CN108684997A - Containing protein beverage - Google Patents

Containing protein beverage Download PDF

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Publication number
CN108684997A
CN108684997A CN201711174029.1A CN201711174029A CN108684997A CN 108684997 A CN108684997 A CN 108684997A CN 201711174029 A CN201711174029 A CN 201711174029A CN 108684997 A CN108684997 A CN 108684997A
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China
Prior art keywords
cellulose
mass
protein beverage
beverage
protein
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CN201711174029.1A
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Chinese (zh)
Inventor
小籏晴子
山崎有亮
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Asahi Kasei Corp
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Asahi Kasei Kogyo KK
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Publication of CN108684997A publication Critical patent/CN108684997A/en
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    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/38—Other non-alcoholic beverages
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/52—Adding ingredients
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/52—Adding ingredients
    • A23L2/66—Proteins

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  • Health & Medical Sciences (AREA)
  • Nutrition Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Non-Alcoholic Beverages (AREA)
  • Dairy Products (AREA)
  • Beans For Foods Or Fodder (AREA)

Abstract

Containing protein beverage without what cohesion, presentation uniform appearance and astringent taste were inhibited the purpose of the present invention is to provide a kind of.The present invention is that one kind containing protein beverage, contains the cellulose of the protein of 0.2 mass % or more, the tannin of 1ppm or more and 0.01 mass % or more, and its loss tangent tan δ are below 3.

Description

Containing protein beverage
Technical field
The present invention relates to containing protein beverage.
Background technology
Back and forth, contain protein beverage (hereinafter, sometimes referred to as " protein beverage ".) due to can simply absorb work For the protein of one of nutritional ingredient, no matter so age and gender, are liked by most people.In recent years, due to increasing Protein content enjoys various tastes, so the food composition diversification as protein source, and into one The seasoning of its beverage of step ground is also diversified.In particular, with cocoa power, coffee, black tea, the seasoning such as smear tea and to mask protein only The beverage of special flavor and taste is loved.
Patent document 1 discloses emulsion stabilizer and its manufacture of a kind of cold-aseptic filling fallen flowers lactogenesis (peanut emulsion) beverage Method.Specifically, it discloses containing by microcrystalline cellulose, xanthans, sodium carboxymethylcellulose, glycerin monostearate, sucrose The peanut milk drink for the stabilizer that aliphatic ester, polyglyceryl fatty acid ester and citrus fruit fibres are formed.It is described, the peanut emulsion Beverage within the shelf-life without bleed and precipitation, quality and good mouthfeel.
Patent document 2 discloses a kind of chocolate and its manufacturing method containing red bean and milk composition.Specifically, It is middle to record, it is added with the raw material of specific ratios and is sought with special flavor with above-mentioned beverage made from particular step It supports and enriches, there is satisfactory stability.
Patent document 3 discloses a kind of coffee beverage and its manufacturing method containing bitter buckwheat and milk composition.Specifically, wherein It describes, is added with lactogenesis, coffee, buckwheat powder and other raw material with specific ratios, and on made from ad hoc approach Beverage is stated, long shelf-life has good flavor, mouthfeel and excellent stability.
[Xian Youjishuwenxian ]
[Zhuan Liwenxian ]
Patent document 1:Chinese patent application discloses No. 104489103 specification
Patent document 2:Chinese patent application discloses No. 104430897 specification
Patent document 3:Chinese patent application discloses No. 103749685 specification
Invention content
[Fa Mingsuoyaoxiejuewenti ]
Patent document 1 describes a kind of by adding the stabilizer containing microcrystalline cellulose to have excellent stability Peanut milk drink.However, in order to various seasonings are enjoyed with the peanut milk drink and when with seasonings such as cocoa, coffee, black tea, meeting There are problems that cohesion, deteriorated appearance occur.
Patent document 2 and 3, which discloses the protein beverage for using chocolate and coffee to season respectively, has excellent edible sense And stability.Although it is few and other effects to describe precipitation, fully appearance stability (no cohesion) is not studied.It is special Be not increase in these beverages cocoa, the content of coffee etc. when assigning dense taste, has the anxiety of cohesion deterioration.
On the other hand, it is known that tannin is cocoa power, coffee, black tea, smears in tea, part fruit (for example, grape, persimmon etc.) Ingredient, can with albumen qualitative response and form compound or salt or cause to agglomerate.In addition, due to tannin meeting when edible Generate astringent taste feel, so in protein beverage with cocoa power, coffee, black tea, smear the seasonings such as tea, fruit when, tax is made It is extremely difficult to give dense taste and the beverage of uniform appearance is presented and goes back while inhibiting astringent taste.
The present invention has been made in view of the above-described circumstances, provide it is a kind of without cohesion, uniform appearance and astringent taste be presented pressed down System contains protein beverage.
[The Shou Duan &#93 solved the problems, such as;
The present inventor is in depth studied in order to achieve the above objectives and repeatedly, as a result, it has been found that, it is drunk containing protein Cellulose is added in material and reduces loss tangent tan δ, uniform appearance can be presented, and inhibit astringent taste without cohesion, from And complete the present invention.
That is, the present invention includes following implementation.
First embodiment of the present invention contains the protein of 0.2 mass % or more, the list of 1ppm or more containing protein beverage Peaceful and 0.01 mass % or more cellulose, and loss tangent tan δ are below 3.
The above-mentioned storage shear modulus G ' (50) containing protein beverage at 50 DEG C is relative to the shearing energy storage at 25 DEG C The ratio between modulus G ' (25) (G ' (50)/G ' (25)) can be 0.8 or more, 3.0 or less.
Above-mentioned tannin can derive from least one kind of in cocoa, coffee, tea and fruit.
The above embodiment can also contain in beans, kind subclass and cereals at least containing protein beverage 1 kind.
[Fa Mingxiaoguo ]
According to the above embodiment, can provide it is a kind of without cohesion, be presented uniform appearance and what astringent taste was inhibited contains egg White matter beverage.
Specific implementation mode
< > containing protein beverage
Contain the protein of 0.2 mass % or more, the list of 1ppm or more containing protein beverage involved by present embodiment Peaceful and 0.01 mass % or more cellulose, and loss tangent tan δ are below 3.
Previous contains in protein beverage, can be solidifying due to occurring when using seasonings such as the coffee containing tannin, cocoas Poly-, precipitation, and there are problems that deteriorated appearance.In addition, assigning dense taste by increasing the content of cocoa, coffee etc. When, it can become strong from the astringent taste of tannin, there are problems that becoming difficult to drink.
And present embodiment contains protein beverage, by adding cellulose, and by loss tangent tan δ tune To 3 hereinafter, to without cohesion and precipitation, uniform appearance is presented, and astringent taste is inhibited.Furthermore it is possible to increase cocoa, coffee Deng content, assign dense taste, therefore be also good in terms of fragrance emission.
In addition, " cohesion " in this specification refers to, because of assembling containing ingredient for beverage, glomeration is formed, and is caused Beverage is inhomogenous, the state of the miscellaneous trace of color spot, spot occurs.
In addition, " astringent taste " in this specification is also referred to as astringent taste, refer to tongue, benumb in oral cavity or shouting pain as sense Feel.It is known that being attached to tongue, the situation on oral mucosa in oral cavity in above-mentioned complex or salt or their condensate Under, it is denaturalized by receptor present on tongue, oral mucosa, the friction with tongue, oral mucosa becomes larger, and is aware of astringent taste.
Contain protein beverage about present embodiment, containing tannin and while protein, loss tangent tan δ also 3 hereinafter, think the average grain diameter of the complex or salt or their condensate that are formed by tannin and protein accordingly It is relatively small by resting on, astringent taste can be inhibited.
&#91;Wu Xing &#93;
(loss tangent tan δ)
The loss tangent tan δ containing protein beverage of present embodiment are 3 hereinafter, it is preferred that 2.9 hereinafter, more excellent 2.8 are selected in hereinafter, further preferably 2.5 hereinafter, particularly preferably below 2.0.
By loss tangent tan δ in above-mentioned upper limit value hereinafter, so as to inhibit the cohesion of beverage, and provide Uniform appearance.
On the other hand, present embodiment containing in protein beverage, the lower limiting value of loss tangent tan δ has no especially It limits, such as can be in 0.5 or more (preferably 1.0 or more).
In addition, " storage shear modulus (G ') " in this specification refers to, strained to keeping giving to containing protein beverage When the storage shear modulus (G ') of stress accumulated of beverage inside measure gained person.
In addition, " loss tangent tan δ " is to indicate, keep to giving beverage inside when strain containing protein beverage Ratio (G "/G ') of the loss shear modulus (G ") for the stress accumulated relative to storage shear modulus (G ').
As the measurement method of loss tangent tan δ, pass through viscoelasticity measurement device (rheology scientific company (Rheometric Scientific, Inc.) is manufactured, ARESG2 types, geometry:Double-deck Ku Aite (the Double Wall Couette) type, temperature:25 DEG C of constant, angular speed:20rad/ seconds, strain:It is scanned in the range of 1 → 794%.), measurement is cut Storage modulus (G ') and loss shear modulus (G ") are cut, is obtained by calculating G "/G '.In addition, about beverage, do not make internal junction Structure destructively uses pipette, puts into inside unit at leisure, after standing 5 minutes, in dynamic strain (Dynamic Strain) under pattern, start measurement.Loss tangent tan δ in present embodiment refer to measuring and cutting at 25 DEG C Storage modulus (G ') and loss shear modulus (G ") are cut, the result that value when by strain 20% calculates.
(ratios of the storage shear modulus G ' (50) relative to the storage shear modulus G ' (25) at 25 DEG C at 50 DEG C (G'(50)/G'(25))
Present embodiment contains in protein beverage, and the storage shear modulus G ' (50) at 50 DEG C is relative at 25 DEG C The ratio between storage shear modulus G ' (25) (G ' (50)/G ' (25)) 3.0 hereinafter, it is preferred that 2.7 hereinafter, more preferably 2.5 with Under, further preferably 2.0 hereinafter, particularly preferably below 1.8.
By the G ' (50) containing protein beverage/G ' (25) of present embodiment in above-mentioned upper limit value hereinafter, so as to Keep the stability for being resistant to temperature change.Furthermore it is possible to have good fragrance emission.
On the other hand, present embodiment containing in protein beverage, the lower limiting value of G ' (50)/G ' (25) has no special limit It is fixed, such as can be in 0.8 or more (preferably 1.0 or more).
