CN108642581A - Long and short fiber technique in a kind of waste silk raw material production high-strength flatness of extra white - Google Patents

Long and short fiber technique in a kind of waste silk raw material production high-strength flatness of extra white Download PDF

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Publication number
CN108642581A
CN108642581A CN201810376226.XA CN201810376226A CN108642581A CN 108642581 A CN108642581 A CN 108642581A CN 201810376226 A CN201810376226 A CN 201810376226A CN 108642581 A CN108642581 A CN 108642581A
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China
Prior art keywords
silk
material particle
waste silk
raw material
noil
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CN201810376226.XA
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Chinese (zh)
Inventor
唐元冰
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Shandong Qilu Textile Co Ltd
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Shandong Qilu Textile Co Ltd
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Priority to CN201810376226.XA priority Critical patent/CN108642581A/en
Publication of CN108642581A publication Critical patent/CN108642581A/en
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    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01DMECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
    • D01D13/00Complete machines for producing artificial threads
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01DMECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
    • D01D1/00Treatment of filament-forming or like material
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01DMECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
    • D01D5/00Formation of filaments, threads, or the like
    • D01D5/08Melt spinning methods
    • DTEXTILES; PAPER
    • D10INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10BINDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B2331/00Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products
    • D10B2331/04Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products polyesters, e.g. polyethylene terephthalate [PET]

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  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Textile Engineering (AREA)
  • Nonwoven Fabrics (AREA)
  • Artificial Filaments (AREA)

Abstract

The invention discloses a kind of waste silk raw materials to produce long and short fiber technique in the high-strength flatness of extra white, and the technique is specific as follows:It is prepared by the first step, raw material:First, secondly main material particle preparation brightens auxiliary material particle preparation, second step, rotary drum dispensing:Third walks, and completes fiber process:Long and short fiber technique in the waste silk raw material production high-strength flatness of extra white of the present invention, it is simple for process, the processing of extra white fiber can be completed using existing production equipment and production line, obtains extra white fiber product, improve product quality.

