CN108625177A - A kind of preparation and application for Pure Cotton Fabric Printing fabric softener - Google Patents
A kind of preparation and application for Pure Cotton Fabric Printing fabric softener Download PDFInfo
- Publication number
- CN108625177A CN108625177A CN201810445732.XA CN201810445732A CN108625177A CN 108625177 A CN108625177 A CN 108625177A CN 201810445732 A CN201810445732 A CN 201810445732A CN 108625177 A CN108625177 A CN 108625177A
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- CN
- China
- Prior art keywords
- atoleine
- speed
- rotating speed
- added
- adjusted
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/53—Polyethers
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G73/00—Recovery or refining of mineral waxes, e.g. montan wax
- C10G73/02—Recovery of petroleum waxes from hydrocarbon oils; Dewaxing of hydrocarbon oils
- C10G73/06—Recovery of petroleum waxes from hydrocarbon oils; Dewaxing of hydrocarbon oils with the use of solvents
- C10G73/08—Organic compounds
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/224—Esters of carboxylic acids; Esters of carbonic acid
- D06M13/2246—Esters of unsaturated carboxylic acids
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/244—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus
- D06M13/248—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus with compounds containing sulfur
- D06M13/256—Sulfonated compounds esters thereof, e.g. sultones
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
- D06M2101/06—Vegetal fibres cellulosic
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/50—Modified hand or grip properties; Softening compositions
Landscapes
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Textile Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
One kind being used for Pure Cotton Fabric Printing fabric softener, and material quality score and preparation method are as follows：It weighs the alkyl phenol polyvinylether of 6 10wt%, fatty alcohol polyoxyethylene ether, this disk series of surfactants, tween surfactants, at least one surfactant such as dodecyl sodium sulfate and double alkyl maleic acid esters, the deionized water that 40 64wt% are added while stirring under the rotating speed of 600 1000r/min with blender at the uniform velocity stirs 30min after mixing, rotating speed is adjusted to 2000 2800r/min again, the atoleine of 30 50wt% is gradually added into the speed of 1 2.5ml/s under conditions of high-speed stirred, rotating speed is adjusted to 3000 3500r/min high-speed stirreds 1h after its whole adds, it completes to prepare.Again with 10 17g/l of intensifier is endured with all one's will, the present invention prepares 8 12g/l of softening agent, and 5 7g/l of cotton sense finishing agent is configured to arrange slurry to printing textile progress final finishing processing；And after the NaCl that 3 8wt% are added into the remaining waste material of final finishing is demulsified, alkane organic matter atoleine can be effectively recycled.
Description
Technical field
The invention belongs to technical field of fine, are related to a kind of softening agent preparation and application for pure cotton textile.
Background technology
Pure cotton textile printing product can make textile touch meeting in the multiple processing of the manufacturing procedures such as preceding processing, stamp
Become coarse, in order to make fabric that there is soft, smooth, comfortable feel, it is necessary to be arranged to it.Softening agent is because of energy
Enough assign fabric has soft pleasant feeling and the important auxiliary agent as finishing process in feel.It can make fibre using softening agent
Dimension itself has the flexible smooth being adapted with processing conditions to avoid damage.Therefore softening agent used for textiles is a kind of important
Textile auxiliary.Softening agent totality main component used at present is main with silicone oil and its derivative and fat and its derivative
Ingredient.National patent CN107869063A is that active ingredient synthesizes softening agent with dimethicone, odium stearate and n-butanol etc.；
National patent CN 107780219A are by using pentaerythritol fatty ester, sorbitan fatty acid ester and ester based quaternary ammonium salt
Equal synthesis have the good softening agent of using effect.But with such method synthesis softening agent exist on printed color influence compared with
Greatly, there is the defect of viscous glutinous sense in pure cotton fabric surface, and silicone oil and its derivative and fat and its derivative cannot recycle again
It utilizes, pollutes the environment.By experimental results demonstrate be made softness using alkane organic matter atoleine as active ingredient
Agent is applied to Pure Cotton Fabric Printing after-finishing of textile products, in addition to it fabric can be made to reach smooth, comfortable and fluffy feel completely,
Influence is nearly free from printed color, fabric surface will not be made to generate viscous glutinous sense, and the waste material after using is carried out simple
Processing can recycle in waste material 80% or more alkane organic matter atoleine, reduce the pollution to environment.
