CN108660542A - Special brush filament of a kind of interior besom and preparation method thereof - Google Patents
Special brush filament of a kind of interior besom and preparation method thereof Download PDFInfo
- Publication number
- CN108660542A CN108660542A CN201810420927.9A CN201810420927A CN108660542A CN 108660542 A CN108660542 A CN 108660542A CN 201810420927 A CN201810420927 A CN 201810420927A CN 108660542 A CN108660542 A CN 108660542A
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- Prior art keywords
- brush filament
- parts
- besom
- cold water
- preparation
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F8/00—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof
- D01F8/04—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers
- D01F8/12—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers with at least one polyamide as constituent
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L77/00—Compositions of polyamides obtained by reactions forming a carboxylic amide link in the main chain; Compositions of derivatives of such polymers
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F8/00—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof
- D01F8/04—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers
- D01F8/14—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers with at least one polyester as constituent
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2237—Oxides; Hydroxides of metals of titanium
- C08K2003/2241—Titanium dioxide
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- General Chemical & Material Sciences (AREA)
- Textile Engineering (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Manufacturing & Machinery (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Treatment Of Fiber Materials (AREA)
Abstract
The present invention provides special brush filament of a kind of indoor besom and preparation method thereof, is related to hairbrush technical field.The brush filament is made of the raw material of following parts by weight：20 40 parts of polybutylene terephthalate (PBT), 40 60 parts of polyamide, 6 10 parts of liquid polysulfide rubber, 0.7 1.2 parts of nano-titanium dioxide, 12 parts of sodium benzoate, 0.8 1.4 parts of di-sec-octyl phthalate, 0.4 0.9 parts of diphenylamines；And the present invention obtains brush filament of the present invention by production processes such as chip drying, mixed melting, spinneret, liquid cooling and shaping, thermal finalizations.The flexibility that brush filament of the present invention improves conventional plastic silk makes it be unlikely to deform, and enhances pliability, is not easy to scratch floor, while having many advantages, such as wear-resisting, durable, at low cost.
Description
Technical field
The present invention relates to hairbrush technical fields, and in particular to special brush filament of a kind of interior besom and preparation method thereof.
Background technology
Brush filament is that one kind is used to make bristle used in various burnishers, and usual brush filament generally has copper wire, steel wire, Buddhist nun
The kinds such as nylon yarn, plastic wire, abrasive filaments, sisal hemp, Arenga engleri Beccari, bristles, wool.Wherein steel wire metalloid brush filament is due to abrasion hardness height
Etc. properties be mainly used for industrial cleaning or road cleaning, bristles, nylon yarn, plastic wire class brush filament due to neither too hard, nor too soft more
For indoor cleaning tool, the natural brush filament of wool class its have many advantages, such as soft, cleaning it is simple be chiefly used in textile article or
Furniture cleans.
With the development of the times, the ceramic tile that people mostly use timber floor or top grade in home improvement is the dress of flooring
Material is repaiied, brush filament used in general burnisher is mostly plastic wire and nylon yarn on the market, but these brush filaments are in material
On it is partially hard, scratch can be caused to influence when cleaning timber floor or ceramic tile beautiful.
Invention content
In view of the shortcomings of the prior art, the present invention provides special brush filament of a kind of indoor besom and preparation method thereof, biography is improved
The flexibility of system plastic wire makes it be unlikely to deform, and enhances pliability, is not easy to scratch floor, while wear-resisting and at low cost.
In order to achieve the above object, technical scheme of the present invention is achieved by the following technical programs：
A kind of special brush filament of interior besom, the brush filament are made of the raw material of following parts by weight：Poly terephthalic acid fourth two
20-40 parts of alcohol ester, 40-60 parts of polyamide, 6-10 parts of liquid polysulfide rubber, 0.7-1.2 parts of nano-titanium dioxide, benzoic acid
1-2 parts of sodium, 0.8-1.4 parts of di-sec-octyl phthalate, 0.4-0.9 parts of diphenylamines.
Preferably, a kind of special brush filament of indoor besom, the brush filament are made of the raw material of following parts by weight：Poly- terephthaldehyde
30 parts of sour butanediol ester, 50 parts of polyamide, 8 parts of liquid polysulfide rubber, 1 part of nano-titanium dioxide, 1.5 parts of sodium benzoate,
1.2 parts of di-sec-octyl phthalate, 0.6 part of diphenylamines.