As the measurement method of G ' (50) and G ' (25), can by viscoelasticity measurement device (rheology scientific company manufactures, ARESG2 types, geometry:Like special type, temperature in the double-deck library:25 DEG C or 50 DEG C of constant, angular speed:20rad/ seconds, strain:1 → It is scanned in the range of 794%.) measure.In addition, about beverage, so that internal structure is destructively used pipette, put at leisure Inside unit, after standing 5 minutes, under dynamic strain pattern, start measurement.G ' (25)/G ' in present embodiment (50) refer to measuring the storage shear modulus G ' at 25 DEG C and 50 DEG C, the result that respective value when by strain 20% calculates.
(viscosity)
Present embodiment has mobility containing protein beverage, can not chew and drink.Present embodiment contains egg The viscosity of white matter beverage is preferably in 200mPas hereinafter, more preferably in 100mPas hereinafter, further preferably in 50mPas Hereinafter, particularly preferably in 30mPas or less.On the other hand, present embodiment containing in protein beverage, the lower limiting value of viscosity It is not particularly limited, such as can be 1mPas or more (preferably in 2.5mPas or more).
The viscosity of beverage can be used for example B shapes viscosimeter (eastern machine industry manufacture, BV-10M) etc. and measure.
Then, following explanation is carried out containing ingredient containing protein beverage to present embodiment.
&#91;Dan Baizhi &#93;
" protein " in this specification refers to, l-amino acid connects macromolecule chemical combination made of (polymerization) with chain majority Object.About protein, according to the number of the amino acid constituted, type or the sequence of bonding, type is different, from molecular weight About 4000 or so substance to from it is tens million of~hundred million unit substance multiple types exist.As long as the protein in present embodiment can It eats, also " polypeptide " of few " peptide ", peptide of the number including connected amino acid linearly to connect.In addition, this reality Animal can be derived from by applying the protein in mode, can derive from plant, they can also be applied in combination.Wherein, this reality It applies the protein in mode and is preferably derived from animal or the raw material containing milk composition from plant.
(raw material containing milk composition)
As " raw material containing milk composition " in this specification, also include from animal and in plant either one Raw material containing milk composition.
As the animal, such as ox, goat, sheep can be enumerated etc., however it is not limited to these.
As the plant, such as beans, kind subclass, cereals can be enumerated etc., however it is not limited to these.
As raw material containing milk composition, more specifically can for example enumerate:Milk, whole milk powder, skimmed milk power, condensed milk, breast Fat, whipping cream, condensed milk (Condensed Milk), Yoghourt, cheese etc. derive from the raw material containing milk composition of animal;Soya-bean milk etc. comes Derived from the raw material containing milk composition of beans, coconut milk, almond milk, peanut emulsion etc. from raw material containing milk composition, the congee of kind of subclass (Rice milk) etc. derives from the raw material containing milk composition etc. of plant from raw material containing milk composition of cereal etc., however it is not limited to this A bit.Raw material containing milk composition can also be solid either liquid.
Wherein, from easiness and ease of handling consideration is obtained, become containing for the source of the protein in present embodiment Milk composition raw material is preferably milk, whole milk powder, skimmed milk power, whipping cream, soya-bean milk, peanut emulsion, almond milk, big rice milk or coconut palm Sub- breast.On the other hand, from the aspect of health, preferably low-calorie and low cholesterol is former containing milk composition from plant Aftermentioned beans, kind subclass and cereals etc. can be used to derive from the raw material containing milk composition of plant for material.
(beans, kind subclass and cereals)
Preferably, also containing other than containing above-mentioned raw material containing milk composition containing protein beverage about present embodiment Have at least one kind of in beans, kind subclass and cereals.By containing them, while inhibiting the increase of calorie, Present embodiment can also further increase protein content containing protein beverage.Beans, kind subclass and cereals can be single Solely use, can also two or more be applied in combination.In addition, can also be used with above-mentioned material combination containing milk composition.
Beans
" beans " in this specification refers to the seed of edible legume.Beans contains a large amount of protein, is It is that plant can by the nitrogen being largely present in air transformation (immobilization) by the rhizobium being present in the root of legume Protein obtained from the form (for example, ammonia etc.) directly used in amino acid (protein) synthesis.As beans, specifically Such as it can enumerate:Chick-pea (Cicer arietinum), opens side hyacinth bean (chana dal), is small chick-pea (garbanzo) It is hyacinth bean, horse grain beans (masoor dal), pea, broad bean, lupin, leaf circular fan beans, Alpha Luna (ア Le Off ァ Le Na), big Beans, mung bean, blackgram (Vigna mungo), black soya bean (urad dal), red bean, climing red bean, soya bean, moth beans (moth bean), Pigeonpea, grass vetch, careless pea, rattan beans, goa bean, cowpea, Bang Bala peanuts (Bambarra groundnut), kidney bean, three Spend beans, hyacinth bean, certain herbaceous plants with big flowers beans, butter bean, Kidney bean (tepary bean), scarlet runner bean, Hua Dou, peanut, peanut etc., however it is not limited to These.Furthermore it is possible to a kind of these beans be used or two or more is applied in combination.
Wherein, consider from obtaining with ease of handling containing beans contained in protein beverage as present embodiment, It is preferred that chick-pea (Cicerarietinum), lens, broad bean, soybean, mung bean, red bean, peanut or peanut.
Beans shape can be the original shape of beans after drying, can also be the state after subtle crushing, It can be paste, can also be oily, however it is not limited to these.Wherein, from the point of view of ease of processing, beans shape is preferred For comminution, paste or oily.
Kind subclass
As " the kind subclass " in this specification, it is the edible seed covered by shell, compared with five cereals, beans, leads to Chang great little biggers, it is almost edible without culinary art (can be with nutrition intake) containing significant quantities of fat ingredient.As kind of a subclass, Specifically can for example it enumerate:Almond, peanut, Bertholletia excelsa, cashew nut, chestnut, coconut (pulp), the seed of flax, fibert, Australia Continent nut (macadamia nuts), hickory nut, pine nut, American pistachios (pistacchio), poppy capsule, sesame, sunflower kind Seed, walnut, strange sub- seed (Chia seed) etc., however it is not limited to these.Furthermore it is possible to by a kind of use of these kind of subclass or 2 kinds Combination of the above uses.
Wherein, hold from easiness is obtained with processing containing the kind subclass for including in protein beverage as present embodiment Easy property consideration, preferably almond, peanut, cashew nut, chestnut, fibert, Queensland nut, sesame, sunflower seed or walnut.
Kind subclass shape can be the original shape of seed after drying, can also be the state after subtle crushing, It can also be paste, can also be oily, however it is not limited to these.Wherein, from the point of view of ease of processing, subclass shape is planted Preferably comminution, paste or oily.
Cereals
As " cereals " in this specification, it is the edible portion of grain plants, generally refers to be referred to as grain (grain/kernel) part.As cereals, specifically can for example enumerate:Wheat, barley, rye, oat, rice, Brown rice, wild rice (wild rice), corn, Fu Niao meter (fonio), millet, broomcorn millet, sorghum, tongue bran (teff), triticale, amaranth Belong to (Amaranthus), buckwheat, quinoa (quinoa) etc., however it is not limited to these.Furthermore it is possible to by a kind of use of these cereals, Or two or more is applied in combination.
Wherein, hold from easiness is obtained with processing containing the cereals for including in protein beverage as present embodiment Easy property consideration, preferably wheat, barley, rye, oat, rice, brown rice or corn.
Cereals shape can be the original shape of seed after drying, can also be the state after subtle crushing, It can also be paste, can also be oily, however it is not limited to these.Wherein, from the point of view of ease of processing, the shape of cereals Shape is preferably comminution.
(content of protein)
The lower limiting value of the content containing the protein in protein beverage of present embodiment is more than 0.2 mass %, preferably More than 0.5 mass %, more preferably more than 1.0 mass %, further preferably more than 1.5 mass %.In addition, in this paragraph " content of protein " refers to, other than the type of protein, further include present embodiment contain protein beverage In include all protein summation.
Previous contains in protein beverage, in the case that the content of protein is more than above-mentioned lower limiting value, generates apparent Cohesion.And even if the content of the protein containing protein beverage of present embodiment more than above-mentioned lower limiting value, remains on inhibition The generation of cohesion, and obtain significant effect.
In addition, the upper limit value of the content containing the protein in protein beverage of present embodiment preferably 10 mass % with Under, more preferably in 8 mass % hereinafter, further preferably below 5 mass %.
By the content containing the protein in protein beverage of present embodiment in above-mentioned upper limit value hereinafter, so as to An adequate amount of protein is easily absorbed, and can become good and drink mouthfeel.
&#91;From the Dan Baizhi &#93 of plant;
On the other hand, it is preferable to use the albumen from plant of low-calorie and low cholesterol from the aspect of health Matter source.For example, aftermentioned beans, the kind raw material containing milk composition such as subclass and cereals or crushed material, paste, oil can be used Deng as protein source.In present embodiment, the albumen quality from plant is more than 0.2 mass %, preferably in 0.5 matter % or more is measured, more preferably more than 1.0 mass %, further preferably more than 1.5 mass %.
Previous contains in protein beverage, derives from situation of the content of the protein of plant more than above-mentioned lower limiting value Under, generate apparent cohesion.And even if the content of the protein containing protein beverage of present embodiment above-mentioned lower limiting value with On, the generation for inhibiting cohesion is remained on, and obtain significant effect.
In addition, the upper limit value of the content containing the protein in protein beverage of present embodiment preferably 10 mass % with Under, more preferably in 8 mass % hereinafter, further preferably below 5 mass %.
In addition, the method as the content containing the protein in protein beverage for measuring present embodiment, such as can arrange It enumerates:The method calculated by proportioning, or quantitative method etc. is carried out using known method.As the well known protein Quantitative approach, such as sour (Bicinchoninic Acid, the BCA) method of dihomocinchonine, Bradford methods, Lowry methods can be enumerated Deng, however it is not limited to these.
