CN108641568A - A kind of high temperature resistant environment-protective preparation method for coating - Google Patents
A kind of high temperature resistant environment-protective preparation method for coating Download PDFInfo
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- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D171/00—Coating compositions based on polyethers obtained by reactions forming an ether link in the main chain; Coating compositions based on derivatives of such polymers
- C09D171/02—Polyalkylene oxides
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- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F289/00—Macromolecular compounds obtained by polymerising monomers on to macromolecular compounds not provided for in groups C08F251/00 - C08F287/00
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- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/18—Fireproof paints including high temperature resistant paints
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/20—Diluents or solvents
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/63—Additives non-macromolecular organic
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/65—Additives macromolecular
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/30—Sulfur-, selenium- or tellurium-containing compounds
- C08K2003/3045—Sulfates
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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Abstract
The invention discloses a kind of high temperature resistant environment-protective preparation method for coating, include the following steps：Palm oil, polyethylene glycol, water are mixed, potassium peroxydisulfate stirring is added, divinylbenzene is added, potassium peroxydisulfate stirring is added in heating stirring, and styrene, methyl methacrylate, heating stirring is added, and cooling obtains mixed material；Polypropylene glycol diglycidyl ether, aqueous alkide resin, mixed material, titanium dioxide, aluminium triphosphate, magnesium phosphate, sepiolite powder, talcum powder, blanc fixe, quartz powder, zinc oxide, ethylene glycol, coalescents, preservative, thickener, dispersant, antifoaming agent, levelling agent, mould inhibitor, water are uniformly mixed and obtain high-temperature resistant epoxy friendly coating.Gained coating high temperature resistance of the invention is good, excellent in mechanical performance, and safety and environmental protection.
Description
Technical field
The present invention relates to technical field of coatings more particularly to a kind of high temperature resistant environment-protective preparation method for coating,
Background technology
Water paint is the technology to grow up in the sixties in last century, with water as solvent, saves vast resources, aqueous
Fire risk when coating eliminates construction is reduced to atmosphere pollution, and water paint improves operating environmental condition, but long-term
Since, for water paint in addition to being good for the environment, other performances are poor, and how to improve the heat-resisting quantity of water paint is always urgently
It solves the problems, such as.
Invention content
Technical problems based on background technology, the present invention propose a kind of high temperature resistant environment-protective preparation method for coating, institute
It is good to obtain coating high temperature resistance, excellent in mechanical performance, and safety and environmental protection.
A kind of high temperature resistant environment-protective preparation method for coating proposed by the present invention, includes the following steps：
S1, palm oil, polyethylene glycol, water are mixed, potassium peroxydisulfate stirring is added, divinylbenzene is added, heat up stirring,
Potassium peroxydisulfate stirring is added, styrene, methyl methacrylate, heating stirring is added, cooling obtains mixed material；
S2, by polypropylene glycol diglycidyl ether, aqueous alkide resin, mixed material, titanium dioxide, aluminium triphosphate,
Magnesium phosphate, sepiolite powder, talcum powder, blanc fixe, quartz powder, zinc oxide, ethylene glycol, coalescents, preservative, thickening
Agent, dispersant, antifoaming agent, levelling agent, mould inhibitor, water, which are uniformly mixed, obtains high-temperature resistant epoxy friendly coating.
Preferably, in S1, palm oil, polyethylene glycol, water are mixed, potassium peroxydisulfate is added and stirs 10-20min, stirring speed
Degree is 1000-2000r/min, and divinylbenzene is added, and is warming up to 80-88 DEG C of stirring 10-25min, potassium peroxydisulfate stirring is added
10-20min, mixing speed 1000-1200r/min are added styrene, methyl methacrylate, are warming up to 80-88 DEG C of stirring
10-20min, cooling obtain mixed material.
Preferably, in S1, palm oil, polyethylene glycol, water, potassium peroxydisulfate, divinylbenzene, potassium peroxydisulfate, styrene, first
The weight ratio of base methyl acrylate is 20-30：0.5-1.5：10-20：0.2-0.3：1-3：0.15-0.25：0.5-2.5：0.5-
1。
Preferably, in S2, polypropylene glycol diglycidyl ether, aqueous alkide resin, mixed material weight ratio be 20-
40：10-20：3-7.
Preferably, in S2, mixed material, titanium dioxide, aluminium triphosphate, magnesium phosphate weight ratio be 3-7：0.5-1.5：
0.5-1：0.5-1.5.
Preferably, in S2, mixed material, sepiolite powder, talcum powder, blanc fixe, quartz powder, zinc oxide weight
Than for 3-7：1-3：1-2：1-3：1-2：1-2.