The preparation method of the special brush filament of the interior besom includes the following steps：
(1) polybutylene terephthalate (PBT) and polyamide are subjected to slice mixing, then mixed resin is put
Enter dry 2-3h in dynamic vacuum drying machine；
(2) liquid polysulfide rubber, nano-titanium dioxide, sodium benzoate, di-sec-octyl phthalate and diphenylamines are pressed
According to parts by weight mix after be heated to 120 DEG C -130 DEG C, stir evenly mixing slurry is spare；
(3) mixing slurry in above-mentioned steps (2) is mixed with the resin in step (1), after pour into extruser plus
Heat extremely melts, and extrusion plastic brush filament；
(4) plastics brush filament is placed in cooling and shaping in cold water, after will plastics brush filament be sent into stretching device in be stretched as thin footpath
Brush filament；
(5) thin footpath brush filament is subcooled after water cooling and is placed in sizing progress thermal finalization 10-15min in constant temperature shaping box again；
(6) the thin footpath brush filament after thermal finalization is again placed in cooling and shaping in cold water, and cuts, collects and obtain this product.
Preferably, in step (4) cold water temperature in 20-30 DEG C, step (5) cold water temperature in 15-25 DEG C, step (6)
Cold water temperature is at 10-15 DEG C.
Preferably, a diameter of 1-3mm of thin footpath brush filament.
Preferably, heat setting temperature is 120-150 DEG C in constant temperature shaping box in step (5).
The present invention provides special brush filament of a kind of indoor besom and preparation method thereof, and advantage is compared with prior art：
(1) brush filament of the present invention selects polybutylene terephthalate (PBT) and polyamide as base-material, can make the present invention
Gained brush filament is neither too hard, nor too soft, and indoor cleaning is suitble to use.
(2) present invention can enhance the toughness of brush filament added with liquid polysulfide rubber, keep brush filament not variable in use
Shape, while coordinating the substances such as addition nano-titanium dioxide, sodium benzoate, di-sec-octyl phthalate and diphenylamines, it can be effective
Enhance the pliability of brush filament, reduces the scratch to timber floor when using.
(3) present invention can effectively enhance brush in manufacturing process first with liquid sizing, again thermal finalization finally liquid sizing again
Silk flexibility reduces the deformation rate of brush filament in use, while the temperature employed in heat-setting process is 120-150 DEG C
Plastic molecules can be made to carry out softening recombination, keep brush filament more soft durable.
Specific implementation mode
In order to make the object, technical scheme and advantages of the embodiment of the invention clearer, with reference to the embodiment of the present invention pair
Technical solution in the embodiment of the present invention is clearly and completely described, it is clear that described embodiment is a part of the invention
Embodiment, instead of all the embodiments.Based on the embodiments of the present invention, those of ordinary skill in the art are not making wound
The every other embodiment obtained under the premise of the property made labour, shall fall within the protection scope of the present invention.
Embodiment 1：
A kind of special brush filament of interior besom, the brush filament are made of the raw material of following parts by weight：Poly terephthalic acid fourth two
20 parts of alcohol ester, 40 parts of polyamide, 6 parts of liquid polysulfide rubber, 0.7 part of nano-titanium dioxide, 1 part of sodium benzoate, adjacent benzene two
0.8 part of formic acid di-sec-octyl, 0.4 part of diphenylamines.
The preparation method of the special brush filament of the interior besom includes the following steps：
(1) polybutylene terephthalate (PBT) and polyamide are subjected to slice mixing, then mixed resin is put
Enter dry 2-3h in dynamic vacuum drying machine；
(2) liquid polysulfide rubber, nano-titanium dioxide, sodium benzoate, di-sec-octyl phthalate and diphenylamines are pressed
According to parts by weight mix after be heated to 120 DEG C -130 DEG C, stir evenly mixing slurry is spare；
(3) mixing slurry in above-mentioned steps (2) is mixed with the resin in step (1), after pour into extruser plus
Heat extremely melts, and extrusion plastic brush filament；
(4) plastics brush filament is placed in cooling and shaping in cold water, after will plastics brush filament be sent into stretching device in be stretched as thin footpath
Brush filament；
(5) thin footpath brush filament is subcooled after water cooling and is placed in sizing progress thermal finalization 10-15min in constant temperature shaping box again；
(6) the thin footpath brush filament after thermal finalization is again placed in cooling and shaping in cold water, and cuts, collects and obtain this product.
Wherein, cold water temperature cold water temperature in 20-30 DEG C, step (5) is cold in 15-25 DEG C, step (6) in step (4)
Coolant-temperature gage is at 10-15 DEG C；A diameter of 1-3mm of thin footpath brush filament；Heat setting temperature is 120- in constant temperature shaping box in step (5)
150℃。
Embodiment 2：
A kind of special brush filament of interior besom, the brush filament are made of the raw material of following parts by weight：Poly terephthalic acid fourth two
40 parts of alcohol ester, 60 parts of polyamide, 10 parts of liquid polysulfide rubber, 1.2 parts of nano-titanium dioxide, 2 parts of sodium benzoate, adjacent benzene two
1.4 parts of formic acid di-sec-octyl, 0.9 part of diphenylamines.
