CN108651847A - Jujube rice stick and processing method - Google Patents
Jujube rice stick and processing method Download PDFInfo
- Publication number
- CN108651847A CN108651847A CN201810477847.7A CN201810477847A CN108651847A CN 108651847 A CN108651847 A CN 108651847A CN 201810477847 A CN201810477847 A CN 201810477847A CN 108651847 A CN108651847 A CN 108651847A
- Authority
- CN
- China
- Prior art keywords
- jujube
- parts
- water
- powder
- soybean protein
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 235000009566 rice Nutrition 0.000 title claims abstract description 47
- 238000003672 processing method Methods 0.000 title description 3
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- 244000126002 Ziziphus vulgaris Species 0.000 title 1
- 241001247821 Ziziphus Species 0.000 claims abstract description 85
- 239000000843 powder Substances 0.000 claims abstract description 72
- 241000209094 Oryza Species 0.000 claims abstract description 46
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- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 claims abstract description 8
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- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 claims description 14
- 239000000661 sodium alginate Substances 0.000 claims description 14
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- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 12
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- LXNHXLLTXMVWPM-UHFFFAOYSA-N pyridoxine Chemical compound CC1=NC=C(CO)C(CO)=C1O LXNHXLLTXMVWPM-UHFFFAOYSA-N 0.000 claims description 10
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- RADKZDMFGJYCBB-UHFFFAOYSA-N pyridoxal hydrochloride Natural products CC1=NC=C(CO)C(C=O)=C1O RADKZDMFGJYCBB-UHFFFAOYSA-N 0.000 claims description 5
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- QORWJWZARLRLPR-UHFFFAOYSA-H tricalcium bis(phosphate) Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O QORWJWZARLRLPR-UHFFFAOYSA-H 0.000 claims description 5
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Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L7/00—Cereal-derived products; Malt products; Preparation or treatment thereof
- A23L7/10—Cereal-derived products
- A23L7/117—Flakes or other shapes of ready-to-eat type; Semi-finished or partly-finished products therefor
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- A—HUMAN NECESSITIES
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- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L19/00—Products from fruits or vegetables; Preparation or treatment thereof
- A23L19/01—Instant products; Powders; Flakes; Granules
-
- A—HUMAN NECESSITIES
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- A23L19/00—Products from fruits or vegetables; Preparation or treatment thereof
- A23L19/09—Mashed or comminuted products, e.g. pulp, purée, sauce, or products made therefrom, e.g. snacks
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- A—HUMAN NECESSITIES
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- A23L29/015—Inorganic compounds
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- A—HUMAN NECESSITIES
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- A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
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- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
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- A23L5/30—Physical treatment, e.g. electrical or magnetic means, wave energy or irradiation
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- A—HUMAN NECESSITIES
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- A23L7/10—Cereal-derived products
- A23L7/161—Puffed cereals, e.g. popcorn or puffed rice
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- A23L7/17—Preparation of puffed cereals involving preparation of meal or dough as an intermediate step by extrusion
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23P—SHAPING OR WORKING OF FOODSTUFFS, NOT FULLY COVERED BY A SINGLE OTHER SUBCLASS
- A23P10/00—Shaping or working of foodstuffs characterised by the products
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Abstract
The present invention relates to a kind of jujube rice stick, process steps include:It prepares red date powder, prepare red jujube polysaccharide, the preparation of rice stick, the present invention adds red date powder, soyabean protein powder, acetate starch on the basis of traditional rice stick, keep its mouthfeel more rich, adding metal, nonmetallic nutrient powder and red jujube polysaccharide simultaneously keeps its nutrition more rich, and jujube rice stick both with mouthfeel, nutrition is made eventually by extrusion.
Description
Technical field
The invention belongs to food processing fields, are related to millet cake processing technology, especially a kind of jujube rice stick and processing method.
Background technology
Rice stick is a kind of leisure dilated food, and small volume and less weight is easy to carry about with one, and can quickly supplement energy.Currently on the market
The rice stick of sale, which is mostly that corn flour is puffing, to be formed, and most taste is single, cannot meet different crowd demand, some add special mouth
The rice stick of taste, easily causes the loss of nutritional ingredient in the production process, and nutritional ingredient is few, influences the expansion of consumer market.
By the retrieval to existing patent document, following discloses patent document is found:
1, the puffing stick (Publication No. CN107950896A) of a kind of instant type Gorgon fruit glutinous rice, characterized in that using gorgon euryale seed powder,
Glutinous rice flour, corn flour, potato starch, milk powder, white granulated sugar, salt, vegetable oil make, and the puffing stick of Gorgon fruit glutinous rice of the present invention relies on
Starchy material is convenient for puffing advantage, and using rich amyloid Gorgon fruit, glutinous rice, corn and potato starch, milk powder, white is added
Granulated sugar, salt and plant oil component, that is, have additional nutrients and flavor adjustment, puffing stick do not add any harmful substance, peace
Quan Xinggao, full of nutrition, brain healthy, crisp and delicious are conducive to digesting and assimilating for human body, are that nourishing suitable for people of all ages is good
Product;Gorgon fruit dilated food of the present invention is easy to carry, storage is convenient, and opening is instant, is that the good leisure rich in nutritional ingredient is eaten
Product.
By comparison, technical solution disclosed above with the present invention there are larger difference, and it is provided by the present invention
Technical solution and the technique effect reached are superior to above-mentioned each patent document.
Invention content
It is an object of the invention in place of overcome the deficiencies in the prior art, provide one kind to add on the basis of traditional rice stick
Red date powder, soyabean protein powder, acetate starch keep its mouthfeel more rich, while it is more to add metal, nonmetallic nutrient powder and jujube
Sugar keeps its nutrition more rich, and jujube rice stick both with mouthfeel, nutrition is made eventually by extrusion.
