CN108654533B - Reaction kettle for water-based titanium alloy cutting fluid - Google Patents
Reaction kettle for water-based titanium alloy cutting fluid Download PDFInfo
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- CN108654533B CN108654533B CN201810478038.8A CN201810478038A CN108654533B CN 108654533 B CN108654533 B CN 108654533B CN 201810478038 A CN201810478038 A CN 201810478038A CN 108654533 B CN108654533 B CN 108654533B
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- polyethylene glycol
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- cutting fluid
- titanium alloy
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/0066—Stirrers
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D19/00—Degasification of liquids
- B01D19/02—Foam dispersion or prevention
- B01D19/04—Foam dispersion or prevention by addition of chemical substances
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D19/00—Degasification of liquids
- B01D19/02—Foam dispersion or prevention
- B01D19/04—Foam dispersion or prevention by addition of chemical substances
- B01D19/0404—Foam dispersion or prevention by addition of chemical substances characterised by the nature of the chemical substance
- B01D19/0409—Foam dispersion or prevention by addition of chemical substances characterised by the nature of the chemical substance compounds containing Si-atoms
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
- B01F23/40—Mixing liquids with liquids; Emulsifying
- B01F23/43—Mixing liquids with liquids; Emulsifying using driven stirrers
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
- B01F35/90—Heating or cooling systems
- B01F35/93—Heating or cooling systems arranged inside the receptacle
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
- B01F35/90—Heating or cooling systems
- B01F35/95—Heating or cooling systems using heated or cooled stirrers
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
- B01F35/90—Heating or cooling systems
- B01F2035/99—Heating
Abstract
The invention discloses a reaction kettle for water-based titanium alloy cutting fluid, which comprises a kettle body, wherein the kettle body comprises a stirring shaft which is driven by a motor arranged at the top and extends into an inner cavity of the kettle body, a stirring paddle is arranged on the stirring shaft, and the other end of the stirring shaft is fixed in a support frame at the bottom; a heating pipe is sleeved outside the stirring shaft; the top of the stirring kettle is also provided with a feeding hole, and the bottom of the stirring kettle is provided with a discharging hole; a spiral turbulence strip is arranged in the inner cavity of the kettle body and clings to the inner wall; and the water-based titanium alloy cutting fluid comprises a polyethylene glycol ester lubricant. The reaction kettle can solve the problem of excessive bubbles caused by excessive emulsification and the problem of demulsification caused by insufficient emulsification in the prior art.
Description
Technical Field
The invention relates to the field of liquid reaction kettles, in particular to a water-based titanium alloy cutting fluid reaction kettle.
Background
Titanium is a structural metal developed in the last 50 th century, and titanium alloy has the advantages of high strength, corrosion resistance, good heat resistance and the like, and is an important alloy for developing aviation and high-end equipment. However, titanium alloys are also difficult to machine due to these properties, and cutting with ordinary metals results in accelerated wear of the tool tip and unacceptable quality of the work piece, and therefore, selection of an appropriate metal cutting fluid is of great importance.
Most of metal cutting fluids in the prior art are emulsified oil products, and the viscosity of the products is not suitable for being used in titanium metal cutting, so that the phenomenon of adhesion and abrasion of the titanium metal can be caused. Therefore, water-based cutting fluids have become the subject of development of titanium metal cutting fluids. Water-based cutting fluids have low oil content or do not contain oily components and therefore have less environmental impact. The water-based cutting fluid is generally an emulsified or galactized product, which contains a large amount of lubricants, emulsifiers and the like, particularly, the conventional oil reaction kettle is adopted for the water-based titanium alloy cutting fluid adopting the polyethylene glycol ester lubricants, so that the demulsification phenomenon caused by uneven stirring or excessive emulsification can be caused, and the product quality of the water-based titanium alloy cutting fluid is greatly influenced. Therefore, a reaction kettle suitable for the water-based titanium alloy cutting fluid needs to be developed.
