CN108690439A - A kind of aqueous anti-muscle transparent priming and preparation method thereof that rises of pine - Google Patents
A kind of aqueous anti-muscle transparent priming and preparation method thereof that rises of pine Download PDFInfo
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- CN108690439A CN108690439A CN201810236338.5A CN201810236338A CN108690439A CN 108690439 A CN108690439 A CN 108690439A CN 201810236338 A CN201810236338 A CN 201810236338A CN 108690439 A CN108690439 A CN 108690439A
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- Prior art keywords
- muscle
- rises
- pine
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- transparent priming
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
- C09D133/04—Homopolymers or copolymers of esters
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/002—Priming paints
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/10—Transparent films; Clear coatings; Transparent materials
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
- C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
Abstract
The present invention relates to technical field of coatings, specifically disclose a kind of aqueous anti-muscle transparent priming and preparation method thereof that rises of pine.The priming paint, is counted in parts by weight, including following component:First water-based acrylic resin:35-47 parts, the second water-based acrylic resin:35-47 parts, coalescents:3-7 parts, levelling agent:0.1-0.5 parts, wetting agent:0.1-0.4 parts, antifoaming agent:0.1-0.6 parts, thickener:0.2-0.4 parts, water:4.4-10.6 part.The aqueous anti-muscle transparent priming that rises of pine provided by the invention, has excellent freeze-thaw resistance, grinability, and adhesive force is high, and storage stability is high, and the anti-muscle that rises is had excellent performance.
Description
Technical field
The present invention relates to technical field of coatings more particularly to a kind of pine aqueous anti-rise muscle transparent priming and its preparation sides
Method.
Background technology
Timber rises muscle or wood grain protrusion, is a phenomenon common in aqueous woodware paint application, and the muscle mechanism that rises is:
Timber needs to cut in process and play is cut, and inevitably cuts off or destroys the integrality of lumber fibre, work as timber
Fiber when being exposed, wood-fibred will suck moisture in timber as suction pipe, cause lumber fibre to expand, protrusion
In wood surface.
Pine color and luster is natural, and texture understands beauty, highly practical, durable, for ease of maintenaince.After furniture is made, fill
Divide and shows the true of material, natural beauty perception.Pine is wooden soft, and material is light, and furniture installation is moved all very convenient therefore loose
The wooden solid wood is the preferred material for manufacturing children furniture.But since pine is wooden soft, it is easy moisture to be drawn into timber, so loose
Wood is easy to the muscle that rises.Thus, it is ensured that in the coating process of pine, prevent pine from rising muscle.
Invention content
For existing pine be easy to rise muscle the problems such as, the present invention provides a kind of pine the aqueous anti-muscle transparent priming that rises.
Further, the present invention also provides a kind of preparation methods of the aqueous anti-muscle transparent priming that rises of pine.
To achieve the above object of the invention, the embodiment of the present invention uses the following technical solution:
A kind of aqueous anti-muscle transparent priming that rises of pine, the priming paint is counted in parts by weight, including following component:
Compared with the existing technology, the aqueous anti-muscle transparent priming that rises of pine provided by the invention, use acrylic emulsion at
Membrane substance has high osmosis and closure, can be combined rapidly with wood fiber component rapidly, then very fast solidification, therefore fiber
Will not expand or degrees of expansion weakens significantly, greatly improve water paint rise in construction muscle the problem of.
Further, the present invention also provides the preparation methods of the aqueous anti-muscle transparent priming that rises of the pine.The preparation method,
It at least includes the following steps:
(1) each component is weighed according to the proportioning of the aqueous anti-muscle transparent priming that rises of above-mentioned pine;
(2) first water-based acrylic resin, the second water-based acrylic resin, water, coalescents are carried out at batch mixing
Reason, obtains the first mixture;
(3) the first mixture, antifoaming agent, wetting agent, levelling agent are subjected to mixing treatment, obtain the second mixture;
(4) thickener is added in the second mixture, is stirred, obtain the aqueous anti-muscle transparent priming that rises of the pine.
Compared with the existing technology, the preparation method of the aqueous anti-muscle transparent priming that rises of pine provided by the invention, preparation method
Simply, process is easy to control, and facilitates industrialized production.