The present invention solves its technical problem and following technical scheme is taken to realize:
A kind of jujube rice stick, process steps are as follows:
(1) red date powder is prepared:
1. after 100-200 portions of jujubes are cleaned, stoning, stripping and slicing is placed in 100-150 DEG C of temperature, pressure 1.2 × 105-2.4
×10540-70min is handled under Pa high-temperature and high-pressure conditions, then digests jujube, selects 0.15%-0.5% celluloses
Enzyme, 0.25%-0.5% pectases, hydrolysis temperature are 30-45 DEG C;
2. by step, 1. treated that jujube is put into that temperature is 60-70 DEG C, and vacuum degree is the vacuum dehydrating at lower temperature of -0.2Mpa
8-10h is dried in case, and compound drying aid maltodextrin 20-30%, beta-cyclodextrin 15-20% is added, to shorten drying time,
Reduce cost;
3. by the jujube of drying, add after -40 DEG C of nitrogen charging ultramicro grinding 10min are carried out under the conditions of ultrasonic power 400-600W
Enter to compound 0.1-0.4 parts of antagonist microcrystalline cellulose, 0.1-0.4 parts of tricalcium phosphate, then crushing, time are for the second time for progress
10min crosses 200 mesh sieve;
4. adding date powder quality improver-endo-xylanase 0.01%-0.03%, Arabic gum 0.35-1.5%, mix
It closes uniformly, red date powder is made, it is spare;
(2) red jujube polysaccharide is prepared:
The first step, it is equal with high speed after cooling in 60-65 DEG C of heated-air drying 5h-10h after stripping and slicing in the jujube through over cleaning
Even pulverizer crushes, rotating speed 500r/min-600r/min, time 8min-10min, and 50 mesh sieve is crossed after grinds, spare;
Second step, magnetic field-Subcritical Water Extraction red jujube polysaccharide:Solid-liquid ratio 1 is added in the red date powder handled through the first step:15
Distilled water, be put into the pressure-resistant glass reactor for 18MPa-22MPa, 2.0L-2.5L that magnetic rotor has been added, reach 125
At DEG C -130 DEG C, it is put into the magnetic field intensity in oil bath pan with 0.1T-0.15T, under the mixing speed of 1200r/min-1500r/min
20min-30min is reacted, is cooled to room temperature, reaction mixture is used into vacuum of the Buchner funnel by 0.02MPa-0.04MPa
Decompression filters, and water-insoluble and jujube juice are detached;
Third walks, and by water-insoluble, i.e. jujube slag carries out heated-air drying 4h-5h in 60-65 DEG C, high-speed uniform is used after cooling
Pulverizer crushes, rotating speed 400r/min-500r/min, time 8min-10min, and 50 mesh sieve is crossed after grinds, spare;
The jujube juice of separation is concentrated into 150mL- by the 4th step in a rotary evaporator in 50 DEG C of -60 DEG C of water bath conditions
200mL is added the absolute ethyl alcohol of jujube juice 3-4 times of volume of concentrate, rear natural sedimentation is sufficiently stirred, in 4 DEG C of refrigerator overnights
It preserves, keeps Thick many candies precipitation complete.Precipitation and alcohol soluble substance supernatant are completely separated with vacuum filtration, obtain jujube Thick many candies.
Alcohol soluble substance supernatant is recycled into ethyl alcohol using rotary evaporator at 50 DEG C -60 DEG C, concentrated supernatant is obtained, is put into 105 DEG C of bakings
Dry 3h-4h obtains red jujube polysaccharide to constant weight in case, spare;
(2) prepared by rice stick
1. by 100-200 parts of red date powders, 100-150 parts of rice meals, 10-50 parts of glutinous rice flours, 10-30 parts of acetate starch,
4-5 parts of 10-20 parts of metal nutrient powders, 10-20 parts of nonmetallic nutrient powders and red jujube polysaccharide are uniformly mixed, and suitable quantity of water is added to adjust
Material moisture is to 10-15%;
2. 1. material that step obtains is placed in double helix exrusion bulking machine, screw speed 150-200r/min, squeeze
It is 155-185 DEG C to press swelling temperature;
3. product is cut after the completion of extrusion, length about 5-8cm, you can obtain jujube rice stick.
Moreover, the metal nutrition powder, preparation method thereof is as follows:
(1) soybean protein:Starch=1.5:1 is dissolved in water, adds 7.5U/g SPI enzymes, under 55 DEG C of pre-heating temperatures, stirs
Starch soybean protein mixed gel obtained after mixing 10-20 minutes;
(2) low temperature expanding:Starch soybean protein mixed gel is sent into puffing can container, air compressor pressurization is reached
To 0.08~0.46Mpa, jet chimney is passed through hot steam, and swelling temperature is 60~80 DEG C, after keeping 5-10min, opens valve
Swelling granular is taken out in pressure release, if there is larger particles need to be crushed, forms the particle of 0.5-1.5mm, is full of inside particle netted
Hole;
(3) 2-3 parts of ferrous sulfate, 1-2 parts of zinc lactates, 2-3 parts of calcium citrate malates are placed in 50-80 parts of water, are made
At composite solution;
(4) swelling granular that step (2) obtains is immersed in the composite solution of step (3), nutritional ingredient is loaded to
The netted hole of swelling granular surface and inside impregnates 10-20 minutes, takes out drying;
(5) secondary roller coating:Particle of the step (4) after dry is immersed in starch soybean protein mixed gel, after stirring,
It is dry, metal nutrient powder of the formation diameter in 0.05-2mm.
