CN108624367A - A kind of Preparation equipment of environment-friendlygasoline gasoline additive and preparation method thereof and the additive - Google Patents
A kind of Preparation equipment of environment-friendlygasoline gasoline additive and preparation method thereof and the additive Download PDFInfo
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- CN108624367A CN108624367A CN201810505783.7A CN201810505783A CN108624367A CN 108624367 A CN108624367 A CN 108624367A CN 201810505783 A CN201810505783 A CN 201810505783A CN 108624367 A CN108624367 A CN 108624367A
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L1/00—Liquid carbonaceous fuels
- C10L1/10—Liquid carbonaceous fuels containing additives
- C10L1/106—Liquid carbonaceous fuels containing additives mixtures of inorganic compounds with organic macromolecular compounds
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L1/00—Liquid carbonaceous fuels
- C10L1/10—Liquid carbonaceous fuels containing additives
- C10L1/14—Organic compounds
- C10L1/16—Hydrocarbons
- C10L1/1608—Well defined compounds, e.g. hexane, benzene
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L1/00—Liquid carbonaceous fuels
- C10L1/10—Liquid carbonaceous fuels containing additives
- C10L1/14—Organic compounds
- C10L1/16—Hydrocarbons
- C10L1/1625—Hydrocarbons macromolecular compounds
- C10L1/1633—Hydrocarbons macromolecular compounds homo- or copolymers obtained by reactions only involving carbon-to carbon unsaturated bonds
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L1/00—Liquid carbonaceous fuels
- C10L1/10—Liquid carbonaceous fuels containing additives
- C10L1/14—Organic compounds
- C10L1/18—Organic compounds containing oxygen
- C10L1/182—Organic compounds containing oxygen containing hydroxy groups; Salts thereof
- C10L1/1822—Organic compounds containing oxygen containing hydroxy groups; Salts thereof hydroxy group directly attached to (cyclo)aliphatic carbon atoms
- C10L1/1824—Organic compounds containing oxygen containing hydroxy groups; Salts thereof hydroxy group directly attached to (cyclo)aliphatic carbon atoms mono-hydroxy
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L1/00—Liquid carbonaceous fuels
- C10L1/10—Liquid carbonaceous fuels containing additives
- C10L1/14—Organic compounds
- C10L1/18—Organic compounds containing oxygen
- C10L1/188—Carboxylic acids; metal salts thereof
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L1/00—Liquid carbonaceous fuels
- C10L1/10—Liquid carbonaceous fuels containing additives
- C10L1/14—Organic compounds
- C10L1/18—Organic compounds containing oxygen
- C10L1/192—Macromolecular compounds
- C10L1/198—Macromolecular compounds obtained otherwise than by reactions involving only carbon-to-carbon unsaturated bonds homo- or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon to carbon double bond, and at least one being terminated by an acyloxy radical of a saturated carboxylic acid, of carbonic acid
- C10L1/1985—Macromolecular compounds obtained otherwise than by reactions involving only carbon-to-carbon unsaturated bonds homo- or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon to carbon double bond, and at least one being terminated by an acyloxy radical of a saturated carboxylic acid, of carbonic acid polyethers, e.g. di- polygylcols and derivatives; ethers - esters
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L1/00—Liquid carbonaceous fuels
- C10L1/10—Liquid carbonaceous fuels containing additives
- C10L1/14—Organic compounds
- C10L1/24—Organic compounds containing sulfur, selenium and/or tellurium
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L1/00—Liquid carbonaceous fuels
- C10L1/10—Liquid carbonaceous fuels containing additives
- C10L1/14—Organic compounds
- C10L1/24—Organic compounds containing sulfur, selenium and/or tellurium
- C10L1/2431—Organic compounds containing sulfur, selenium and/or tellurium sulfur bond to oxygen, e.g. sulfones, sulfoxides
- C10L1/2437—Sulfonic acids; Derivatives thereof, e.g. sulfonamides, sulfosuccinic acid esters
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- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Inorganic Chemistry (AREA)
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- General Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Liquid Carbonaceous Fuels (AREA)
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Abstract
The present invention provides a kind of environment-friendlygasoline gasoline additive and preparation method thereof and the Preparation equipment of the additive, constituent is made of following ratio in parts by weight：8 15 parts of ethylene, 36 parts of butadiene, 25 parts of TBHQ, 30 45 parts of poly- a alkene, 5 10 parts of silicone oil, 48 parts of polyoxyethylene polyoxypropylene polyethers, 26 parts of octadecanoid acid, 6 10 parts of oleic acid ethylene glycol junket, 59 parts of sulfuration cottonseed oil, 25 parts of sulfonate, 3 10 parts of fatty alcohol polyoxyethylene ether, 23 parts of tea polyphenols, 8 10 parts of ethyl alcohol.The present invention prepares method by using special Preparation equipment, produces a kind of environment-friendlygasoline gasoline additive, the trouble for avoiding previous additive environmental protection poor.
