CN108651603A - A kind of phosphate-free water-retaining agent and its application in aquatic products - Google Patents
A kind of phosphate-free water-retaining agent and its application in aquatic products Download PDFInfo
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- CN108651603A CN108651603A CN201810339178.7A CN201810339178A CN108651603A CN 108651603 A CN108651603 A CN 108651603A CN 201810339178 A CN201810339178 A CN 201810339178A CN 108651603 A CN108651603 A CN 108651603A
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- phosphate
- retaining agent
- free water
- aquatic products
- water
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23B—PRESERVING, e.g. BY CANNING, MEAT, FISH, EGGS, FRUIT, VEGETABLES, EDIBLE SEEDS; CHEMICAL RIPENING OF FRUIT OR VEGETABLES; THE PRESERVED, RIPENED, OR CANNED PRODUCTS
- A23B4/00—General methods for preserving meat, sausages, fish or fish products
- A23B4/14—Preserving with chemicals not covered by groups A23B4/02 or A23B4/12
- A23B4/18—Preserving with chemicals not covered by groups A23B4/02 or A23B4/12 in the form of liquids or solids
- A23B4/20—Organic compounds; Microorganisms; Enzymes
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23B—PRESERVING, e.g. BY CANNING, MEAT, FISH, EGGS, FRUIT, VEGETABLES, EDIBLE SEEDS; CHEMICAL RIPENING OF FRUIT OR VEGETABLES; THE PRESERVED, RIPENED, OR CANNED PRODUCTS
- A23B4/00—General methods for preserving meat, sausages, fish or fish products
- A23B4/14—Preserving with chemicals not covered by groups A23B4/02 or A23B4/12
- A23B4/18—Preserving with chemicals not covered by groups A23B4/02 or A23B4/12 in the form of liquids or solids
- A23B4/24—Inorganic compounds
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Abstract
A kind of application the invention discloses phosphate-free water-retaining agent and its in aquatic products.It includes, by percentage to the quality, soybean fiber 6.7%~42.9%, acidity regulator 30.8%~88.9%, glycine 0~28.6%, trehalose 0~44.4%.Dosage of the phosphate-free water-retaining agent in aquatic products soak is 0.1%~5.0%.The phosphate-free water-retaining agent of the present invention can significantly improve retentiveness of the aquatic products in immersion, chilled storage, defrosting and digestion process, prevent juice loss of aquatic products during processing and storage, and not phosphorus element-containing, the phosphate excessive problem brought because adding excessive phosphoric acid salt water-retaining agent can be avoided.To improving the quality of frozen fish, develops safe and nontoxic phosphate-free water-retaining agent and be of great significance.
Description
Technical field
The invention belongs to technical field of aquatic product processing, and in particular to a kind of phosphate-free water-retaining agent and its answering in aquatic products
With.
Background technology
Aquatic products, since solute concentration and ice crystal are formed, easily cause aquatic products meat to change in freezing, with
The extension of cooling time, the protein freeze denaturalization contained in aquatic products, retentiveness, gelling, tenderness and nutritive value
Deterioration occurs.When defrosting or boiling aquatic products, juice loss increases, and it is hard, frangible just to will appear carnification, coarse mouthfeel,
Phenomena such as appearance luster changes.Aquatic products common water-retaining agent is freezed when phosphate, it can improve the pH value of aquatic products itself, and make
It is maintained at neutral left and right；Cause the increase of ionic strength；Dissociation and the chelated metal ions for promoting actomyosin, to
The water retention property and gel strength of aquatic products can be improved.But long-term intake phosphate can influence human calcium's phosphorus balance, endanger body
Body health.Therefore, it to improve the quality of frozen fish, develops safe and nontoxic phosphate-free water-retaining agent and is of great significance.
Invention content
The purpose of this part is to summarize some aspects of the embodiment of the present invention and briefly introduce some preferably to implement
Example.It may do a little simplified or be omitted to avoid our department is made in this section and the description of the application and the title of the invention
Point, the purpose of abstract of description and denomination of invention it is fuzzy, and this simplification or omit and cannot be used for limiting the scope of the invention.