Moreover, the nonmetallic nutrition powder, preparation method thereof is as follows:
(1) 2-5 parts of multi-vitamins, 1-3 parts of amino acid, 2-3 parts of carboxymethyl celluloses is taken to mix all mentioned components
In suitable quantity of water, uniform complex is formed, the multi-vitamins are vitamin B5, vitamin B6, vitamin C, described
Amino acid be threonine, tryptophan;
(2) preparation of soybean protein porous gel:Soyabean protein powder is scattered in deionized water, 1-4h is stirred, is prepared
At the soy bean proteinous soln of 3-5% (w/w), then it is placed in 4 DEG C of refrigerator and stands overnight, soybean protein is made fully to liquefy,
Then, 10-30min will be heated in water-bath that the solution is placed under certain temperature, so that soybean protein is fully denaturalized, is cooled to room temperature
Afterwards, the MTGase enzymes of 4-6U/g are added in the pH to 6.5-7.0 for adjusting solution, use homogenizer right at 5000r/min immediately after
It carries out homogeneous 0.5-1min, rear to place plastic at room temperature;
(3) complex of step (1) is added in the soybean protein porous gel of step (2), gel is made to carry out it
Load is wrapped up, complex hydrogel is formed;
(4) the complex hydrogel prepared with step (3) is core material, and sodium alginate is that wall material prepares microcapsules, specifically
Steps are as follows:
1. the configuration of solution:A concentration of 3-4% sodium alginates are weighed, it is multiple gradual on a small quantity to be dissolved in distilled water;
2. being vented:It transfers the solution into glass bomb, the air in solution is excluded using ultrasonic wave, is connected to and makes
Grain machine;
3. sampling:80-120mL hydrogels are drawn with threaded syringe, are connected to comminutor.
4. adjusting pressure:Air pump is opened, adjusting inlet pressure can be flowed continually out up to sodium alginate soln, while into
Sample;
5. being granulated:On-load voltage 3000V adjusts frequency, wall material and core material is made to pass through concentric 200 μm of nozzles of the higher-order of oscillation
Microcapsules are formed, microcapsules are scattered in a concentration of 2%-3%CaCl2Cured in solution, cured stir speed (S.S.) is 30-
50%, hardening time 30-40min;
6. finished product:Sample is obtained by filtration, the raffinate of sample surfaces is repeatedly rinsed with deionized water, through vacuum freeze drying 8-
The nonmetallic nutrient powder of a diameter of 0.05-0.2mm is made after 10h, it is spare.
The advantages and positive effects of the present invention are:
1, the processing innovation of red date powder cooperates with crushing technology, jujube using secondary interval low temperature-ultrasonic vibration in the present invention
Compounding anticaking agent microcrystalline cellulose 0.1-0.5g, phosphorus is added after carrying out -40 DEG C of nitrogen charging ultramicro grinding 10min under ultrasound condition in powder
Sour tricalcium 0.1-0.5g, then carries out crushing for second.Secondary interval low temperature-ultrasonic vibration collaboration crushing technology can accelerate powder
Broken speed reduces the loss of heat-sensitive materials, reduces caking, and improve the micromeritis features such as date powder fineness, mobility.
2, the present invention extracts red jujube polysaccharide, extracts technology using jujube-magnetic field-subcritical water, can effectively drop blood
Sugared reducing blood lipid improves the health-care efficacy of bright pink jujube rice stick, retains the nutritional ingredient of polysaccharide in jujube to greatest extent.
3, the present invention adds metal and the nutrients such as nonmetallic in the process of jujube rice stick, is sought using metal
The form addition for supporting powder and nonmetallic dietary powder forms complex water by preparing complex, soybean protein porous gel
Gel, complex hydrogel are core material, and sodium alginate prepares microcapsules for wall material and ultimately forms non-aqueous gel nutritional granular, multiple
Closing microcapsules nutritional granular and is immersed in starch soybean protein mixture puffing particle compound by low temperature expanding soybean protein
In solution, nutritional ingredient is loaded in starch soybean protein mixture puffing particle surface and the reticular structure of inside, effectively
It improves nutritive element content and avoids the mesotrophic loss of baking process.
4, nonmetallic and metal nutriment of the invention enters in puffing soybean protein particle, after puffing
Soybean protein has the specific surface area of bigger, can load is more nonmetallic and metal nutriments, according to experiment, after puffing
The capacity value of 50-60% can be increased, and add hydrogel nutritional granular and composite micro-capsule nutritional granular, Combination in product
Good, nutriment is uniformly dispersed, and improves edible mouthfeel and subsequent absorption, in addition, manufactured product can be realized to battalion
It fully wraps up with supporting substance, while also improving the whole embedding rate of nutriment.
5, the present invention adds red date powder, soyabean protein powder, acetate starch on the basis of traditional rice stick, makes its mouthfeel more
It is abundant, while adding metal, nonmetallic nutrient powder and red jujube polysaccharide keeps its nutrition more rich, and mouth is made eventually by extrusion
Jujube rice stick both with sense, nutrition.
Specific implementation mode
Below by specific embodiment, the invention will be further described, and following embodiment is descriptive, is not limit
Qualitatively, protection scope of the present invention cannot be limited with this.