Description
Technical field
The invention belongs to additive technology fields, specifically, being related to a kind of environment-friendlygasoline gasoline additive and preparation method thereof
And the Preparation equipment of the additive.
Background technology
Environmentally protective to become modern theme with the requirement of social development, the continuous development of automobile industry causes global change
The hidden danger such as warm, need timely processing.There are labile elements in fuel oil, generate oxidative dimerization at high temperature, form carbon distribution
Particle is added the clean kept type additive in gasoline, these carbon particulates is surrounded from all quarter, forms oil-soluble one by one
Micella prevents them from assembling and becomes larger, can not be deposited on metal surface using intermicellar electrostatic repulsion and steric hindrance, to
Improve fuel qualities.
Invention content
In view of this, technical problem to be solved by the invention is to provide a kind of environment-friendlygasoline gasoline additive and its preparation sides
The Preparation equipment of method and the additive prepares method by using special Preparation equipment, produces a kind of environment protection gasoline
Additive, the trouble for avoiding previous additive environmental protection poor.
In order to solve the above-mentioned technical problem, the invention discloses a kind of environment-friendlygasoline gasoline additives comprising raw material composition at
Divide and is made of in parts by weight following ratio：8-15 parts of ethylene, 3-6 parts of butadiene, TBHQ2-5 parts, 30-45 parts of poly- a alkene, silicon
5-10 parts oily, 4-8 parts of polyoxyethylene polyoxypropylene polyethers, 2-6 parts of octadecanoid acid, 6-10 parts of oleic acid ethylene glycol junket, vulcanization cottonseed
5-9 parts oily, 2-5 parts of sulfonate, 3-10 parts of fatty alcohol polyoxyethylene ether, 2-3 parts of tea polyphenols, 8-10 parts of ethyl alcohol.
According to an embodiment of the present invention, the wherein preparation method of environment-friendlygasoline gasoline additive, including：
Step A, under an atmospheric pressure, ethylene, butadiene, poly- a alkene and silicone oil are subjected to mixing polycondensation, ethyl alcohol is catalysis
Agent, 250-340 DEG C of temperature obtain mixture A；
Step B, octadecanoid acid, fatty alcohol polyoxyethylene ether, sulfuration cottonseed oil and oleic acid ethylene glycol junket mixing is carried out to stir
It mixes, polyoxyethylene polyoxypropylene polyethers is slowly added in four times after uniform, until PH is 6.5-6.8, obtain mixture B；
Step C, TBHQ and sulfonate are mixed, mixture A is added and stirs evenly, stir speed (S.S.) 700-800r/
Min, 15-20min obtain mixture C；
Step D, mixture C addition mixture B is stirred, tea polyphenols is added, puts into and carries out water oil in centrifuge
From centrifugation unit frequency is 8000-9000HZ, and rotating speed 7000-8000r/min takes out supernatant liquor after filtering, obtains product.
According to an embodiment of the present invention, the wherein Preparation equipment of environment-friendlygasoline gasoline additive, which is characterized in that including：
The rooms mixture A, the rooms mixture A are connected to butadiene room, ethylene room and poly- a alkene room by tracheae, and pass through water conservancy diversion
Pipe is connected to silicone oil room and ethyl alcohol room, and wherein tracheae is equipped with valve with diversion pipe；
The rooms mixture B, the rooms mixture B open or close octadecane sour room, fatty alcohol polyoxyethylene ether by hydraulic selector
Room, sulfuration cottonseed oil room, oleic acid ethylene glycol junket room and polyoxyethylene polyoxypropylene polyethers room, wherein set rotation in the rooms mixture B
The spiral shell of mixing component and adjacent octadecane sour room, fatty alcohol polyoxyethylene ether room, sulfuration cottonseed oil room and oleic acid ethylene glycol junket room
Revolve conveying assembly；
The mixture C room of the rooms mixture A and the rooms mixture B is connected to by hydraulic selector, mixture C room side passes through valve
It is connected to the rooms TBHQ and sulfonate room, the other side is connected to tea polyphenols room by hydraulic selector, wherein sets Stirring in mixture C room
Component；
And the centrifuge of mixture C room is connected to by hydraulic selector；
Wherein, butadiene room, ethylene room, poly- a alkene room, silicone oil room, ethyl alcohol room, octadecane sour room, fatty alcohol polyoxy second
Alkene ether room, sulfuration cottonseed oil room, oleic acid ethylene glycol junket room, polyoxyethylene polyoxypropylene polyethers room, the rooms TBHQ, sulfonate room and tea
Polyphenol room is respectively provided with feed inlet.