Description

Long and short fiber technique in a kind of waste silk raw material production high-strength flatness of extra white
Technical field
The present invention relates to a kind of waste silk raw materials recovery processing technologys, and in particular to a kind of waste silk raw material production extra white is high-strength low Middle long and short fiber technique is stretched, regeneration extra white fibre process technical field is belonged to.
Background technology
In the process of manufacture of polyester fiber fused mass directly spinning, due to lousiness, broken end phenomena such as appearance can lead to one The generation of fixed number amount waste silk, with the increase of polyester fiber production capacity, the waste silk doses in production process also can accordingly increase;How Simply and effectively this part waste silk material of reuse, for saving raw material dosage, reduction production cost improves the economic benefit of enterprise, Suffer from larger realistic meaning;The recycling application method of the polyester waste silks industrially used at present is broadly divided into two kinds;One is Using the chemical methodes such as alcoholysis or basic hydrolysis degradation polyester waste silks, is recycled through row in the form of monomer, chemically gathered Process is complicated when ester waste silk reuse, will produce three wastes problem, and product all Shortcomings in economy and quality;The second is will gather Ester waste silk re-melts extrusion and plastics or low-grade fiber is made, but polyester waste silks can cause to glue during remelted because being pyrolyzed Degree reduce, therefore using polyester waste silks be raw material re-melt extrusion made from polyester fiber it is second-rate, can only generally be used as cotton for wadding Or non-woven fabrics;It also lacks a kind of effective method at present, realizes following for waste silk in polyester fiber control system in melt direct spinning production process Ring utilizes;For this purpose, Chinese Patent Application No.:201210335518.1 disclosing a kind of returning online for fused mass directly spinning oil-free waste silk With method, the specific steps are:(1) pre-treatment (2) melting (3) viscosifies (4) online reuse, and waste silk melt pipe passes through metering system Melt conveying pipeline is accessed, the waste silk melt after thickening enters melt conveying pipeline via waste silk melt pipe, in order to ensure to gather The stability of ester fiber production technology and performance, the flow-rate ratio for controlling waste silk melt and spinning melt is 1: 20 ~ 1: 5;Waste silk is molten Body is mixed with spinning melt through melt conveying process is full and uniform, continues to participate in the production process of polyester fiber fused mass directly spinning;This Invention can effectively save raw material dosage by the oil-free waste silk generated during online recycled polyester fused mass directly spinning, real Waste silk recycles in existing polyester fiber control system in melt direct spinning production process;Waste silk melt is viscosified by the way that chain extender is added, The problem of waste silk melt be can effectively solve the problem that because molecular weight and viscosity decline, influence spinning technique performance;But it is not improved The utility value of waste silk, waste silk later stage preparation product quality is not high enough, and can not be carried out at later stage recycling to oily waste silk well Reason.
Invention content
To solve the above problems, the present invention proposes long and short fiber work in a kind of waste silk raw material production high-strength flatness of extra white Skill can realize the exploitation of extra white fiber, obtain extra white fiber product, improve product quality.
Long and short fiber technique in the waste silk raw material production high-strength flatness of extra white of the present invention, the technique are specific as follows:
It is prepared by the first step, raw material:
First, main material particle preparation, obtains melt directly spinning filament and lands waste silk, and the waste silk according to no silk noil and is had silk noil Categorised collection stores, and after having silk noil to deoil, dry by vertical centrifugal hydroextractor washing, obtains silk noil, will go silk noil with No silk noil is cut off with filament cutter respectively, and shearing length is 20 ~ 30cm, and without silk noil and silk noil is gone to mix completion cut-out, then Pass through chemical fibre granule mechanism winner feed particles;Often packet 25Kg is fixed packs again, and stacking is spare;
Secondly, auxiliary material particle preparation is brightened, using the dedicated granule machine of chemical fibre, while above-mentioned making main material particle, By a certain amount of fluorescent brightening master batch containing blue powder B12, stopping that chemical fibre is added in input waste silk to this preceding time that discharges In granule machine, the fluorescent brightening master batch weight and the no silk noil and total weight ratio is after going silk noil to mix:5~10Kg: 100Kg;By the high speed rotation of its stationary knife of chemical fibre granule machine, the fluorescent brightening master batch and silk noil is gone and it melts wadding state without silk noil Material uniformly mixing, adds water blowing that the auxiliary material particle of whitening effect is made, and then often packet 25Kg is fixed packs again, and stacking is spare;
Second step, rotary drum dispensing:
According to main material particle:The weight ratio for brightening auxiliary material particle and dacron chip base indigo plant X-ray is followed successively by 45 ~ 44:1~5:0.2 In ~ 0.6 input rotary drum;
Third walks, and completes fiber process:Spinning and postprocessing working procedures before being sequentially completed;It is spun before described specific as follows:Drying → screw rod Melt extruded → filtering → metering squeezes out strand → ring, which is blown, to be cooled and shaped → oil → draw and feed → fall bucket;The post-processing work Sequence is specific as follows:Boundling → water-bath stretching → steam bath stretching → anxiety thermal finalization → curling → relaxation heat setting → cut-out → packet Dress;The dry moisture is 80 ± 10ppm, the extrusion strand its hole diameter of spinneret 0.32mm, draw ratio 2:1:It is described to squeeze Go out its spinning speed of strand for 900 ~ 1200m/min;It is 3.4 ~ 4.6 that the water-bath, which stretches its draw ratio,;The vapour bath stretches Its draw ratio is 1.10 ~ 1.16;Described its setting temperature of anxiety thermal finalization is 170 ~ 200 DEG C;Its sizing of the laxation shaping Temperature is 60 ~ 130 DEG C;Its specification of the fiber is 2.5D ╳ 51mm.