Preferably, in S2, mixed material, ethylene glycol, coalescents, preservative, thickener, dispersant, antifoaming agent, levelling
Agent, mould inhibitor, water weight ratio be 3-7：2-5：1-2.5：0.5-1.5：1-2：0.5-1.5：1-2：0.5-1.5：1-2：1-3.
In S1 of the present invention, using palm oil as kernel, after divinylbenzene is appropriately crosslinked, in one layer of hard of outer layers of polymer
It is good to be allowed to not only toughening effect for shell；And mixed material and polypropylene glycol diglycidyl ether, aqueous alkide resin compatibility are excellent
It is good, it cooperates with coalescents and titanium dioxide, aluminium triphosphate, magnesium phosphate, forms network-like cross-linked structure, mechanical property
Good, high temperature resistance is excellent, and can be improved strong with coated substrate cohesive force, and adhesion property is excellent；Sepiolite powder, talcum powder,
The intersolubility of blanc fixe, quartz powder and soybean oil compound is good, and binding force is strong, and mechanical property is fabulous.
The present invention reduces the use of a large amount of volatile organic solvents in construction with water as solvent, be beneficial to environmental protection and
The health of construction personnel, compared with existing water paint, high temperature resistance is good, strong adhesive force, good fluidity, mechanical property
It is excellent.
Specific implementation mode
In the following, technical scheme of the present invention is described in detail by specific embodiment.
Embodiment 1
A kind of high temperature resistant environment-protective preparation method for coating, includes the following steps：
S1,20kg palm oils, 1.5kg polyethylene glycol, 10kg water are mixed, 0.3kg potassium peroxydisulfates are added and stir 10min,
Mixing speed is 2000r/min, and 1kg divinylbenzenes are added, and is warming up to 88 DEG C of stirring 10min, 0.25kg potassium peroxydisulfates are added
10min, mixing speed 1200r/min are stirred, 0.5kg styrene, 1kg methyl methacrylates is added, is warming up to 80 DEG C and stirs
20min is mixed, cooling obtains mixed material；
S2, by 20kg polypropylene glycol diglycidyl ethers, 20kg aqueous alkide resins, 3kg mixed materials, 1.5kg dioxies
Change titanium, 0.5kg aluminium triphosphates, 1.5kg magnesium phosphates, 1kg sepiolite powders, 2kg talcum powder, 1kg blanc fixes, 2kg quartz
Mountain flour, 1kg zinc oxide, 5kg ethylene glycol, 1kg coalescents, 1.5kg preservatives, 1kg thickeners, 1.5kg dispersants, 1kg disappear
Infusion, 1.5kg levelling agents, 1kg mould inhibitors, 3kg water, which are uniformly mixed, obtains high-temperature resistant epoxy friendly coating.
Embodiment 2
A kind of high temperature resistant environment-protective preparation method for coating, includes the following steps：
S1,30kg palm oils, 0.5kg polyethylene glycol, 20kg water are mixed, 0.2kg potassium peroxydisulfates are added and stir 20min,
Mixing speed is 1000r/min, and 3kg divinylbenzenes are added, and is warming up to 80 DEG C of stirring 25min, 0.15kg potassium peroxydisulfates are added
20min, mixing speed 1000r/min are stirred, 2.5kg styrene, 0.5kg methyl methacrylates is added, is warming up to 88 DEG C
10min is stirred, cooling obtains mixed material；
S2, by 40kg polypropylene glycol diglycidyl ethers, 10kg aqueous alkide resins, 7kg mixed materials, 0.5kg dioxies
Change titanium, 1kg aluminium triphosphates, 0.5kg magnesium phosphates, 3kg sepiolite powders, 1kg talcum powder, 3kg blanc fixes, 1kg quartzs
Powder, 2kg zinc oxide, 2kg ethylene glycol, 2.5kg coalescents, 0.5kg preservatives, 2kg thickeners, 0.5kg dispersants, 2kg disappear
Infusion, 0.5kg levelling agents, 2kg mould inhibitors, 1kg water, which are uniformly mixed, obtains high-temperature resistant epoxy friendly coating.