According to an embodiment of the present invention, gas outlet is arranged in tracheae one end wherein in the rooms said mixture A, and installs temperature
Meter.
According to an embodiment of the present invention, wherein above-mentioned hydraulic selector is beaten by built-in hydraulic cylinder startup slide damper
Each chamber is closed on or off.
According to an embodiment of the present invention, wherein the above-mentioned external shell of helical feed component, covers at octadecane sour room, fat
The hydraulic selector of fat alcohol polyoxyethylene ether room, sulfuration cottonseed oil room and oleic acid ethylene glycol junket room, and the rooms mixture B are connected to, including
The screw rod driven by first motor.
According to an embodiment of the present invention, wherein above-mentioned Stirring component includes passing through the second motor-driven active
Axis, driving shaft has sets the fixed fixing axle of bearing by interior；It is arranged at intervals at the stirring rod of driving shaft side；It is set to actively
The supporting rod of the axis other side；Multiple shafts of supporting rod are inserted in by bearing, multiple shaft height are different；And it is installed on and turns
The blade of shaft end；Wherein, multiple institute's shafts are located at the transmission shaft driven inside supporting rod by boring tooth engagement, transmission shaft with consolidate
Dead axle is by boring tooth engagement.
Compared with prior art, the present invention can be obtained including following technique effect：
1) material is easy to get, at low cost, and environment-friendly and green, stability is strong, and oxidation resistance is good, and film is formed in metal surface,
Effective antirust improves lubricity, and abrasion resistance index is high, and frictional index is small, effectively promotes power, and water-oil separation effect is good, quickly clear
Except carbon deposit, oil circuit is cleaned, fuel oil is saved, prolongs the service life.
2) tri- Room mixture A, B, C of Preparation equipment cooperates, and auxiliary stirring, mixing is more uniformly distributed, and prepares additive
It is more environmentally friendly.
Certainly, implementing any of the products of the present invention must be not necessarily required to reach all the above technique effect simultaneously.
Description of the drawings
Attached drawing described herein is used to provide further understanding of the present invention, and constitutes the part of the present invention, this hair
Bright illustrative embodiments and their description are not constituted improper limitations of the present invention for explaining the present invention.In the accompanying drawings：
Fig. 1 is the Preparation equipment schematic diagram of the environment-friendlygasoline gasoline additive of the embodiment of the present invention；
Fig. 2 is the region A schematic diagrames of Fig. 1；
Fig. 3 is the mixture B chamber interior schematic diagrames of the embodiment of the present invention.
Reference numeral
The rooms mixture A 10, butadiene room 11, ethylene room 12, poly- a alkene room 13, silicone oil room 14, ethyl alcohol room 15, tracheae 20,
Diversion pipe 21, valve 22, the rooms mixture B 30, octadecane sour room 31, fatty alcohol polyoxyethylene ether room 32, sulfuration cottonseed oil room 33,
Oleic acid ethylene glycol junket room 34, polyoxyethylene polyoxypropylene polyethers room 35, hydraulic selector 40, hydraulic cylinder 41, slide damper 42, rotation
Turn mixing component 50, the second motor 51, driving shaft 52, fixing axle 53, stirring rod 54, supporting rod 55, shaft 56, blade 57, biography
Moving axis 58, helical feed component 60, first motor 61, screw rod 62, mixture C room 70, the rooms TBHQ 71, sulfonate room 72, tea
Polyphenol room 73, centrifuge 90, feed inlet 100, gas outlet 210, thermometer 220, region A.
Specific implementation mode
Carry out the embodiment that the present invention will be described in detail below in conjunction with accompanying drawings and embodiments, thereby how the present invention is applied
Technological means solves technical problem and reaches the realization process of technical effect to fully understand and implement.