Embodiment 1
A kind of jujube rice stick, process steps are as follows:
(1) red date powder is prepared:
1. after 100 portions of jujubes are cleaned, stoning, stripping and slicing is placed in 100 DEG C of temperature, pressure 1.2 × 105Pa high temperature and pressure items
40min is handled under part, then digests jujube, selects 0.15% cellulase, 0.25% pectase, hydrolysis temperature 30
℃;
2. by step, 1. treated that jujube is put into that temperature is 60 DEG C, and vacuum degree is the vacuum dehydrating at lower temperature case of -0.2Mpa
Middle drying 8h, and compound drying aid maltodextrin 20% is added, beta-cyclodextrin 15% reduces cost to shorten drying time;
3. by the jujube of drying, it is added again after -40 DEG C of nitrogen charging ultramicro grinding 10min are carried out under the conditions of ultrasonic power 400W
It with 0.1 part of antagonist microcrystalline cellulose, 0.1 part of tricalcium phosphate, then carries out crushing for second, time 10min crosses 200 mesh
Sieve;
4. adding date powder quality improver-endo-xylanase 0.01%, Arabic gum 0.35%, it is uniformly mixed, is made
Red date powder, it is spare;
(2) red jujube polysaccharide is prepared:
The first step, in 60 DEG C of heated-air drying 5h after stripping and slicing, high-speed uniform pulverizer is used after cooling in the jujube through over cleaning
It crushes, rotating speed 500r/min, time 8min, 50 mesh sieve is crossed after grinds, it is spare;
Second step, magnetic field-Subcritical Water Extraction red jujube polysaccharide:Solid-liquid ratio 1 is added in the red date powder handled through the first step:15
Distilled water, be put into the pressure-resistant glass reactor for 18MPa, 2.0L that magnetic rotor has been added, when reaching 125 DEG C, be put into oil
To react 20min under the magnetic field intensity of 0.1T, the mixing speed of 1200r/min in bath, it is cooled to room temperature, by reaction mixture
It is filtered by the vacuum decompression of 0.02MPa using Buchner funnel, water-insoluble and jujube juice is detached;
Third walks, and by water-insoluble, i.e. jujube slag carries out heated-air drying 4h in 60 DEG C, high-speed uniform pulverizer is used after cooling
It crushes, rotating speed 400r/min, time 8min, 50 mesh sieve is crossed after grinds, it is spare;
The jujube juice of separation is concentrated into 150mL in 50 DEG C of water bath conditions, jujube is added by the 4th step in a rotary evaporator
The absolute ethyl alcohol of 3 times of volumes of juice concentrate, is sufficiently stirred rear natural sedimentation, is preserved in 4 DEG C of refrigerator overnights, Thick many candies is made to precipitate
Completely.Precipitation and alcohol soluble substance supernatant are completely separated with vacuum filtration, obtain jujube Thick many candies.By alcohol soluble substance supernatant in 50
Ethyl alcohol is recycled using rotary evaporator at DEG C, obtains concentrated supernatant, dry 3h is put into 105 DEG C of baking ovens to constant weight, obtains red
Jujube polysaccharide, it is spare;
(2) prepared by rice stick
1. by 100 parts of red date powders, 100 parts of rice meals, 10 parts of glutinous rice flours, 10 parts of acetate starch, 10 parts of metal nutrient powders,
4 parts of 10 parts of nonmetallic nutrient powders and red jujube polysaccharide are uniformly mixed, and suitable quantity of water is added to adjust material moisture to 10%;
2. 1. material that step obtains is placed in double helix exrusion bulking machine, screw speed 150r/min, squeeze swollen
It is 155 DEG C to change temperature;
3. product is cut after the completion of extrusion, length about 5cm, you can obtain jujube rice stick.
Moreover, the metal nutrition powder, preparation method thereof is as follows:
(1) soybean protein:Starch=1.5:1 is dissolved in water, adds 7.5U/g SPI enzymes, under 55 DEG C of pre-heating temperatures, stirs
Mix starch soybean protein mixed gel obtained after ten minutes;
(2) low temperature expanding:Starch soybean protein mixed gel is sent into puffing can container, air compressor pressurization is reached
To 0.08Mpa, jet chimney is passed through hot steam, and swelling temperature is 60 DEG C, after keeping 5min, opens valve pressure release, takes out puffing
Particle forms the particle of 0.5mm, is full of netted hole inside particle if there is larger particles need to be crushed;
(3) 2 parts of ferrous sulfate, 1 part of zinc lactate, 2 parts of calcium citrate malates are placed in 50 parts of water, are made compound molten
Liquid;
(4) swelling granular that step (2) obtains is immersed in the composite solution of step (3), nutritional ingredient is loaded to
The netted hole of swelling granular surface and inside impregnates 10 minutes, takes out drying;
(5) secondary roller coating:Particle of the step (4) after dry is immersed in starch soybean protein mixed gel, after stirring,
It is dry, metal nutrient powder of the formation diameter in 0.05mm.
Moreover, the nonmetallic nutrition powder, preparation method thereof is as follows:
(1) 2 parts of multi-vitamins, 1 part of amino acid, 2 parts of carboxymethyl celluloses is taken to be mixed in all mentioned components in right amount
In water, uniform complex is formed, the multi-vitamins are vitamin B5, vitamin B6, vitamin C, the amino
Acid is threonine, tryptophan;
(2) preparation of soybean protein porous gel:Soyabean protein powder is scattered in deionized water, 1h is stirred, is configured to
The soy bean proteinous soln of 3% (w/w), is then placed in 4 DEG C of refrigerator and stands overnight, soybean protein is made fully to liquefy, then,
10min will be heated in water-bath that the solution is placed under certain temperature, soybean protein is made fully to be denaturalized, after being cooled to room temperature, adjusted
The MTGase enzymes of 4U/g are added in the pH to 6.5 of solution, carry out homogeneous to it at 5000r/min with homogenizer immediately after
0.5min, it is rear to place plastic at room temperature;
(3) complex of step (1) is added in the soybean protein porous gel of step (2), gel is made to carry out it
Load is wrapped up, complex hydrogel is formed;
(4) the complex hydrogel prepared with step (3) is core material, and sodium alginate is that wall material prepares microcapsules, specifically
Steps are as follows:
1. the configuration of solution:A concentration of 3% sodium alginate is weighed, it is multiple gradual on a small quantity to be dissolved in distilled water;
2. being vented:It transfers the solution into glass bomb, the air in solution is excluded using ultrasonic wave, is connected to and makes
Grain machine;
3. sampling:80mL hydrogels are drawn with threaded syringe, are connected to comminutor.
4. adjusting pressure:Air pump is opened, adjusting inlet pressure can be flowed continually out up to sodium alginate soln, while into
Sample;
5. being granulated:On-load voltage 3000V adjusts frequency, wall material and core material is made to pass through concentric 200 μm of nozzles of the higher-order of oscillation
Microcapsules are formed, microcapsules are scattered in a concentration of 2%CaCl2Cured in solution, cured stir speed (S.S.) is 30%, solidification
Time 30min;
6. finished product:Sample is obtained by filtration, the raffinate of sample surfaces is repeatedly rinsed with deionized water, through vacuum freeze drying 8-
The nonmetallic nutrient powder of a diameter of 0.05mm is made after 10h, it is spare.
