CN108671866A - A kind of industrial chemicals reaction unit and reaction method - Google Patents
A kind of industrial chemicals reaction unit and reaction method Download PDFInfo
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- CN108671866A CN108671866A CN201810554835.XA CN201810554835A CN108671866A CN 108671866 A CN108671866 A CN 108671866A CN 201810554835 A CN201810554835 A CN 201810554835A CN 108671866 A CN108671866 A CN 108671866A
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- drain pipe
- revolving part
- tube
- reative cell
- room
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
- B01J19/0013—Controlling the temperature of the process
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/0066—Stirrers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B9/00—Cleaning hollow articles by methods or apparatus specially adapted thereto
- B08B9/02—Cleaning pipes or tubes or systems of pipes or tubes
- B08B9/027—Cleaning the internal surfaces; Removal of blockages
- B08B9/032—Cleaning the internal surfaces; Removal of blockages by the mechanical action of a moving fluid, e.g. by flushing
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B9/00—Cleaning hollow articles by methods or apparatus specially adapted thereto
- B08B9/08—Cleaning containers, e.g. tanks
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
- B01J2219/00092—Tubes
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- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Treatment Of Fiber Materials (AREA)
Abstract
The invention discloses a kind of industrial chemicals reaction units of chemical reaction technical field,Including pedestal,The base top offers motor room,Reative cell is installed at the top of the pedestal,The reative cell surface wrap has constant warm tube,It is provided with tapping room at the top of the woven hose,The tapping chamber surface is provided with feeding device,Chamber is provided with drain pipe in the tapping room,Drain pipe surface upper end is provided with screw element,The drain pipe surface is provided with force-applying piece,The drain pipe surface offers liquid-leaking nozzle,The infusion bottom of the tube is mounted on helix tube,It is connected with lower revolving part at the top of the electric machine rotational axis,It is installed with transmission gear at the top of the upper revolving part bottom and lower revolving part,The present invention is convenient for adjusting reaction temperature,Liquid outlet quantity is more accurate,It ensure that reaction effect,Upper revolving part and lower revolving part direction of rotation are opposite,It ensure that the mixing effect of reaction solution.
Description
Technical field
The present invention relates to chemical reaction technical field, specially a kind of industrial chemicals reaction unit and reaction method.
Background technology
When making industrial chemicals, majority is produced by chemical reaction, and certain reactions need specific reaction temperature, have
A little reactions need to carry out at a certain temperature, and traditional temperature control mode is obtained by agent burns when needing higher temperature
Heat, this heating mode, temperature are extremely unstable, it is difficult to control, and temperature distribution is uneven, traditional reaction solution manually thing
It first controls and adds, this mode accuracy is low, and efficiency is slow, affects production efficiency, and traditional agitating mode is artificial
Stirring, this agitating mode are time-consuming and laborious, it is difficult to stir evenly, agitating device on the market is also mostly single revolving part, rotation
Mode is single, is easy that reaction solution is made to form whirlpool, so that reactant is deposited on bottom, keep stirring uneven.
A kind of novel chemical industrial chemicals reaction units of Chinese patent CN201620969553.2, including pedestal, motor,
Shell and air-heater；Pedestal is arranged on the ground；Be provided on pedestal motor fixing frame, reaction unit fixed frame, air box and
Clinker case；Motor fixing frame is set on the base；Reaction unit fixed mount setting is on pedestal；Air box is set on the base,
And air-heater is provided in air box, and air box and pedestal are fixed together；Clinker case is set on the base；Motor setting exists
In motor fixing frame, although reactant can be made to reach required temperature, heating tube heating effect is limited, it is difficult to homogeneous heating.
Invention content
The purpose of the present invention is to provide a kind of industrial chemicals reaction unit and reaction methods, to solve above-mentioned background technology
The problem of middle proposition.