Invention content
Very little, pure cotton fabric surface are influenced on printed color in order to solve the above technical problem, the present invention provides a kind of
The preparation method and application of softening agent without viscous glutinous sense.
One kind being used for Pure Cotton Fabric Printing fabric softener, and material quality score and preparation method are as follows：It weighs 6-
The alkyl phenol polyvinylether of 10wt%, fatty alcohol polyoxyethylene ether, this disk series of surfactants, tween surfactants, ten
At least one surfactant such as dialkyl sulfonates and double alkyl maleic acid esters, with blender 600-1000r/min's
The deionized water that 40-64wt% is added under rotating speed while stirring at the uniform velocity stirs 30min and after mixing, then by rotating speed is adjusted to
2000-2800r/min is gradually added the atoleine of 30-50wt% with the speed of 1-2.5ml/s under conditions of high-speed stirred
Enter, rotating speed is adjusted to 3000-3500r/min high-speed stirred 1h after its whole adds, completes to prepare.
Further, since alkane organic matter atoleine itself is insoluble in water, the present invention is will by surfactant
Its emulsification forms colloid and keeps its evenly dispersed in deionized water, so 3-8wt% is added in the remaining waste material of final finishing
NaCl be demulsified after, alkane organic matter atoleine can be detached with water-soluble substances and water, pass through liquid separation method recycle alkane
Hydrocarbon organic matter atoleine.
Further, prepared by final finishing stenter composite mortar：Stiffening intensifier 10-17g/l, the present invention prepare softening agent
8-12g/l, cotton sense finishing agent 5-7g/l.
Specific implementation mode
The technical scheme in the embodiments of the invention will be clearly and completely described below, it is clear that described implementation
Example is only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, this field is common
All other embodiment that technical staff is obtained without making creative work belongs to what the present invention protected
Range.
Embodiment 1
It is prepared by softening agent：It weighs the alkyl phenol polyvinylether of 8wt%, fatty alcohol polyoxyethylene ether, this disk series surface-active
At least one surfactant such as agent, tween surfactants, dodecyl sodium sulfate and double alkyl maleic acid esters, with stirring
The deionized water that 45wt% is added in machine while stirring under the rotating speed of 600-1000r/min at the uniform velocity stirs 30min after mixing,
Rotating speed is adjusted to 2000-2800r/min again, by the atoleine of 47wt% with the speed of 2ml/s under conditions of high-speed stirred
It is gradually added into, rotating speed is adjusted to 3000-3500r/min high-speed stirred 1h after its whole adds, complete to prepare.
It is prepared by final finishing stenter composite mortar：Stiffening intensifier 15g/l, the present invention prepare softening agent 12g/l, cotton sense finishing agent
5g/l。
The recycling of active ingredient alkane type organic atoleine：Final finishing stenter after being arranged to fabric
7wt%NaCl is added in composite mortar, allows its uniform dissolution, standing 10min to recycle upper layer clear solution, as alkanes are organic
Object atoleine, rate of recovery position 86%.
Embodiment 2
It is prepared by softening agent：It weighs the alkyl phenol polyvinylether of 10wt%, fatty alcohol polyoxyethylene ether, this disk series surface-active
At least one surfactant such as agent, tween surfactants, dodecyl sodium sulfate and double alkyl maleic acid esters, with stirring
The deionized water that 40wt% is added in machine while stirring under the rotating speed of 600-1000r/min at the uniform velocity stirs 30min after mixing,
Rotating speed is adjusted to 2000-2800r/min again, by the atoleine of 50wt% with the speed of 1.5ml/s under conditions of high-speed stirred
Degree is gradually added into, and rotating speed is adjusted to 3000-3500r/min high-speed stirred 1h after its whole adds, and completes to prepare.
It is prepared by final finishing stenter composite mortar：Stiffening intensifier 12g/l, the present invention prepare softening agent 9g/l, cotton sense finishing agent
6g/l。
The recycling of active ingredient alkane type organic atoleine：Final finishing stenter after being arranged to fabric
5wt%NaCl is added in composite mortar, allows its uniform dissolution, standing 10min to recycle upper layer clear solution, as alkanes are organic
Object atoleine, rate of recovery position 92%.