Embodiment 3
A kind of high temperature resistant environment-protective preparation method for coating, includes the following steps：
S1,22kg palm oils, 1.2kg polyethylene glycol, 12kg water are mixed, 0.28kg potassium peroxydisulfates are added and stir 12min,
Mixing speed is 1800r/min, and 1.5kg divinylbenzenes are added, and is warming up to 86 DEG C of stirring 15min, 0.22kg persulfuric acid is added
Potassium stirs 13min, mixing speed 1150r/min, and 1kg styrene, 0.8kg methyl methacrylates is added, is warming up to 82 DEG C
18min is stirred, cooling obtains mixed material；
S2, by 25kg polypropylene glycol diglycidyl ethers, 18kg aqueous alkide resins, 4kg mixed materials, 1.2kg dioxies
Change titanium, 0.6kg aluminium triphosphates, 1.2kg magnesium phosphates, 1.5kg sepiolite powders, 1.8kg talcum powder, 1.5kg blanc fixes,
1.7kg quartz powders, 1.4kg zinc oxide, 4kg ethylene glycol, 1.5kg coalescents, 1.2kg preservatives, 1.3kg thickeners,
1.2kg dispersants, 1.3kg antifoaming agent, 1.2kg levelling agents, 1.3kg mould inhibitors, 2.5kg water, which are uniformly mixed, obtains high temperature resistant environment-protective
Coating.
Embodiment 4
A kind of high temperature resistant environment-protective preparation method for coating, includes the following steps：
S1,28kg palm oils, 0.8kg polyethylene glycol, 18kg water are mixed, 0.22kg potassium peroxydisulfates are added and stir 18min,
Mixing speed is 1200r/min, and 2.5kg divinylbenzenes are added, and is warming up to 82 DEG C of stirring 20min, 0.18kg persulfuric acid is added
Potassium stirs 17min, mixing speed 1050r/min, and 2kg styrene, 0.6kg methyl methacrylates is added, is warming up to 86 DEG C
12min is stirred, cooling obtains mixed material；
S2, by 35kg polypropylene glycol diglycidyl ethers, 12kg aqueous alkide resins, 6kg mixed materials, 0.8 titanium dioxide
Titanium, 0.8kg aluminium triphosphates, 0.8kg magnesium phosphates, 2.5kg sepiolite powders, 1.2kg talcum powder, 2.5kg blanc fixes,
1.3kg quartz powders, 1.8kg zinc oxide, 3kg ethylene glycol, 2kg coalescents, 0.8kg preservatives, 1.7kg thickeners, 0.8kg
Dispersant, 1.7kg antifoaming agent, 0.8kg levelling agents, 1.7kg mould inhibitors, 1.5kg water, which are uniformly mixed, obtains high-temperature resistant epoxy friendly coating.
Embodiment 5
A kind of high temperature resistant environment-protective preparation method for coating, includes the following steps：
S1,25kg palm oils, 1kg polyethylene glycol, 15kg water are mixed, 0.25kg potassium peroxydisulfates is added and stir 15min, stir
It is 1500r/min to mix speed, and 2kg divinylbenzenes are added, and is warming up to 84 DEG C of stirring 18min, the stirring of 0.2kg potassium peroxydisulfates is added
15min, mixing speed 1100r/min are added 1.5kg styrene, 0.7kg methyl methacrylates, are warming up to 84 DEG C of stirrings
15min, cooling obtain mixed material；
S2, by 30kg polypropylene glycol diglycidyl ethers, 15kg aqueous alkide resins, 5kg mixed materials, 1kg titanium dioxides
Titanium, 0.7kg aluminium triphosphates, 1kg magnesium phosphates, 2kg sepiolite powders, 1.5kg talcum powder, 2kg blanc fixes, 1.5kg quartz
Mountain flour, 1.6kg zinc oxide, 3.5kg ethylene glycol, 1.8kg coalescents, 1kg preservatives, 1.5kg thickeners, 1kg dispersants,
1.5kg antifoaming agent, 1kg levelling agents, 1.5kg mould inhibitors, 2kg water, which are uniformly mixed, obtains high-temperature resistant epoxy friendly coating.
The foregoing is only a preferred embodiment of the present invention, but scope of protection of the present invention is not limited thereto,
Any one skilled in the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention and its
Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.
Claims (7)
1. a kind of high temperature resistant environment-protective preparation method for coating, which is characterized in that include the following steps：
S1, palm oil, polyethylene glycol, water are mixed, potassium peroxydisulfate stirring is added, divinylbenzene is added, heating stirring is added
Potassium peroxydisulfate stirs, and styrene, methyl methacrylate, heating stirring is added, and cooling obtains mixed material；
S2, by polypropylene glycol diglycidyl ether, aqueous alkide resin, mixed material, titanium dioxide, aluminium triphosphate, phosphoric acid
Magnesium, sepiolite powder, talcum powder, blanc fixe, quartz powder, zinc oxide, ethylene glycol, coalescents, preservative, thickener,
Dispersant, antifoaming agent, levelling agent, mould inhibitor, water, which are uniformly mixed, obtains high-temperature resistant epoxy friendly coating.