Disclosure of Invention
Aiming at the defects in the prior art, the invention provides the reaction kettle suitable for the water-based titanium alloy cutting fluid, in particular suitable for the water-based titanium alloy cutting fluid containing the polyethylene glycol ester lubricant, and the reaction kettle has the advantages of good emulsification effect, difficult demulsification of finished products and the like.
The polyethylene glycol esters are generally used in the fields of chemical industry, papermaking, spinning and the like, are used as emulsifying agents, have good emulsifying, lubricating and softening properties, can be dissolved in various organic solvents, and are generally dispersed in water. The water-based titanium alloy cutting fluid is generally used as a lubricant, but when the water-based titanium alloy cutting fluid is added into a water phase and is conventionally emulsified by a common reaction kettle, a large amount of bubbles are generated in the emulsification process due to the presence of a spoiler in the reaction kettle, which is fatal to the reaction kettle, so that the dosage of an antifoaming agent needs to be increased in raw materials, the antifoaming agent commonly used in the field is siloxane, the adhesion abrasion phenomenon of the water-based titanium alloy cutting fluid is increased due to the introduction of a large amount of siloxane, and the phenomenon of insufficient emulsification and easy demulsification exists in the reaction kettle without the spoiler.
The inventor surprisingly finds that the spiral spoiler strip is adopted to replace a common vertical spoiler through careful research, so that the phenomenon of excessive bubbles and demulsification caused by insufficient emulsification in the prior art caused by excessive emulsification can be solved. The specific technical scheme of the invention is as follows:
a reaction kettle for water-based titanium alloy cutting fluid comprises a kettle body, wherein the kettle body comprises a stirring shaft which is driven by a motor arranged at the top and extends into an inner cavity of the kettle body, a stirring paddle is arranged on the stirring shaft, and the other end of the stirring shaft is fixed in a support frame at the bottom; a heating pipe is sleeved outside the stirring shaft; the top of the stirring kettle is also provided with a feeding hole, and the bottom of the stirring kettle is provided with a discharging hole; a spiral turbulence strip is arranged in the inner cavity of the kettle body and clings to the inner wall; and the water-based titanium alloy cutting fluid comprises a polyethylene glycol ester lubricant.
In a preferred embodiment of the invention, the stirring paddle has 4 to 6 blades, and the blades are all in a plane vertical to the stirring shaft. The paddle is formed by overlapping a lower paddle and an upper paddle. Preferably, the upper paddle has a slightly smaller area than the lower paddle. More preferably, the cross-sections of the upper and lower blades form a step shape.
In a preferred embodiment of the invention, the number of the stirring paddles is 3, and the stirring paddles are uniformly distributed on the stirring shaft; correspondingly, the number of the heating pipes is 2, and the heating pipes are positioned between two adjacent stirring paddles. Preferably, the diameter of the heating pipe is larger than the length of the paddle. The stirring and dissolving process of the polyethylene glycol ester system needs heating, and the heating is beneficial to dissolving the components under normal conditions, so that the process time can be reduced, the production flow can be shortened, and the cost can be reduced.
In a preferred embodiment of the invention, the spiral direction of the turbulence strips is consistent with the rotation direction of the stirring paddle, the included angle between the turbulence strips and the horizontal plane is 15-45 degrees, and the width of the turbulence strips is 1/8-1/15 of the inner diameter of the kettle body. It is believed that the included angle of the turbulence strip and the horizontal plane is too large, so that the turbulence effect is enhanced, bubbles are more easily generated, and when the included angle of the turbulence strip and the horizontal plane is too small, the turbulence effect is too weak, the emulsification effect is poor, and therefore the selection of a proper included angle plays a crucial role in the stability of the water-based titanium alloy cutting fluid. Preferably, the included angle between the turbulence strips and the horizontal plane is 30 degrees, and the width of the turbulence strips is 1/10 of the inner diameter of the kettle body.