More specifically, for example, the quantitative approach of the protein measured by BCA methods can based on the reaction in 2 stages, with Following sequence carries out.First, in the 1st stage, by being bonded containing the peptide in protein beverage, bivalent cupric ion (Cu2+) gone back Originally it was univalent copper ion (Cu+).The Cu being reduced2+Amount it is proportional to the amount for the protein for including in solution.Then, the 2nd In stage, the BCA of 2 molecules is in Cu+Upper coordination is formed in the bluish violet complex that display absorbs by force at 562nm.By with light splitting Photometer measures it and carries out colorimetric assay, can quantify the content of the protein in beverage.More specifically, for example may be used To use the TaKaRaBCAProtein of precious wine brewing company manufacture to measure kit (TaKaRaBCAProtein Assay Kit), The content of protein in beverage is quantified.
&#91;Dan Ning &#93;
" tannin " in this specification refers to, derives from plant, is reacted with protein, alkaloid or metal ion, securely It is bonded and is formed the general name of the water soluble compound of indissoluble salt.Tannin generally existing in plant kingdom.In addition, tannin is that have The complicated aromatic compound of most phenolic hydroxyl group.As the raw-food material in the source as tannin, such as can enumerate Tea, cocoa, coffee, grape wine, fruit etc., however it is not limited to these.
Cocoa
" cocoa " in this specification is Malvaceae (Krona Qwest (Cronquist) system or new Engler (Engler) in system, snake woman belong to (Waltheria) section) evergreen tree, refer to be also known as cocoa chocolate tree (cacao tree), The substance of cocoa chocolate tree (cocoa tree).As the cocoa (cacao) in the source as the tannin in present embodiment, as long as Object is used as raw-food material, specifically can for example enumerate cocoa mass (cacao mass), cocoa butter (cocoa Butter), cocoa power, chocolate etc., however it is not limited to these.
Coffee
" coffee " in this specification refers to, the seed acquired from coffee tree.Coffee can be intact after producing The life beans of raw state can also be the baking beans after heated processing.No matter in addition, the type in the place of production of coffee, beans, as long as It is mixing gains.Can be the state after crushing in addition, the shape of coffee can be the original state of beans, it can be with It is the extracting solution of coffee, or can is gained person's (for example, the extracting solution of coffee is granulated and is made powdered etc.) after processing.
Tea
" tea " in this specification refers to being moved by the leaf of tea tree, stem, fruit, petal, root etc. or from Mycophyta Made of the machining object of object.As the tea in the source as the tannin in present embodiment, specifically can for example enumerate:It is green Tea, white tea, yellow tea, green tea, black tea, black tea, jasmine tea etc..Also include the outer tea of tea in addition, as the tea in present embodiment.Make For tea outside the tea, such as can enumerate:Wheat tea, native Changshan tea, balsam pear tea, coca tea (coca tea), Louis boss's tea (rooibos tea), silvenine tea, climing tea, Job's tears tea, citron tea, South Africa honey tree tea (honeybush tea), orange peel tea, fish Raw meat grass tea, Indocalamus leaf tea (Xiong Bamboo grass tea), bamboo tea, vanilla tea, kelp tea, plum kelp tea, Ilex paraguarensis (mate tea), buckwheat Tea, coffee senna tea, Sweet tea, purple perilla tea, arhat tea, mushroom tea etc..These tea can use a kind or two or more be applied in combination.
In addition, the shape of tea can be the original sample of tealeaves, it can be gained person after crushed, can be extracting solution, or Can be gained person's (for example, the extracting solution of tea is granulated and is made powdered etc.) after processing.
Wherein, the tea as the source as the tannin in present embodiment, from fragrance and to containing protein beverage The good consideration reconciled, preferably green tea, black tea or black tea.
Fruit
As " fruit " in the source as the tannin in present embodiment, as long as edible, particularly, not at Contain a large amount of tannin in ripe fruit.As fruit, specifically can for example enumerate:Oblonga, Chinese pear, Li, Quinces Quince (marmelo), the pomaceous fruits such as Western oblonga, the certain kind of berries in June (juneberry), Shipova, apple;U.S.'s cherry, apricot, plum, The kernel approaches such as cherry, tart fruit cherry (Prunuscerasus), blackthorn (Prunusspinosa), plum, peach;Almond, silver The shell fruits such as apricot, chestnut, walnut, hickory nut;Valencia orange, navel orange, blood orange, refined method orange (jaffaorange), bergamot (bergamot), chinotto, grape fruit, Orangelo, shaddock, bigarabe, bitter orange, sour tangerine (sudachi), lemon, flat real lemon Lemon, limette (lime), citron, bergamot, summer mandarin orange, eight north (hassaku), day to summer, Jia Bala citruses (jabara), Austria Blue shaddock (sweetie), do not know fiery (Dekopon), chicken tail shaddock (Cocktailfruit), she give mandarin orange, see clearly, the spring sees, bucket mandarin orange (tankan), Mo Kete (Murcott), Seminole (Seminole), ugly tangerine, tangelo (tangelo), pomelo, Manda are rather orange (Mandarinorange), the citruses such as satsuma orange, Ponkan, vertical flower tangerine (tachibana), discipline state mandarin orange, cherry island mandarin orange, golden mandarin orange Class;The evergreenness fruit such as olive, loquat, mountain peach;Cocoa, great Hua cocoas (cupuassu), durian (durian), star apple (star apple), miracle fruit (miracle fruit), fruit olive category (lucuma), tower Mali sieve (tree tomato;Tamarillo), Pineapple, banana, Qi Wanuo fruits (kiwano), papaya (papaya), babaco, mountain papaw (mountain papaya), waist Fruit, mango, Annona glabra (monkey apple;Pond apple), button mangosteen (button mangosteen), mammee (mammee apple), mangosteen, lemon drop mangosteen (lemon drop mangosteen), carambola (star fruit), Carissa carandas (conkerberry), the tropical fruit such as Malpighia coccigera (acerola), Nance, guava (guava), Garbo fruit (jaboticaba) Tree;The certain kind of berries classes such as Cranberry (cranberry), cowberry (bilberry), blackberry, blueberry, blueberry, raspberry;Akebi (akebia), without flower Fruit, persimmon, rasp berry, Kiwi berry (kiwifruit), thorny elaeagnus, mulberry, tongue peach, pomegranate, ape pears (tara vine), sea-buckthorn (seabuckthorn), Grossulariaceae (Grossulariaceae), jujube, Yu Li, gooseberry, grape, papaw (pawpaw), five Taste, Nanking cherry (Mei Tao;Prunustomentosa) etc., however it is not limited to these.These fruits can use a kind or 2 kinds with On be applied in combination.
Can also be jam shape, pureed, fruit juice in addition, the shape of fruit, can entirely use fresh fruit, will it is entire or After incision after partial desiccation or drying gained person or it is powdered (for example, fruit juice be granulated be made it is powdered, by fresh fruit It is entire carry out freeze-drying be made it is powdered etc.).
Wherein, the fruit as the source as the tannin in present embodiment, preferably certain kind of berries class, grape, persimmon, apple, Peach, banana or pineapple.
(content of tannin)
The lower limiting value of the content containing the tannin in protein beverage of present embodiment is in 1ppm or more, preferably in 20ppm More than, more preferably in 80ppm or more, further preferably in 125ppm or more.
By the content containing the tannin in protein beverage of present embodiment more than above-mentioned lower limiting value, so as to enjoy Changed by the taste containing protein beverage, in addition it can cover the unique aroma and flavor of protein.In addition, previous contains In protein beverage, in the case where tannin and protein coexist, they form complex, salt etc., cause to agglomerate.In contrast, this reality Even if applying the content of the tannin containing protein beverage of mode more than above-mentioned lower limiting value, the generation for inhibiting cohesion is remained on, and Obtain significant effect.
On the other hand, the upper limit value of the content containing the tannin in protein beverage of present embodiment is not particularly limited, Such as it can be in 6000ppm or less.By the content containing the tannin in protein beverage of present embodiment above-mentioned upper limit value with Under, so as to be difficult to feel the bitter taste and astringent taste from tannin, become the taste for being easy to drink.
In addition, the method as the content containing the tannin in protein beverage for measuring present embodiment, such as can enumerate Go out to use the LowenthalShi methods (permanganimetric method) etc. of photometric titration apparatus.The specific measurement of LowenthalShi methods Method can analyze book (Tokyo department of agriculture of university of empire chemurgy classroom/work) according to chemurgy and measure.
&#91;Xian Weisu &#93;
" cellulose " in this specification, in addition to the cellulose of the definition usually received according to those skilled in the art, The general name of the polysaccharide for the construction being formed by connecting with β 1-4 bondings with D- glucopyranoses is (hereinafter, otherwise referred to as " usually Cellulose ".) except, further include aftermentioned avicel cellulose complex and microfibre shape cellulose complex and they Mixture.
In addition, " cellulosic material " refers to, the substance containing cellulose in the raw material for including in containing protein beverage.It is fine The plain raw material of dimension is either the solid contents such as powdered, graininess, can also be that cellulose is made to be scattered in water-medium and obtain Dispersion liquid.
(physical property)
Average degree of polymerization
As the average degree of polymerization containing the cellulose for including in protein beverage of present embodiment, it is not particularly limited. In addition, the average degree of polymerization of cellulose can be according to basis"15th revision Japanese Pharmacopoeia"(the Japanese officina of the 15th correction Just) the reduced viscosity of the cupri-ethylene diamine solution described in the validation test (3) of the avicel cellulose of paraphrase sheet (distribution of Guang Chuan bookstores) Method measures.Wherein, when being measured according to the validation test of avicel cellulose (3), the range of the value of relative viscosity in conversion table When outer, according to the validation test (3) of cellulose powder, the sample initially weighed is changed to 0.25g, is carried out with similarly sequence It measures.
Shape of particle
The shape of particle containing the cellulose for including in protein beverage of present embodiment can be fine shape of particle.
In addition, shape of particle of the cellulose in aqueous dispersion can be measured by method as follows.First, Modulate the pure water suspension of the cellulose containing 0.1 mass %.Then, with high-shear homogenizing machine (homogenizer) (Japan's essence Machine manufactures, trade name " EXCELAUTO homogenizer ED-7 ", treatment conditions:Rotating speed 15,000rpm × 5 minute), it is allowed to Dispersion.Then, the aqueous dispersion of gained will be carried out with digit microscope (HIROX is manufactured, trade name " HIROXKH-1300 ") The major diameter (L) of particle image and the ratio (L/D) of minor axis (D) that shape is obtained when observing are set to the index of shape of particle, using work For 100~150 cellulose granules average value and counted value.In addition, the value of L/D is bigger, then mean fiber Element is more elongated shape.