Embodiment 2
A kind of jujube rice stick, process steps are as follows:
(1) red date powder is prepared:
1. after 200 portions of jujubes are cleaned, stoning, stripping and slicing is placed in 150 DEG C of temperature, pressure 2.4 × 105Pa high temperature and pressure items
70min is handled under part, then digests jujube, selects 0.5% cellulase, 0.5% pectase, hydrolysis temperature 45
℃;
2. by step, 1. treated that jujube is put into that temperature is 70 DEG C, and vacuum degree is the vacuum dehydrating at lower temperature case of -0.2Mpa
Middle drying 10h, and compound drying aid maltodextrin 30% is added, beta-cyclodextrin 20% reduces cost to shorten drying time;
3. by the jujube of drying, it is added again after -40 DEG C of nitrogen charging ultramicro grinding 10min are carried out under the conditions of ultrasonic power 600W
It with 0.4 part of antagonist microcrystalline cellulose, 0.4 part of tricalcium phosphate, then carries out crushing for second, time 10min crosses 200 mesh
Sieve;
4. adding date powder quality improver-endo-xylanase 0.03%, Arabic gum 1.5%, it is uniformly mixed, is made red
Date powder, it is spare;
(2) red jujube polysaccharide is prepared:
The first step, in 65 DEG C of heated-air drying 10h after stripping and slicing, is crushed after cooling with high-speed uniform in the jujube through over cleaning
Machine crushes, rotating speed 600r/min, time 10min, and 50 mesh sieve is crossed after grinds, spare;
Second step, magnetic field-Subcritical Water Extraction red jujube polysaccharide:Solid-liquid ratio 1 is added in the red date powder handled through the first step:15
Distilled water, be put into the pressure-resistant glass reactor for 22MPa, 2.5L that magnetic rotor has been added, when reaching 130 DEG C, be put into oil
It to react 30min under the magnetic field intensity of 0.15T, the mixing speed of 1500r/min in bath, is cooled to room temperature, reaction is mixed
Object is filtered using Buchner funnel by the vacuum decompression of 0.04MPa, and water-insoluble and jujube juice are detached;
Third walks, and by water-insoluble, i.e. jujube slag carries out heated-air drying 5h in 65 DEG C, high-speed uniform pulverizer is used after cooling
It crushes, rotating speed 500r/min, time 10min, 50 mesh sieve is crossed after grinds, it is spare;
The jujube juice of separation is concentrated into 200mL in 60 DEG C of water bath conditions, jujube is added by the 4th step in a rotary evaporator
The absolute ethyl alcohol of 4 times of volumes of juice concentrate, is sufficiently stirred rear natural sedimentation, is preserved in 4 DEG C of refrigerator overnights, Thick many candies is made to precipitate
Completely.Precipitation and alcohol soluble substance supernatant are completely separated with vacuum filtration, obtain jujube Thick many candies.By alcohol soluble substance supernatant in 60
Ethyl alcohol is recycled using rotary evaporator at DEG C, obtains concentrated supernatant, dry 4h is put into 105 DEG C of baking ovens to constant weight, obtains red
Jujube polysaccharide, it is spare;
(2) prepared by rice stick
1. by 200 parts of red date powders, 150 parts of rice meals, 50 parts of glutinous rice flours, 30 parts of acetate starch, 20 parts of metal nutrient powders,
5 parts of 20 parts of nonmetallic nutrient powders and red jujube polysaccharide are uniformly mixed, and suitable quantity of water is added to adjust material moisture to 15%;
2. 1. material that step obtains is placed in double helix exrusion bulking machine, screw speed 200r/min, squeeze swollen
It is 185 DEG C to change temperature;
3. product is cut after the completion of extrusion, length about 8cm, you can obtain jujube rice stick.
Moreover, the metal nutrition powder, preparation method thereof is as follows:
(1) soybean protein:Starch=1.5:1 is dissolved in water, adds 7.5U/g SPI enzymes, under 55 DEG C of pre-heating temperatures, stirs
Starch soybean protein mixed gel obtained after mixing 10-20 minutes;
(2) low temperature expanding:Starch soybean protein mixed gel is sent into puffing can container, air compressor pressurization is reached
To 0.46Mpa, jet chimney is passed through hot steam, and swelling temperature is 80 DEG C, after keeping 10min, opens valve pressure release, takes out puffing
Particle forms the particle of 1.5mm, is full of netted hole inside particle if there is larger particles need to be crushed;
(3) 3 parts of ferrous sulfate, 2 parts of zinc lactates, 3 parts of calcium citrate malates are placed in 80 parts of water, are made compound molten
Liquid;
(4) swelling granular that step (2) obtains is immersed in the composite solution of step (3), nutritional ingredient is loaded to
The netted hole of swelling granular surface and inside impregnates 20 minutes, takes out drying;
(5) secondary roller coating:Particle of the step (4) after dry is immersed in starch soybean protein mixed gel, after stirring,
It is dry, metal nutrient powder of the formation diameter in 2mm.
Moreover, the nonmetallic nutrition powder, preparation method thereof is as follows:
(1) 5 parts of multi-vitamins, 3 parts of amino acid, 3 parts of carboxymethyl celluloses is taken to be mixed in all mentioned components in right amount
In water, uniform complex is formed, the multi-vitamins are vitamin B5, vitamin B6, vitamin C, the amino
Acid is threonine, tryptophan;
(2) preparation of soybean protein porous gel:Soyabean protein powder is scattered in deionized water, 4h is stirred, is configured to
The soy bean proteinous soln of 5% (w/w), is then placed in 4 DEG C of refrigerator and stands overnight, soybean protein is made fully to liquefy, then,
30min will be heated in water-bath that the solution is placed under certain temperature, soybean protein is made fully to be denaturalized, after being cooled to room temperature, adjusted
The MTGase enzymes of 6U/g are added in the pH to 7.0 of solution, carry out homogeneous to it at 5000r/min with homogenizer immediately after
1min, it is rear to place plastic at room temperature;
(3) complex of step (1) is added in the soybean protein porous gel of step (2), gel is made to carry out it
Load is wrapped up, complex hydrogel is formed;
(4) the complex hydrogel prepared with step (3) is core material, and sodium alginate is that wall material prepares microcapsules, specifically
Steps are as follows:
1. the configuration of solution:A concentration of 4% sodium alginate is weighed, it is multiple gradual on a small quantity to be dissolved in distilled water;
2. being vented:It transfers the solution into glass bomb, the air in solution is excluded using ultrasonic wave, is connected to and makes
Grain machine;
3. sampling:120mL hydrogels are drawn with threaded syringe, are connected to comminutor.