In view of above-mentioned technological deficiency, it is proposed that the present invention.
Therefore, as one aspect of the present invention, the present invention overcomes the deficiencies in the prior art, provides a kind of nothing
Phosphorus water-retaining agent.
In order to solve the above technical problems, the present invention provides following technical solutions：A kind of phosphate-free water-retaining agent comprising, with
Mass percent meter,
A kind of preferred embodiment as phosphate-free water-retaining agent of the present invention comprising, by percentage to the quality,
As a kind of preferred embodiment of phosphate-free water-retaining agent of the present invention, wherein：The soybean fiber includes that soybean is more
Sugar.
As a kind of preferred embodiment of phosphate-free water-retaining agent of the present invention, wherein：The acidity regulator includes carbonic acid
One or both of sodium, sodium citrate, sodium bicarbonate or three kinds.
As a kind of preferred embodiment of phosphate-free water-retaining agent of the present invention, wherein：The acidity regulator is sodium carbonate：
Sodium citrate in mass ratio 2：1 compounding.
As another aspect of the present invention, the present invention overcomes the deficiencies of the prior art and provide phosphate-free water-retaining agent in aquatic products
Application in product.
As a kind of preferred embodiment of application of the phosphate-free water-retaining agent of the present invention in aquatic products, wherein：It is described without phosphorus
Dosage of the water-retaining agent in aquatic products is by quality ratio 0.1%~5.0%.
As a kind of preferred embodiment of application of the phosphate-free water-retaining agent of the present invention in aquatic products, wherein：It is described without phosphorus
Dosage of the water-retaining agent in aquatic products is by quality ratio 1%~3%.
As a kind of preferred embodiment of application of the phosphate-free water-retaining agent of the present invention in aquatic products, wherein：The aquatic products
Product, including fish, shrimps.
A kind of preferred embodiment as application of the phosphate-free water-retaining agent of the present invention in aquatic products comprising, it will be described
Aquatic products are soaked in the phosphate-free water-retaining agent, impregnate 4~10h in 4~8 DEG C.
Beneficial effects of the present invention：The phosphate-free water-retaining agent of the present invention can significantly improve aquatic products in immersion, chilled storage, solution
Retentiveness in jelly and digestion process, prevents juice loss of aquatic products during processing and storage, and not phosphorus element-containing, can
Avoid the phosphate excessive problem brought because adding excessive phosphoric acid salt water-retaining agent.To improving the quality of frozen fish, open
The phosphate-free water-retaining agent for sending out safe and nontoxic is of great significance.
Specific implementation mode
In order to make the foregoing objectives, features and advantages of the present invention clearer and more comprehensible, with reference to specific embodiment pair
The specific implementation mode of the present invention is described in detail.
Many details are elaborated in the following description to facilitate a thorough understanding of the present invention, still the present invention can be with
Implemented different from other manner described here using other, those skilled in the art can be without prejudice to intension of the present invention
In the case of do similar popularization, therefore the present invention is not limited by following public specific embodiment.
Secondly, " one embodiment " or " embodiment " referred to herein refers to that may be included at least one realization side of the present invention
A particular feature, structure, or characteristic in formula." in one embodiment " that different places occur in the present specification not refers both to
The same embodiment, nor the individual or selective embodiment mutually exclusive with other embodiment.
Embodiment 1：
A kind of phosphate-free water-retaining agent compounds mixing by following raw material, is calculated according to weight, including：Soybean fiber
10%, acidity regulator 60%, glycine 10%, trehalose 10%.The dosage of the phosphate-free water-retaining agent is 1.0% (quality percentage
Content).