Present embodiment containing the cellulose for including in protein beverage be minuteness particle shape in the case of, cellulose L/D is preferably 9 hereinafter, more preferably 7 hereinafter, further preferably 6 hereinafter, particularly preferably below 5.The L/D of cellulose is excellent Choosing is more than 1, more preferably 2 or more, further preferably 3 or more.Within the above range by the L/D of cellulose, to contain egg White matter beverage tends to be difficult to feel harsh feeling when edible, and it is excellent to cross larynx sense.
(cellulosic material)
Common cellulose
Common cellulose in present embodiment either by the acquisitions such as vegetation class, microorganism, animal natural fibre Dimension element, can also be chemically synthesized synthetic cellulose.As the native cellulose, such as can enumerate:Timber, bamboo, wheat Stalk, rice straw, cotton, ramie, bagasse, mestha, beet, ascidian, bacteria cellulose etc. containing cellulose from natural goods Cellulosic materials.It, among those, both can be with about present embodiment containing the common cellulose for including in protein beverage Using a kind, two or more use can also be mixed.As generally commercially available common cellulose, specifically can for example enumerate Go out:The common cellulose of the powder morphologies such as cellulose flock (cellulose flock), avicel cellulose is (hereinafter, sometimes Referred to as " cellulose powder ".).
Cellulose powder (the common cellulose of powder morphology)
" cellulose powder " in present embodiment refers to, to the alpha fibre obtained as paper pulp and from fibrous plant It after element is handled, refines, substance obtained from mechanicalness crushes.For example, being equivalent to"15th revision Japanese Pharmacopoeia" " cellulose powder " recorded in paraphrase sheet (distribution of Guang Chuan bookstores), the average degree of polymerization of cellulose powder are defined as being more than 440. As cellulose powder, specifically such as " the KCFLOCK series " that can enumerate Nippon Paper manufacture.
Avicel cellulose
" avicel cellulose " in present embodiment refers to the alpha fibre that will be obtained as paper pulp and from fibrous plant Element carries out part depolymerization with acid, carries out substance obtained from refining.For example, being equivalent to"15th revision Japanese Pharmacopoeia"Paraphrase " avicel cellulose " described in this (distribution of Guang Chuan bookstores).The average degree of polymerization of avicel cellulose preferably 350 hereinafter, in order to It is good with the harmonicity of other food materials, more preferably below 300.
The method of average degree of polymerization as control fiber element, can enumerate hydrolysis process etc..Pass through hydrolysis process, fiber Depolymerization occurs for the noncrystalline cellulose inside cellulose fiber matter, and average degree of polymerization becomes smaller.
The method of the hydrolysis process is such as can enumerate sour water solution, pyrohydrolysis, vapour explosion, microwave decomposition, not It is limited to these.These methods both may be used alone, two or more kinds can also be used.
In the acid-hydrolyzed method, for example, in the alpha-cellulose for making to obtain as paper pulp from fibrous plant point In the state of being dispersed in water-medium, Bronsted acid, carboxylic acid, lewis acid, heteropoly acid etc. are added in right amount, is heated while stirring, according to This can easily control average degree of polymerization.Although the reaction conditions such as temperature, pressure, time at this time are because of cellulose type, fibre The plain concentration of dimension, sour type, acid concentration and difference, but appropriate adjust to may achieve target average degree of polymerization.More specifically, Such as following condition can be enumerated:Using 2 mass % inorganic acid aqueous solutions below, under 100 DEG C or more, pressurization, processing is fine It ties up 10 minutes plain or more.When the condition, the catalyst components such as acid infiltrate into inside cellulose fibre, and hydrolysis is promoted, and is made Catalyst component content tails off, and refined also become thereafter is easy.
In addition, avicel cellulose and cellulose powder, state when it being made to be dispersed in water is different.If making cellulose point It dissipates in water, is ground with homogenizer, make dispersion liquid, visually observe the state and be compared, then in the moisture of avicel cellulose In dispersion liquid, the whole creams shape that White-opalescent is presented does not generate separation.In contrast, in the aqueous dispersions of cellulose powder In, separation is generated, supernatant and precipitation are separated into.
As the comparative approach of aqueous dispersions state, such as can be carried out by method as follows.First, measure water and Cellulose, so that content of cellulose becomes 10 mass %.Then, under 25 DEG C of atmosphere, TK homogeneous mixers are used (homomixer) (special machine chemical industry (strain) manufacture, " MARK II "), is stirred 10 minutes with 12,000rpm, makes and divide Dispersion liquid.Then, which is carried out at high pressure homogenizer (APV is manufactured, " Manton-Gaulin homogenizers ", pressure 15MPa) Reason.Then, the white suspension of gained is compared with the suspending stabilized state after being stood 1 hour at 25 DEG C.
Avicel cellulose powder
Above-mentioned avicel cellulose can be pulverulence.In this specification, " avicel cellulose powder " refers to crystalline fibers Element is through substance obtained from powdered, with " cellulose powder " different from.
Native cellulose as the raw material of avicel cellulose powder can derive from plant, animal or microorganism.Wherein, It is preferably derived from plant.As the plant, such as timber, bamboo, cotton, ramie, ascidian, bagasse, mestha, bacterium can be enumerated The cellulosic materials from natural goods containing cellulose such as cellulose.In above-mentioned cellulosic materials, a kind can be both used, It can also use and mix two or more and obtain person.
In addition, native cellulose uses preferably in the form of refined pulp.The process for purification of paper pulp is not particularly limited, example Any one of dissolving slurry, kraft pulp, NBKP paper pulp paper pulp can such as be used.
The average grain diameter (dry powder, secondary aggregation body) of avicel cellulose powder preferably 20 μm or more, 100 μm with Under.Within the above range by the average grain diameter of avicel cellulose powder, to contain beans, seed in containing protein beverage In the case of the solid constituents such as class, it can be easy to reconcile.
It, can be by dry powder, in secondary aggregation body in addition, the measurement method of the average grain diameter of avicel cellulose Under state, pass through the vibration of avicel cellulose powder, separation, method etc. of the measurement relative to the weight frequency of grain size on sieve The well known method measured of sieving carries out.Typically, first, by RO-TAP formulas vibrating sieving machine (manufactured by flat work, vibrating sieving machine (sieveshaker) A types), using JIS standard screens (Z8801-1987), sample 10g sieve within 10 minutes, is divided accordingly. Then, it is 50% grain size, the average grain of the drying powder as avicel cellulose by the accumulating weight in the size distribution of gained Diameter.
As the manufacturing method of avicel cellulose powder, such as can be by will be carried out through the native cellulose after hydrolysis process It dries and obtains.Both it can be separately separated in this case, from the reaction solution as obtained by hydrolysis process containing through hydrolysis The solid constituent of treated cellulose, makes it be dispersed in medium appropriate and modulates and obtain dispersion liquid, by the dispersion of gained Liquid is dried, can also be in the case where same hydrolysis solution forms cellulose dispersion liquid with direct state, by the dispersion Liquid convection drying.
In the manufacturing method of avicel cellulose powder, as make the solid containing the cellulose after hydrolysis process at Divide the medium used in the case of being subsequently dispersed in medium appropriate, is had no especially as long as industrial used substance It limits, at least any one in water and organic solvent can be used for example.As the organic solvent, can enumerate:Such as first The alcohols such as alcohol, ethyl alcohol, isopropanol, butanol, 2- methyl butanols, benzylalcohol;The hydro carbons such as pentane, hexane, heptane, hexamethylene;Acetone, second Ketones such as ylmethyl ketone etc..Wherein, as the organic solvent used as medium, the substance preferably used in pharmaceuticals, More preferably"Pharmaceuticals additive topical reference book 2000"The substance of solvent is classified as in (Yao Shi newspaper offices (strain) distribution).
For example, can make, containing the cellulose solids ingredient after hydrolysis process, first for the time being to be divided with a kind of medium After dissipating, the medium is removed, it is then made to be dispersed in different media.
In the manufacturing method of avicel cellulose powder, as the drying side of dispersion liquid that is allowed to be scattered in medium and modulate Method is not particularly limited.As the drying means, can enumerate:Such as freeze-drying (freeze-drying), spray drying, rotary drum do Dry, tray dried, pneumatic conveying drying, vacuum drying and organic solvent are carried out at the same time dry drying means etc..
The aqueous dispersions of cellulose
" aqueous dispersions of cellulose " in present embodiment refer to making the cellulose powder, the avicel cellulose Or the avicel cellulose powder decile dissipate in water obtained from solution.
The average grain diameter (primary particle (primary particle) diameter) of the aqueous dispersions of cellulose is preferably smaller than 50 μm, More preferably at 30 μm hereinafter, further preferably at 15 μm hereinafter, particularly preferably at 11 μm or less.Pass through the aqueous dispersions of cellulose Average grain diameter in above-mentioned upper limit value hereinafter, to when being added to containing in protein beverage, be easy uniform dispersion.Therefore, Can get be difficult to feel harsh feeling, cross larynx sense become good, mouldability it is excellent contain protein beverage.In addition, the water of cellulose In the case that the average grain diameter of dispersion liquid is more than above-mentioned upper limit value, is preferably adjusting the aqueous dispersions of cellulose and will be averaged in advance Grain size is adjusted to be added to containing the method in protein beverage in the state of above-mentioned upper limit value or less.
On the other hand, there is no particular limitation for the lower limiting value of the average grain diameter of the aqueous dispersions of cellulose, such as can be at 1 μm More than.
In addition, in this specification, " average grain diameter of the aqueous dispersion of cellulose " refers to the body relative to particle whole Product, the spherical conversion diameter of particle of the cumulative volume at 50%, also referred to as median particle diameter.
The measurement method of the average grain diameter of aqueous dispersion as cellulose, can be used for example method as follows into Row.First, the aqueous dispersions of the cellulose of 1 mass % of modulation are as sample.Then, for the sample of gained, by using sharp Optical diffraction scatters formula particle size distribution measurement device, and (for example, manufactured by the making of hole field, trade name " LA-910 ", ultrasonication 1 is divided Clock, refractive index 1.20) laser diffractometry, measure.Then, as described above, will be obtained by laser diffractometry The distribution of volume frequency granularity in be accumulated as 50% grain size as " average grain diameters of the aqueous dispersions of cellulose ".