4. adjusting pressure:Air pump is opened, adjusting inlet pressure can be flowed continually out up to sodium alginate soln, while into
Sample;
5. being granulated:On-load voltage 3000V adjusts frequency, wall material and core material is made to pass through concentric 200 μm of nozzles of the higher-order of oscillation
Microcapsules are formed, microcapsules are scattered in a concentration of 3%CaCl2Cured in solution, cured stir speed (S.S.) is 50%, solidification
Time 40min;
6. finished product:Sample is obtained by filtration, the raffinate of sample surfaces is repeatedly rinsed with deionized water, through vacuum freeze drying
The nonmetallic nutrient powder of a diameter of 0.015mm is made after 10h, it is spare.
Embodiment 3
A kind of jujube rice stick, process steps are as follows:
(1) red date powder is prepared:
1. after 150 portions of jujubes are cleaned, stoning, stripping and slicing is placed in 125 DEG C of temperature, pressure 1.8 × 105Pa high temperature and pressure items
65min is handled under part, then digests jujube, selects 0.35% cellulase, 0.35% pectase, hydrolysis temperature 35
℃;
2. by step, 1. treated that jujube is put into that temperature is 65 DEG C, and vacuum degree is the vacuum dehydrating at lower temperature case of -0.2Mpa
Middle drying 9h, and compound drying aid maltodextrin 25% is added, beta-cyclodextrin 18% reduces cost to shorten drying time;
3. by the jujube of drying, it is added again after -40 DEG C of nitrogen charging ultramicro grinding 10min are carried out under the conditions of ultrasonic power 500W
It with 0.3 part of antagonist microcrystalline cellulose, 0.3 part of tricalcium phosphate, then carries out crushing for second, time 10min crosses 200 mesh
Sieve;
4. adding date powder quality improver-endo-xylanase 0.02%, Arabic gum 0.85%, it is uniformly mixed, is made
Red date powder, it is spare;
(2) red jujube polysaccharide is prepared:
The first step, in 63 DEG C of heated-air drying 8h after stripping and slicing, high-speed uniform pulverizer is used after cooling in the jujube through over cleaning
It crushes, rotating speed 550r/min, time 9min, 50 mesh sieve is crossed after grinds, it is spare;
Second step, magnetic field-Subcritical Water Extraction red jujube polysaccharide:Solid-liquid ratio 1 is added in the red date powder handled through the first step:15
Distilled water, be put into the pressure-resistant glass reactor for 20MPa, 2.3L that magnetic rotor has been added, when reaching 128 DEG C, be put into oil
It to react 25min under the magnetic field intensity of 0.13T, the mixing speed of 13500r/min in bath, is cooled to room temperature, reaction is mixed
Object is filtered using Buchner funnel by the vacuum decompression of 0.03MPa, and water-insoluble and jujube juice are detached;
Third walks, and by water-insoluble, i.e. jujube slag carries out heated-air drying 4.5h in 63 DEG C, crushed with high-speed uniform after cooling
Machine crushes, rotating speed 450r/min, time 9min, and 50 mesh sieve is crossed after grinds, spare;
The jujube juice of separation is concentrated into 180mL in 55 DEG C of water bath conditions, jujube is added by the 4th step in a rotary evaporator
The absolute ethyl alcohol of 3.5 times of volumes of juice concentrate, is sufficiently stirred rear natural sedimentation, is preserved in 4 DEG C of refrigerator overnights, keeps Thick many candies heavy
It forms sediment complete.Precipitation and alcohol soluble substance supernatant are completely separated with vacuum filtration, obtain jujube Thick many candies.By alcohol soluble substance supernatant in
Ethyl alcohol is recycled using rotary evaporator at 55 DEG C, obtains concentrated supernatant, dry 3.5h is put into 105 DEG C of baking ovens to constant weight, obtains
It is spare to red jujube polysaccharide;
(2) prepared by rice stick
1. by 150 parts of red date powders, 120 parts of rice meals, 40 parts of glutinous rice flours, 20 parts of acetate starch, 15 parts of metal nutrient powders,
4.5 parts of 15 parts of nonmetallic nutrient powders and red jujube polysaccharide are uniformly mixed, and suitable quantity of water is added to adjust material moisture to 13%;
2. 1. material that step obtains is placed in double helix exrusion bulking machine, screw speed 180r/min, squeeze swollen
It is 170 DEG C to change temperature;
3. product is cut after the completion of extrusion, length about 6cm, you can obtain jujube rice stick.
Moreover, the metal nutrition powder, preparation method thereof is as follows:
(1) soybean protein:Starch=1.5:1 is dissolved in water, adds 7.5U/g SPI enzymes, under 55 DEG C of pre-heating temperatures, stirs
Starch soybean protein mixed gel obtained after mixing 10-20 minutes;
(2) low temperature expanding:Starch soybean protein mixed gel is sent into puffing can container, air compressor pressurization is reached
To 0.35Mpa, jet chimney is passed through hot steam, and swelling temperature is 70 DEG C, after keeping 8min, opens valve pressure release, takes out puffing
Particle forms the particle of 1.2mm, is full of netted hole inside particle if there is larger particles need to be crushed;
(3) 2.5 parts of ferrous sulfate, 1.5 parts of zinc lactates, 2.5 parts of calcium citrate malates are placed in 70 parts of water, are made multiple
Close solution;
(4) swelling granular that step (2) obtains is immersed in the composite solution of step (3), nutritional ingredient is loaded to
The netted hole of swelling granular surface and inside impregnates 15 minutes, takes out drying;
(5) secondary roller coating:Particle of the step (4) after dry is immersed in starch soybean protein mixed gel, after stirring,
It is dry, metal nutrient powder of the formation diameter in 0.1mm.
