-90% is dried 3 minutes under 100 degrees Celsius;
Step 4: carrying out antibiotic finish:Fabric is subjected to two leachings two in the antiseptic prepared and rolls antibiotic finish, bath raio 1:
30, then dip time 30 minutes, pick-up 80-90% is dried 3 minutes under 100 degrees Celsius, then is dried under 135 degrees Celsius
It is 3 minutes dry;
Step 5: performance test:Carry out anti-microbial property and water repellency test.
2. the manufacture craft of antibacterial water-proof function fabric according to claim 1, it is characterised in that:The bleeding agent is
Fatty alcohol polyoxyethylene ether accelerates process for reducing the surface tension of fabric to promote infiltration of the various types of materials to fiber
Process.
3. the manufacture craft of antibacterial water-proof function fabric according to claim 1, it is characterised in that:The finishing agent is
Quaternary cationics.
4. the manufacture craft of antibacterial water-proof function fabric according to claim 1, it is characterised in that:The water repellent finish
Agent is paraffin class finishing agent or modified fat acid or polysiloxane emulsion or finishing agent containing fluoroalkyl.
5. the manufacture craft of antibacterial water-proof function fabric according to claim 4, it is characterised in that:It is described to contain fluoroalkyl
Finishing agent is fluoroalkyl Type of Collective object or acrylic acid fluorocarbon sulfonamides base ethyl ester or Quilone water repellents.
6. the manufacture craft of antibacterial water-proof function fabric according to claim 1, it is characterised in that:The crosslinking agent is
Amide-formaldehyde class compound or urea aldehyde compound or Polycarboxylic acids or epoxide or ethylene imide compound or
Organosilicon compound.
7. the manufacture craft of antibacterial water-proof function fabric according to claim 1, it is characterised in that:The anti-microbial property
Test is using AATCC-90 haloing test method(s)s.
8. the manufacture craft of antibacterial water-proof function fabric according to claim 1, it is characterised in that:The water repellency
Test uses AATCC22-1977 fabric surface moisture resistance methods of testing.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810503298.6A CN108691194A (en) | 2018-05-23 | 2018-05-23 | A kind of manufacture craft of antibacterial water-proof function fabric |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810503298.6A CN108691194A (en) | 2018-05-23 | 2018-05-23 | A kind of manufacture craft of antibacterial water-proof function fabric |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108691194A true CN108691194A (en) | 2018-10-23 |
Family
ID=63847725
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|---|---|---|---|
| CN201810503298.6A Pending CN108691194A (en) | 2018-05-23 | 2018-05-23 | A kind of manufacture craft of antibacterial water-proof function fabric |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110747635A (en) * | 2019-12-06 | 2020-02-04 | 湖州菠萝蜜服饰有限公司 | Antibacterial treatment method of pure cotton fabric |
| CN115519883A (en) * | 2022-09-16 | 2022-12-27 | 邦威防护科技股份有限公司 | Preparation method of highly-comfortable waterproof and moisture-permeable nano protective clothing fabric |
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| CN103334306A (en) * | 2013-05-18 | 2013-10-02 | 安徽工程大学 | Silver-carrying chitosan composite antibacterial agent, preparation method of the silver-carrying chitosan composite antibacterial agent, and fabric compounding finishing method |
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| CN103334306A (en) * | 2013-05-18 | 2013-10-02 | 安徽工程大学 | Silver-carrying chitosan composite antibacterial agent, preparation method of the silver-carrying chitosan composite antibacterial agent, and fabric compounding finishing method |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110747635A (en) * | 2019-12-06 | 2020-02-04 | 湖州菠萝蜜服饰有限公司 | Antibacterial treatment method of pure cotton fabric |
| CN115519883A (en) * | 2022-09-16 | 2022-12-27 | 邦威防护科技股份有限公司 | Preparation method of highly-comfortable waterproof and moisture-permeable nano protective clothing fabric |
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