In addition, the aqueous dispersions of cellulose used as sample in measuring, for example, can by method as follows into Row modulation.First, sample and pure water are measured in the SUS beakers of 2L capacity, so that solid component concentration is 1%, dispersion liquid Total amount is 1,500mL.Then, using the propeller(type)stirrer (agitator mixer) (Three- for being equipped with general stirring wing cross-shaped paddle (radius 35mm) One Motor, HEIDON manufactures, BL-600), at 25 DEG C, dispersion 20 minutes, modulation are carried out with 500rpm.
Avicel cellulose complex
" avicel cellulose complex " in this specification refers to the high water solubility in the avicel cellulose as principal component Molecule substance obtained from Composite.Herein, " Composite " refer to, the surface of avicel cellulose by chemical bonds such as hydrogen bonds, Form obtained from being coated through water soluble polymer.Therefore, avicel cellulose complex is not only by crystalline cellulose powder End and the mixed state of water soluble polymer, but the state on water soluble polymer covering avicel cellulose surface.Therefore, such as Fruit makes avicel cellulose complex be scattered in water-medium, then water soluble polymer is from avicel cellulose sur-face peeling, But the construction from the radial stretching, extension in surface is formed, it is in water colloidal.With the colloidal, existing avicel cellulose is multiple Zoarium can form higher-dimension reticular structure by interactions such as respective electrostatic repulsion, steric repulsion, Van der Waals forces.
" water soluble polymer " in this specification refers to hydrophilic macromolecule substance, in cold water and warm water at least The substance for dissolving or being swollen in either one.Herein, " hydrophily " refers to that there is a part to be dissolved in the ion exchange water of room temperature In characteristic.If quantitatively defining " hydrophily ", as described below.First, (pass through stirring-head etc.) under stirring, make water solubility Macromolecule 0.05g is dissolved in the ion exchange water of 50mL, until balance.Then, it is handled with the membrane filter in 1 μm of aperture When, by content of the ingredient of the membrane filter in water soluble polymer more than 1 mass % when, judgement have it is hydrophilic Property.
The keratinization of cellulose from each other when having the function of preventing dry due to water soluble polymer, so and water Avicel cellulose composite bulk phase after soluble macromolecular complex is for other powder, it is easier to which uniform mixing is also more held It is easily dispersed in water-medium.Therefore, present embodiment containing in protein beverage, in order to can further easy equably will Cellulose is blended in other raw materials containing protein beverage, and preferably comprises avicel cellulose complex.
As the avicel cellulose for forming complex, either microfibre shape, can also be microgranular.Wherein, make To form the avicel cellulose of complex, preferably microgranular, more preferably L/D is in 9 particles below, further preferably L/ D is still more preferably L/D in 6 particles below in 7 particles below, and particularly preferably L/D is in 5 particles below.
In addition, preferably being crystallized containing the avicel cellulose complex for including in protein beverage as present embodiment The complex of cellulose and water-soluble polysaccharides.
As the water-soluble polysaccharides, can enumerate:Such as xanthans, Karaya Gum (karaya gum), gellan gum, Psyllium seed gum (psyllium seed gum), locust bean gum (locust bean gum), guar gum, enzyme decompose guar gum, sieve Shop sign in the form of a streamer glue (tamarind seed gum), Wen Quince glue (quince seed gum), tara gum (tara gum), yellow alpine yarrow Glue, Arabic gum (arabic gum), arabogalactan, ghatti gum (ghatti gum), curdlan (curdlan), Carrageenan (carrageenan), furcellaran (furcellaran), pulullan polysaccharide (pullulan), glucan (dextran), glucomannans (glucomannan), agar, gelatin, indigestible dextrins, pectin (pectin), poly- grape Sugared (polydextrose), soluble soybean polysaccharide class, chitosan, azotobacter vinelandii glue, alginic acid and its salt, fiber Plain derivative etc..
Can be any one of HM pectin and LM pectin as the pectin.
As the alginate, can enumerate such as sodium alginate, calcium alginate, propylene glycol alginate.
As the cellulose derivative, it is fine that such as sodium carboxymethylcellulose, calcium carboxymethylcellulose, methyl can be enumerated Dimension element, hydroxypropyl cellulose and hydroxyethyl cellulose etc..
About the water-soluble polysaccharides for forming complex with avicel cellulose, they can both be used with a kind, can also be 2 kinds It is used in combination above.
Wherein, as the water-soluble polysaccharides for forming complex with avicel cellulose, preferably anionic property polysaccharide.One As, " anionic property polysaccharide " refers to, when being dispersed or dissolved in water, cation dissociation, its own becomes anion Substance.Anionic property polysaccharide is easy and cellulose Composite, so the avicel cellulose complex of gained is suspending stabilized Property it is high.Therefore, the avicel cellulose is easy to mix with containing the uniform component in protein beverage, and it is good to can get larynx sense Beverage, so be suitable.
As the anionic property polysaccharide, can enumerate:Such as xanthans, Karaya Gum, psyllium seed gum, gellan gum, Carrageenan, alginic acid, sodium alginate, calcium alginate, sodium carboxymethylcellulose, calcium carboxymethylcellulose, HM pectin, LM fruits Glue etc..About these anionic property polysaccharides, both can with only a kind with avicel cellulose carry out Composite, can also combine 2 kinds with Upper and avicel cellulose carries out Composite.
Wherein, as anionic property polysaccharide, preferably xanthans, Karaya Gum, gellan gum or sodium carboxymethylcellulose.
As the content of the avicel cellulose in avicel cellulose complex, preferably more than 20 mass %, 99 mass % Hereinafter, more preferably more than 30 mass %, 99 mass % hereinafter, further preferably more than 40 mass %, 95 mass % hereinafter, Particularly preferably more than 50 mass %, 95 mass % are hereinafter, most preferably more than 60 mass %, 90 mass % or less.
In addition, the content as the water soluble polymer in avicel cellulose complex, preferably more than 1 mass %, 80 Quality % is hereinafter, more preferably more than 1 mass %, 70 mass % are hereinafter, further preferably more than 2 mass %, 60 mass % Below.
Within the above range by the content of avicel cellulose and water soluble polymer, to avicel cellulose and water solubility High molecular Composite is easy to be promoted, and in containing protein beverage, can inhibit cohesion and the precipitation of avicel cellulose.
As the manufacturing method of avicel cellulose complex, such as can be manufactured by following methods:In compounding procedure, Apply mechanical shear stress to avicel cellulose and water soluble polymer makes water solubility while making avicel cellulose miniaturization Macromolecule is in avicel cellulose surface recombination.When the miniaturization of avicel cellulose, it can also add other than water soluble polymer Other additives etc..In particular, hydroaropic substance, it both can be in avicel cellulose and water soluble polymer Composite Process is added together, can also be added after forming complex.The mixture obtained in compounding procedure can be dried when necessary. About present embodiment containing the avicel cellulose complex added in protein beverage, pass through above-mentioned mechanical shearing, Either undried substance, can also be substance after drying.
As the method for application mechanical shear stress, such as the method being kneaded using kneading machine etc. may be appropriately used Deng.As the kneading machine, kneader, extruder, planetary-type mixer, mixing and kneading machine etc. can be enumerated, either continous way, It can also be interval (Batch) formula.These kneading machines both can be used alone, can also machine of more than two kinds be applied in combination.This A little kneading machines are suitably selected according to progress such as tack requirements in various uses.
The temperature when mixing of cellulose and water soluble polymer is not particularly limited, preferably 20 DEG C or more, 100 DEG C with Under, more preferably in 30 DEG C or more, 100 DEG C hereinafter, further preferably at 50 DEG C or more, 100 DEG C or less.Pass through temperature when mixing Within the above range, so as to be easy to promote avicel cellulose grind and Composite with water soluble polymer.In addition, because The deterioration of water soluble polymer is inhibited caused by heat, can obtain the crystalline fibers for foring the high reticular structure of density Plain complex.In addition, because be kneaded when Composite reaction, friction etc. due tos adstante febre, can also while except it is hot while be kneaded.In order to control Temperature can carry out casing cooling, heat release etc. except heat.
Solid component content when mixing is preferably more than 20 mass %, further excellent more preferably more than 30 mass % 35 mass % or more are selected in, particularly preferably more than 40 mass %.Pass through solid component content when mixing in above-mentioned lower limiting value More than, it is transferred to mixture to which mixing energy becomes easy, Composite is promoted.
On the other hand, the upper limit value of solid component content when mixing is not particularly limited, but preferably 90 mass % with Under, more preferably in 70 mass % hereinafter, further preferably below 60 mass %.Pass through solid component content when mixing upper Upper limit value is stated hereinafter, so as to be fully kneaded, obtains uniform kneaded state.
In addition, in order to which solid component content to be adjusted in above range, as the opportunity point of addition water, work can be kneaded Necessary amount is carried out before sequence adds water, and water can also be added during compounding procedure, can also separate part from whole amount of water, Add water before and during compounding procedure in this two benches.
In addition, in the manufacturing method of avicel cellulose complex, when drying the mixture obtained by above-mentioned compounding procedure, Drying side well known to tray drying, spray drying, belt drying, fluidized bed drying, freeze-drying, microwave drying etc. can be used Method.
Preferably, when mixture is supplied to drying process, water is not added in mixture, maintains consolidating for compounding procedure Body constituent concentration, is supplied to drying process.The moisture content of avicel cellulose complex after drying be preferably 20 mass % hereinafter, More preferably in 15 mass % hereinafter, further preferably below 10 mass %.Pass through the avicel cellulose complex after drying Moisture content in above-mentioned upper limit value hereinafter, to become difficult to generate it is tacky, addle the problems such as and carry or transport in cost The problem of.
On the other hand, the lower limiting value of the moisture content of the avicel cellulose complex after drying is preferably more than 1 mass %, more It is preferred that more than 1.5 mass %.By the moisture content of the avicel cellulose complex after drying more than the lower limiting value, to It can prevent by dispersed deterioration caused by over-drying.
In addition, the avicel cellulose complex obtained after drying process, preferably crushes processing, becomes powder shaped. Wherein, in the case where using spray drying as drying means, since dry and powdered can be carried out at the same time, so do not have Necessity crushes processing.
In the case where that will be crushed through dried avicel cellulose complex, can be used for example cutting type pulverizer, Method well known to beater grinder, pin bar disintegrator (pin mill), jet pulverizer etc..As degree of grinding, through powder Broken treated substance is more preferable all by the sieve in 425 μm of aperture preferably all by the sieve of aperture 1mm, and powder Average particle size (weight average particle diameter) is broken at 10 μm or more, 250 μm or less.
