CN108645995A - For the ore quality detection device and detection method after lepidolite ore dressing - Google Patents

For the ore quality detection device and detection method after lepidolite ore dressing Download PDF

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Publication number
CN108645995A
CN108645995A CN201810404862.9A CN201810404862A CN108645995A CN 108645995 A CN108645995 A CN 108645995A CN 201810404862 A CN201810404862 A CN 201810404862A CN 108645995 A CN108645995 A CN 108645995A
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transmission block
ore
quality detection
reative cell
lepidolite
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CN201810404862.9A
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CN108645995B (en
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南伟
蒋章铭
欧阳欣
郭亮
吴进方
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Yichun Jindi Lithium Industry Co Ltd
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Yichun Jindi Lithium Industry Co Ltd
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
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Abstract

The invention discloses a kind of ore quality detection devices for after lepidolite ore dressing,Including body,The outer surface of the body is provided with touch display screen,The side of the body is provided with handle,The bottom of the body is provided with pedestal,The lower inside of the body is respectively arranged with supporting rod and gas storage chamber,This kind is used for the ore quality detection device after lepidolite ore dressing,Internal body is provided with evaporator and reative cell,Lithium ore powder mixed with powdery solid highly basic 20 40 minutes to uniformly after,It is passed directly into high steam,Utilize the moisture in high steam,The powdery solid highly basic in reactant is set to be reacted in dissolving,Under conditions of high temperature and pressure,It is reacted with lithium ore and generates complete solable matter,It can allow lithium in lithium ore,Sodium,Potassium,Rubidium,Cesium ion is completely dissolved into solution,The bottom for being sent into sensing chamber by expansion bend again is detected,Generated cost when detection is saved,And environmental pollution is reduced when detecting.