To achieve the above object, the present invention provides the following technical solutions：A kind of industrial chemicals reaction unit, including pedestal,
The base top offers motor room, is provided with motor, the position that the base top is kept right in the motor room straight up
It installs and is equipped with mounting plate, water pump is installed on the left of the mounting plate, reative cell, the reative cell are installed at the top of the pedestal
Surface wrap has constant warm tube, the constant warm tube upper end to connect pump outlet, and the constant warm tube lower end connects pump intake, institute
It states constant temperature pipe surface and the position of water pump is provided with heating device, there are two structure is identical defeated for reative cell top setting
Liquid pipe, and run through reative cell at the top of woven hose, it is provided with tapping room at the top of the woven hose, the tapping room and woven hose connect
Support device is connect, the support device is arranged in base top, and the tapping chamber surface is provided with feeding device, the tapping room
Inner cavity is provided with drain pipe, and tapping ceiling portion is run through at the top of the drain pipe, and tapping room bottom is run through in the drain pipe lower end, and
Drain pipe lower end is plugged on infusion tube cavity upper end, and the woven hose inner cavity top is fixedly installed rubber ring, the rubber ring
Inner wall fits with drain pipe surface, and drain pipe surface upper end is provided with screw element, and connection tapping room at the top of screw element
Inner cavity top, the drain pipe surface are provided with force-applying piece, and the drain pipe surface offers liquid-leaking nozzle, the infusion bottom of the tube
It is mounted on helix tube, and helix tube fits with reaction chamber wall, the electric machine rotational axis is through reative cell bottom center of circle position
It sets, the reative cell bottom is equipped with sealing ring, and electric machine rotational axis runs through sealing ring, is connected at the top of the electric machine rotational axis
Lower revolving part, the lower fixing piece of lower revolving part top connection, the lower fixing piece are mounted on reaction chamber wall, the reative cell
Inner wall is equipped with upper fixing element, and fixed part bottom is equipped with revolving part, the upper revolving part bottom and lower revolving part
Top is installed with transmission gear, and the transmission gear is mutually twisted, and the reative cell left bottom is provided with outlet tube,
The outlet tube runs through reative cell left side wall, and the outlet tube surface is equipped with liquid valve close to one end of reative cell.
Preferably, the support device includes clamping ring, and the clamping ring is mounted on tapping chamber surface, the clamping ring back of the body
Face is connected with support column, and the support column is arranged in base top rearward position, and the woven hose surface crown is equipped with solid
Determine ring, the fixed ring back side is equipped with extension arm, and the extension arm other end connects support column.
Preferably, the upper revolving part includes rotary shaft, and there are five the identical rotations of structure for the rotating shaft surface installation
Support arm, and the identical rotating arm of five structures is in same level, and the identical rotating arm of five structures circumferentially type
Arrangement, the one end of the rotating arm far from support column is equipped with stirring sheet.
Preferably, the screw element inner cavity is provided with screw thread, and drain pipe surface is provided with and matches outer spiral shell with screw element
Line.
Preferably, the drain pipe surface is provided with the identical indicator of three structures, and the identical instruction of three structures
Needle is parallel with liquid-leaking nozzle bottom, and the tapping chamber surface is provided with scale, and scale is as unit of ten milliliters.
Preferably, the feeding device upper end is funnel-form, and tapping room table wall is run through in the feeding device lower end.