Specific implementation mode
In order to make the purpose , technical scheme and advantage of the present invention be clearer, with reference to embodiments, to the present invention
It is further elaborated.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, it is not used to
Limit the present invention.
The embodiment of the present invention provides a kind of pine the aqueous anti-muscle transparent priming that rises, and the priming paint is counted in parts by weight, including
Following component:
Compared with the existing technology, the aqueous anti-muscle transparent priming that rises of pine provided by the invention, use acrylic emulsion at
Membrane substance has high osmosis and closure, can be combined rapidly with wood fiber component rapidly, then very fast solidification, therefore fiber
Will not expand or degrees of expansion weakens significantly, greatly improve water paint rise in construction muscle the problem of.
Specifically, preferably described first water-based acrylic resin is the self-crosslinking acrylic lotion of nucleocapsid, glass
It is 23-27 DEG C to change temperature, solid content 42-47%.Second water-based acrylic resin is the selfing bipropenyl of nucleocapsid
Yogurt liquid, glass transition temperature are 43-47 DEG C, solid content 42-47%.
Glass transition temperature Tg (also referred to as glass state temperature) refers to the temperature that high polymer is changed into glassy state by elastic stage,
It is an important performance indexes of high polymer.High polymer demonstrates flexibility above this temperature, and high polymer table is put in the temperature
Reveal brittleness.Polymer emulsion is one kind of high polymer, and glass transition temperature reflects hardness after polymer emulsion forms film
Size.The resin of low Tg has excellent film forming, and coating is contributed to form a film.The resin of high glass transition temperature has
Good anti-muscle effect of rising, Anti- tarnishing effect is excellent, can meet loose wooden japanning requirement.Therefore two kinds of different glass are selected
The acrylic emulsion of temperature cooperates, and not only contributes to coating film forming, can also meet the requirement of the anti-muscle that rises.
Preferably, the coalescents are dipropylene, dipropylene glycol methyl ether, alcohol ester-12,2- amino-2-methyls-
At least one of 1- propyl alcohol.
At least one of above-mentioned coalescents are selected, not only improve gloss, the rub resistance of paint film, while to paint film
Surface drying is done solid work the time and is had an impact.
Preferably, the levelling agent is polyether-modified dimethyl silicone polymer.Preferred levelling agent can improve solution
Mobility, and can make paint film that there is slippery feel, while also there is high-compatibility, it can be compatible well with unclassified stores.Together
When the recoatability of lower one of finishing coat is had no adverse effect, and the levelling wetability of priming paint can be significantly improved.
Preferably, the antifoaming agent is polyether siloxane copolymer.
Polyether siloxane copolymer has the advantages that two kinds of antifoaming agent of ethers and organic silicon, and stability is good, low toxicity, antioxygen
Change, defoaming ability is high.
Preferably, the thickener is association type polyurethane thickener.
Association thickener makes macromolecular chain generate intramolecular and Interpolymer Association, is brought greatly to the rheological characteristic of aqueous solution
It influences, while the lipophilic group in associative thickener can adsorb emulsion particle and granules of pigments, forms physical mesh (crosslinking)
Structure, the reticular structure can gradually be destroyed in shearing field, therefore can be with the flowing property of control system.Such association
It disengages at high shear rates, viscosity is made to reduce, shearing is formed again after removing, and viscosity is made to restore, but the formation associated needs
The time is wanted, so the recovery of viscosity is fast unlike cellulose family, to give certain flowing time, is conducive to levelling,
Be conducive to the raising of gloss.
The present invention provide the pine it is aqueous it is anti-rise muscle transparent priming under the premise of, it is aqueous to still further provide the pine
The preparation method of the anti-muscle transparent priming that rises.
In any embodiment, which at least includes the following steps:
(1) each component is weighed according to the proportioning of the aqueous anti-muscle transparent priming that rises of above-mentioned pine;
(2) first water-based acrylic resin, the second water-based acrylic resin, coalescents are subjected to mixing treatment,
Obtain the first mixture;
(3) the first mixture, water, antifoaming agent, wetting agent, levelling agent are subjected to mixing treatment, obtain the second mixture;
(4) thickener is added in the second mixture, is stirred, obtain the aqueous anti-muscle transparent priming that rises of the pine.