2, long and short fiber technique in the waste silk raw material production high-strength flatness of extra white according to claim 1, feature exist In:The rotary drum dispensing its to 358 type rotary drum dispensings, often 90 ~ 98 packet main material particles are added in drum, and 2 ~ 10 packets brighten auxiliary material Grain, adds 10 ~ 30Kg dacron chip base indigo plant X-rays.
As preferred embodiment, the fiber process is completed on producing 50 tons of high-strength flatness cotton production lines daily.
It is described to brighten auxiliary material particle preparation it uses individual chemical fibre granule machine and main original as preferred embodiment Expect the chemical fibre granule machine synchronous working of particle preparation, or special using chemical fibre by the chemical fibre granule machine configuration of main material particle preparation Granule machine batch operation, gap obtain main material particle and brighten auxiliary material particle.
As preferred embodiment, the melt directly spinning filament landing waste silk is collected by production line or external buying obtains It takes.
Compared with prior art, waste silk raw material of the invention produces long and short fiber work in the high-strength flatness of extra white to the present invention Skill, it is simple for process, the processing of extra white fiber can be completed using existing production equipment and production line, obtain the production of extra white fiber Product improve product quality.
Specific implementation mode
Embodiment 1:
Long and short fiber technique in a kind of waste silk raw material production high-strength flatness of extra white, the technique are specific as follows:
It is prepared by the first step, raw material:
First, main material particle preparation, obtains melt directly spinning filament and lands waste silk, and the waste silk according to no silk noil and is had silk noil Categorised collection stores, and after having silk noil to deoil, dry by vertical centrifugal hydroextractor washing, obtains silk noil, will go silk noil with No silk noil is cut off with filament cutter respectively, and shearing length is 20 ~ 30cm, and without silk noil and silk noil is gone to mix completion cut-out, then Pass through chemical fibre granule mechanism winner feed particles;Often packet 25Kg is fixed packs again, and stacking is spare;
Secondly, auxiliary material particle preparation is brightened, using the dedicated granule machine of chemical fibre, while above-mentioned making main material particle, By a certain amount of fluorescent brightening master batch containing blue powder B12, stopping that chemical fibre is added in input waste silk to this preceding time that discharges In granule machine, the fluorescent brightening master batch weight and the no silk noil and total weight ratio is after going silk noil to mix:5~10Kg: 100Kg;By the high speed rotation of its stationary knife of chemical fibre granule machine, the fluorescent brightening master batch and silk noil is gone and it melts wadding state without silk noil Material uniformly mixing, adds water blowing that the auxiliary material particle of whitening effect is made, and then often packet 25Kg is fixed packs again, and stacking is spare;
Second step, rotary drum dispensing:
According to main material particle:The weight ratio for brightening auxiliary material particle and dacron chip base indigo plant X-ray is followed successively by 45 ~ 44:1~5:0.2 In ~ 0.6 input rotary drum;
Third walks, and completes fiber process:Spinning and postprocessing working procedures before being sequentially completed;It is spun before described specific as follows:Drying → screw rod Melt extruded → filtering → metering squeezes out strand → ring, which is blown, to be cooled and shaped → oil → draw and feed → fall bucket;The post-processing work Sequence is specific as follows:Boundling → water-bath stretching → steam bath stretching → anxiety thermal finalization → curling → relaxation heat setting → cut-out → packet Dress;The dry moisture is 80 ± 10ppm, the extrusion strand its hole diameter of spinneret 0.32mm, draw ratio 2:1:It is described to squeeze Go out its spinning speed of strand for 900 ~ 1200m/min;It is 3.4 ~ 4.6 that the water-bath, which stretches its draw ratio,;The vapour bath stretches Its draw ratio is 1.10 ~ 1.16;Described its setting temperature of anxiety thermal finalization is 170 ~ 200 DEG C;Its sizing of the laxation shaping Temperature is 60 ~ 130 DEG C;Its specification of the fiber is 2.5D ╳ 51mm.
Embodiment 2:
The rotary drum dispensing its to 358 type rotary drum dispensings, often 90 ~ 98 packet main material particles are added in drum, and 2 ~ 10 packets brighten auxiliary material Particle adds 10 ~ 30Kg dacron chip base indigo plant X-rays.
Embodiment 3:
The fiber process is completed on producing 50 tons of high-strength flatness cotton production lines daily.
It is described to brighten auxiliary material particle preparation it uses individual chemical fibre granule machine and main material particle in another embodiment The chemical fibre granule machine of preparation works asynchronously, or utilizes the dedicated group of chemical fibre by the chemical fibre granule machine configuration of main material particle preparation Grain machine batch operation, gap obtain main material particle and brighten auxiliary material particle.
In another embodiment, the melt directly spinning filament landing waste silk is collected by production line or external buying obtains.
Above-described embodiment is only the better embodiment of the present invention, therefore all structures according to described in present patent application range It makes, the equivalent change or modification that feature and principle are done, is included within the scope of present patent application.