Preferably, a kind of industrial chemicals reaction unit and reaction method include the following steps：
S1. force-applying piece is rotated, so that drain pipe is increased by screw element, liquid-leaking nozzle is made to rise to extreme higher position, confirms that liquid valve is
Closed state checks transmission gear occluding relation, starts water pump, the water in constant warm tube is made constantly to recycle, and keeps temperature unified, if instead
It is higher than water temperature in requisition for temperature, then opens heating device, the water temperature in constant warm tube is made to increase, start motor, ensures its normal rotation
Turn；
S2. reaction solution is poured by two feeding devices in tapping room respectively, starting water pump keeps the water in constant warm tube continuous
Lower water temperature in constant warm tube is rotated force-applying piece, drain pipe is made to decline by cycle by heating device to required temperature is reacted,
When liquid-leaking nozzle drops to liquid level or less, reaction solution flow to woven hose from liquid-leaking nozzle, and then, reaction solution flows into helix tube, spiral
Pipe fits with reaction chamber wall, and reaction solution temperature in helix tube opens motor, motor drives constantly close to constant warm tube temperature
Lower revolving part rotation, lower revolving part drive upper revolving part to reversely rotate by transmission gear, lower revolving part and the agitation of upper revolving part
Reaction solution makes reaction solution be sufficiently mixed reaction, after the completion of reaction, opens liquid valve, the liquid after reaction is discharged from outlet tube；
S3. after use, force-applying piece is rotated, so that liquid-leaking nozzle is risen to extreme higher position, distilled water is poured into feeding device, directly
Highest is risen to liquid level, force-applying piece is rotated, drain pipe is made slowly to decline, distilled water is left to helix tube by woven hose, cleaning
Reactant residue in helix tube, distilled water are flowed by helix tube in reative cell, and motor is started, and motor drives revolving part to turn
It is dynamic, reaction chamber wall is cleaned, liquid valve is opened, distilled water is made to flow out, completes cleaning, for use next time.
Compared with prior art, the beneficial effects of the invention are as follows：
1. the present invention opens up liquid-leaking nozzle by drain pipe surface, then in such a way that screw element connects the inner wall in tapping ceiling portion,
Convenient for controlling the liquid outlet quantity of reaction solution, keeps liquid outlet quantity more accurate, ensure that reaction effect；
2. constant warm tube fits with reacting outdoor wall, water pump makes water in constant warm tube constantly flow, and heating device controls water temperature, is convenient for
Reaction temperature is adjusted, reaction effect is further ensured；
Revolving part and lower revolving part direction of rotation are on the contrary, ensure that the mixing effect of reaction solution on 3..
Description of the drawings
Fig. 1 is schematic structural view of the invention；
Fig. 2 is support device structure diagram of the present invention；
Fig. 3 is the upper revolving part structural schematic diagram of the present invention；
Fig. 4 is indicator of the present invention and drain pipe installation relation schematic diagram；
Fig. 5 is reative cell top view of the present invention.
In figure：It is 1 pedestal, 2 motor rooms, 3 motors, 4 mounting plates, 5 water pumps, 6 heating devices, 7 reative cells, 8 constant warm tubes, 9 defeated
Liquid pipe, 10 tapping rooms, 11 feeding devices, 12 drain pipes, 13 rubber rings, 14 screw elements, 15 force-applying pieces, 16 liquid-leaking nozzles, 17 spirals
Pipe, 18 sealing rings, 19 times revolving parts, 20 times fixing pieces, revolving part on 21,211 rotary shafts, 212 rotating arms, 213 stirring sheets,
22 upper fixing elements, 23 transmission gears, 24 outlet tubes, 25 liquid valves, 26 support devices, 261 clamping rings, 262 fixed rings, 263 are prolonged
Long-armed, 264 support columns, 27 indicators.
Specific implementation mode
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete
Site preparation describes, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on
Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts every other
Embodiment shall fall within the protection scope of the present invention.