2. high temperature resistant environment-protective preparation method for coating according to claim 1, which is characterized in that in S1, by palm oil, poly- second two
Alcohol, water mixing, are added potassium peroxydisulfate and stir 10-20min, mixing speed 1000-2000r/min, divinylbenzene is added, rise
Temperature is added potassium peroxydisulfate and stirs 10-20min, mixing speed 1000-1200r/min adds to 80-88 DEG C of stirring 10-25min
Enter styrene, methyl methacrylate, be warming up to 80-88 DEG C of stirring 10-20min, cooling obtains mixed material.
3. high temperature resistant environment-protective preparation method for coating according to claim 1 or claim 2, which is characterized in that in S1, palm oil, poly- second
Glycol, water, potassium peroxydisulfate, divinylbenzene, potassium peroxydisulfate, styrene, methyl methacrylate weight ratio be 20-30：
0.5-1.5：10-20：0.2-0.3：1-3：0.15-0.25：0.5-2.5：0.5-1.
4. according to any one of the claim 1-3 high temperature resistant environment-protective preparation method for coating, which is characterized in that in S2, poly- the third two
Alcohol diglycidyl ether, aqueous alkide resin, mixed material weight ratio be 20-40：10-20：3-7.
5. according to any one of the claim 1-4 high temperature resistant environment-protective preparation method for coating, which is characterized in that in S2, mixture
Material, titanium dioxide, aluminium triphosphate, magnesium phosphate weight ratio be 3-7：0.5-1.5：0.5-1：0.5-1.5.
6. according to any one of the claim 1-5 high temperature resistant environment-protective preparation method for coating, which is characterized in that in S2, mixture
Material, sepiolite powder, talcum powder, blanc fixe, quartz powder, zinc oxide weight ratio be 3-7：1-3：1-2：1-3：1-2：1-
2。
7. according to any one of the claim 1-6 high temperature resistant environment-protective preparation method for coating, which is characterized in that in S2, mixture
Material, ethylene glycol, coalescents, preservative, thickener, dispersant, antifoaming agent, levelling agent, mould inhibitor, water weight ratio be 3-7：
2-5：1-2.5：0.5-1.5：1-2：0.5-1.5：1-2：0.5-1.5：1-2：1-3.
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| CN201810287587.7A CN108641568A (en) | 2018-03-30 | 2018-03-30 | A kind of high temperature resistant environment-protective preparation method for coating |
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| CN201810287587.7A CN108641568A (en) | 2018-03-30 | 2018-03-30 | A kind of high temperature resistant environment-protective preparation method for coating |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112812650A (en) * | 2021-02-06 | 2021-05-18 | 全通电缆股份有限公司 | Composite cable coating and preparation method thereof |
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| CN103265672A (en) * | 2013-05-22 | 2013-08-28 | 云南大学 | Method for preparing plant oil-based core-shell structural flexibilizer |
| CN105969032A (en) * | 2016-06-03 | 2016-09-28 | 浙江天女集团制漆有限公司 | Water-based alkyd paint and preparation method thereof |
| CN106349869A (en) * | 2016-08-27 | 2017-01-25 | 安徽省金盾涂料有限责任公司 | High-temperature-resistant epoxy coating with excellent mechanical properties |
| CN106519849A (en) * | 2016-11-21 | 2017-03-22 | 大连华漫环保精细材料有限公司 | Water-based environment-friendly antirust paint and preparation method thereof |
| CN107828317A (en) * | 2017-12-01 | 2018-03-23 | 李晓强 | Good corrosion resistant bridge framework of steel reinforcement coating of freeze-thaw resistance and preparation method thereof |
-
2018
- 2018-03-30 CN CN201810287587.7A patent/CN108641568A/en not_active Withdrawn
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103265672A (en) * | 2013-05-22 | 2013-08-28 | 云南大学 | Method for preparing plant oil-based core-shell structural flexibilizer |
| CN105969032A (en) * | 2016-06-03 | 2016-09-28 | 浙江天女集团制漆有限公司 | Water-based alkyd paint and preparation method thereof |
| CN106349869A (en) * | 2016-08-27 | 2017-01-25 | 安徽省金盾涂料有限责任公司 | High-temperature-resistant epoxy coating with excellent mechanical properties |
| CN106519849A (en) * | 2016-11-21 | 2017-03-22 | 大连华漫环保精细材料有限公司 | Water-based environment-friendly antirust paint and preparation method thereof |
| CN107828317A (en) * | 2017-12-01 | 2018-03-23 | 李晓强 | Good corrosion resistant bridge framework of steel reinforcement coating of freeze-thaw resistance and preparation method thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112812650A (en) * | 2021-02-06 | 2021-05-18 | 全通电缆股份有限公司 | Composite cable coating and preparation method thereof |
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Application publication date: 20181012 |