Claims (5)

1. long and short fiber technique in a kind of waste silk raw material production high-strength flatness of extra white, it is characterised in that:The technique is specific as follows:
It is prepared by the first step, raw material:
First, main material particle preparation, obtains melt directly spinning filament and lands waste silk, and the waste silk according to no silk noil and is had silk noil Categorised collection stores, and after having silk noil to deoil, dry by vertical centrifugal hydroextractor washing, obtains silk noil, will go silk noil with No silk noil is cut off with filament cutter respectively, and shearing length is 20 ~ 30cm, and without silk noil and silk noil is gone to mix completion cut-out, then Pass through chemical fibre granule mechanism winner feed particles;Often packet 25Kg is fixed packs again, and stacking is spare;
Secondly, auxiliary material particle preparation is brightened, using the dedicated granule machine of chemical fibre, while above-mentioned making main material particle, By a certain amount of fluorescent brightening master batch containing blue powder B12, stopping that chemical fibre is added in input waste silk to this preceding time that discharges In granule machine, the fluorescent brightening master batch weight and the no silk noil and total weight ratio is after going silk noil to mix:5~10Kg: 100Kg;By the high speed rotation of its stationary knife of chemical fibre granule machine, the fluorescent brightening master batch and silk noil is gone and it melts wadding state without silk noil Material uniformly mixing, adds water blowing that the auxiliary material particle of whitening effect is made, and then often packet 25Kg is fixed packs again, and stacking is spare;
Second step, rotary drum dispensing:
According to main material particle:The weight ratio for brightening auxiliary material particle and dacron chip base indigo plant X-ray is followed successively by 45 ~ 44:1~5:0.2 In ~ 0.6 input rotary drum;
Third walks, and completes fiber process:Spinning and postprocessing working procedures before being sequentially completed;It is spun before described specific as follows:Drying → screw rod Melt extruded → filtering → metering squeezes out strand → ring, which is blown, to be cooled and shaped → oil → draw and feed → fall bucket;The post-processing work Sequence is specific as follows:Boundling → water-bath stretching → steam bath stretching → anxiety thermal finalization → curling → relaxation heat setting → cut-out → packet Dress;The dry moisture is 80 ± 10ppm, the extrusion strand its hole diameter of spinneret 0.32mm, draw ratio 2:1:It is described to squeeze Go out its spinning speed of strand for 900 ~ 1200m/min;It is 3.4 ~ 4.6 that the water-bath, which stretches its draw ratio,;The vapour bath stretches Its draw ratio is 1.10 ~ 1.16;Described its setting temperature of anxiety thermal finalization is 170 ~ 200 DEG C;Its sizing of the laxation shaping Temperature is 60 ~ 130 DEG C;Its specification of the fiber is 2.5D ╳ 51mm.
2. long and short fiber technique in the waste silk raw material production high-strength flatness of extra white according to claim 1, it is characterised in that:Institute State rotary drum dispensing its to 358 type rotary drum dispensings, often 90 ~ 98 packet main material particles are added in drum, and 2 ~ 10 packets brighten auxiliary material particle, then 10 ~ 30Kg dacron chip base indigo plant X-rays are added.
3. long and short fiber technique in the waste silk raw material production high-strength flatness of extra white according to claim 1, it is characterised in that:Institute Fiber process is stated to complete on producing 50 tons of high-strength flatness cotton production lines daily.
4. long and short fiber technique in the waste silk raw material production high-strength flatness of extra white according to claim 1, it is characterised in that:Institute It states and brightens auxiliary material particle preparation it uses individual chemical fibre granule machine work synchronous with the chemical fibre granule machine of main material particle preparation Make, or utilizes the dedicated granule machine batch operation of chemical fibre, gap to obtain by the chemical fibre granule machine configuration of main material particle preparation Main material particle and brighten auxiliary material particle.
5. long and short fiber technique in the waste silk raw material production high-strength flatness of extra white according to claim 1, it is characterised in that:Institute Melt directly spinning filament landing waste silk is stated to obtain by production line collection or external buying.
CN201810376226.XA 2018-04-25 2018-04-25 Long and short fiber technique in a kind of waste silk raw material production high-strength flatness of extra white Pending CN108642581A (en)