- 5 are please referred to Fig.1, the present invention provides a kind of technical solution：A kind of industrial chemicals reaction unit, including pedestal 1, institute
It states 1 top of pedestal and offers motor room 2, be easily installed motor 3, state and be provided with motor 3 in motor room 2 straight up, for rotation
Part provides power, and the position that 1 top of the pedestal is kept right is provided with mounting plate 4, for installing water pump 5,4 left side of the mounting plate
Water pump 5 is installed, the top of the pedestal 1 is equipped with reative cell 7, and 7 surface wrap of the reative cell has constant warm tube 8, makes reaction
Room 7 keeps constant temperature, 8 upper end of the constant warm tube to connect 5 water outlet of water pump, and 8 lower end of the constant warm tube connects 5 water inlet of water pump, institute
It states 8 surface of constant warm tube and the position of water pump 5 is provided with heating device 6, the water in heated constant temperature pipe 8,7 top of the reative cell
There are two the identical woven hoses 9 of structure for setting, and reative cell 7 is run through at 9 top of woven hose, and 9 top of the woven hose, which is provided with, puts
Liquid chamber 10, for the solution before placing response, the tapping room 10 and woven hose 9 are all connected with support device 26, are used to support and put
Liquid chamber 10, the setting of the support device 26 is at 1 top of pedestal, and 10 surface of tapping room is provided with feeding device 11, convenient for anti-
Liquid is answered to enter tapping room 10,10 inner cavity of tapping room is provided with drain pipe 12 and is pushed up for reaction solution, the drain pipe 12 to be discharged
Portion is through 10 top of tapping room, and 10 bottom of tapping room is run through in 12 lower end of the drain pipe, and 12 lower end of drain pipe is plugged on infusion
9 inner cavity upper end of pipe, 9 inner cavity top of the woven hose is fixedly installed rubber ring 13, for sealing, 13 inner wall of the rubber ring with
12 surface of drain pipe fits, and 12 surface upper end of the drain pipe is provided with screw element 14, and 14 top of screw element connects tapping
10 inner cavity top of room, 12 surface of the drain pipe are provided with force-applying piece 15, and 12 surface of the drain pipe offers liquid-leaking nozzle 16, just
It is leaked out in reaction solution, 9 bottom of the woven hose is mounted on helix tube 17, and helix tube 17 fits with 7 inner wall of reative cell, makes
Reacting liquid temperature is consistent with constant warm tube 8, and 3 rotary shaft of the motor runs through 7 bottom center location of reative cell, 7 bottom of the reative cell
Portion is equipped with sealing ring 18, and 3 rotary shaft of motor runs through sealing ring 18, enclosed reaction chamber 7, and 3 rotary shaft of motor top connects
It is connected to lower revolving part 19, the lower fixing piece 20 of 19 top connection of the lower revolving part, the lower fixing piece 20 is mounted in reative cell 7
Wall, 7 inner wall of the reative cell are equipped with upper fixing element 22, and 22 bottom of fixed part is equipped with revolving part 21, it is described on
21 bottom of revolving part and 19 top of lower revolving part are installed with transmission gear 23, and the transmission gear 23 is mutually twisted, band
Dynamic upper revolving part 21 rotates, and 7 left bottom of the reative cell is provided with outlet tube 24, and the outlet tube 24 is left through reative cell 7
Side wall, 24 surface of the outlet tube are equipped with liquid valve 25, control liquid discharge close to one end of reative cell 7.
Wherein, the support device 26 includes clamping ring 261, and the clamping ring 261 is mounted on 10 surface of tapping room, described
261 back side of clamping ring is connected with support column 264, and the support column 264 is arranged in 1 top rearward position of pedestal, the infusion
9 surface crown of pipe is equipped with fixed ring 262, and 262 back side of the fixed ring is equipped with extension arm 263, and the extension arm 263 is another
End connection support column 264, support tapping room 10；
The upper revolving part 21 includes rotary shaft 211, and there are five the identical rotating arms of structure for the installation of 211 surface of the rotary shaft