1 a kind of environment-friendlygasoline gasoline additive of embodiment and preparation method thereof, raw material constituent in parts by weight by comparing below
Example composition：10 parts of ethylene, 5 parts of butadiene, 3 parts of TBHQ, 35 parts of poly- a alkene, 8 parts of silicone oil, polyoxyethylene polyoxypropylene polyethers 6
Part, 4 parts of octadecanoid acid, 8 parts of oleic acid ethylene glycol junket, 7 parts of sulfuration cottonseed oil, 3 parts of sulfonate, 5 parts of fatty alcohol polyoxyethylene ether, tea
2 parts of polyphenol, 9 parts of ethyl alcohol.
Preparation method is as follows：A, under an atmospheric pressure, ethylene, butadiene, poly- a alkene and silicone oil are subjected to mixing contracting
Poly-, ethyl alcohol is catalyst, and 300 DEG C of temperature obtains mixture A；B, by octadecanoid acid, fatty alcohol polyoxyethylene ether, sulfuration cottonseed oil
It is mixed with oleic acid ethylene glycol junket, polyoxyethylene polyoxypropylene polyethers is slowly added in four times after uniform, until PH is
6.7, obtain mixture B；C, TBHQ and sulfonate are mixed, mixture A is added and stirs evenly, stir speed (S.S.) 720r/
Min, 18min obtain mixture C；D, mixture C addition mixture B is stirred, tea polyphenols is added, puts into centrifuge and carries out
Water-oil separation, centrifugation unit frequency are 8200HZ, and rotating speed 7500r/min takes out supernatant liquor after filtering, obtains product.
2 a kind of environment-friendlygasoline gasoline additive of embodiment and preparation method thereof, raw material constituent in parts by weight by comparing below
Example composition：15 parts of ethylene, 4 parts of butadiene, 3 parts of TBHQ, 45 parts of poly- a alkene, 10 parts of silicone oil, polyoxyethylene polyoxypropylene polyethers 4
Part, 2 parts of octadecanoid acid, 6 parts of oleic acid ethylene glycol junket, 6 parts of sulfuration cottonseed oil, 3 parts of sulfonate, 3 parts of fatty alcohol polyoxyethylene ether, tea
3 parts of polyphenol, 8 parts of ethyl alcohol.
Preparation method is as follows：A, under an atmospheric pressure, ethylene, butadiene, poly- a alkene and silicone oil are subjected to mixing contracting
Poly-, ethyl alcohol is catalyst, and 320 DEG C of temperature obtains mixture A；B, by octadecanoid acid, fatty alcohol polyoxyethylene ether, sulfuration cottonseed oil
It is mixed with oleic acid ethylene glycol junket, polyoxyethylene polyoxypropylene polyethers is slowly added in four times after uniform, until PH is
6.6, obtain mixture B；C, TBHQ and sulfonate are mixed, mixture A is added and stirs evenly, stir speed (S.S.) 800r/
Min, 15-20min obtain mixture C；D, mixture C addition mixture B is stirred, tea polyphenols is added, put into centrifuge
Water-oil separation is carried out, centrifugation unit frequency is 8400HZ, and rotating speed 7600r/min takes out supernatant liquor after filtering, obtains product.
3 a kind of environment-friendlygasoline gasoline additive of embodiment and preparation method thereof, raw material constituent in parts by weight by comparing below
Example composition：13 parts of ethylene, 3 parts of butadiene, 3 parts of TBHQ, 45 parts of poly- a alkene, 5 parts of silicone oil, polyoxyethylene polyoxypropylene polyethers 4
Part, 3 parts of octadecanoid acid, 7 parts of oleic acid ethylene glycol junket, 8 parts of sulfuration cottonseed oil, 3 parts of sulfonate, 5 parts of fatty alcohol polyoxyethylene ether, tea
3 parts of polyphenol, 8 parts of ethyl alcohol.
Preparation method is as follows：A, under an atmospheric pressure, ethylene, butadiene, poly- a alkene and silicone oil are subjected to mixing contracting
Poly-, ethyl alcohol is catalyst, and 280 DEG C of temperature obtains mixture A；B, by octadecanoid acid, fatty alcohol polyoxyethylene ether, sulfuration cottonseed oil
It is mixed with oleic acid ethylene glycol junket, polyoxyethylene polyoxypropylene polyethers is slowly added in four times after uniform, until PH is
6.8, obtain mixture B；C, TBHQ and sulfonate are mixed, mixture A is added and stirs evenly, stir speed (S.S.) 780r/
Min, 15-20min obtain mixture C；D, mixture C addition mixture B is stirred, tea polyphenols is added, put into centrifuge
Water-oil separation is carried out, centrifugation unit frequency is 8200HZ, and rotating speed 8000r/min takes out supernatant liquor after filtering, obtains product.