The reaction kettle of the invention is mainly used for water-based titanium alloy cutting fluid, in particular to water-based titanium alloy cutting fluid containing polyethylene glycol fatty acid ester, wherein the polyethylene glycol fatty acid ester comprises, but is not limited to: polyethylene glycol monostearate, polyethylene glycol distearate, polyethylene glycol monolaurate, polyethylene glycol dilaurate, polyethylene glycol monooleate, polyethylene glycol dioleate, polyethylene glycol monomyristate, polyethylene glycol dimyristate, polyethylene glycol monoricinoleate, polyethylene glycol bisricinoleate, polyethylene glycol mono-arachidate, polyethylene glycol bisarachidate, polyethylene glycol monobehenate, polyethylene glycol bisbehenate, polyethylene glycol monopalmitate, and polyethylene glycol dipalmitate. In a preferred embodiment of the present invention, the polyethylene glycol ester lubricant is selected from one or more of polyethylene glycol monostearate, polyethylene glycol distearate, polyethylene glycol monolaurate, polyethylene glycol dilaurate, polyethylene glycol monooleate, and polyethylene glycol dioleate. The above polyethylene glycol fatty acid esters provide similar lubricating properties.
The reaction kettle of the water-based titanium alloy cutting fluid is mainly used for mixing and stirring the water-based titanium alloy cutting fluid. The raw materials of the lubricant comprise polyethylene glycol ester lubricant and water, and also comprise auxiliary materials and fillers which are commonly used in the field, wherein the auxiliary materials or fillers comprise but are not limited to: auxiliary lubricants such as phosphorus-based lubricants, bentonite lubricants, and the like; pH adjusting agents such as ammonia compounds, hydroxides, etc.; defoaming agents such as siloxanes, polyoxyethylene ethers, polyoxypropylene ethers and the like.
According to the reaction kettle of the water-based titanium alloy cutting fluid, water and water-soluble auxiliary materials such as a pH regulator and the like are sequentially added through a top feeding hole, a heating pipe is used for heating a system to 70-80 ℃, stirring is kept, then polyethylene glycol ester lubricants, auxiliary lubricants, defoaming agents and other components are added, stirring is continued under a heating condition, when uniform emulsion is formed, the temperature is reduced to normal temperature, and then a finished product of the water-based titanium alloy cutting fluid can be discharged from a bottom discharging hole. The stirring speed in the process is not too high, preferably 30-50 rpm.
The invention has the beneficial effects that:
1. compared with the common spoiler, the reaction kettle for the water-based titanium alloy cutting fluid reduces the spoiler effect, avoids the phenomenon of excessive bubbles caused by excessive emulsification, reduces the use of a defoaming agent, and reduces the adhesive wear caused by the cutting fluid by arranging the spiral spoiler strip.
2. The reaction kettle of the water-based titanium alloy cutting fluid avoids using a conventional propeller type stirring paddle, and adopts the same plane paddle stirring paddle, so that the vortex generated by stirring can be further reduced, micro bubbles formed in the vortex are avoided, the use of a defoaming agent is further reduced, and the adhesive wear caused by the cutting fluid is reduced.
3. The reaction kettle for the water-based titanium alloy cutting fluid is suitable for the water-based titanium alloy cutting fluid containing the polyethylene glycol ester lubricant, and has the advantages of good emulsification effect and difficult demulsification of a finished product.
Drawings
FIG. 1 is a schematic structural diagram of a preferred embodiment of the present invention;
FIG. 2 is a schematic structural diagram of a spoiler in accordance with a preferred embodiment of the present invention;
FIG. 3 is a schematic diagram of the structure of a stirring paddle in a preferred embodiment of the invention;
the method comprises the following steps of 1-a kettle body, 2-a stirring shaft, 3-a stirring paddle, 31-a blade, 311-an upper blade, 312-a lower blade, 4-a support frame, 5-a motor, 6-a heating pipe, 7-a turbulence strip, 8-a feeding port and 9-a discharging port.