Description

For the ore quality detection device and detection method after lepidolite ore dressing
Technical field
The present invention relates to ore quality detection field, specially a kind of ore quality detection dress for after lepidolite ore dressing It sets and detection method.
Background technology
Stone ore detects the object phase quantitative analysis for referring to all kinds of mineral products(Constituent analysis), elemental analysis, chemical analysis, ore mirror Fixed, single element quantitative analysis, physical property test chemical etc..Can according to the standards such as GB, ASTM, TP, ISO, UOP, JIS, EN into Row test analysis.
The existing ore quality detection device method for after lepidolite ore dressing is carried by raw material of lepidolite It takes, current extracting mode is sulfuric acid process or potassium sulfate and limestone calcination connection, because limestone calcination method uses high-temperature calcination Mode, temperature is generally at 1000 DEG C or so, thus energy consumption is high, and material circulation is big and the lithium rate of recovery is low, testing cost is high, Sulfuric acid process pollutes environment influence greatly using the concentrated sulfuric acid and lepidolite high-temperature roasting, carbonate sinker, same high energy consumption, exhaust gas It discharges larger, larger pressure is caused to environment.
Invention content
The purpose of the present invention is to provide a kind of ore quality detection device and detection method for after lepidolite ore dressing, To solve to propose in above-mentioned background technology to cause energy consumption high and lithium using sulfuric acid process or potassium sulfate and limestone calcination connection The problem of rate of recovery is low, product cost is high and sulfuric acid process uses the environmental pollution caused by the concentrated sulfuric acid and lepidolite high-temperature roasting.
To achieve the above object, the detection device of an object of the present invention is to provide following technical solution:One kind is used for The outer surface of ore quality detection device after lepidolite ore dressing, including body, the body is provided with touch display screen, described The side of body is provided with handle, and the bottom of the body is provided with pedestal, and the lower inside of the body is respectively arranged with branch The side of strut and gas storage chamber, the gas storage chamber is provided with snorkel, and one end of the snorkel is provided with valve, The other end of the snorkel is provided with evaporator, and the interior side of the body is provided with sensing chamber, the bottom of the sensing chamber Portion is provided with transmission block, and the both sides of the transmission block are both provided with sliding groove and slider roller, the inside setting of the transmission block There are expansion bend, one end of the transmission block to be provided with reactive tank, buckle is provided at the top of the transmission block, the transmission block Outer surface is provided with reative cell, and the top activated carbon ventilation opening of the reative cell, the inside of the activated carbon ventilation opening is set respectively It is equipped with activated carbon taste removal adsorption layer and wind turbine, the side of the ventilation opening is provided with air outlet net-shaped protective cover.
Preferably, the expansion bend is connected to the side of reactive tank using multiple-segment telescopic tube and extension, and it uses hydraulic pressure It is flexible that power mode carries out transmission.
Preferably, the side for snapping through welding connecting mode and being fixed on reative cell, and buckle internal by pneumatic It is telescopically connected on the top of transmission block.
Preferably, at the top of the reactive tank it is in " recessed " type, and holds sample area inside it and use tempered glass materials institute System, and reactive tank inner wall smooth.
Preferably, the snorkel is connected to through evaporator external inside evaporator.
Preferably, it is made using absorbent charcoal material inside the activated carbon taste removal adsorption layer, and its outer surface is in " bee Nest shape ".
Another object of the present invention utilizes the above-mentioned ore quality detection device for after lepidolite ore dressing to select lepidolite The detection method that ore quality after mine carries out, method are as follows:
1)The parameter set by internal body is controlled by touch display screen,
2)The buckle of reative cell side is opened by touch display screen, then pulls handrail to side, by pulling handrail to top Transmission block is opened at end, and sample and reaction raw materials are put into reactive tank, are then pushed into transmission block,
3)It is by touch display screen that buckle is stuck with transmission block, it is then turned on evaporator progress high steam and is reacted, steam By being moved into reative cell, the raw material in reactive tank is reacted with reaction raw materials,
4)Reaction terminates, and reactive tank is contracted to below sensing chamber by expansion bend, then is detected to it by sensing chamber, is detected Data are shown to touch display screen after completion, are analyzed its raw material by data analysis,
5)Finally transmission block is extracted out again, takes out raw material, the movement at the top of reative cell is opened by touch display screen after taking-up Reative cell internal gas is discharged baffle by activated carbon ventilation opening, is carried out to internal gas by activated carbon taste removal adsorption layer Purification is discharged by air outlet again.
Compared with prior art, the advantageous effect of detection device of the invention and detection method is:This kind is used for lepidolite Ore quality detection device after ore dressing is provided with evaporator and reative cell in internal body, and lithium ore powder and powdery solid are strong Alkali mixing 20-40 minutes is passed directly into high steam, using the moisture in high steam, makes the powder in reactant to after uniformly Shape solid alkali react in dissolving, and under conditions of high temperature and pressure, the complete solable matter of generation is reacted with lithium ore, can be with Lithium, sodium, potassium, rubidium, the cesium ion allowed in lithium ore is completely dissolved into solution, then by expansion bend be sent into the bottom of sensing chamber into Row detection, has saved generated cost when detection, and reduce environmental pollution when detecting.
Description of the drawings
Fig. 1 is schematic structural view of the invention;
Fig. 2 is side structure schematic diagram of the present invention;
Fig. 3 is partial structural diagram of the present invention.
In figure:1, body, 2, touch display screen, 3, handle, 4, pedestal, 5, expansion bend, 6, sliding groove, 7, slider roller, 8, it buckles, 9, evaporator, 10, reactive tank, 11, reative cell, 12, activated carbon ventilation opening, 13, supporting rod, 14, gas storage chamber, 15, valve, 16, snorkel, 17, sensing chamber, 18, activated carbon taste removal adsorption layer, 19, wind turbine, 20, air outlet net-shaped protective cover, 21, transmission block.
Specific implementation mode
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete Site preparation describes, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts every other Embodiment belongs to the range of the protection of the present invention.
- 3 are please referred to Fig.1, the present invention provides a kind of technical solution:A kind of ore quality detection for after lepidolite ore dressing Device, including body 1, touch display screen 2, handle 3, pedestal 4, expansion bend 5, sliding groove 6, slider roller 7, buckle 8, evaporator 9, reactive tank 10, reative cell 11, activated carbon ventilation opening 12, supporting rod 13, gas storage chamber 14, valve 15, snorkel 16, detection Room 17, activated carbon taste removal adsorption layer 18, wind turbine 19, air outlet net-shaped protective cover 20 and transmission block 21, the outer surface of the body 1 It is provided with touch display screen 2, the side of the body 1 is provided with handle 3, and the bottom of the body 1 is provided with pedestal 4, described The lower inside of body 1 is respectively arranged with supporting rod 13 and gas storage chamber 14, and the side of the gas storage chamber 14 is provided with One end of snorkel 16, the snorkel 16 is provided with valve 15, and the other end of the snorkel 15 is provided with evaporator 9, institute The interior side for stating body 1 is provided with sensing chamber 17, and the bottom of the sensing chamber 17 is provided with transmission block 21, the transmission block 21 Both sides be both provided with sliding groove 6 and slider roller 7, the transmission block 21 is internally provided with expansion bend 5, the transmission block 21 One end be provided with reactive tank 10, the top of the transmission block 21 is provided with buckle 8, and the outer surface of the transmission block 21 is provided with Reative cell 11, the top activated carbon ventilation opening 12 of the reative cell 11, the inside of the activated carbon ventilation opening 12 is respectively arranged with The side of activated carbon taste removal adsorption layer 18 and wind turbine 19, the ventilation opening 12 is provided with air outlet net-shaped protective cover 20.
Preferably, the expansion bend 5 is connected to the side of reactive tank 10 using multiple-segment telescopic tube and extension, and it uses liquid Pressure power mode carries out transmission and stretches, and sample is sent into 17 bottom of sensing chamber by expansion bend 5 after the reaction was completed and is examined It surveys.
Preferably, the buckle 8 is fixed on the side of reative cell 6 by welding connecting mode, and buckles and pass through gas inside 8 The dynamic top for being telescopically connected on transmission block 21 can utilize buckle when sample is sent into reative cell due to reative cell internal high pressure Its device is stuck.
Preferably, 10 top of the reactive tank is in " recessed " type, and holds sample area inside it and use tempered glass materials It is made, and 10 inner wall smooth of reactive tank, sample can be made adequately to be reacted carrying out reative cell, and be more favorable for detecting Room is detected.
Preferably, the snorkel 16 is connected to through 9 outer surface of evaporator inside evaporator 9, is steamed into horizontal high voltage It can be reacted by internal-combustion when way of steam processing and generate high steam.
Preferably, 18 inside of the activated carbon taste removal adsorption layer is made using absorbent charcoal material, and its outer surface is in The gas of reative cell 11 can be passed through activity by " cellular " after the reaction by certain time by opening flapper The activated carbon taste removal adsorption layer 18 being arranged in charcoal ventilation opening 12 is discharged after filtering, and reduces the discharge of pernicious gas.
Detection method and operation principle:The device is positioned over smooth place first, is controlled by touch display screen 2 Parameter set by 1 inside of body, the buckle 8 of 11 side of reative cell is opened by touch display screen 2, is then pulled and is helped to side Sample and reaction raw materials are put into reactive tank 10, then by transmission block by hand 3 by pulling handrail 3 to top to open transmission block 21 21 push-in, it is by touch display screen 2 that buckle 8 is stuck with transmission block 21, it is anti-to be then turned on the progress high steam progress of evaporator 9 It answers, by being moved into reative cell 11, the raw material in reactive tank is reacted steam with reaction raw materials, after waiting for certain time, Reaction terminates, and reactive tank 10 is contracted to 17 lower section of sensing chamber by expansion bend 5, then be detected to it by sensing chamber 17, examined Data after completing are surveyed to analyze its raw material by data analysis by display to touch display screen 2, it finally again will transmission Block is extracted out, and raw material are taken out, and the moving stop at 11 top of reative cell is opened after taking-up by touch display screen 2, by reative cell 11 Internal gas is discharged by activated carbon ventilation opening 12, is purified again internal gas by going out by activated carbon taste removal adsorption layer 18 Air port is discharged.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with Understanding without departing from the principles and spirit of the present invention can carry out these embodiments a variety of variations, modification, replace And modification, the scope of the present invention is by appended claims and its equivalent limits.