4 a kind of environment-friendlygasoline gasoline additive of embodiment and preparation method thereof, raw material constituent in parts by weight by comparing below
Example composition：8 parts of ethylene, 3 parts of butadiene, 2 parts of TBHQ, 30 parts of poly- a alkene, 5 parts of silicone oil, polyoxyethylene polyoxypropylene polyethers 4
Part, 2 parts of octadecanoid acid, 6 parts of oleic acid ethylene glycol junket, 5 parts of sulfuration cottonseed oil, 2 parts of sulfonate, 3 parts of fatty alcohol polyoxyethylene ether, tea
2 parts of polyphenol, 8 parts of ethyl alcohol.
Preparation method is as follows：A, under an atmospheric pressure, ethylene, butadiene, poly- a alkene and silicone oil are subjected to mixing contracting
Poly-, ethyl alcohol is catalyst, and 340 DEG C of temperature obtains mixture A；B, by octadecanoid acid, fatty alcohol polyoxyethylene ether, sulfuration cottonseed oil
It is mixed with oleic acid ethylene glycol junket, polyoxyethylene polyoxypropylene polyethers is slowly added in four times after uniform, until PH is
6.8, obtain mixture B；C, TBHQ and sulfonate are mixed, mixture A is added and stirs evenly, stir speed (S.S.) 800r/
Min, 20min obtain mixture C；D, mixture C addition mixture B is stirred, tea polyphenols is added, puts into centrifuge and carries out
Water-oil separation, centrifugation unit frequency are 9000HZ, and rotating speed 8000r/min takes out supernatant liquor after filtering, obtains product.
5 a kind of environment-friendlygasoline gasoline additive of embodiment and preparation method thereof, raw material constituent in parts by weight by comparing below
Example composition：10 parts of ethylene, 5 parts of butadiene, 3 parts of TBHQ, 42 parts of poly- a alkene, 6 parts of silicone oil, polyoxyethylene polyoxypropylene polyethers 7
Part, 3 parts of octadecanoid acid, 8 parts of oleic acid ethylene glycol junket, 6 parts of sulfuration cottonseed oil, 4 parts of sulfonate, 5 parts of fatty alcohol polyoxyethylene ether, tea
3 parts of polyphenol, 10 parts of ethyl alcohol.
Preparation method is as follows：A, under an atmospheric pressure, ethylene, butadiene, poly- a alkene and silicone oil are subjected to mixing contracting
Poly-, ethyl alcohol is catalyst, and 320 DEG C of temperature obtains mixture A；B, by octadecanoid acid, fatty alcohol polyoxyethylene ether, sulfuration cottonseed oil
It is mixed with oleic acid ethylene glycol junket, polyoxyethylene polyoxypropylene polyethers is slowly added in four times after uniform, until PH is
6.6, obtain mixture B；C, TBHQ and sulfonate are mixed, mixture A is added and stirs evenly, stir speed (S.S.) 750r/
Min, 18min obtain mixture C；D, mixture C addition mixture B is stirred, tea polyphenols is added, puts into centrifuge and carries out
Water-oil separation, centrifugation unit frequency are 8000HZ, and rotating speed 7000r/min takes out supernatant liquor after filtering, obtains product.
In above example, embodiment 5 is most preferred embodiment, and lubricant effect is more preferable, and permeability is strong, and stability is good；Step B
In be slowly added in four times polyoxyethylene polyoxypropylene polyethers ensure emulsion resistance machine uniformity, improve antifoaming speed.
Referring to FIG. 1, Fig. 1 is the Preparation equipment schematic diagram of the environment-friendlygasoline gasoline additive of the embodiment of the present invention.It is of the invention public
A kind of Preparation equipment of environment-friendlygasoline gasoline additive, including the rooms mixture A 10 are opened, the rooms mixture A 10 are connected to fourth by tracheae 20
Diene room 11, ethylene room 12 and poly- a alkene room 13, and silicone oil room 14 and ethyl alcohol room 15, wherein tracheae are connected to by diversion pipe 21
20 are equipped with valve 22 with diversion pipe 21.The rooms mixture A 10 import the main component of mixture A.