The preparation method of the special brush filament of the interior besom includes the following steps：
(1) polybutylene terephthalate (PBT) and polyamide are subjected to slice mixing, then mixed resin is put
Enter dry 2-3h in dynamic vacuum drying machine；
(2) liquid polysulfide rubber, nano-titanium dioxide, sodium benzoate, di-sec-octyl phthalate and diphenylamines are pressed
According to parts by weight mix after be heated to 120 DEG C -130 DEG C, stir evenly mixing slurry is spare；
(3) mixing slurry in above-mentioned steps (2) is mixed with the resin in step (1), after pour into extruser plus
Heat extremely melts, and extrusion plastic brush filament；
(4) plastics brush filament is placed in cooling and shaping in cold water, after will plastics brush filament be sent into stretching device in be stretched as thin footpath
Brush filament；
(5) thin footpath brush filament is subcooled after water cooling and is placed in sizing progress thermal finalization 10-15min in constant temperature shaping box again；
(6) the thin footpath brush filament after thermal finalization is again placed in cooling and shaping in cold water, and cuts, collects and obtain this product.
Wherein, cold water temperature cold water temperature in 20-30 DEG C, step (5) is cold in 15-25 DEG C, step (6) in step (4)
Coolant-temperature gage is at 10-15 DEG C；A diameter of 1-3mm of thin footpath brush filament；Heat setting temperature is 120- in constant temperature shaping box in step (5)
150℃。
Embodiment 3：
A kind of special brush filament of interior besom, the brush filament are made of the raw material of following parts by weight：Poly terephthalic acid fourth two
30 parts of alcohol ester, 50 parts of polyamide, 8 parts of liquid polysulfide rubber, 1 part of nano-titanium dioxide, 1.5 parts of sodium benzoate, adjacent benzene two
1.2 parts of formic acid di-sec-octyl, 0.6 part of diphenylamines.
The preparation method of the special brush filament of the interior besom includes the following steps：
(6) polybutylene terephthalate (PBT) and polyamide are subjected to slice mixing, then mixed resin is put
Enter dry 2-3h in dynamic vacuum drying machine；
(7) liquid polysulfide rubber, nano-titanium dioxide, sodium benzoate, di-sec-octyl phthalate and diphenylamines are pressed
According to parts by weight mix after be heated to 120 DEG C -130 DEG C, stir evenly mixing slurry is spare；
(8) mixing slurry in above-mentioned steps (2) is mixed with the resin in step (1), after pour into extruser plus
Heat extremely melts, and extrusion plastic brush filament；
(9) plastics brush filament is placed in cooling and shaping in cold water, after will plastics brush filament be sent into stretching device in be stretched as thin footpath
Brush filament；
(10) thin footpath brush filament is subcooled after water cooling and is placed in sizing progress thermal finalization 10-15min in constant temperature shaping box again；
(6) the thin footpath brush filament after thermal finalization is again placed in cooling and shaping in cold water, and cuts, collects and obtain this product.
Wherein, cold water temperature cold water temperature in 20-30 DEG C, step (5) is cold in 15-25 DEG C, step (6) in step (4)
Coolant-temperature gage is at 10-15 DEG C；A diameter of 1-3mm of thin footpath brush filament；Heat setting temperature is 120- in constant temperature shaping box in step (5)
150℃。
It should be noted that herein, relational terms such as first and second and the like are used merely to a reality
Body or operation are distinguished with another entity or operation, are deposited without necessarily requiring or implying between these entities or operation
In any actual relationship or order or sequence.Moreover, the terms "include", "comprise" or its any other variant are intended to
Non-exclusive inclusion, so that the process, method, article or equipment including a series of elements is not only wanted including those
Element, but also include other elements that are not explicitly listed, or further include for this process, method, article or equipment
Intrinsic element.In the absence of more restrictions, the element limited by sentence "including a ...", it is not excluded that
There is also other identical elements in process, method, article or equipment including the element.
The above embodiments are merely illustrative of the technical solutions of the present invention, rather than its limitations；Although with reference to the foregoing embodiments
Invention is explained in detail, it will be understood by those of ordinary skill in the art that：It still can be to aforementioned each implementation
Technical solution recorded in example is modified or equivalent replacement of some of the technical features；And these modification or
It replaces, the spirit and scope for various embodiments of the present invention technical solution that it does not separate the essence of the corresponding technical solution.
Claims (6)
1. a kind of special brush filament of interior besom, which is characterized in that the brush filament is made of the raw material of following parts by weight：Gather to benzene two
20-40 parts of formic acid butanediol ester, 40-60 parts of polyamide, 6-10 parts of liquid polysulfide rubber, nano-titanium dioxide 0.7-1.2
Part, 1-2 parts of sodium benzoate, 0.8-1.4 parts of di-sec-octyl phthalate, 0.4-0.9 parts of diphenylamines.