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Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101736444A (en) * 2010-01-25 2010-06-16 桐乡市中驰化纤有限公司 Method for recycling polyester waste silks
CN102828276A (en) * 2012-09-04 2012-12-19 福建鑫华股份有限公司 Preparation method of biodegradable regenerated polyester staple fibers
CN102899729A (en) * 2012-10-19 2013-01-30 宁波大发化纤有限公司 Method for processing regenerated polyester staple fiber by using waste polyester textile
CN103668534A (en) * 2012-08-31 2014-03-26 福建百宏聚纤科技实业有限公司 Online recycling method of melt direct-spun oil-free waste silk
CN104911748A (en) * 2015-06-02 2015-09-16 龙福环能科技股份有限公司 Method for industrial production of polyester filament yarn by using polyester waste yarn
CN105839199A (en) * 2016-04-22 2016-08-10 孔祥明 Process for spinning chemical fibers from waste polyester cloth
CN105887233A (en) * 2016-06-27 2016-08-24 福建鑫华股份有限公司 Method for preparing extra white regenerated polyester short fiber
CN105937064A (en) * 2016-06-27 2016-09-14 福建鑫华股份有限公司 Preparation method of high strength and high tensile regenerated polyester staple fiber dedicated for non-weaving

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101736444A (en) * 2010-01-25 2010-06-16 桐乡市中驰化纤有限公司 Method for recycling polyester waste silks
CN103668534A (en) * 2012-08-31 2014-03-26 福建百宏聚纤科技实业有限公司 Online recycling method of melt direct-spun oil-free waste silk
CN102828276A (en) * 2012-09-04 2012-12-19 福建鑫华股份有限公司 Preparation method of biodegradable regenerated polyester staple fibers
CN102899729A (en) * 2012-10-19 2013-01-30 宁波大发化纤有限公司 Method for processing regenerated polyester staple fiber by using waste polyester textile
CN104911748A (en) * 2015-06-02 2015-09-16 龙福环能科技股份有限公司 Method for industrial production of polyester filament yarn by using polyester waste yarn
CN105839199A (en) * 2016-04-22 2016-08-10 孔祥明 Process for spinning chemical fibers from waste polyester cloth
CN105887233A (en) * 2016-06-27 2016-08-24 福建鑫华股份有限公司 Method for preparing extra white regenerated polyester short fiber
CN105937064A (en) * 2016-06-27 2016-09-14 福建鑫华股份有限公司 Preparation method of high strength and high tensile regenerated polyester staple fiber dedicated for non-weaving

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Application publication date: 20181012