The rooms mixture B 30, the rooms mixture B 30 open or close octadecane sour room 31, poly alkyl alcohol by hydraulic selector 40
Ethylene oxide ether room 32, sulfuration cottonseed oil room 33, oleic acid ethylene glycol junket room 34 and polyoxyethylene polyoxypropylene polyethers room 35, wherein mixed
Close Stirring component 50 and adjacent octadecane sour room 31, fatty alcohol polyoxyethylene ether room 32, sulfuration cottonseed oil built in the rooms object B 20
The helical feed component 60 of room 33 and oleic acid ethylene glycol junket room 34.The rooms mixture B 30 import the main component of mixture B.
The mixture C room 70 of the rooms mixture A 10 and the rooms mixture B 30, mixture C room 70 1 are connected to by hydraulic selector 40
Side is connected to the rooms TBHQ 71 and sulfonate room 72 by valve 22, and the other side is connected to tea polyphenols room 73 by hydraulic selector 40, wherein
Main mixing component 80 built in mixture C room 70.
And the centrifuge 90 of mixture C room 70 is connected to by hydraulic selector 40.
Wherein, butadiene room 11, ethylene room 12, poly- a alkene room 13, silicone oil room 14, ethyl alcohol room 15, octadecane sour room 31,
Fatty alcohol polyoxyethylene ether room 32, sulfuration cottonseed oil room 33, oleic acid ethylene glycol junket room 34, polyoxyethylene polyoxypropylene polyethers room
35, the rooms TBHQ 71, sulfonate room 72 and tea polyphenols room 73 are respectively provided with feed inlet 100.
In the present embodiment, feed inlet 100 is provided in each chamber, and the raw material of corresponding chambers is directed respectively into for it.So
Flow is controlled by valve 22 or hydraulic selector 40 afterwards, determines proportioning, and then imported into the rooms corresponding mixture A 10 and mix instead
It answers, generates mixture A；30 hybrid reaction of the rooms mixture B generates mixture B；It imported into mixture C room 70 later according to this hair
Bright step C and step D, prepares mixing finished product, is finally centrifuged by centrifuge 90, filters out finished product product, and one step of equipment arrives
Position, it is easy to use.
It is opened or closed respectively it is noted that hydraulic selector 40 starts slide damper 42 by built-in hydraulic cylinder 41
A chamber, it is simple in structure, it is easy to operate.
Referring to FIG. 2, Fig. 2 is the region A schematic diagrames of Fig. 1.Gas outlet 210 is arranged in 10 interior tracheae of the rooms mixture A, 20 one end,
To and thermometer 220 be installed.Thermometer 220 is mounted on tracheae 20 and close to gas outlet 210, temperature sensor, feedback information, control
System reaction, it is convenient and practical.
It is 30 schematic internal view of the rooms mixture B of the embodiment of the present invention please continue to refer to Fig. 1 and Fig. 3, Fig. 3.Helical feed
60 external shell of component covers at octadecane sour room 31, fatty alcohol polyoxyethylene ether room 32, sulfuration cottonseed oil room 33 and oleic acid second
The hydraulic selector 40 of glycol junket room 34, and the rooms mixture B 30 are connected to, include the screw rod 62 driven by first motor 61.Spiral shell
Rotation conveying assembly 60 is placed in octadecane sour room 31, fatty alcohol polyoxyethylene ether room 32, sulfuration cottonseed oil room 33 and oleic acid ethylene glycol
The lower section of junket room 34, it is uniform for the octadecanoid acid of importing, fatty alcohol polyoxyethylene ether, sulfuration cottonseed oil and oleic acid ethylene glycol junket
Conveying, is fully stirred to polyoxyethylene polyoxypropylene polyether reactant, is uniformly mixed, and the Stirring component 50 after being convenient for is anti-
It answers.
Stirring component 50 includes the driving shaft 52 driven by the second motor 51, and driving shaft 52 has sets axis by interior
Hold fixed fixing axle 53；It is arranged at intervals at the stirring rod 54 of 52 side of driving shaft；It is set to the branch for stating 52 other side of driving shaft
Strut 55；Multiple shafts 56 of supporting rod 55 are inserted in by bearing, 56 height of multiple shafts is different；And it is installed on shaft 56
The blade 57 of end；Wherein, multiple shafts 56 are located at the transmission of the transmission shaft 58 inside supporting rod 55, transmission shaft by boring tooth engagement
58 pass through cone tooth engagement with fixing axle 53.In the present embodiment, the second motor 51 drives driving shaft 52, rotation to drive stirring rod
54 and supporting rod 55, stirring rod 54 stirs mixture B, and supporting rod 55 drives multiple shafts 56 so that 57 stress of blade of end
Rotation, to more fully stir the reactant of liquid and gas, moreover, the shaft 56 of setting different height, can react from
Top-down all reactants of the rooms mixture B 30, are stirred evenly.Meanwhile the biography that multiple shafts 56 pass through cone tooth engagement
Moving axis 58, transmission is more convenient, and efficiency is faster.