212, and the identical rotating arm of five structures 212 keeps stirring range broader, and five structure phases not in same level
Circumferentially type arranges same rotating arm 212, and the one end of the rotating arm 212 far from support column is equipped with stirring sheet 213, uses
In agitated liquid；
14 inner cavity of the screw element is provided with screw thread, and 12 surface of drain pipe is provided with and matches external screw thread with screw element 14, just
In moving up and down for control drain pipe；
The identical indicator 27 of structure that there are three the settings of 12 surface of the drain pipe, and the identical indicator 27 of three structures and leakage
16 bottom of fluid apertures is parallel, keeps tapping more accurate, and 10 surface of tapping room is provided with scale, and scale is single with ten milliliters
Position releases the volume of liquid convenient for observation；
11 upper end of the feeding device is funnel-form, and the entrance of reaction solution, 11 lower end of the feeding device is convenient for run through tapping room
10 table walls；
A kind of industrial chemicals reaction unit and reaction method include the following steps：
S1. force-applying piece 15 is rotated, so that drain pipe 12 is increased by screw element 14, liquid-leaking nozzle 16 is made to rise to extreme higher position, confirm
Liquid valve 25 is in off state, and checks 23 occluding relation of transmission gear, starts water pump 5, the water in constant warm tube 8 is made constantly to recycle,
Keep temperature unified, if reaction needs temperature to be higher than water temperature, open heating device 6, the water temperature in constant warm tube 8 is made to increase, starts
Motor 3 ensures its normal rotation；
S2. reaction solution is poured by two feeding devices 11 in tapping room 10 respectively, starting water pump 5 makes in constant warm tube 8
Water constantly recycles, and by heating device 6 rotates force-applying piece 15, makes row the lower water temperature in constant warm tube 8 to required temperature is reacted
Liquid pipe 12 declines, and when liquid-leaking nozzle 16 drops to liquid level or less, reaction solution flow to woven hose 9, then, reaction solution from liquid-leaking nozzle 16
Flow into helix tube 17, helix tube 17 fits with 7 inner wall of reative cell, reaction solution in helix tube 17 temperature constantly close to constant warm tube
8 temperature open motor 3, and motor 3 drives lower revolving part 19 to rotate, and lower revolving part 19 drives upper revolving part by transmission gear 23
21 reversely rotate, and lower revolving part 19 and upper revolving part 21 stir reaction solution, and reaction solution is made to be sufficiently mixed reaction, after the completion of reaction,
Liquid valve 25 is opened, the liquid after reaction is discharged from outlet tube；
S3. after use, force-applying piece 15 is rotated, so that liquid-leaking nozzle 16 is risen to extreme higher position, distillation is poured into feeding device
Water rotates force-applying piece 15 until liquid level rises to highest, and drain pipe 12 is made slowly to decline, and distilled water is left to spiral shell by woven hose 9
Coil 17 cleans the reactant residue in helix tube 17, and distilled water is flowed by helix tube 17 in reative cell 7, and motor is started
3, motor 3 drives revolving part rotation, cleans 7 inner wall of reative cell, opens liquid valve 25, distilled water is made to flow out, and completes cleaning, so as to
Next time uses.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
Understanding without departing from the principles and spirit of the present invention can carry out these embodiments a variety of variations, modification, replace
And modification, the scope of the present invention is defined by the appended.
Claims (7)
1. a kind of industrial chemicals reaction unit, including pedestal（1）, it is characterised in that：The pedestal（1）Top offers motor room
（2）, the motor room（2）It is inside provided with motor straight up（3）, the pedestal（1）The position that top is kept right is provided with installation
Plate（4）, the mounting plate（4）Left side is equipped with water pump（5）, the pedestal（1）Top reative cell is installed（7）, described anti-
