CN108690440A - A kind of production technology of water packet sand continuous phase coating - Google Patents

A kind of production technology of water packet sand continuous phase coating Download PDF

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Publication number
CN108690440A
CN108690440A CN201810361040.7A CN201810361040A CN108690440A CN 108690440 A CN108690440 A CN 108690440A CN 201810361040 A CN201810361040 A CN 201810361040A CN 108690440 A CN108690440 A CN 108690440A
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China
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parts
weight
added
water
minutes
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CN201810361040.7A
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Chinese (zh)
Inventor
李志强
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Zhejiang Changxin Kai Shi Coatings Co Ltd
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Zhejiang Changxin Kai Shi Coatings Co Ltd
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Priority to CN201810361040.7A priority Critical patent/CN108690440A/en
Publication of CN108690440A publication Critical patent/CN108690440A/en
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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D143/00Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and containing boron, silicon, phosphorus, selenium, tellurium, or a metal; Coating compositions based on derivatives of such polymers
    • C09D143/04Homopolymers or copolymers of monomers containing silicon
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40Additives
    • C09D7/60Additives non-macromolecular
    • C09D7/61Additives non-macromolecular inorganic
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40Additives
    • C09D7/60Additives non-macromolecular
    • C09D7/63Additives non-macromolecular organic
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40Additives
    • C09D7/65Additives macromolecular
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K2201/00Specific properties of additives
    • C08K2201/014Additives containing two or more different additives of the same subgroup in C08K
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/02Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/02Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
    • C08L2205/025Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/03Polymer mixtures characterised by other features containing three or more polymers in a blend
    • C08L2205/035Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Paints Or Removers (AREA)

Abstract

The invention discloses a kind of production technologies of water packet sand continuous phase coating, including 1), by water, antifoaming agent, SD-5W solution changes agent, 996AD and 80-120 sand are added in reaction kettle, stir to get mixed liquor A;2), TT935 and water are added in mixed liquor A, stir to get mixed liquid B;3), propylene glycol, AMP-95, coalescents and thickener are added in mixed liquid B, stir to get mixed liquor C;4) mixed liquor C, is stood 2-3 hours, obtains finished product.Continuous phase coating produced by the present invention has good water resistance, and stable storing, efficiently solves the problems in background technology.