In addition, mixture C room 70 is also provided with mutually isostructural Stirring component 50, further realizes environment protection gasoline and add
Add the mixing of agent, it is convenient and practical to formulate finished product.
Above description shows to describe several preferred embodiments of the present invention, but as previously described, it should be understood that the present invention is simultaneously
It is not limited to form disclosed herein, is not to be taken as excluding other embodiments, and can be used for various other combinations, repair
Change and environment, and can in the scope of the invention is set forth herein, by the above teachings or related fields of technology or knowledge into
Row change.And changes and modifications made by those skilled in the art do not depart from the spirit and scope of the present invention, then it all should be in the present invention
In the protection domain of appended claims.
Claims (7)
1. a kind of environment-friendlygasoline gasoline additive, which is characterized in that including：
Raw material constituent is made of following ratio in parts by weight：8-15 parts of ethylene, 2-5 parts of TBHQ, gathers 3-6 parts of butadiene
30-45 parts of a alkene, 5-10 parts of silicone oil, 4-8 parts of polyoxyethylene polyoxypropylene polyethers, 2-6 parts of octadecanoid acid, oleic acid ethylene glycol junket
6-10 parts, 5-9 parts of sulfuration cottonseed oil, 2-5 parts of sulfonate, 3-10 parts of fatty alcohol polyoxyethylene ether, 2-3 parts of tea polyphenols, ethyl alcohol 8-
10 parts.
2. a kind of preparation method of environment-friendlygasoline gasoline additive according to claim 1, it is characterised in that：
Step A, under an atmospheric pressure, ethylene, butadiene, poly- a alkene and silicone oil are subjected to mixing polycondensation, ethyl alcohol is catalyst,
250-340 DEG C of temperature obtains mixture A；
Step B, octadecanoid acid, fatty alcohol polyoxyethylene ether, sulfuration cottonseed oil and oleic acid ethylene glycol junket are mixed,
Polyoxyethylene polyoxypropylene polyethers is slowly added to after even in four times, until PH is 6.5-6.8, obtains mixture B；
Step C, TBHQ and sulfonate are mixed, mixture A is added and stirs evenly, stir speed (S.S.) 700-800r/min,
15-20min obtains mixture C；
Step D, mixture C addition mixture B is stirred, tea polyphenols is added, puts into centrifuge and carries out water-oil separation, from
Scheming frequency is 8000-9000HZ, and rotating speed 7000-8000r/min takes out supernatant liquor after filtering, obtains product.
3. a kind of Preparation equipment of environment-friendlygasoline gasoline additive according to claim 1, which is characterized in that including：
The rooms mixture A (10), the rooms the mixture A (10) by tracheae (20) connection butadiene room (11), ethylene room (12) and
Poly- a alkene room (13), and by diversion pipe (21) connection silicone oil room (14) and ethyl alcohol room (15), wherein the tracheae (20) and institute
It states diversion pipe (21) and is equipped with valve (22)；
The rooms mixture B (30), the rooms the mixture B (30) by hydraulic selector (40) open or close octadecane sour room (31),
Fatty alcohol polyoxyethylene ether room (32), sulfuration cottonseed oil room (33), oleic acid ethylene glycol junket room (34) and polyoxyethylene polyoxypropylene
Polyethers room (35), wherein Stirring component (50) built in the rooms the mixture B (20) and the adjacent octadecane sour room (31),
The fatty alcohol polyoxyethylene ether room (32), the sulfuration cottonseed oil room (33) and the oleic acid ethylene glycol junket room (34) spiral
Conveying assembly (60)；
The mixture C room (70) of the rooms the mixture A (10) and the rooms the mixture B (30) is connected to by hydraulic selector (40),
Mixture C room (70) side is connected to the rooms TBHQ (71) and sulfonate room (72) by valve (22), and the other side passes through hydraulic selector
(40) tea polyphenols room (73) are connected to, wherein the Stirring component (50) built in the mixture C room (70)；
And the centrifuge (90) of the mixture C room (70) is connected to by hydraulic selector (40)；
Wherein, the butadiene room (11), ethylene room (12), poly- a alkene room (13), silicone oil room (14), ethyl alcohol room (15), 18
Alkanoic acid room (31), fatty alcohol polyoxyethylene ether room (32), sulfuration cottonseed oil room (33), oleic acid ethylene glycol junket room (34), polyoxy second
Alkene polyoxypropylene polyether room (35), the rooms TBHQ (71), sulfonate room (72) and tea polyphenols room (73) are respectively provided with feed inlet
(100)。
4. a kind of Preparation equipment of environment-friendlygasoline gasoline additive according to claim 3, which is characterized in that the wherein described mixing
Gas outlet (210) are arranged in the rooms object A (10) interior tracheae (20) one end, and install thermometer (220).