Detailed Description
In order to make the technical means, the creation characteristics, the achievement purposes and the effects of the invention easy to understand, the invention is further explained below by combining the drawings and the specific embodiments.
Example 1:
as shown in fig. 1, the reaction kettle for water-based titanium alloy cutting fluid comprises a kettle body 1, wherein the kettle body 1 comprises a stirring shaft 2 which is driven by a motor 5 arranged at the top and extends into an inner cavity of the kettle body, a stirring paddle 3 is arranged on the stirring shaft 2, and the other end of the stirring shaft 2 is fixed in a support frame 4 at the bottom; a heating pipe 6 is sleeved outside the stirring shaft 2; the top of the kettle body 1 is also provided with a feeding hole 8, and the bottom is provided with a discharging hole 9; the reaction kettle is used for stirring and mixing the water-based titanium alloy cutting fluid containing the polyethylene glycol ester lubricant. Further, as shown in fig. 2, a spiral turbulence strip 7 is arranged in the inner cavity of the kettle body 1 and clings to the inner wall.
Further, the schematic structure of the stirring paddle 3 is shown in fig. 3, and preferably, the stirring paddle 3 has 6 blades 31 with central symmetry, and the blades 31 are all in a plane perpendicular to the stirring shaft 2. The blade 31 is formed by overlapping a lower blade 312 and an upper blade 311, wherein the area of the upper blade 311 is slightly smaller than that of the lower blade 312, and the cross sections of the upper blade 311 and the lower blade 312 form a step shape. Further, the number of the stirring paddles 3 is 3, and the stirring paddles are uniformly distributed on the stirring shaft 2.
The reaction kettle for the water-based titanium alloy cutting fluid is based on the purpose of accelerating dissolving and stirring, an inner cavity of a kettle body 1 is provided with 2 heating pipes 6, and the heating pipes 6 are positioned between two adjacent stirring paddles 3.
Preferably, the included angle between the turbulence strips 7 and the horizontal plane is 30 degrees, the downward spiral direction of the turbulence strips 7 is consistent with the rotation direction of the stirring paddle, and the width of the turbulence strips 7 is 1/10 of the inner diameter of the kettle body.
The working process of the reaction kettle for the water-based titanium alloy cutting fluid comprises the following steps: sequentially adding water and water-soluble auxiliary materials such as a pH regulator and the like through a top feeding hole, heating the system to 70-80 ℃ through a heating pipe, keeping stirring, then adding polyethylene glycol ester lubricant, an auxiliary lubricant, a defoaming agent and other components, continuously stirring under a heating condition, cooling to normal temperature when uniform emulsion is formed, and discharging a finished product of the water-based titanium alloy cutting fluid from a bottom discharging hole. The reaction kettle for the water-based titanium alloy cutting fluid is combined with the stirring paddle with a special structure through the spiral turbulence strips, so that the turbulence degree is reduced, the excessive emulsification of the polyethylene glycol ester lubricant is avoided, and the final product has the advantages of uniform emulsification and long storage time.
The above embodiment is only one embodiment of the present invention, and the description thereof is specific and detailed, but not construed as limiting the scope of the present invention. It should be noted that, for a person skilled in the art, several variations and modifications can be made without departing from the inventive concept, which falls within the scope of the present invention. Therefore, the protection scope of the present patent shall be subject to the appended claims.