Description

A kind of production technology of water packet sand continuous phase coating
Technical field
The invention belongs to coating process fields, specifically, being related to a kind of production technology of water packet sand continuous phase coating.
Background technology
Coating, in the entitled paint of Chinese tradition, so-called coating be coated in the body surface being protected or decorated, and The continuous film of firm attachment can be formed with coated article, typically based on resin or oil or lotion, add or do not add face Material, filler add corresponding additive, the thick liquid being formulated with organic solvent or water.
Currently, architectural decoration coating material Water-borne modification has become inevitable development trend, the building decorated using water paint True stone texture is strong, is ideal building and ornament materials, but conventional water paint does not have good water-fast weathering performance, this master To depend on the Recipe of aqueous continuous phase coating.
Invention content
In view of the above-mentioned problems, the present invention provides a kind of production technology of water packet sand continuous phase coating, the painting produced Material has preferable water-fast weather resistance, to effectively solve the problems, such as to point out in background technology.
The technical solution adopted by the present invention is:
A kind of production technology of water packet sand continuous phase coating, includes the following steps:
1) 168 parts by weight water, 1.5 parts by weight antifoaming agent, 2.5 parts by weight SD-5W solutions, are become into agent, 550 parts by weight 996AD It is added in reaction kettle with 200 parts by weight 80-120 sand, with 5-10 points of the rotating speed of 800-1000r/min stirring at 15-25 DEG C Clock obtains mixed liquor A;
2), 3.5 parts by weight TT935 and 21 parts by weight water are added in mixed liquor A, with 800- at 15-25 DEG C The rotating speed of 1000r/min stirs 25-35 minutes, obtains mixed liquid B;
3), 18.5 parts by weight of propylene glycol, 1 parts by weight AMP-95,27.5 parts by weight coalescents and 3.5 parts by weight are thickened Agent is added in mixed liquid B, is stirred 5-10 minutes with the rotating speed of 400-500r/min at 15-25 DEG C, is obtained mixed liquor C;
4) mixed liquor C, is stood 2-3 hours, obtains finished product.
Preferably, the preparation method of the antifoaming agent is:First, ointment is prepared, by the proportion ingredient of following component, with Weight part ratio meter, White Mineral Oil:White carbon:Polyethers:Polyether polyol:Castor oil=(10-45) part:(2-10) part:(10-35) Part:(10-30) part:(10-35) part;Then above-mentioned dispensing is added into the reaction kettle equipped with stirring slurry, motor and heating system, It will be uniformly mixed under dispensing room temperature, stir 1 hour blowing;80 parts of the ointment that above-mentioned Recipe is worked it out is taken, is added certainly Each 20 parts of newborn silicone oil, tributyl phosphate, 10 parts of blended emulsifier stir evenly, and 280 parts of water is then added and makes its phase inversion, turns 16 parts of thickener is added after mutually complete and is used for thickening tune viscosity to 1500CS-2000CS, then discharging is packaged dress, you can is disappeared Infusion.
Preferably, the preparation method of the preservative is:By the dodecyl dimethyl Benzylmagnesium chloride of weight Ammonium, myristyl benzyl dimethyl ammonium chloride, cetalkonium chloride and octadecyl dimethyl benzyl chlorination The composition and didecyl Dimethy ammonium chloride of one or more of ammonium are put into blender and are stirred, stirring Time is 30-120 minutes;When needing that stabilizer is added, stabilizer is added in deionized water and is dissolved, then will be dissolved with The deionized water solution of stabilizer is poured into the blender and is stirred, and mixing time is 30-120 minutes;It only needs to be added When deionized water, directly deionized water is poured into the blender and is stirred, mixing time is similarly 30-120 minutes;So By finished product head tank is pumped into after filtering, analysis qualification, it is put into clean empty bottle in Irrigation Machine or slack tank starts filling and screw capping, Obtain preservative.
Continuous phase coating produced by the present invention has good water resistance, and stable storing, efficiently solves background skill The problems in art.
Specific implementation mode
The present invention is described in further detail below by specific embodiment.
Embodiment
A kind of production technology of water packet sand continuous phase coating, includes the following steps:
1) 168 parts by weight water, 1.5 parts by weight antifoaming agent, 2.5 parts by weight SD-5W solutions, are become into agent, 550 parts by weight 996AD It is added in reaction kettle with 200 parts by weight 80-120 sand, with 5-10 points of the rotating speed of 800-1000r/min stirring at 15-25 DEG C Clock obtains mixed liquor A;
2), 3.5 parts by weight TT935 and 21 parts by weight water are added in mixed liquor A, with 800- at 15-25 DEG C The rotating speed of 1000r/min stirs 25-35 minutes, obtains mixed liquid B;
3), 18.5 parts by weight of propylene glycol, 1 parts by weight AMP-95,27.5 parts by weight coalescents and 3.5 parts by weight are thickened Agent is added in mixed liquid B, is stirred 5-10 minutes with the rotating speed of 400-500r/min at 15-25 DEG C, is obtained mixed liquor C;
4) mixed liquor C, is stood 2-3 hours, obtains finished product.
The preparation method of the antifoaming agent is:First, ointment is prepared, by the proportion ingredient of following component, with weight part ratio Meter, White Mineral Oil:White carbon:Polyethers:Polyether polyol:Castor oil=(10-45) part:(2-10) part:(10-35) part:(10-30) Part:(10-35) part;Then above-mentioned dispensing is added into the reaction kettle equipped with stirring slurry, motor and heating system, by dispensing room temperature It is lower to be uniformly mixed, stir 1 hour blowing;80 parts of the ointment that above-mentioned Recipe is worked it out is taken, is added from newborn silicone oil, phosphoric acid Each 20 parts of tributyl, 10 parts of blended emulsifier stir evenly, and 280 parts of water is then added and makes its phase inversion, 16 are added after phase inversion is complete The thickener of part, which is used for thickening, adjusts viscosity to 1500CS-2000CS, and then discharging, which is packaged, fills, you can obtains antifoaming agent.
The preparation method of the preservative is:By the dodecyl benzyl dimethyl ammonium chloride of weight, the tetradecane One kind in base dimethyl benzyl ammonium chloride, cetalkonium chloride and stearyl dimethyl benzyl ammonium chloride Or two or more compositions and didecyl Dimethy ammonium chloride is put into blender and is stirred, mixing time 30- 120 minutes;When needing that stabilizer is added, stabilizer is added in deionized water and is dissolved, it then will be dissolved with stabilizer Deionized water solution is poured into the blender and is stirred, and mixing time is 30-120 minutes;It only needs that deionized water is added When, directly deionized water is poured into the blender and is stirred, mixing time is similarly 30-120 minutes;Then pass through Be pumped into finished product head tank after filter, analysis are qualified, be put into clean empty bottle in Irrigation Machine or slack tank start filling and screw capping to get to Preservative.