The hydroaropic substance of on-macromolecular substance
As present embodiment containing the cellulose contained by protein beverage, either the object being only made of cellulose Matter can also be the purpose for raising to the dispersibility of water-medium, and also contain non-high score while containing cellulose The substance of the hydroaropic substance of sub- substance.The hydroaropic substance is as the disintegration when making cellulose be scattered in water-medium Agent or water guide agent play a role.Therefore, before being mixed with the raw material other than containing protein beverage, in advance by cellulose It is mixed with hydroaropic substance, by adding the cellulose coated through hydroaropic substance, cellulose becomes easier to accordingly Disperse in containing protein beverage.
As present embodiment containing the cellulose contained by protein beverage, cellulose and water-soluble polysaccharide are preferably comprised The avicel cellulose complex of class, the hydroaropic substance with on-macromolecular substance.
In this specification, " hydroaropic substance of on-macromolecular substance " refers to, high to the dissolubility of cold water, hardly brings The organic substance of viscosity.As the hydroaropic substance of on-macromolecular substance, specifically can for example enumerate:Glucidtemns adds The relatively low polysaccharide of work starch equimolecular quantity;Oligofructose (oligofructose), galactooligosaccharide (oligo- Galactose), oligomeric maltose (oligo-maltose), oligoisomaltose (oligo-isomaltose), lactose, malt The oligosaccharides such as sugar, sucrose, alpha-cyclodextrin, beta-cyclodextrin, gamma-cyclodextrin;The monosaccharides such as glucose, fructose, sorbose;Malt Glycitols such as sugar alcohol, D-sorbite, antierythrite etc..
As the glucidtemns, dextrin class can be enumerated.
As the producing starch, can enumerate:Acetylation hexane diacid-crosslinked starch, acetylated oxidized starch, acetylation Phosphoric acid crosslinked starch, starch Sodium Octenyl Succinate, amylcose acetate, hydroxyalkylation phosphoric acid crosslinked starch, hydroxyalkylated starch, phosphorus Sour crosslinked starch, phosphoric acid esterification phosphoric acid crosslinked starch, sodium starch glycol, starch phosphate sodium etc..
In addition, the starch as the raw material as these producing starch, can be αization processing gains, can also be portion Divide αization to process gains, can also be non-alpha machining object.
Wherein, as the cellulose in present embodiment contained by hydroaropic substance, be preferably selected from glucidtemns and One or more of producing starch, is more preferably selected from one or more of dextrin and producing starch, further preferably dextrin and plus Both work starch.
In addition, present embodiment containing the cellulose contained by protein beverage be not with water soluble polymer complex When the cellulose of change, although little by little, due to the function as water soluble polymer, and particularly preferably containing paste Essence.
In addition, the content of the hydroaropic substance relative to cellulose, it is contemplated that the type of cellulose, the kind of hydroaropic substance Class etc. can be adjusted suitably to the degree that will not interfere dispersibility and its stability in water-medium.
(content of cellulose)
The lower limiting value of the content containing the cellulose in protein beverage of present embodiment is more than 0.01 mass %, preferably More than 0.05 mass %, more preferably more than 0.15 mass %, further preferably more than 0.20 mass %.
By the content containing the cellulose in protein beverage of present embodiment more than the lower limiting value, so as to The uniform eyed structure of cellulose is formed in the beverage, so can inhibit to agglomerate and precipitate, forms uniform appearance.Further Ground can become difficult to feel the astringent taste from tannin.
On the other hand, the upper limit value of the content containing the cellulose in protein beverage of present embodiment has no special limit It is fixed, such as can be below 3.00 mass %.By the content containing the cellulose in protein beverage of present embodiment above-mentioned Upper limit value is hereinafter, so as to be made the beverage of good larynx sense excessively, tongue sense of touch.
&#91;Qi Tacailiao &#93;
It can include the substance of act set forth below as other materials containing protein beverage about present embodiment.
(rutin)
Present embodiment can also contain rutin containing protein beverage.
The molecular formula of rutin is with C27H30O16It indicates, β-rutin is combined on the 3rd of quercetin (quercetin) oxygen The flavonoids glycosides of sugared (rutinose) (6-O- α-L- rhamnopyranosyl (rhamnosyl)-β-D-Glucoses) (flavonoid glycoside).In the flavonoids of the polyphenol with strength antioxidation, also referred to as vitamin P.Rutin is water-soluble.
It is 1.8mg or less in the preferably every 100mL of the content containing the rutin in protein beverage of present embodiment.Pass through this The content containing the rutin in protein beverage of embodiment in above-mentioned upper limit value hereinafter, to from rutin bitter taste by Inhibit, the good beverage of taste can be made.
High performance liquid chromatography can be used for example in the content of rutin, and as the HPLC of its an example, (Tianjin Island System makees manufactured 870UV type UV, visible lights spectrophotometric detector, the Luo Danni (Rheodyne) that LC-6A pumps, Japan's branch school industry manufacture are manufactured 7125 syringe, Island Jin System make manufactured Chromatpac CR4A data processing equipments) it measures.
As specific measurement method, first, 3 water salt 54.4mg of rutin (is dissolved in methanol by rutin standard solution 50mL gains are made), with the mixed solution (methanol of methanol, water and 0.5M oxalic acid:Water:Oxalic acid=5 0.5M:44:1) it carries out Dilution makes calibration curve from the height at peak by its 40 μ L injection HPLC according to Absolute Calibration curve method.Then, reed will be contained For the sample 10g weighings of fourth in the eggplant type flask of 200mL, addition methanol 50mL is heated to reflux 60 points in 90 DEG C of water-bath Clock.Then, after cooling, in the volumetric flask of 100mL, addition methanol is so that total amount is 100mL, under conditions of 2500rpm, from The heart detaches 5 minutes.Then, it takes supernatant 10mL in the eggplant type flask of 100mL, solvent is carried out to be dried under reduced pressure solidification, it will be residual After staying object to be dissolved in 0.5mL methanol, with 0.01M oxalic acid 5mL and the mixed solution (methanol of methanol, water and 0.5M oxalic acid: Water:Oxalic acid=25 0.5M:24:1) 10mL is dissolved out.Then, dissolution fluid is carried out being dried under reduced pressure solidification, it will with methanol 0.5mL After residue dissolving, 0.01M oxalic acid is added so that total amount 5.0mL.Then, it using HPLC, in the same manner as titer, surveys The height at amount peak can find out content according to calibration curve.
(stabilizer)
Present embodiment can also contain thickening polysaccharide containing protein beverage.As the thickening polysaccharide, can enumerate Go out:Such as locust bean gum, guar gum, tamarind gum, Karaya Gum, chitosan, Arabic gum, agar, Irish moss are poly- Sugar, alginic acid, sodium alginate, HM pectin, LM pectin, azotobacter vinelandii glue, xanthans, curdlan, pulullan polysaccharide, Portugal are poly- Sugar, gellan gum, gelatin, cellulose derivative are (for example, sodium carboxymethylcellulose, calcium carboxymethylcellulose, methylcellulose, hydroxyl Propyl cellulose, hydroxyethyl cellulose etc.), dextrin, starch etc..These thickening polysaccharides can use a kind or two or more group It closes and uses.
Wherein, hold from the reconciliation with beverage containing the thickening polysaccharide for including in protein beverage as present embodiment Easy property consideration, preferably guar gum, Karaya Gum, Arabic gum, carrageenan, xanthans, gellan gum or carboxymethyl cellulose Plain sodium.
(other materials)
Present embodiment can contain other materials other than the above containing protein beverage.As other materials, as long as It is edible ingredient, for the purpose of seasoning, preservation etc., additive can be enumerated.As other materials, can enumerate Go out:Such as the grease types such as vegetable oil, animal oil, vegetable constituent, meat ingredient, mushroom constituent, starch, seasoning, emulsifier, table Face activating agent, resistance to deposits modifier, antiseptic, disintegrant, antifoaming agent, foaming agent, food fiber, fortification at thickening polysaccharide Agent, pH adjusting agent, fragrance, antioxidant, acid flavoring, swelling agent, pigment etc..As the seasoning, salt, Portugal can be enumerated The carbohydrates such as grape sugar, fructose, granulated sugar, sweetener, sugar alcohol, various extracts, amino acid etc., onion, clear soup (consomm é), sauce Oil, salt, spice etc..
As long as the content of these materials does not damage the effect in present embodiment, there is no limit, can be from the balance of fragrance Equal considerations are suitably adjusted.
Manufacturing method >s of the < containing protein beverage
As the manufacturing method containing protein beverage of present embodiment, it is not particularly limited.For example, raw material are thrown Enter in water, is stirred manufacture.More specifically, for example, first, mixed raw material input is adjusted to 80 DEG C in advance Temperature water in.Then, using Three-One Motor, make the uniform dispersion of the mixed liquor.Then, pressure type homogenizer (Manton-Gaulin homogenizers) can manufacture present embodiment accordingly by homogenizing under the pressure of 20MPa Containing protein beverage.Further, it for long-term preservation, can both sterilize, and can also be filled to and preserve in container.
(preserving container)
As the preservation container containing protein beverage of filling present embodiment, it is not particularly limited.For example, can enumerate Go out the vessel such as glass, mug;Polyethylene terephthalate (Polyethyleneterephthalate with lid: PET container, tank, bottle, paper bag, the Freezing cup etc.) manufactured, but it is not limited to these.Wherein, as container is preserved, due to that can grow Phase preserves, so container, tank or paper bag that preferably the PET with lid is manufactured, due to inhibiting the with obvious effects of cohesion, therefore And the container of more preferably PET manufactures.
&#91;Shi Shili &#93;
In conjunction with following embodiments etc., the present invention will be described.But these do not limit the scope of the invention.
< < evaluation method > >
In Examples 1 to 9 and comparative example 1~4 as follows it is obtained containing protein beverage evaluation method is as follows It is shown.
Loss tangent tan δ >s of the < containing protein beverage
Loss tangent tan δ containing protein beverage are measured, are found out as shown below.
First, after beverage obtained being preserved 1 day at 25 DEG C, pass through viscoelasticity measurement device (rheology scientific company Manufacture;ARESG2 types;Geometry:Double-deck Ku Aite (the Double Wall Couette) type;Temperature:25 DEG C constant;Angle speed Degree:20rad/ seconds;Strain:It is scanned in the range of 1 → 794%.), measure storage shear modulus (G ') at 25 DEG C and Loss shear modulus (G ").In addition, about beverage, using pipette without destroying internal structure, put into inside unit at leisure, After standing 5 minutes, under dynamic strain pattern, start to measure.Then, from the storage shear modulus at 25 DEG C obtained (G ') and loss shear modulus (G ") calculates G "/G ' i.e. loss tangent tan δ.