Moreover, the nonmetallic nutrition powder, preparation method thereof is as follows:
(1) 3 parts of multi-vitamins, 2 parts of amino acid, 2.5 parts of carboxymethyl celluloses is taken to be mixed in all mentioned components suitable
It measures in water, forms uniform complex, the multi-vitamins are vitamin B5, vitamin B6, vitamin C, the ammonia
Base acid is threonine, tryptophan;
(2) preparation of soybean protein porous gel:Soyabean protein powder is scattered in deionized water, 1-4h is stirred, is prepared
At the soy bean proteinous soln of 3-5% (w/w), then it is placed in 4 DEG C of refrigerator and stands overnight, soybean protein is made fully to liquefy,
Then, 15min will be heated in water-bath that the solution is placed under certain temperature, soybean protein is made fully to be denaturalized, after being cooled to room temperature,
The pH to 6.8 for adjusting solution, is added the MTGase enzymes of 5U/g, is carried out to it at 5000r/min with homogenizer immediately after
Matter 0.8min, it is rear to place plastic at room temperature;
(3) complex of step (1) is added in the soybean protein porous gel of step (2), gel is made to carry out it
Load is wrapped up, complex hydrogel is formed;
(4) the complex hydrogel prepared with step (3) is core material, and sodium alginate is that wall material prepares microcapsules, specifically
Steps are as follows:
1. the configuration of solution:A concentration of 3.5% sodium alginate is weighed, it is multiple gradual on a small quantity to be dissolved in distilled water;
2. being vented:It transfers the solution into glass bomb, the air in solution is excluded using ultrasonic wave, is connected to and makes
Grain machine;
3. sampling:100mL hydrogels are drawn with threaded syringe, are connected to comminutor.
4. adjusting pressure:Air pump is opened, adjusting inlet pressure can be flowed continually out up to sodium alginate soln, while into
Sample;
5. being granulated:On-load voltage 3000V adjusts frequency, wall material and core material is made to pass through concentric 200 μm of nozzles of the higher-order of oscillation
Microcapsules are formed, microcapsules are scattered in a concentration of 2%-3%CaCl2Being cured in solution, cured stir speed (S.S.) is 40%,
Hardening time 35min;
6. finished product:Sample is obtained by filtration, the raffinate of sample surfaces is repeatedly rinsed with deionized water, through vacuum freeze drying 9h
The nonmetallic nutrient powder of a diameter of 0.15mm is made afterwards, it is spare.
The content of each substance is as follows in finished product after measured:
Although disclosing the embodiment of the present invention for the purpose of illustration, it will be appreciated by those skilled in the art that:Not
Be detached from the present invention and spirit and scope of the appended claims in, various substitutions, changes and modifications be all it is possible, therefore, this
The range of invention is not limited to embodiment disclosure of that.
Claims (3)
1. a kind of jujube rice stick, it is characterised in that:Process steps are as follows:
(1) red date powder is prepared:
1. after 100-200 portions of jujubes are cleaned, stoning, stripping and slicing is placed in 100-150 DEG C of temperature, pressure 1.2 × 105-2.4×
10540-70min is handled under Pa high-temperature and high-pressure conditions, then digests jujube, selects 0.15%-0.5% cellulases,
0.25%-0.5% pectases, hydrolysis temperature are 30-45 DEG C;
2. by step, 1. treated that jujube is put into that temperature is 60-70 DEG C, and vacuum degree is in the vacuum dehydrating at lower temperature case of -0.2Mpa
8-10h is dried, and compound drying aid maltodextrin 20-30%, beta-cyclodextrin 15-20% is added, to shorten drying time, is reduced
Cost;
3. by the jujube of drying, it is added again after -40 DEG C of nitrogen charging ultramicro grinding 10min are carried out under the conditions of ultrasonic power 400-600W
It with 0.1-0.4 parts of antagonist microcrystalline cellulose, 0.1-0.4 parts of tricalcium phosphate, then carries out crushing for second, time 10min,
Cross 200 mesh sieve;
4. adding date powder quality improver-endo-xylanase 0.01%-0.03%, Arabic gum 0.35-1.5%, mixing is equal
It is even, red date powder is made, it is spare;
(2) red jujube polysaccharide is prepared:
The first step, in 60-65 DEG C of heated-air drying 5h-10h after stripping and slicing, high-speed uniform powder is used after cooling in the jujube through over cleaning
Broken machine crushes, rotating speed 500r/min-600r/min, time 8min-10min, and 50 mesh sieve is crossed after grinds, spare;
Second step, magnetic field-Subcritical Water Extraction red jujube polysaccharide:Solid-liquid ratio 1 is added in the red date powder handled through the first step:15 steaming
Distilled water is put into the pressure-resistant glass reactor for 18MPa-22MPa, 2.0L-2.5L that magnetic rotor has been added, reach 125 DEG C-
At 130 DEG C, it is put into the magnetic field intensity in oil bath pan with 0.1T-0.15T, anti-under the mixing speed of 1200r/min-1500r/min
20min-30min is answered, is cooled to room temperature, reaction mixture is subtracted using Buchner funnel by the vacuum of 0.02MPa-0.04MPa
Pressure filters, and water-insoluble and jujube juice are detached;
Third walks, and by water-insoluble, i.e. jujube slag carries out heated-air drying 4h-5h in 60-65 DEG C, crushed with high-speed uniform after cooling
Machine crushes, rotating speed 400r/min-500r/min, time 8min-10min, and 50 mesh sieve is crossed after grinds, spare;
The jujube juice of separation is concentrated into 150mL-200mL by the 4th step in a rotary evaporator in 50 DEG C of -60 DEG C of water bath conditions,
The absolute ethyl alcohol of jujube juice 3-4 times of volume of concentrate is added, is sufficiently stirred rear natural sedimentation, preserves, makes in 4 DEG C of refrigerator overnights
Thick many candies precipitation is complete.Precipitation and alcohol soluble substance supernatant are completely separated with vacuum filtration, obtain jujube Thick many candies.By alcohol soluble substance
Supernatant recycles ethyl alcohol at 50 DEG C -60 DEG C using rotary evaporator, obtains concentrated supernatant, is put into 105 DEG C of baking ovens dry
3h-4h obtains red jujube polysaccharide to constant weight, spare;
(2) prepared by rice stick
1. by 100-200 parts of red date powders, 100-150 parts of rice meals, 10-50 parts of glutinous rice flours, 10-30 parts of acetate starch, 10-20
4-5 parts of part metal nutrient powder, 10-20 parts of nonmetallic nutrient powders and red jujube polysaccharide are uniformly mixed, and suitable quantity of water is added to adjust material
Water content is to 10-15%;
2. 1. material that step obtains is placed in double helix exrusion bulking machine, screw speed 150-200r/min, squeeze swollen
It is 155-185 DEG C to change temperature;
3. product is cut after the completion of extrusion, length about 5-8cm, you can obtain jujube rice stick.