Claims (7)

1. a kind of ore quality detection device for after lepidolite ore dressing, including body(1), it is characterised in that:The body (1)Outer surface be provided with touch display screen(2), the body(1)Side be provided with handle(3), the body(1)Bottom Portion is provided with pedestal(4), the body(1)Lower inside be respectively arranged with supporting rod(13)And gas storage chamber(14), institute State gas storage chamber(14)Side be provided with snorkel(16), the snorkel(16)One end be provided with valve(15), institute State snorkel(16)The other end be provided with evaporator(9), the body(1)Interior side be provided with sensing chamber(17), institute State sensing chamber(17)Bottom be provided with transmission block(21), the transmission block(21)Both sides be both provided with sliding groove(6)With cunning Dynamic idler wheel(7), the transmission block(21)Be internally provided with expansion bend(5), the transmission block(21)One end be provided with reaction Slot(10), the transmission block(21)Top be provided with buckle(8), the transmission block(21)Outer surface be provided with reative cell (11), the reative cell(11)Top activated carbon ventilation opening(12), the activated carbon ventilation opening(12)Inside be respectively set Active charcoal taste removal adsorption layer(18)And wind turbine(19), the ventilation opening(12)Side be provided with air outlet net-shaped protective cover (20).
2. a kind of ore quality detection device for after lepidolite ore dressing according to claim 1, it is characterised in that:Institute State expansion bend(5)Reactive tank is connected to using multiple-segment telescopic tube and extension(10)Side, and its use hydraulic power mode into Row transmission is flexible.
3. a kind of ore quality detection device for after lepidolite ore dressing according to claim 1, it is characterised in that:Institute State buckle(8)It is fixed on reative cell by welding connecting mode(6)Side, and buckle(8)Inside is connected by Pneumatic extension In transmission block(21)Top.
4. a kind of ore quality detection device for after lepidolite ore dressing according to claim 1, it is characterised in that:Institute State reactive tank(10)Top is in " recessed " type, and holds sample area inside it and use tempered glass materials made, and reactive tank (10)Inner wall smooth.
5. a kind of ore quality detection device for after lepidolite ore dressing according to claim 1, it is characterised in that:Institute State snorkel(16)Through evaporator(9)Outer surface, and extend to evaporator(9)It is internal.
6. a kind of ore quality detection device for after lepidolite ore dressing according to claim 1, it is characterised in that:Institute State activated carbon taste removal adsorption layer(18)Inside is made using absorbent charcoal material, and its outer surface is in " cellular ".
7. a kind of basis is used for the ore quality detection method after lepidolite ore dressing, it is characterised in that including following method:
1)The parameter set by 1 inside of body is controlled by touch display screen 2,
2)The buckle 8 of 11 side of reative cell is opened by touch display screen 2, then pulls handrail 3 to side, by pulling handrail 3 open transmission block 21 to top, and sample and reaction raw materials are put into reactive tank 10, are then pushed into transmission block 21,
3)It is by touch display screen 2 that buckle 8 is stuck with transmission block 21, it is then turned on the progress high steam of evaporator 9 and is reacted, Steam is reacted by being moved into reative cell 11, the raw material in reactive tank with reaction raw materials,
4)Reaction terminates, and reactive tank 10 is contracted to 17 lower section of sensing chamber by expansion bend 5, then examined to it by sensing chamber 17 It surveys, data are shown to touch display screen 2 after detection is completed, and are analyzed its raw material by data analysis,
5)Finally transmission block is extracted out again, takes out raw material, opens the shifting at 11 top of reative cell after taking-up by touch display screen 2 Dynamic baffle, 11 internal gas of reative cell is discharged by activated carbon ventilation opening 12, by activated carbon taste removal adsorption layer 18 to inside Gas is purified to be discharged by air outlet again.
CN201810404862.9A 2018-04-28 2018-04-28 Device and method for detecting ore quality after lepidolite mineral separation Active CN108645995B (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111638101A (en) * 2020-05-08 2020-09-08 中蓝长化工程科技有限公司 Wet alkali fusion method for simultaneously determining content of lithium and calcium in lithium ore