Gs ' (50) of the < containing protein beverage/G ' (25) >
G ' (50) containing protein beverage/G ' (25) is measured, is found out as described below.
First, after beverage obtained being preserved 1 day at 25 DEG C and 50 DEG C, pass through viscoelasticity measurement device (rheology section Company manufactures;ARESG2 types;Geometry:Like special type in the double-deck library;Temperature:25 DEG C constant or 50 DEG C constant;Angular speed: 20rad/ seconds;Strain:It is scanned in the range of 1 → 794%.), measure the storage shear modulus (G ') at 25 DEG C and 50 DEG C. In addition, about beverage, using pipette without destroying internal structure, put into inside unit at leisure, after standing 5 minutes, Under dynamic strain pattern, start to measure.The value of the storage shear modulus G ' at 25 DEG C and 50 DEG C when then, by strain 20% Respectively as G ' (25), G ' (50), it is calculated than (G ' (50)/G ' (25)).
Cohesion >s of the < containing protein beverage
The cohesion containing protein beverage is checked by visual observation, is based on following 4 benchmark ratings.
◎:Nothing;○:A part of a small amount of generation;△:It is a small amount of on the whole to generate;×:It is a large amount of on the whole to generate
Precipitation >s of the < containing protein beverage
The precipitation containing protein beverage is checked by visual observation, is based on following 4 benchmark ratings.
◎:Nothing;○:A part of a small amount of generation;△:It is a small amount of on the whole to generate;×:It is a large amount of on the whole to generate
Fragrance emission >s of the < containing protein beverage
By 20 years old~50 years old 5 group members of men and women, examination by sensory organs is implemented to the fragrance emission containing protein beverage. Evaluation criteria is based on following 4 benchmark ratings.In addition, in 5 Team Conference spokesmans, most answers is evaluation result.
◎:It is excellent;○:It is slightly excellent;△:It is slightly poor;×:Difference
Astringent taste >s of the < containing protein beverage
By 20 years old~50 years old 5 judging panels of men and women, examination by sensory organs is implemented to the astringent taste containing protein beverage.Evaluation criteria Based on following 4 benchmark ratings.In addition, in 5 Team Conference spokesmans, most answers is evaluation result.
◎:It is excellent (not puckery);○:It is slightly excellent (less puckery);△:It is slightly poor (slightly puckery);×:Poor (puckery)
&#91;Embodiment 1&#93;Manufacture containing protein beverage 1
(1) manufacture of avicel cellulose complex A
After commercially available DP paper pulp is shredded, in the hydrochloric acid of 2.5mol/L, after being hydrolyzed 15 minutes at 105 DEG C, water is carried out It washes, filter, the cellulose for the wet cake shape that manufacture solid constituent is 55%.Average degree of polymerization is 220.Then, by the fibre of wet cake shape Dimension is plain and as water-soluble carboxymethyl cellulose (carboxymethyl cellulose;CMC commercially available CMC-Na) is (sub- assorted Blue (Ashland) manufacture, FL-9A, degree of substitution 0.93), be with cellulose/water solubility CMC=85/15, solid component concentration The mode of 48% (being adjusted with ion exchange water) is put into two axis kneading machines (DSM Xplore manufactures, Compounder15), with 393 (s of shear velocity-1) be kneaded 12 minutes, obtain avicel cellulose complex A.In addition, the disposable full doses of water solubility CMC Input.Melting temperature is 70 DEG C.
(2) manufacture containing protein beverage 1
Then, manufacture contains protein beverage.Formula:Oat (japanese food manufacture) is 2 mass %;Soya-bean milk (text manufacture of recording) For 1 mass %;Avicel cellulose complex A is 0.01 mass %;Cocoa power (VANHOUTEN) is 0.5 mass %;Granulated sugar is 5 Quality % (the first sugar industry).In these raw materials, the powder material that is pre-mixed other than soya-bean milk.In addition, using ion exchange water, adjust It is whole extremely to amount to 100 mass %.As manufacturing method, first, in the ion exchange water for being heated up to 80 DEG C, come into operation Three- One Motor (HEIDEN is manufactured, BL-600), with the 500rpm powder materials being obtained by mixing while stirring and soya-bean milk, stirring 5 Minute.Using pressure type homogenizer (Manton-Gaulin homogenizers, SMT manufactures), primary pressure processing is carried out with 15MPa to it, Secondary pressure processing is carried out with 5MPa.Further, using UHT sterilization machines, sterilization 60 seconds is carried out at 140 DEG C, manufacture contains egg White matter beverage 1.
Protein content containing protein beverage 1 is 0.5 mass %, and tannin 20ppm, loss tangent tan δ are 1.3, G ' (50)/G ' (25) is 0.84, and it is zero to agglomerate, and is precipitated as △, fragrance emission △, astringent taste zero.The above results such as 1 institute of table Show.
&#91;Embodiment 2&#93;Manufacture containing protein beverage 2
Using the avicel cellulose complex A obtained in (1) of embodiment 1, manufacture contains protein beverage.Formula:Knot Crystalline cellulose complex is 0.08 mass %;Skimmed milk power (Seichin manufacture) is 1 mass %;Peanut powder (MINOYA (body room) Manufacture) it is 3 mass %;Cocoa power (VANHOUTEN) is 0.5 mass %;Granulated sugar is 5 mass % (the first sugar industry).These powders Raw material is pre-mixed.In addition, using ion exchange water, adjust to 100 mass % of total.As manufacturing method, first, heating Into 80 DEG C of ion exchange waters, the Three-One Motor that come into operation (HEIDEN is manufactured, BL-600) are stirred with the sides 500rpm Powder raw material obtained from side is pre-mixed are mixed, are stirred 5 minutes.Use pressure type homogenizer (Manton-Gaulin homogeneous Machine, SMT manufactures), primary pressure processing is carried out with 15MPa to it, secondary pressure processing is carried out with 5MPa.Further, it is killed using UHT Bacterium machine, carries out sterilization 60 seconds at 140 DEG C, and manufacture contains protein beverage 2.
Protein content containing protein beverage 2 is 1.1 mass %, and tannin 20ppm, loss tangent tan δ are 2.7, G ' (50)/G ' (25) is 1.9, is agglomerated for △, is precipitated as zero, fragrance emission zero, astringent taste zero.The above results are as shown in table 1.
&#91;Embodiment 3&#93;Manufacture containing protein beverage 3
Using the avicel cellulose complex A obtained in (1) of embodiment 1, manufacture contains protein beverage.Formula:Knot Crystalline cellulose complex is 0.16 mass %;Skimmed milk power (Seichin manufacture) is 4 mass %;Peanut powder (MINOYA manufactures) is 8 Quality %;Cocoa power (VANHOUTEN manufactures) is 0.5 mass %;Granulated sugar is 5 mass % (the first sugar industry).These powder materials It is pre-mixed.In addition, using ion exchange water, adjust to 100 mass % of total.As manufacturing method, using same with embodiment 2 The method of sample, manufacture contain protein beverage 3.
Protein content containing protein beverage 3 is 3.5 mass %, and tannin 20ppm, loss tangent tan δ are 2.4, G ' (50)/G ' (25) is 1.5, and it is zero to agglomerate, and is precipitated as zero, fragrance emission zero, astringent taste zero.The above results are as shown in table 1.
&#91;Embodiment 4&#93;Manufacture containing protein beverage 4
Using the avicel cellulose complex A obtained in (1) of embodiment 1, manufacture contains protein beverage.Formula:Knot Crystalline cellulose complex is 0.16 mass %;Whole milk powder (Seichin manufacture) is 10 mass %;Soy meal (ball rice (Marukome) Manufacture) it is 6.4 mass %;Cocoa power (VANHOUTEN manufactures) is 0.5 mass %;Granulated sugar is 5 mass % (the first sugar industry).This A little powder materials are pre-mixed.In addition, using ion exchange water, adjust to 100 mass % of total.As manufacturing method, use Method similarly to Example 2, manufacture contain protein beverage 4.
Protein content containing protein beverage 4 is 4.8 mass %, and tannin 20ppm, loss tangent tan δ are 2.8, G ' (50)/G ' (25) is 1.3, and it is zero to agglomerate, and is precipitated as zero, fragrance emission ◎, astringent taste zero.The above results are as shown in table 1.
&#91;Embodiment 5&#93;Manufacture containing protein beverage 5
Using the avicel cellulose complex A obtained in (1) of embodiment 1, manufacture contains protein beverage.Formula:Knot Crystalline cellulose complex is 0.2 mass %;Skimmed milk power (Seichin manufacture) is 2 mass %;Peanut powder (MINOYA manufactures) is 4 matter Measure %;Cocoa power (VANHOUTEN manufactures) is 2 mass %;Granulated sugar is 5 mass % (manufacture of the first sugar industry).These powder materials It is pre-mixed.In addition, using ion exchange water, adjust to 100 mass % of total.As manufacturing method, using same with embodiment 2 The method of sample, manufacture contain protein beverage 5.
Protein content containing protein beverage 5 is 1.7 mass %, and tannin 81ppm, loss tangent tan δ are 1.4, G ' (50)/G ' (25) is 2.2, agglomerates for ◎, is precipitated as ◎, fragrance emission zero, astringent taste ◎.The above results are as shown in table 1.
&#91;Embodiment 6&#93;Manufacture containing protein beverage 6
Using the avicel cellulose complex A obtained in (1) of embodiment 1, manufacture contains protein beverage.Formula:Knot Crystalline cellulose complex is 0.2 mass %;Skimmed milk power (Seichin manufacture) is 2 mass %;Peanut powder (MINOYA manufactures) is 4 matter Measure %;Coffee (AGF manufactures) is 1 mass %;Granulated sugar is 5 mass % (manufacture of the first sugar industry).These powder materials are pre-mixed. In addition, using ion exchange water, adjust to 100 mass % of total.As manufacturing method, using method similarly to Example 2, Manufacture contains protein beverage 6.
Protein content containing protein beverage 6 is 1.7 mass %, and tannin 125ppm, loss tangent tan δ are 1.6, G ' (50)/G ' (25) is 1.8, agglomerates for ◎, is precipitated as ◎, fragrance emission ◎, astringent taste ◎.The above results such as table 1 It is shown.