By taking the silver carp flesh of fish as an example, phosphate-free water-retaining agent of the present invention is as follows applied to the silver carp flesh of fish：
1) by fresh Silver Carp decaptitating, truncate, scale, remove internal organ, flesh of fish thickness is 2cm when slice, cleans, drains standby
With；
2) the silver carp flesh of fish is soaked in the phosphate-free water-retaining agent fully dissolved, 4 DEG C of immersion 6h are dried after immersion with paper handkerchief
Surface solution；
3) the silver carp flesh of fish after impregnating, which is placed in -20 DEG C of refrigerators, to be freezed one week；
4) silver carp flesh of fish placement is thawed after a certain period of time, and carries out boiling, digestion time 4min.
By taking Roche shrimp as an example, it is as follows applied to Roche shrimp：
1) by fresh Roche shrimp decaptitating, truncate, remove shrimp line, clean, drain it is rear spare；
2) Roche shrimp is soaked in the phosphate-free water-retaining agent fully dissolved, 4 DEG C of immersion 6h are dried after immersion with paper handkerchief
Surface solution；
3) the Roche shrimp after impregnating, which is placed in -20 DEG C of refrigerators, to be freezed one week；
4) Roche shrimp placement is thawed after a certain period of time, and carries out boiling, digestion time 2min.
Embodiment 2：
A kind of phosphate-free water-retaining agent compounds mixing by following raw material, is calculated according to weight, including：Soybean fiber
14.3%, acidity regulator 85.7%.The dosage of the phosphate-free water-retaining agent is 3.0%.Specific implementation step such as embodiment 1.
Embodiment 3：
A kind of phosphate-free water-retaining agent compounds mixing by following raw material, is calculated according to weight, including：Soybean fiber
42.9%, acidity regulator 45.0%, trehalose 12.1%.The dosage of the phosphate-free water-retaining agent is 3.0%.Specific implementation step is such as
Embodiment 1.
Embodiment 4：
A kind of phosphate-free water-retaining agent compounds mixing by following raw material, is calculated according to weight, including：Soybean fiber
8.3%, acidity regulator 88.9%, glycine 2.8%.The dosage of the phosphate-free water-retaining agent is 3.0%.Specific implementation step is strictly according to the facts
Apply example 1.
Embodiment 5 (comparative example 1)：
A kind of phosphate-free water-retaining agent compounds mixing by following raw material, is calculated according to weight, including：Acidity adjustment
Agent 60%, glycine 10%, trehalose 20%.The dosage of the phosphate-free water-retaining agent is 1.0%.Specific implementation step such as embodiment 1.
Embodiment 6 (comparative example 2)：
A kind of common phosphate-free water-retaining agent formula compounds mixing by following raw material, is calculated according to weight, wrapped
It includes：Sodium carbonate 20%, sodium bicarbonate 35%, sodium citrate 25%, edible salt 15%, L MALIC ACID 5%.The phosphate-free water-retaining agent
Dosage is 3.0%.Specific implementation step such as embodiment 1.
Embodiment 7 (comparative example 3)：
Using commercially available phosphorous water-retaining agent, the dosage of the phosphorous water-retaining agent is 3.0%.Specific implementation step such as embodiment 1.
Embodiment 8 (comparative example 4)：
A kind of phosphate-free water-retaining agent compounds mixing by following raw material, is calculated according to weight, including：Acidity adjustment
Agent 90%, trehalose 10%.The dosage of the phosphate-free water-retaining agent is 1.0%.Specific implementation step such as embodiment 1.
Embodiment 9 (comparative example 5)：
A kind of phosphate-free water-retaining agent compounds mixing by following raw material, is calculated according to weight, including：Acidity adjustment
Agent 90%, glycine 10%.The dosage of the phosphate-free water-retaining agent is 1.0%.Specific implementation step such as embodiment 1.
Acidity regulator of the present invention includes one or both of sodium carbonate, sodium citrate, sodium bicarbonate or three kinds, preferably
For sodium carbonate：Sodium citrate in mass ratio 2：1 compounding.
Soybean fiber used in the present invention, preferably soybean polyoses.