Compared with the existing technology, the preparation method of the aqueous anti-muscle transparent priming that rises of pine provided by the invention, preparation method
Simply, process is easy to control, and facilitates industrialized production.
Explanation is further explained to above-mentioned preparation method below:
Specifically, preferably mixing treatment process described in step (2) is:By first water-based acrylic resin,
Two water-based acrylic resins stir 4-6min with the speed of 400-600rpm, and water is added under the speed of 700-900rpm,
Coalescents are added under the speed of 900-1200rpm, stir 15-20min.
It is mainly that system viscosity is larger to select the stirring at low speed of 400-600rpm, and stirring at low speed is not easy bubble stirring into body
In system, and high-speed stirred is readily incorporated bubble, and when viscosity is big, bubble is not easy to be precipitated, and can influence filming performance, so selection is low
Speed mixes the first water-based acrylic resin, the second water-based acrylic resin;Water is added in the speed of 700-900rpm, it is main
It wants to contain film forming matter in system, rate influences very much system performance soon, so selecting the stir speed (S.S.) that system is made to reach uniform effect
Fruit;The high-speed stirred of 900-1200rpm helps to disperse.
Mixing treatment process is described in step (3):Under the mixing speed of 800-1000rpm, by antifoaming agent, wetting
Agent, levelling agent are added sequentially in first mixture, are often added a kind of ingredient and are stirred 8- with the speed of 800-1000rpm
12min。
Preferably, mixing speed described in step (4) is 800-1200rpm, mixing time 13-17min.Select 800-
The speed of 1200rpm stirs, and is conducive to disperse.
Explanation is further explained to above-mentioned preparation method below:
It is provided in an embodiment of the present invention in order to better illustrate, it is illustrated below by embodiment is further.
Embodiment 1
The embodiment of the present invention provides a kind of pine the aqueous anti-muscle transparent priming that rises, and the priming paint is counted in parts by weight, including
Following component:First water-based acrylic resin:35 parts, the second water-based acrylic resin:47 parts, coalescents:7 parts, levelling agent:
0.5 part, wetting agent:0.4 part, antifoaming agent:0.6 part, thickener:0.2 part, water:9.3 part.
Above-mentioned first water-based acrylic resin is hold high high chemical industry (China) Co., Ltd 4298, glass transition temperature 25
DEG C, solid content 45%;Second water-based acrylic resin is hold high high chemical industry (China) Co., Ltd 4088, and glass transition temperature is
45 DEG C, solid content 45%;Coalescents are the mixture of 2 parts of dipropylene glycol methyl ethers, 4 dipropylenes, 1 part of alcohol ester 12;
Levelling agent is BYK346;Wetting agent is TEGO 270;The mixing for the TEGO 902W and 0.3 part of TEGO 825 that antifoaming agent is 0.3 part
Object;Thickener is COATEX high Thailands 2025.
The preparation method of the aqueous anti-muscle transparent priming that rises of above-mentioned pine, includes the following steps:
(1) each component is weighed according to the proportioning of the aqueous anti-muscle transparent priming that rises of above-mentioned pine;
(2) first water-based acrylic resin, the second water-based acrylic resin are stirred into 5min with the speed of 500rpm,
Water is added under the speed of 800rpm, coalescents are added under the speed of 1000rpm, stirs 15min, obtains the first mixing
Object;
(3) under the mixing speed of 1000rpm, antifoaming agent, wetting agent, levelling agent are added sequentially to first mixing
In object, often adds a kind of ingredient and 10min is stirred with the speed of 1000rpm, obtain the second mixture;
(4) thickener is added in the second mixture, mixing speed 1000rpm, mixing time 15min is obtained
The aqueous anti-muscle transparent priming that rises of the pine.
Embodiment 2
The embodiment of the present invention provides a kind of pine the aqueous anti-muscle transparent priming that rises, and the priming paint is counted in parts by weight, including
Following component:First water-based acrylic resin:42 parts, the second water-based acrylic resin:42 parts, coalescents:5 parts, levelling agent:
0.3 part, wetting agent:0.3 part, antifoaming agent:0.5 part, thickener:0.3 part, water:9.5 part.