Answer room（7）Surface wrap has constant warm tube（8）, the constant warm tube（8）Upper end connects water pump（5）Water outlet, the constant warm tube（8）Under
End connection water pump（5）Water inlet, the constant warm tube（8）Surface is close to water pump（5）Position be provided with heating device（6）, described
Reative cell（7）There are two the identical woven hoses of structure for top setting（9）, and woven hose（9）Reative cell is run through at top（7）, described
Woven hose（9）Top is provided with tapping room（10）, the tapping room（10）And woven hose（9）It is all connected with support device（26）, institute
State support device（26）It is arranged in pedestal（1）Top, the tapping room（10）Surface is provided with feeding device（11）, the tapping
Room（10）Inner cavity is provided with drain pipe（12）, the drain pipe（12）Tapping room is run through at top（10）Top, the drain pipe
（12）Tapping room is run through in lower end（10）Bottom, and drain pipe（12）Lower end is plugged on woven hose（9）Inner cavity upper end, the woven hose
（9）Inner cavity top is fixedly installed rubber ring（13）, the rubber ring（13）Inner wall and drain pipe（12）Surface fits, described
Drain pipe（12）Surface upper end is provided with screw element（14）, and screw element（14）Top connects tapping room（10）Inner cavity top, institute
State drain pipe（12）Surface is provided with force-applying piece（15）, the drain pipe（12）Surface offers liquid-leaking nozzle（16）, the infusion
Pipe（9）Bottom is mounted on helix tube（17）, and helix tube（17）With reative cell（7）Inner wall fits, the motor（3）Rotation
Axis runs through reative cell（7）Bottom center location, the reative cell（7）Bottom is equipped with sealing ring（18）, and motor（3）Rotary shaft
Through sealing ring（18）, the motor（3）It is connected with lower revolving part at the top of rotary shaft（19）, the lower revolving part（19）Top connects
Connect lower fixing piece（20）, the lower fixing piece（20）Mounted on reative cell（7）Inner wall, the reative cell（7）Inner wall is equipped with
Fixing piece（22）, fixed part（22）Bottom is equipped with revolving part（21）, the upper revolving part（21）Bottom and backspin
Turn part（19）Top is installed with transmission gear（23）, the transmission gear（23）It is mutually twisted, the reative cell（7）It is left
Side bottom is provided with outlet tube（24）, the outlet tube（24）Through reative cell（7）Left side wall, the outlet tube（24）Surface is leaned on
Proximal response room（7）One end liquid valve is installed（25）.
2. a kind of industrial chemicals reaction unit according to claim 1, it is characterised in that：The support device（26）Including
Clamping ring（261）, the clamping ring（261）Mounted on tapping room（10）Surface, the clamping ring（261）The back side is connected with support
Column（264）, the support column（264）It is arranged in pedestal（1）Top rearward position, the woven hose（9）Surface crown is installed
There is fixed ring（262）, the fixed ring（262）The back side is equipped with extension arm（263）, the extension arm（263）The other end connects
Support column（264）.
3. a kind of industrial chemicals reaction unit according to claim 1, it is characterised in that：The upper revolving part（21）Including
Rotary shaft（211）, the rotary shaft（211）There are five the identical rotating arms of structure for surface installation（212）, and five structure phases
Same rotating arm（212）Not in same level, and the identical rotating arm of five structures（212）Circumferentially type arranges, institute
State rotating arm（212）One end far from support column is equipped with stirring sheet（213）.
4. a kind of industrial chemicals reaction unit according to claim 1, it is characterised in that：The screw element（14）Inner cavity is set
It is equipped with screw thread, and drain pipe（12）Surface is provided with and screw element（14）Match external screw thread.
5. a kind of industrial chemicals reaction unit according to claim 1 or 4, it is characterised in that：The drain pipe（12）Table
There are three the identical indicators of structure for face setting（27）, and the identical indicator of three structures（27）With liquid-leaking nozzle（16）Bottom phase
It is parallel, the tapping room（10）Surface is provided with scale, and scale is as unit of ten milliliters.
6. a kind of industrial chemicals reaction unit according to claim 1, it is characterised in that：The feeding device（11）Upper end
For funnel-form, the feeding device（11）Tapping room is run through in lower end（10）Table wall.