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CN103823075A (en) * 2014-03-22 2014-05-28 山东理工大学 Translation iron ore analysis device
CN203816488U (en) * 2014-04-30 2014-09-10 南京农业大学 Fume-cupboard-free digesting and automatic waste gas collecting integrated device for experimental sample
CN206308026U (en) * 2016-12-13 2017-07-07 宜春银锂新能源有限责任公司 One kind is applied to lepidolite lithium carbonate processing unit (plant)
CN206828619U (en) * 2017-05-11 2018-01-02 江西南氏锂电新材料有限公司 Elemental lithium extraction element in a kind of lepidolite ore
CN206881259U (en) * 2017-06-23 2018-01-16 山东元本检测技术有限公司 A kind of detection means of water Mineral Elements in Jadeite Shellfish
CN206930543U (en) * 2017-06-10 2018-01-26 辽宁精研药物评价试验平台有限公司 A kind of chemical rapid detector
CN107739039A (en) * 2017-10-16 2018-02-27 福州大学 A kind of method that defluorinate lepidolite pipeline dissolution carries lithium
CN107826633A (en) * 2017-11-24 2018-03-23 苏州富强科技有限公司 A kind of pull-out mechanism for air tightness detection equipment

Patent Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103290217A (en) * 2013-06-20 2013-09-11 江西省科学院应用化学研究所 Technology for extracting lithium by processing lithium ores through high-pressure steaming process
CN103823075A (en) * 2014-03-22 2014-05-28 山东理工大学 Translation iron ore analysis device
CN203816488U (en) * 2014-04-30 2014-09-10 南京农业大学 Fume-cupboard-free digesting and automatic waste gas collecting integrated device for experimental sample
CN206308026U (en) * 2016-12-13 2017-07-07 宜春银锂新能源有限责任公司 One kind is applied to lepidolite lithium carbonate processing unit (plant)
CN206828619U (en) * 2017-05-11 2018-01-02 江西南氏锂电新材料有限公司 Elemental lithium extraction element in a kind of lepidolite ore
CN206930543U (en) * 2017-06-10 2018-01-26 辽宁精研药物评价试验平台有限公司 A kind of chemical rapid detector
CN206881259U (en) * 2017-06-23 2018-01-16 山东元本检测技术有限公司 A kind of detection means of water Mineral Elements in Jadeite Shellfish
CN107739039A (en) * 2017-10-16 2018-02-27 福州大学 A kind of method that defluorinate lepidolite pipeline dissolution carries lithium
CN107826633A (en) * 2017-11-24 2018-03-23 苏州富强科技有限公司 A kind of pull-out mechanism for air tightness detection equipment

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111638101A (en) * 2020-05-08 2020-09-08 中蓝长化工程科技有限公司 Wet alkali fusion method for simultaneously determining content of lithium and calcium in lithium ore

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