Above-mentioned first water-based acrylic resin is hold high high chemical industry (China) Co., Ltd 4298, glass transition temperature 25
DEG C, solid content 45%;Second water-based acrylic resin is hold high high chemical industry (China) Co., Ltd 4088, and glass transition temperature is
45 DEG C, solid content 45%;Coalescents be 1 part of dipropylene glycol methyl ether, 2.5 dipropylenes, 1.5 parts of alcohol ester-12s it is mixed
Close object;Levelling agent is BYK346;Wetting agent is TEGO 270;The TEGO 902W and 0.3 part of TEGO 825 that antifoaming agent is 0.2 part
Mixture;Thickener is COATEX high Thailands 2025.
A kind of preparation method of the aqueous anti-muscle transparent priming that rises of above-mentioned pine is as described in Example 1, repeats no more.
Embodiment 3
The embodiment of the present invention provides a kind of pine the aqueous anti-muscle transparent priming that rises, and the priming paint is counted in parts by weight, including
Following component:First water-based acrylic resin:47 parts, the second water-based acrylic resin:38 parts, coalescents:6 parts, levelling agent:
0.3 part, wetting agent:0.4 part, antifoaming agent:0.3 part, thickener:0.4 part, water:9.3 part.
Above-mentioned first water-based acrylic resin is hold high high chemical industry (China) Co., Ltd 4298, glass transition temperature 25
DEG C, solid content 45%;Second water-based acrylic resin is hold high high chemical industry (China) Co., Ltd 4088, and glass transition temperature is
45 DEG C, solid content 45%;Coalescents are the mixture of 2 parts of dipropylene glycol methyl ethers, 2 dipropylenes, 2 parts of alcohol ester-12s;
Levelling agent is BYK346;Wetting agent is TEGO 270;TEGO 902W's that antifoaming agent is 0.15 part and 0.15 part of TEGO 825 is mixed
Close object;Thickener is COATEX high Thailands 2025.
A kind of preparation method of the aqueous anti-muscle transparent priming that rises of above-mentioned pine is as described in Example 1, repeats no more.
It, below will be real in order to better illustrate the characteristic of the aqueous anti-muscle transparent priming that rises of pine provided in an embodiment of the present invention
The aqueous anti-muscle transparent priming that rises of pine for applying the preparation of example 1,2,3 carries out performance detection, and test result is as shown in table 1.
1 the performance test results of table
From table 1, it is apparent that the aqueous anti-muscle transparent priming that rises of pine provided by the invention, has excellent freeze-thawing resistant
Property, grinability, adhesive force is high, and storage stability is high.
Further, anti-rise by muscle transparent priming according to following work by pine that 1-3 of the embodiment of the present invention is prepared is aqueous
Skill carries out application to deal board (40cm*60cm), and carries out anti-muscle performance test of rising.Above-mentioned technique includes the following steps:
(1) by deal board (40cm*60cm) deburring, first deal board is polished flat with 240# sand paper;
(2) the aqueous anti-muscle transparent priming even application that rises of pine that embodiment 1-3 is provided is polished flat in step (1)
Deal board on, wait for quietly 4 hours;
(3) again with 400# sand paper by step (2) through first spraying after deal board polish it is whole;
(4) one-component clear finish even application is waited for quietly 4 hours on through step (3) treated deal board;
(5) deal board in step (4) after second sprays polished with 600# sand paper again whole;
(6) one-component clear finish even application is waited for quietly 12 hours on through step (5) treated deal board, is seen
Deal board is examined to rise muscle effect.
It is anti-to rise that muscle test result is as follows shown in table 2.
Table 2
| Project | Embodiment 1 | Embodiment 2 | Embodiment 3 |
| The anti-muscle effect that rises | It is excellent | It is excellent | It is excellent |
From table 2 it can be seen that the aqueous anti-muscle transparent priming that rises of pine that 1-3 of the embodiment of the present invention is provided, has excellent
The anti-muscle effect that rises.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all essences in the present invention
Any modification, equivalent replacement or improvement etc., should all be included in the protection scope of the present invention made by within refreshing and principle.
Claims (10)
1. a kind of aqueous anti-muscle transparent priming that rises of pine, it is characterised in that:The priming paint, is counted in parts by weight, including such as the following group
Point:
2. the aqueous anti-muscle transparent priming that rises of pine as described in claim 1, it is characterised in that:The first water soluble acrylic acid tree
Fat is the self-crosslinking acrylic lotion of nucleocapsid, and glass transition temperature is 23-27 DEG C, solid content 42-47%.