2. a kind of jujube rice stick according to claim 1, it is characterised in that:The metal nutrition powder, preparation method thereof is such as
Under:
(1) soybean protein:Starch=1.5:1 is dissolved in water, adds 7.5U/g SPI enzymes, under 55 DEG C of pre-heating temperatures, stirs 10-
Starch soybean protein mixed gel obtained after twenty minutes;
(2) low temperature expanding:Starch soybean protein mixed gel is sent into puffing can container, air compressor pressurization is reached
0.08~0.46Mpa, jet chimney are passed through hot steam, and swelling temperature is 60~80 DEG C, after keeping 5-10min, open valve and let out
Pressure takes out swelling granular, if there is larger particles need to be crushed, forms the particle of 0.5-1.5mm, is full of netted sky inside particle
Cave;
(3) 2-3 parts of ferrous sulfate, 1-2 parts of zinc lactates, 2-3 parts of calcium citrate malates are placed in 50-80 parts of water, are made multiple
Close solution;
(4) swelling granular that step (2) obtains is immersed in the composite solution of step (3), nutritional ingredient is loaded to puffing
The netted hole of particle surface and inside impregnates 10-20 minutes, takes out drying;
(5) secondary roller coating:Particle of the step (4) after dry is immersed in starch soybean protein mixed gel, after stirring, is done
It is dry, metal nutrient powder of the formation diameter in 0.05-2mm.
3. a kind of jujube rice stick according to claim 1, it is characterised in that:The nonmetallic nutrition powder, preparation method thereof is such as
Under:
(1) 2-5 parts of multi-vitamins, 1-3 parts of amino acid, 2-3 parts of carboxymethyl celluloses is taken to be mixed in all mentioned components suitable
It measures in water, forms uniform complex, the multi-vitamins are vitamin B5, vitamin B6, vitamin C, the ammonia
Base acid is threonine, tryptophan;
(2) preparation of soybean protein porous gel:Soyabean protein powder is scattered in deionized water, 1-4h is stirred, is configured to 3-
The soy bean proteinous soln of 5% (w/w), is then placed in 4 DEG C of refrigerator and stands overnight, soybean protein is made fully to liquefy, then,
10-30min will be heated in water-bath that the solution is placed under certain temperature, soybean protein is made fully to be denaturalized, after being cooled to room temperature, adjusted
Save solution pH to 6.5-7.0, the MTGase enzymes of 4-6U/g are added, immediately after use homogenizer at 5000r/min to its into
Row homogeneous 0.5-1min, it is rear to place plastic at room temperature;
(3) complex of step (1) is added in the soybean protein porous gel of step (2), gel is made to wrap up it
Load forms complex hydrogel;
(4) for the complex hydrogel prepared with step (3) for core material, sodium alginate is that wall material prepares microcapsules, specific steps
It is as follows:
1. the configuration of solution:A concentration of 3-4% sodium alginates are weighed, it is multiple gradual on a small quantity to be dissolved in distilled water;
2. being vented:It transfers the solution into glass bomb, the air in solution is excluded using ultrasonic wave, is connected to granulation
Machine;
3. sampling:80-120mL hydrogels are drawn with threaded syringe, are connected to comminutor.
4. adjusting pressure:Air pump is opened, adjusting inlet pressure can be flowed continually out up to sodium alginate soln, while sample introduction;
5. being granulated:On-load voltage 3000V adjusts frequency, concentric 200 μm of nozzles that wall material and core material pass through the higher-order of oscillation is made to be formed
Microcapsules, microcapsules are scattered in a concentration of 2%-3%CaCl2Being cured in solution, cured stir speed (S.S.) is 30-50%,
Hardening time 30-40min;
6. finished product:Sample is obtained by filtration, the raffinate of sample surfaces is repeatedly rinsed with deionized water, through vacuum freeze drying 8-10h
The nonmetallic nutrient powder of a diameter of 0.05-0.2mm is made afterwards, it is spare.
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN112075603A (en) * | 2020-09-25 | 2020-12-15 | 新疆天辰智慧信息科技有限公司 | Red date superfine powder and preparation method thereof |
CN113208029A (en) * | 2021-05-27 | 2021-08-06 | 上海应用技术大学 | Method for preparing red date powder by vacuum drying |
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CN101999728A (en) * | 2010-10-15 | 2011-04-06 | 陕西科技大学 | Microwave drying instant red date powder and production method thereof |
CN102079792A (en) * | 2010-12-09 | 2011-06-01 | 江南大学 | Gold thread jujube acidic polysaccharide extraction and structural characterization |
CN103783121A (en) * | 2014-03-04 | 2014-05-14 | 刘少伟 | Puffed grain energy bar |
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CN101999728A (en) * | 2010-10-15 | 2011-04-06 | 陕西科技大学 | Microwave drying instant red date powder and production method thereof |
CN102079792A (en) * | 2010-12-09 | 2011-06-01 | 江南大学 | Gold thread jujube acidic polysaccharide extraction and structural characterization |
CN103783121A (en) * | 2014-03-04 | 2014-05-14 | 刘少伟 | Puffed grain energy bar |
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Publication number | Priority date | Publication date | Assignee | Title |
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CN112075603A (en) * | 2020-09-25 | 2020-12-15 | 新疆天辰智慧信息科技有限公司 | Red date superfine powder and preparation method thereof |
CN113208029A (en) * | 2021-05-27 | 2021-08-06 | 上海应用技术大学 | Method for preparing red date powder by vacuum drying |
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