Claims (2)
1. The reaction method of the reaction kettle for the water-based titanium alloy cutting fluid comprises a kettle body and is characterized in that: the kettle body comprises a stirring shaft which is driven by a motor arranged at the top and extends into the inner cavity of the kettle body, a stirring paddle is arranged on the stirring shaft, and the other end of the stirring shaft is fixed in a support frame at the bottom; a heating pipe is sleeved outside the stirring shaft; the top of the kettle body is also provided with a feeding hole, and the bottom of the kettle body is provided with a discharging hole; a spiral turbulence strip is arranged in the inner cavity of the kettle body and clings to the inner wall;
and the water-based titanium alloy cutting fluid comprises a polyethylene glycol ester lubricant;
the stirring paddle is provided with 4-6 blades which are all positioned in a plane vertical to the stirring shaft;
the paddle is formed by overlapping a lower paddle and an upper paddle, the area of the upper paddle is slightly smaller than that of the lower paddle, and the sections of the upper paddle and the lower paddle form a step shape;
the number of the stirring paddles is 3, and the stirring paddles are uniformly distributed on the stirring shaft; the number of the heating pipes is 2, and the heating pipes are positioned between two adjacent stirring paddles;
the included angle between the turbulence strips and the horizontal plane is 30 degrees, the width of the turbulence strips is 1/10 of the inner diameter of the kettle body, and the downward spiral direction of the turbulence strips is consistent with the rotation direction of the stirring paddle;
the polyethylene glycol esters comprise polyethylene glycol fatty acid esters;
the reaction method of the reaction kettle adopting the water-based titanium alloy cutting fluid comprises the steps of sequentially adding water and water-soluble auxiliary materials through a top feeding hole, heating a system to 70-80 ℃ through a heating pipe, keeping stirring, then adding the rest components, wherein the rest components comprise polyethylene glycol ester lubricants, auxiliary lubricants and defoaming agents, continuously stirring under a heating condition, cooling to normal temperature when uniform emulsion is formed, and discharging a finished product of the water-based titanium alloy cutting fluid from a bottom discharging hole; the reaction kettle for the water-based titanium alloy cutting fluid is combined with the stirring paddle through the spiral turbulence strips, so that the turbulence degree is reduced, and the excessive emulsification of the polyethylene glycol ester lubricant is avoided.
2. The reaction method of the reaction kettle for the water-based titanium alloy cutting fluid according to claim 1, characterized in that: the polyethylene glycol fatty acid ester is selected from one or more of polyethylene glycol monostearate, polyethylene glycol distearate, polyethylene glycol monolaurate, polyethylene glycol dilaurate, polyethylene glycol monooleate and polyethylene glycol dioleate.
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WO2007054340A1 (en) * | 2005-11-10 | 2007-05-18 | Vortex-Nanofluid Gmbh | Device comprising guiding devices and method for producing nanodispersions |
JP2014036925A (en) * | 2012-08-15 | 2014-02-27 | Denki Kagaku Kogyo Kk | Agitator and manufacturing method of small size plate member |
CN205925520U (en) * | 2016-08-18 | 2017-02-08 | 海志电源技术(赣州)有限公司 | Agitating unit of release agent |
CN107617400A (en) * | 2017-11-07 | 2018-01-23 | 盐城市大丰匀力机械制造厂 | High-speed stirred reactor |
Family Cites Families (3)
Publication number | Priority date | Publication date | Assignee | Title |
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CN203002369U (en) * | 2012-12-10 | 2013-06-19 | 赣州虔东稀土集团股份有限公司 | Reaction kettle |
CN203990634U (en) * | 2014-08-22 | 2014-12-10 | 倍合德华强(连云港)医药化工科技有限公司 | A kind of vertical response still with function of temperature control |
CN106479657B (en) * | 2016-09-18 | 2019-07-12 | 清华大学天津高端装备研究院 | A kind of water base fully synthetic titanium alloy cutting liquid |
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Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2007054340A1 (en) * | 2005-11-10 | 2007-05-18 | Vortex-Nanofluid Gmbh | Device comprising guiding devices and method for producing nanodispersions |
JP2014036925A (en) * | 2012-08-15 | 2014-02-27 | Denki Kagaku Kogyo Kk | Agitator and manufacturing method of small size plate member |
CN205925520U (en) * | 2016-08-18 | 2017-02-08 | 海志电源技术(赣州)有限公司 | Agitating unit of release agent |
CN107617400A (en) * | 2017-11-07 | 2018-01-23 | 盐城市大丰匀力机械制造厂 | High-speed stirred reactor |
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