3. the aqueous anti-muscle transparent priming that rises of pine as described in claim 1, it is characterised in that:The second water soluble acrylic acid tree
Fat is the self-crosslinking acrylic lotion of nucleocapsid, and glass transition temperature is 43-47 DEG C, solid content 42-47%.
4. the aqueous anti-muscle transparent priming that rises of pine as described in claim 1, it is characterised in that:The coalescents are dipropyl two
At least one of alcohol butyl ether, dipropylene glycol methyl ether, alcohol ester-12,2-amino-2-methyl-1-propanol.
5. the aqueous anti-muscle transparent priming that rises of pine as described in claim 1, it is characterised in that:The levelling agent is polyether-modified
Dimethyl silicone polymer.
6. the aqueous anti-muscle transparent priming that rises of pine as described in claim 1, it is characterised in that:The antifoaming agent is polyethers silica
Alkyl copolymer.
7. the aqueous anti-muscle transparent priming that rises of pine as described in claim 1, it is characterised in that:The thickener is poly- for association type
Urethane thickener.
8. a kind of preparation method of the aqueous anti-muscle transparent priming that rises of pine, it is characterised in that:It at least includes the following steps:
(1) each component is weighed according to the proportioning of the aqueous anti-muscle transparent priming that rises of the pine as described in any one of claim 1~7;
(2) first water-based acrylic resin, the second water-based acrylic resin, water, coalescents are subjected to mixing treatment, obtained
To the first mixture;
(3) the first mixture, antifoaming agent, wetting agent, levelling agent are subjected to mixing treatment, obtain the second mixture;
(4) thickener is added in the second mixture, is stirred, obtain the aqueous anti-muscle transparent priming that rises of the pine.
9. the preparation method of the aqueous anti-muscle transparent priming that rises of pine as claimed in claim 8, it is characterised in that:In step (2)
The mixing treatment process is:By first water-based acrylic resin, the second water-based acrylic resin with 400-600rpm's
Speed stirs 4-6min, and water is added under the speed of 700-900rpm, coalescents are added under the speed of 900-1200rpm,
Stir 15-20min;And/or
Mixing treatment process is described in step (3):Under the mixing speed of 800-1000rpm, by antifoaming agent, wetting agent, stream
Flat agent is added sequentially in first mixture, is often added a kind of ingredient and is stirred 8-12min with the speed of 800-1000rpm.
10. the preparation method of the aqueous anti-muscle transparent priming that rises of pine as claimed in claim 8, it is characterised in that:In step (4)
The mixing speed is 800-1200rpm, mixing time 13-17min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810236338.5A CN108690439A (en) | 2018-03-21 | 2018-03-21 | A kind of aqueous anti-muscle transparent priming and preparation method thereof that rises of pine |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810236338.5A CN108690439A (en) | 2018-03-21 | 2018-03-21 | A kind of aqueous anti-muscle transparent priming and preparation method thereof that rises of pine |
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| CN109370305A (en) * | 2018-10-26 | 2019-02-22 | 江门市新会区明洋化工实业有限公司 | A kind of water-based ink wear-resisting, water-fast, toughness is strong, transparency is high |
| CN109370306A (en) * | 2018-10-26 | 2019-02-22 | 江门市新会区明洋化工实业有限公司 | The anti-muscle water-based ink that rises of one kind |
| CN110317509A (en) * | 2019-07-30 | 2019-10-11 | 德美特涂料(北京)有限公司 | The preparation method of interior wall latex finishing coat suitable for mopping wallpaper |
| CN110423524A (en) * | 2019-08-01 | 2019-11-08 | 广东千叶松化工有限公司 | A kind of aqueous woodware varnish lacquer and preparation method thereof |
| CN110527426A (en) * | 2019-09-04 | 2019-12-03 | 浙江大风范家具股份有限公司 | A kind of solid wood furniture filling conduit coating at cement underseal bottom and preparation method thereof |
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| CN110527426A (en) * | 2019-09-04 | 2019-12-03 | 浙江大风范家具股份有限公司 | A kind of solid wood furniture filling conduit coating at cement underseal bottom and preparation method thereof |
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Application publication date: 20181023 |