Index determining：
1) water absorption rate (%)=(weight-original weight after immersion)/original weight × 100%
2) defrosting weight-loss ratio (%)=(weight after original weight-defrosting)/original weight × 100%
3) weight × 100% after cooking loss rate (%)=(weight after weight-boiling after defrosting)/defrosting
Water absorption rate, defrosting weight-loss ratio and the cooking loss rate of 1 aquatic products of table
From comparative example 1 and comparative example 2 as can be seen that the addition of soybean fiber keeps the defrosting loss of aquatic products and cooking loss bright
It is aobvious to reduce, illustrate that soybean fiber can improve the frost resistance of aquatic products.Loss main cause of thawing is the muscle in frozen storage
Internal water forms ice crystal, make protein molecule be squeezed concentrations, agglomerate mutually, while destroying cell membrane, lead to protein
Denaturation causes water loss.Fribrillin is the main component freezed in the flesh of fish, the fish meat protein meeting in frozen storage
Two kinds of denaturation occur, when the aggregation of protein molecule, second is that the expansion of protein and peptide chain.Combination water in structure of fish muscle with
Protein molecule is firmly combined with, and with the extension of refrigeration time, freezing rate increases, and is taken off in conjunction with protein molecule is made after water crystallization
Water causes certain reactive groups to be assembled, and causes the solidifying of protein by forming disulfide bond, hydrophobic bond, hydrogen bond etc. and be combineding with each other
Fusion.The distribution of chemical bond and surrounding water molecules state are closely related in protein molecule.When moisture does not freeze, protein point
Sub- height aquation, the non-polar group on polypeptide chain are located at intramolecule, and macroscopic property is more stable, between non-polar group
Chemical bond also make this state more stablize.When moisture freezes, the degree of hydration of protein declines, in addition ice crystal mutually squeezes
Pressure, makes protein molecule higher structure change, the expansion of protein is caused to be denaturalized.Soybean fiber may pass through capillary etc.
Active force penetrates into muscle, interacts with muscle protein, to increase the space between meat fiber, moisture can enter
In muscle fibril structure；Soybean fiber may form one layer of fine and close wrap film on aquatic products surface simultaneously, make the moisture of infiltration more
Good is retained in muscle, reduces the loss of internal Free water and unbound water.
Sensory evaluation is tested：After aquatic products boiling, subjective appreciation experiment is carried out.Experiment sensory evaluation group is to have received profession
The composition of personnel of sense organ training shares 5 people, scores indexs of correlation such as the flavour of sample, texture, appearances, standards of grading
It is as follows：
2 sensory evaluation scores standard of table
3 sensory evaluation scores table of table
| Project | Flavour | Texture | Appearance |
| Embodiment 1 | 29 | 29 | 29 |
| Embodiment 2 | 28 | 27 | 29 |
| Embodiment 3 | 26 | 26 | 28 |
| Embodiment 4 | 26 | 26 | 26 |
| Comparative example 1 | 22 | 21 | 21 |
| Comparative example 2 | 19 | 16 | 20 |
| Comparative example 3 | 11 | 26 | 26 |
From comparative example 2 and comparative example 3 as can be seen that acidity regulator can not improve the freeze proof water retention property of aquatic products,
Meanwhile although can improve the texture and appearance of aquatic products containing phosphatic water-retaining agent, obtained product has apparent puckery
Mouthfeel and metallic taste.
Embodiment 10：
A kind of phosphate-free water-retaining agent compounds mixing by following raw material, is calculated according to weight, including：Soybean fiber
10%, acidity regulator 60%, glycine 10%, trehalose 10%.The dosage of the phosphate-free water-retaining agent is 0.1%.
By taking the silver carp flesh of fish as an example, phosphate-free water-retaining agent of the present invention is as follows applied to the silver carp flesh of fish：
1) by fresh Silver Carp decaptitating, truncate, scale, remove internal organ, flesh of fish thickness is 2cm when slice, cleans, drains standby
With；
2) the silver carp flesh of fish is soaked in the phosphate-free water-retaining agent fully dissolved, 4 DEG C of immersion 6h are dried after immersion with paper handkerchief
Surface solution；
3) the silver carp flesh of fish after impregnating, which is placed in -20 DEG C of refrigerators, to be freezed one week；
4) silver carp flesh of fish placement is thawed after a certain period of time, and carries out boiling, digestion time 4min.