&#91;Embodiment 7&#93;Manufacture containing protein beverage 7
Using the avicel cellulose complex A obtained in (1) of embodiment 1, manufacture contains protein beverage.Formula:Knot Crystalline cellulose complex is 0.2 mass %;Skimmed milk power (Seichin manufacture) is 2 mass %;Peanut powder (MINOYA manufactures) is 4 matter Measure %;Black tea (Lipton (Lipton) manufacture) is 3 mass % as tealeaves;Granulated sugar is 5 mass % (manufacture of the first sugar industry).These In raw material, the powder material that is pre-mixed other than black tea.In addition, using ion exchange water, adjust to 100 mass % of total.Make For manufacturing method, first, in the ion exchange water for being heated to 90 DEG C, input black tea is as tealeaves, so as to add up to 3 matter % is measured, is extracted, black tea liquid is obtained.Then, in the black tea liquid for being heated up to 80 DEG C, come into operation Three-One Motor (HEIDEN is manufactured, BL-600) is stirred 5 minutes with the 500rpm powder materials being obtained by mixing while stirring and soya-bean milk.It uses Pressure type homogenizer (Manton-Gaulin homogenizers, SMT manufacture) carries out primary pressure processing to it with 15MPa, with 5MPa into The secondary pressure processing of row.Further, using UHT sterilization machines, sterilization 60 seconds is carried out at 140 DEG C, manufacture contains protein beverage 7。
Protein content containing protein beverage 7 is 1.7 mass %, and tannin 330ppm, loss tangent tan δ are 1.8, G ' (50)/G ' (25) is 1.5, agglomerates for ◎, is precipitated as ◎, fragrance emission ◎, astringent taste ◎.The above results such as table 1 It is shown.
&#91;Embodiment 8&#93;Manufacture containing protein beverage 8
Using the avicel cellulose complex A obtained in (1) of embodiment 1, manufacture contains protein beverage.Formula:Knot Crystalline cellulose complex is 0.2 mass %;Skimmed milk power (Seichin manufacture) is 2 mass %;Peanut powder (MINOYA manufactures) is 4 matter Measure %;Coffee (AGF manufactures) is 5 mass %;Granulated sugar is 5 mass % (manufacture of the first sugar industry).These powder materials are pre-mixed. In addition, using ion exchange water, adjust to 100 mass % of total.As manufacturing method, using method similarly to Example 2, Manufacture contains protein beverage 8.
Protein content containing protein beverage 8 is 1.7 mass %, and tannin 6,000ppm, loss tangent tan δ are 2.2, G ' (50)/G ' (25) is 1.9, agglomerates for ◎, is precipitated as zero, fragrance emission ◎, astringent taste △.The above results such as table 1 It is shown.
&#91;Embodiment 9&#93;Manufacture containing protein beverage 9
Using the avicel cellulose complex A obtained in (1) of embodiment 1, manufacture contains protein beverage.Formula:Knot Crystalline cellulose complex is 3 mass %;Skimmed milk power (Seichin manufacture) is 2 mass %;Peanut powder (MINOYA manufactures) is 4 matter Measure %;Cocoa (VANHOUTEN manufactures) is 3 mass %;Granulated sugar is 5 mass % (manufacture of the first sugar industry).These powder materials are pre- First mix.In addition, using ion exchange water, adjust to 100 mass % of total.As manufacturing method, using similarly to Example 2 Method, manufacture contain protein beverage 9.
Protein content containing protein beverage 9 is 1.7 mass %, and tannin 125ppm, loss tangent tan δ are 0.8, G ' (50)/G ' (25) is 2.7, agglomerates for ◎, is precipitated as ◎, fragrance emission ◎, astringent taste zero.The above results such as table 1 It is shown.
&#91;Table 1&#93;
&#91;Comparative example 1&#93;Manufacture containing protein beverage 10
Without using the avicel cellulose complex A obtained in (1) of embodiment 1, manufacture contains protein beverage.Formula: Avicel cellulose complex is 0 mass %;Skimmed milk power (Seichin manufacture) is 2 mass %;Peanut powder (MINOYA manufactures) is 4 matter Measure %;Cocoa (VANHOUTEN manufactures) is 3 mass %;Granulated sugar is 5 mass % (manufacture of the first sugar industry).These powder materials are pre- First mix.In addition, using ion exchange water, adjust to 100 mass % of total.As manufacturing method, using similarly to Example 9 Method, manufacture contain protein beverage 10.
Protein content containing protein beverage 10 is 1.7 mass %, and tannin 125ppm, loss tangent tan δ are 0.4, G ' (50)/G ' (25) be 0.5, agglomerate for ×, be precipitated as ×, fragrance emission be ×, astringent taste be ×.The above results such as table 2 It is shown.
&#91;Comparative example 2&#93;Manufacture containing protein beverage 11
As the replacement of the avicel cellulose complex A obtained in (1) of embodiment 1, used with the amount of 0.3 mass % Gellan gum (LT-100, three Rong Yuan F.F.I. manufactures), manufacture contains protein beverage.Formula:Gellan gum is 0.3 mass %;Degreasing Milk powder (Seichin manufacture) is 2 mass %;Peanut powder (MINOYA manufactures) is 4 mass %;Cocoa (VANHOUTEN manufactures) is 3 matter Measure %;Granulated sugar is 5 mass % (manufacture of the first sugar industry).These powder materials are pre-mixed.In addition, using ion exchange water, adjust It is whole extremely to amount to 100 mass %.As manufacturing method, using method same as comparative example 1, manufacture contains protein beverage 11.
Protein content containing protein beverage 11 is 1.7 mass %, and tannin 125ppm, loss tangent tan δ are 4.8, G ' (50)/G ' (25) is 0.6, agglomerate for ×, be precipitated as △, fragrance emission is ×, astringent taste is ×.The above results such as table 2 It is shown.
&#91;Comparative example 3&#93;Manufacture containing protein beverage 12
By the avicel cellulose complex A obtained in (1) of embodiment 1 and gellan gum (LT-100, three Rong Yuan F.F.I. Manufacture) it is used in combination, manufacture contains protein beverage.Formula:Avicel cellulose complex is 0.08 mass %;Gellan gum is 0.2 matter Measure %;Skimmed milk power (Seichin manufacture) is 2 mass %;Peanut powder (MINOYA manufactures) is 4 mass %;Cocoa (VANHOUTEN systems Make) it is 3 mass %;Granulated sugar is 5 mass % (manufacture of the first sugar industry).These powder materials are pre-mixed.In addition, being handed over using ion Water is changed, is adjusted to 100 mass % of total.As manufacturing method, using method same as comparative example 1, manufacture is drunk containing protein Material 12.
Protein content containing protein beverage 12 is 1.7 mass %, and tannin 125ppm, loss tangent tan δ are 3.5, G ' (50)/G ' (25) is 0.9, is agglomerated for △, is precipitated as △, fragrance emission is ×, astringent taste is ×.The above results such as table 2 It is shown.
&#91;Comparative example 4&#93;Manufacture containing protein beverage 13
Using the avicel cellulose complex A obtained in (1) of embodiment 1, cocoa is not added, manufacture is drunk containing protein Material.Formula:Avicel cellulose complex A is 0.2 mass %;Skimmed milk power (Seichin manufacture) is 2 mass %;Peanut powder (MINOYA manufactures) is 4 mass %;Granulated sugar is 5 mass % (manufacture of the first sugar industry).These powder materials are pre-mixed.In addition, Using ion exchange water, adjust to 100 mass % of total.As manufacturing method, method same as comparative example 1, manufacture are used Containing protein beverage 13.
Protein content containing protein beverage 13 is 1.7 mass %, and tannin 0ppm, loss tangent tan δ are 1.1, G ' (50)/G ' (25) is 1.0, is agglomerated for ◎, is precipitated as △, fragrance emission is ×, astringent taste zero.Containing protein beverage 13 due to Without tannin, therefore without agglomerating, astringent taste is also less felt, but fragrance emission is poor, precipitation is more.
&#91;Table 2&#93;
By Tables 1 and 2 it is found that in containing protein and tannin containing protein beverage, by adding cellulose, and Loss tangent tan δ are less than 3.5 (preferably below 3.0), to without cohesion and precipitation, show uniform appearance, and Astringent taste, further fragrance emission can be inhibited also good.
&#91;Chan Yeshangkeliyongxing &#93;
Present embodiment is the cohesion of protein and tannin and the beverage that precipitation is suppressed containing protein beverage.Separately Outside, present embodiment contains protein beverage, and since fragrance emission is good, the astringent taste from tannin is suppressed, so quotient Product value is high.

Claims (8)

1. one kind containing protein beverage, which is characterized in that
The tannin of protein, 1ppm or more containing 0.2 mass % or more and the cellulose of 0.01 mass % or more, and
Loss tangent tan δ are below 3.
2. according to claim 1 contain protein beverage, which is characterized in that the protein is derived from selected from beans, kind At least one kind of raw material containing milk composition in subclass and cereals.
3. protein beverage according to claim 1, which is characterized in that contain 0.2 mass % or more, 10 mass % or less Plant-derived protein.
4. according to claim 1 contain protein beverage, which is characterized in that the cutting at 50 DEG C containing protein beverage Cut storage modulus G ' (50) relative to the ratio between storage shear modulus G ' (25) at 25 DEG C G ' (50)/G ' (25) 0.8 or more, 3.0 following.
5. according to claim 2 contain protein beverage, which is characterized in that the cutting at 50 DEG C containing protein beverage Cut storage modulus G ' (50) relative to the ratio between storage shear modulus G ' (25) at 25 DEG C G ' (50)/G ' (25) 0.8 or more, 3.0 following.
6. according to claim 3 contain protein beverage, which is characterized in that the cutting at 50 DEG C containing protein beverage Cut storage modulus G ' (50) relative to the ratio between storage shear modulus G ' (25) at 25 DEG C G ' (50)/G ' (25) 0.8 or more, 3.0 following.
7. containing protein beverage according to according to any one of claims 1 to 6, which is characterized in that the tannin is derived from and is selected from It is at least one kind of in cocoa, coffee, tea and fruit.
8. containing protein beverage according to according to any one of claims 1 to 6, which is characterized in that also contain selected from beans, kind It is at least one kind of in subclass and cereals.
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Application publication date: 20181023