7. a kind of industrial chemicals reaction unit according to claim 1-6, it is characterised in that：A kind of industrial chemicals is anti-
Device and reaction method is answered to include the following steps：
S1. force-applying piece is rotated（15）, pass through screw element（14）Make drain pipe（12）Rise, makes liquid-leaking nozzle（16）Rise to highest order
It sets, confirms liquid valve（25）It is in off state, checks transmission gear（23）Occluding relation starts water pump（5）, make constant warm tube（8）
Interior water constantly recycles, and keeps temperature unified, if reaction needs temperature to be higher than water temperature, opens heating device（6）, make constant warm tube
（8）Interior water temperature increases, and starts motor（3）, ensure its normal rotation；
S2. reaction solution is passed through into two feeding devices respectively（11）It is poured into tapping room（10）In, start water pump（5）Make constant warm tube
（8）Interior water constantly recycles, and passes through heating device（6）By constant warm tube（8）Interior lower water temperature is applied to required temperature, rotation is reacted
Power part（15）, make drain pipe（12）Decline, works as liquid-leaking nozzle（16）When dropping to liquid level or less, reaction solution is from liquid-leaking nozzle（16）It flow to
Woven hose（9）, then, reaction solution flows into helix tube（17）, helix tube（17）With reative cell（7）Inner wall fits, and reaction solution exists
Helix tube（17）Interior temperature is constantly close to constant warm tube（8）Temperature opens motor（3）, motor（3）Drive lower revolving part（19）Turn
It is dynamic, lower revolving part（19）Pass through transmission gear（23）Revolving part in drive（21）It reversely rotates, lower revolving part（19）With upper rotation
Part（21）Reaction solution is stirred, reaction solution is made to be sufficiently mixed reaction, after the completion of reaction, opens liquid valve（25）, the liquid after reaction
It is discharged from outlet tube；
S3. after use, force-applying piece is rotated（15）, make liquid-leaking nozzle（16）Extreme higher position is risen to, is poured into feeding device
Distilled water rotates force-applying piece until liquid level rises to highest（15）, make drain pipe（12）Slowly decline, distilled water passes through infusion
Pipe（9）It is left to helix tube（17）, clean helix tube（17）Interior reactant residue, distilled water pass through helix tube（17）It flows into anti-
Answer room（7）It is interior, start motor（3）, motor（3）Revolving part rotation is driven, reative cell is cleaned（7）Inner wall opens liquid valve（25）,
So that distilled water is flowed out, completes cleaning, for use next time.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810554835.XA CN108671866A (en) | 2018-06-01 | 2018-06-01 | A kind of industrial chemicals reaction unit and reaction method |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810554835.XA CN108671866A (en) | 2018-06-01 | 2018-06-01 | A kind of industrial chemicals reaction unit and reaction method |
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| Publication Number | Publication Date |
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| CN108671866A true CN108671866A (en) | 2018-10-19 |
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| CN201810554835.XA Pending CN108671866A (en) | 2018-06-01 | 2018-06-01 | A kind of industrial chemicals reaction unit and reaction method |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114768665A (en) * | 2022-05-26 | 2022-07-22 | 北京慕湖仪器制造有限公司 | Laboratory is with compound system of automatic water-reducing agent |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105617491A (en) * | 2014-10-25 | 2016-06-01 | 刘亚江 | Heating bottle of infusion tube |
| CN205288388U (en) * | 2015-11-02 | 2016-06-08 | 国家电网公司 | Chemical reaction cauldron structure that nano -fluids generated |
| CN207085896U (en) * | 2017-06-29 | 2018-03-13 | 江苏欣舟化工科技有限公司 | A kind of coaxial double rotating type quick reaction kettle |
-
2018
- 2018-06-01 CN CN201810554835.XA patent/CN108671866A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105617491A (en) * | 2014-10-25 | 2016-06-01 | 刘亚江 | Heating bottle of infusion tube |
| CN205288388U (en) * | 2015-11-02 | 2016-06-08 | 国家电网公司 | Chemical reaction cauldron structure that nano -fluids generated |
| CN207085896U (en) * | 2017-06-29 | 2018-03-13 | 江苏欣舟化工科技有限公司 | A kind of coaxial double rotating type quick reaction kettle |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114768665A (en) * | 2022-05-26 | 2022-07-22 | 北京慕湖仪器制造有限公司 | Laboratory is with compound system of automatic water-reducing agent |
| CN114768665B (en) * | 2022-05-26 | 2023-12-12 | 北京慕湖新材料技术有限公司 | Automatic water reducing agent compound system for laboratory |
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