Claims (3)

1. a kind of production technology of water packet sand continuous phase coating, which is characterized in that include the following steps:
1) 168 parts by weight water, 1.5 parts by weight antifoaming agent, 2.5 parts by weight SD-5W solutions, are become into agent, 550 parts by weight 996AD and 200 Parts by weight 80-120 sand is added in reaction kettle, is stirred 5-10 minutes, is obtained with the rotating speed of 800-1000r/min at 15-25 DEG C To mixed liquor A;
2), 3.5 parts by weight TT935 and 21 parts by weight water are added in mixed liquor A, with 800-1000r/min at 15-25 DEG C Rotating speed stir 25-35 minutes, obtain mixed liquid B;
3), 18.5 parts by weight of propylene glycol, 1 parts by weight AMP-95,27.5 parts by weight coalescents and 3.5 parts by weight of thickening agent are added Enter into mixed liquid B, is stirred 5-10 minutes with the rotating speed of 400-500r/min at 15-25 DEG C, obtain mixed liquor C;
4) mixed liquor C, is stood 2-3 hours, obtains finished product.
2. a kind of production technology of water packet sand continuous phase coating according to claim 1, which is characterized in that the antifoaming agent Preparation method be:First, ointment is prepared, by the proportion ingredient of following component, in terms of weight part ratio, White Mineral Oil:White carbon:It is poly- Ether:Polyether polyol:Castor oil=(10-45) part:(2-10) part:(10-35) part:(10-30) part:(10-35) part;Then to Above-mentioned dispensing is added in reaction kettle equipped with stirring slurry, motor and heating system, will be uniformly mixed under dispensing room temperature, stirring 1 is small When blowing;80 parts of the ointment that above-mentioned Recipe is worked it out is taken, is added from newborn silicone oil, each 20 parts of tributyl phosphate, mixing 10 parts of emulsifier, stirs evenly, and 280 parts of water is then added and makes its phase inversion, and 16 parts of thickener is added after phase inversion is complete and is used for increasing Thick tune viscosity to 1500CS-2000CS, then discharging is packaged dress, you can obtains antifoaming agent.
3. a kind of production technology of water packet sand continuous phase coating according to claim 1, which is characterized in that the preservative Preparation method be:By the dodecyl benzyl dimethyl ammonium chloride of weight, myristyl benzyl dimethyl ammonium chloride, The composition of one or more of cetalkonium chloride and stearyl dimethyl benzyl ammonium chloride And didecyl Dimethy ammonium chloride is put into blender and is stirred, mixing time is 30-120 minutes;It needs to be added steady When determining agent, stabilizer is added in deionized water and is dissolved, the deionized water solution dissolved with stabilizer is then poured into institute It states in blender and is stirred, mixing time is 30-120 minutes;When only needing that deionized water is added, directly deionized water is fallen Enter and be stirred in the blender, mixing time is similarly 30-120 minutes;Then it is pumped into finished product after filtering, analyzing qualification Head tank, is put into clean empty bottle in Irrigation Machine or slack tank starts filling and screw capping to get to preservative.
CN201810361040.7A 2018-04-20 2018-04-20 A kind of production technology of water packet sand continuous phase coating Pending CN108690440A (en)

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CN201810361040.7A CN108690440A (en) 2018-04-20 2018-04-20 A kind of production technology of water packet sand continuous phase coating

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Application Number Priority Date Filing Date Title
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Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105505073A (en) * 2015-12-26 2016-04-20 铃鹿复合建材(上海)有限公司 Sand-in-water multicolor paint
CN107652726A (en) * 2017-10-30 2018-02-02 惠州市华昱美实业有限公司 A kind of stone-like coating and its preparation technology

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105505073A (en) * 2015-12-26 2016-04-20 铃鹿复合建材(上海)有限公司 Sand-in-water multicolor paint
CN107652726A (en) * 2017-10-30 2018-02-02 惠州市华昱美实业有限公司 A kind of stone-like coating and its preparation technology

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Application publication date: 20181023