Embodiment 3
It is prepared by softening agent：Weigh the alkyl phenol polyvinylether of 5wt%, fatty alcohol polyoxyethylene ether, this disk series of surfactants,
At least one surfactant such as tween surfactants, dodecyl sodium sulfate and double alkyl maleic acid esters, uses blender
The deionized water that 45wt% is added while stirring under the rotating speed of 600-1000r/min at the uniform velocity stirs 30min after mixing, then
Rotating speed is adjusted to 2000-2800r/min, by the atoleine of 50wt% with the speed of 1.5ml/s under conditions of high-speed stirred
It is gradually added into, rotating speed is adjusted to 3000-3500r/min high-speed stirred 1h after its whole adds, complete to prepare.
It is prepared by final finishing stenter composite mortar：Stiffening intensifier 17g/l, the present invention prepare softening agent 7g/l, cotton sense finishing agent
6g/l。
The recycling of active ingredient alkane type organic atoleine：Final finishing stenter after being arranged to fabric
3wt%NaCl is added in composite mortar, allows its uniform dissolution, standing 10min to recycle upper layer clear solution, as alkanes are organic
Object atoleine, rate of recovery position 87%.
Stamp pure cotton after final finishing stenter composite mortar by softening agent prepared by the present invention is added arranges is weaved
Product, the fluffy softness of feel, fabric surface is not cunning coarse but without viscous glutinous sense, while being influenced on printed color small yet；After use
The waste material of final finishing stenter composite mortar carry out demulsification processing, in waste material 80% or more the organic thing liquid of alkane can be recycled
Body paraffin reduces the pollution to environment.
Claims (3)
1. a kind of preparation and application for Pure Cotton Fabric Printing fabric softener, it is characterised in that include the following steps：
1）It weighs the alkyl phenol polyvinylether of 6-10wt%, fatty alcohol polyoxyethylene ether, this disk series of surfactants, tween
At least one surfactant such as surfactant, dodecyl sodium sulfate and double alkyl maleic acid esters, is existed with blender
Be added while stirring under the rotating speed of 600-1000r/min 40-64wt% deionized water at the uniform velocity stir 30min be uniformly mixed,
2）Rotating speed is adjusted to 2000-2800r/min again, by the atoleine of 30-50wt% with 1- under conditions of high-speed stirred
The speed of 2.5ml/s is gradually added into, and rotating speed is adjusted to 3000-3500r/min high-speed stirred 1h after its whole adds, and completes system
It is standby.
2. further, since alkane organic matter atoleine itself is insoluble in water, the present invention be by surfactant by its
Emulsification forms colloid and keeps its evenly dispersed in deionized water, so being added 3-8wt%'s in the remaining waste material of final finishing
After NaCl is demulsified, alkane organic matter atoleine can be detached with water-soluble substances and water, and alkane is recycled by liquid separation method
Organic matter atoleine.
3. further, prepared by final finishing stenter composite mortar：Stiffening intensifier 10-17g/l, the present invention prepare softening agent 8-
12g/l, cotton sense finishing agent 5-7g/l.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810445732.XA CN108625177A (en) | 2018-05-11 | 2018-05-11 | A kind of preparation and application for Pure Cotton Fabric Printing fabric softener |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810445732.XA CN108625177A (en) | 2018-05-11 | 2018-05-11 | A kind of preparation and application for Pure Cotton Fabric Printing fabric softener |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108625177A true CN108625177A (en) | 2018-10-09 |
Family
ID=63692722
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810445732.XA Pending CN108625177A (en) | 2018-05-11 | 2018-05-11 | A kind of preparation and application for Pure Cotton Fabric Printing fabric softener |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108625177A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111794004A (en) * | 2020-06-28 | 2020-10-20 | 宣城凯欧纺织有限公司 | Process for nano printing of cotton-like handfeel polyester fabric |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111794004A (en) * | 2020-06-28 | 2020-10-20 | 宣城凯欧纺织有限公司 | Process for nano printing of cotton-like handfeel polyester fabric |
| CN111794004B (en) * | 2020-06-28 | 2022-09-27 | 宣城凯欧纺织有限公司 | Process for nano printing of cotton-like handfeel polyester fabric |
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Application publication date: 20181009 |
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