5. a kind of Preparation equipment of environment-friendlygasoline gasoline additive according to claim 3, which is characterized in that the wherein described hydraulic pressure
Switch (40) starts slide damper (42) by built-in hydraulic cylinder (41) and opens or closes each chamber.
6. a kind of Preparation equipment of environment-friendlygasoline gasoline additive according to claim 3, which is characterized in that the wherein described spiral
Conveying assembly (60) external shell covers at the octadecane sour room (31), the fatty alcohol polyoxyethylene ether room (32), described
The hydraulic selector (40) of sulfuration cottonseed oil room (33) and the oleic acid ethylene glycol junket room (34), and it is connected to the rooms the mixture B
(30), include the screw rod (62) driven by first motor (61).
7. a kind of Preparation equipment of environment-friendlygasoline gasoline additive according to claim 6, which is characterized in that the wherein described rotation
Mixing component (50) includes the driving shaft (52) driven by the second motor (51), and the driving shaft (52) has sets axis by interior
Hold fixed fixing axle (53)；It is arranged at intervals at the stirring rod (54) of the driving shaft (52) side；It is set to the driving shaft
(52) supporting rod (55) of the other side；It is inserted in multiple shafts (56) of the supporting rod (55) by bearing, the multiple turn
Axis (56) height is different；And it is installed on the blade (57) of the shaft (56) end；Wherein, multiple shafts (56) pass through
Cone tooth engagement is located at internal transmission shaft (58) transmission of the supporting rod (55), the transmission shaft (58) and the fixing axle (53)
By boring tooth engagement.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810505783.7A CN108624367A (en) | 2018-05-24 | 2018-05-24 | A kind of Preparation equipment of environment-friendlygasoline gasoline additive and preparation method thereof and the additive |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810505783.7A CN108624367A (en) | 2018-05-24 | 2018-05-24 | A kind of Preparation equipment of environment-friendlygasoline gasoline additive and preparation method thereof and the additive |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20040065002A1 (en) * | 2001-02-01 | 2004-04-08 | Shibin Hu | Fuel oil additive and fuel oil products containing the fuel oil additive |
| CN107298993A (en) * | 2017-08-25 | 2017-10-27 | 马鞍山中粮生物化学有限公司 | A kind of environment-friendlygasoline gasoline additive and preparation method thereof |
| CN207287418U (en) * | 2017-08-05 | 2018-05-01 | 葛毅鹏 | A kind of horizontal efficient stirring reaction unit of shock reducing type temperature controllable |
| CN108031329A (en) * | 2017-12-28 | 2018-05-15 | 郑州源冉生物技术有限公司 | A kind of Western medicine standby raw material mixing apparatus with dual mixed function |
-
2018
- 2018-05-24 CN CN201810505783.7A patent/CN108624367A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20040065002A1 (en) * | 2001-02-01 | 2004-04-08 | Shibin Hu | Fuel oil additive and fuel oil products containing the fuel oil additive |
| CN207287418U (en) * | 2017-08-05 | 2018-05-01 | 葛毅鹏 | A kind of horizontal efficient stirring reaction unit of shock reducing type temperature controllable |
| CN107298993A (en) * | 2017-08-25 | 2017-10-27 | 马鞍山中粮生物化学有限公司 | A kind of environment-friendlygasoline gasoline additive and preparation method thereof |
| CN108031329A (en) * | 2017-12-28 | 2018-05-15 | 郑州源冉生物技术有限公司 | A kind of Western medicine standby raw material mixing apparatus with dual mixed function |
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