2. a kind of special brush filament of indoor besom according to claim 1, which is characterized in that the brush filament is by following parts by weight
Raw material be made：30 parts of polybutylene terephthalate (PBT), 50 parts of polyamide, 8 parts of liquid polysulfide rubber, nanometer titanium dioxide
1 part of titanium, 1.5 parts of sodium benzoate, 1.2 parts of di-sec-octyl phthalate, 0.6 part of diphenylamines.
3. a kind of special brush filament of indoor besom according to claim 1, which is characterized in that the preparation method packet of the brush filament
Include following steps：
(1) polybutylene terephthalate (PBT) and polyamide are subjected to slice mixing, then mixed resin is put into very
Dry 2-3h in empty dynamic drier；
(2) by liquid polysulfide rubber, nano-titanium dioxide, sodium benzoate, di-sec-octyl phthalate and diphenylamines according to weight
Amount part mixing after be heated to 120 DEG C -130 DEG C, stir evenly mixing slurry is spare；
(3) mixing slurry in above-mentioned steps (2) is mixed with the resin in step (1), after pour into extruser and be heated to
Melting, and extrusion plastic brush filament；
(4) plastics brush filament is placed in cooling and shaping in cold water, after will plastics brush filament be sent into stretching device in be stretched as thin footpath brush filament；
(5) thin footpath brush filament is subcooled after water cooling and is placed in sizing progress thermal finalization 10-15min in constant temperature shaping box again；
(6) the thin footpath brush filament after thermal finalization is again placed in cooling and shaping in cold water, and cuts, collects and obtain this product.
4. a kind of preparation method of the special brush filament of indoor besom according to claim 3, it is characterised in that：In step (4)
Cold water temperature in 20-30 DEG C, step (5) cold water temperature in 15-25 DEG C, step (6) cold water temperature at 10-15 DEG C.
5. a kind of preparation method of the special brush filament of indoor besom according to claim 3, it is characterised in that：Thin footpath brush filament
A diameter of 1-3mm.
6. a kind of preparation method of the special brush filament of indoor besom according to claim 3, it is characterised in that：In step (5)
Heat setting temperature is 120-150 DEG C in constant temperature shaping box.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810420927.9A CN108660542A (en) | 2018-05-04 | 2018-05-04 | Special brush filament of a kind of interior besom and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810420927.9A CN108660542A (en) | 2018-05-04 | 2018-05-04 | Special brush filament of a kind of interior besom and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108660542A true CN108660542A (en) | 2018-10-16 |
Family
ID=63781872
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810420927.9A Pending CN108660542A (en) | 2018-05-04 | 2018-05-04 | Special brush filament of a kind of interior besom and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108660542A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110644413A (en) * | 2019-08-23 | 2020-01-03 | 安徽鑫宏源刷业有限公司 | Environment-friendly snow sweeping brush and preparation method thereof |
| CN111719191A (en) * | 2020-06-08 | 2020-09-29 | 台州利丰洁具有限公司 | Method for preparing brush wire of indoor cleaning tool |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105420849A (en) * | 2015-12-08 | 2016-03-23 | 安徽天瑞塑业有限公司 | Fire-retardant-adding environment-friendly brush wire |
| CN105420850A (en) * | 2015-12-08 | 2016-03-23 | 安徽天瑞塑业有限公司 | Diamond abrasive brush wire component and production technology thereof |
| CN105821520A (en) * | 2016-05-10 | 2016-08-03 | 潜山县福达橡胶刷业制品厂 | Efficient environment-friendly inflaming-retarding brush wire production technology |
-
2018
- 2018-05-04 CN CN201810420927.9A patent/CN108660542A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105420849A (en) * | 2015-12-08 | 2016-03-23 | 安徽天瑞塑业有限公司 | Fire-retardant-adding environment-friendly brush wire |
| CN105420850A (en) * | 2015-12-08 | 2016-03-23 | 安徽天瑞塑业有限公司 | Diamond abrasive brush wire component and production technology thereof |
| CN105821520A (en) * | 2016-05-10 | 2016-08-03 | 潜山县福达橡胶刷业制品厂 | Efficient environment-friendly inflaming-retarding brush wire production technology |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110644413A (en) * | 2019-08-23 | 2020-01-03 | 安徽鑫宏源刷业有限公司 | Environment-friendly snow sweeping brush and preparation method thereof |
| CN111719191A (en) * | 2020-06-08 | 2020-09-29 | 台州利丰洁具有限公司 | Method for preparing brush wire of indoor cleaning tool |
| CN111719191B (en) * | 2020-06-08 | 2021-06-15 | 台州利丰洁具有限公司 | Method for preparing brush wire of indoor cleaning tool |
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Application publication date: 20181016 |