By taking Roche shrimp as an example, it is as follows applied to Roche shrimp：
1) by fresh Roche shrimp decaptitating, truncate, remove shrimp line, clean, drain it is rear spare；
2) Roche shrimp is soaked in the phosphate-free water-retaining agent fully dissolved, 4 DEG C of immersion 6h are dried after immersion with paper handkerchief
Surface solution；
3) the Roche shrimp after impregnating, which is placed in -20 DEG C of refrigerators, to be freezed one week；
4) Roche shrimp placement is thawed after a certain period of time, and carries out boiling, digestion time 2min.
Embodiment 11：
A kind of phosphate-free water-retaining agent compounds mixing by following raw material, is calculated according to weight, including：Soybean fiber
10%, acidity regulator 60%, glycine 10%, trehalose 10%.The dosage of the phosphate-free water-retaining agent is 5.0%.
By taking the silver carp flesh of fish as an example, phosphate-free water-retaining agent of the present invention is as follows applied to the silver carp flesh of fish：
1) by fresh Silver Carp decaptitating, truncate, scale, remove internal organ, flesh of fish thickness is 2cm when slice, cleans, drains standby
With；
2) the silver carp flesh of fish is soaked in the phosphate-free water-retaining agent fully dissolved, 4 DEG C of immersion 6h are dried after immersion with paper handkerchief
Surface solution；
3) the silver carp flesh of fish after impregnating, which is placed in -20 DEG C of refrigerators, to be freezed one week；
4) silver carp flesh of fish placement is thawed after a certain period of time, and carries out boiling, digestion time 4min.
By taking Roche shrimp as an example, it is as follows applied to Roche shrimp：
1) by fresh Roche shrimp decaptitating, truncate, remove shrimp line, clean, drain it is rear spare；
2) Roche shrimp is soaked in the phosphate-free water-retaining agent fully dissolved, 4 DEG C of immersion 6h are dried after immersion with paper handkerchief
Surface solution；
3) the Roche shrimp after impregnating, which is placed in -20 DEG C of refrigerators, to be freezed one week；
4) Roche shrimp placement is thawed after a certain period of time, and carries out boiling, digestion time 2min.
To sum up, aquatic products phosphate-free water-retaining agent of the invention contains soybean fiber, acidity regulator, glycine, trehalose,
Using when be uniformly mixed according to a certain percentage.The phosphate-free water-retaining agent can significantly improve the water retention property and texture of aquatic products,
Its freezing, freeze thaw stability is improved, juice loss is prevented, adsorbs free moisture.In the present invention, glucide can by with egg
White matter reactive group combines, and so that protein is in saturation state to avoid the aggregation between protein from being denaturalized, free hydroxyl group is also
Free water can be promoted to be converted into conjunction with water, to reduce " eutectic point " temperature, the quantity for forming ice crystal is reduced, slow down albumen
The mutual aggregation of matter, to prevent the cohesion of albumen to be denaturalized.Sodium carbonate, sodium citrate and sodium bicarbonate play the work of deacidification agent
With, and Water-saving effect is good.Amino acid contains the functional group of the hydroxyls such as carboxyl, and being added in aquatic product can be with protein phase
Good water conservation and cryoprotective effects are played in interaction.
The phosphate-free water-retaining agent of the present invention can significantly improve aquatic products in immersion, chilled storage, defrosting and digestion process
Retentiveness prevents juice loss of aquatic products during processing and storage, and not phosphorus element-containing, can avoid because adding excessively
The phosphate excessive problem that phosphoric acid salt water-retaining agent is brought.To improving the quality of frozen fish, develop safe and nontoxic without phosphorus
Water-retaining agent is of great significance.
It should be noted that the above examples are only used to illustrate the technical scheme of the present invention and are not limiting, although with reference to preferable
Embodiment describes the invention in detail, it will be understood by those of ordinary skill in the art that, it can be to the technology of the present invention
Scheme is modified or replaced equivalently, and without departing from the spirit of the technical scheme of the invention and range, should all be covered in this hair
In bright right.
Claims (10)
1. a kind of phosphate-free water-retaining agent, it is characterised in that：Including, by percentage to the quality,
。
2. phosphate-free water-retaining agent as described in claim 1, it is characterised in that：Including, by percentage to the quality,
。
3. phosphate-free water-retaining agent as claimed in claim 1 or 2, it is characterised in that：The soybean fiber includes soybean polyoses.
4. phosphate-free water-retaining agent as claimed in claim 1 or 2, it is characterised in that：The acidity regulator includes sodium carbonate, lemon
One or both of sour sodium, sodium bicarbonate or three kinds.
5. phosphate-free water-retaining agent as claimed in claim 4, it is characterised in that：The acidity regulator is sodium carbonate：Sodium citrate
In mass ratio 2：1 compounding.
6. application of any phosphate-free water-retaining agent of Claims 1 to 5 in aquatic products.
7. application as claimed in claim 6, it is characterised in that：Dosage of the phosphate-free water-retaining agent in aquatic products, with quality
It is 0.1%~5.0% than meter.
8. the use as claimed in claim 7, it is characterised in that：Dosage of the phosphate-free water-retaining agent in aquatic products, with quality
It is 1%~3% than meter.
9. application as claimed in claim 7 or 8, it is characterised in that：The aquatic products, including fish, shrimps.
10. application as claimed in claim 7 or 8, it is characterised in that：Including the aquatic products are soaked in the without phosphorus guarantor
In aqua, 4~10h is impregnated in 4~8 DEG C.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810339178.7A CN108651603A (en) | 2018-04-16 | 2018-04-16 | A kind of phosphate-free water-retaining agent and its application in aquatic products |
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|---|---|---|---|
| CN201810339178.7A CN108651603A (en) | 2018-04-16 | 2018-04-16 | A kind of phosphate-free water-retaining agent and its application in aquatic products |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109601598A (en) * | 2018-12-27 | 2019-04-12 | 青岛中信源食品科技有限公司 | A kind of without phosphorus squid water-retaining agent and its application |
| CN114747741A (en) * | 2022-05-11 | 2022-07-15 | 中国水产科学研究院南海水产研究所 | Instant fish freeze-dried product and preparation method thereof |
| CN115444126A (en) * | 2022-09-14 | 2022-12-09 | 福建创新食品科技有限公司 | Production method of water retention agent of plant-based dietary fiber |
| CN116473109A (en) * | 2023-04-27 | 2023-07-25 | 海南云富渔业有限公司 | Phosphorus-free water-retaining agent for frozen fish slices and preparation method and application thereof |
| CN116965447A (en) * | 2023-07-31 | 2023-10-31 | 佛山科学技术学院 | Preparation method of prefabricated black fish slices |
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| CN1935029A (en) * | 2006-09-22 | 2007-03-28 | 南宁中诺生物工程有限责任公司 | Frozen tilapia mossambica slice and its processing method |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109601598A (en) * | 2018-12-27 | 2019-04-12 | 青岛中信源食品科技有限公司 | A kind of without phosphorus squid water-retaining agent and its application |
| CN114747741A (en) * | 2022-05-11 | 2022-07-15 | 中国水产科学研究院南海水产研究所 | Instant fish freeze-dried product and preparation method thereof |
| CN115444126A (en) * | 2022-09-14 | 2022-12-09 | 福建创新食品科技有限公司 | Production method of water retention agent of plant-based dietary fiber |
| CN115444126B (en) * | 2022-09-14 | 2023-09-22 | 福建创新食品科技有限公司 | Production method of water retention agent of plant-based dietary fiber |
| CN116473109A (en) * | 2023-04-27 | 2023-07-25 | 海南云富渔业有限公司 | Phosphorus-free water-retaining agent for frozen fish slices and preparation method and application thereof |
| CN116965447A (en) * | 2023-07-31 | 2023-10-31 | 佛山科学技术学院 | Preparation method of prefabricated black fish slices |
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